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Astm G57
Astm G57
for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: G57 − 20
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Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
FIG. 1 Typical Connections for Use of Soil Box with Various Types of Instruments
5191.5 aR ~ a in ft! 4.4 For soil contained in a soil box similar to the one shown
in Fig. 1, the resistivity, ρ, is:
where:
ρ, Ω·cm 5 R A/a (4)
a = electrode separation, and
R = resistance, Ω. where:
Using dimensional analysis, the correct unit for resistivity is R = resistance, Ω,
ohm-centimeter. A = cross sectional area of the container perpendicular to the
current flow, cm2, and
4.3 If the current-carrying (outside) electrodes are not a = inner electrode spacing, cm.
spaced at the same interval as the potential-measuring (inside)
electrodes, the resistivity, ρ, is: NOTE 1—The spacing between the inner electrodes should be measured
from the inner edges of the electrode pins, and not from the center of the
ρ, Ω·cm 5 95.76bR~ 11b⁄a ! (2) electrodes.
5. Significance and Use different depths. The meter utilized may limit the upper range
5.1 Measurement of soil resistivity is used for assessment of resistivity, which can be measured. In such cases, the
and control of corrosion of buried structures. Soil resistivity is resistivity should be reported as greater than the meter’s upper
used both for the estimation of expected corrosion rates and for limit.
the design of cathodic protection systems. As an essential 6.1.4 Voltmeter—The voltmeter shall not draw appreciable
design parameter for cathodic protection systems, it is impor- current from the circuit to avoid influencing the results. A
tant to take as many measurements as necessary so as to get a galvanometer type of movement is preferred but an electronic
sufficiently representative characterization of the soil environ- type instrument will yield satisfactory results if the meter input
ment to which the entire buried structure will be exposed. impedance is at least 10 megaohm.
6.1.5 Electrodes fabricated from mild steel or martensitic
6. Apparatus stainless steel 0.475 cm to 0.635 cm (3⁄16 in. to 1⁄4 in.) in
6.1 At-Grade Measurements in situ: diameter and 30 cm to 60 cm (1 ft to 2 ft) in length are
6.1.1 The equipment required for field resistivity measure- satisfactory for most field measurements. Both materials may
ments to be taken at grade consists of a current source, a four require heat treatment so that they are sufficiently rigid to be
terminal soil resistance meter, suitable voltmeter, ammeter, or inserted in dry soils, or soils containing rocks or gravel. The
galvanometer, four metal electrodes, and the necessary wiring electrodes should be formed with a handle and a terminal for
to make the connections shown in Fig. 2. wire attachment.
6.1.2 Current Source—An ac source, usually 97 Hz, is 6.1.6 Wiring, 18 gauge to 22 gauge insulated stranded cop-
preferred since the use of dc will cause polarization of most per wire. Terminals should be of good quality to ensure that
metal electrodes, resulting in error. The current can be provided low-resistance contact is made at the electrodes and at the
by either a cranked ac generator or a vibrator-equipped dc meter. Where regular surveys are to be made at fixed electrode
source, which is internal to many soil resistance meters. An spacing, a shielded multiconductor cable can be fabricated with
unaltered dc source can be used if the electrodes are abraded to terminals permanently located at the required intervals.
bright metal before immersion, polarity is regularly reversed 6.2 Soil Sample Measurement (that is, soil box):
during measurement, and measurements are averaged for each 6.2.1 The equipment required for the measurement of the
polarity. resistivity of soil samples, either in the field or in the
6.1.3 Four Terminal Soil Resistance Meter—Commercially laboratory, is identical to that needed for at-grade measure-
available, four terminal soil resistance meters are commonly ments except that the electrodes are replaced with an inert
used for measuring soil resistivity. They offer convenience, container containing four mounted electrodes (see Fig. 1).
ease of use, and repeatability. Soil resistance meters yield 6.2.2 Four-electrode soil boxes can be constructed in vari-
direct readings in ohms. Some meters allow readings to be ous sizes provided the inside dimensions are known. Design
taken at multiple depths using electrodes spaced at pre- and construction shall incorporate materials that are durable
determined intervals. These meters allow switching between and machinable. The two end plate electrodes shall be con-
electrode sets without having to rearrange electrodes and can structed of a clean, polished, corrosion-resistant metal or alloy
calculate resistivity from the entered geometry and measured (that is, UNS Designation type S30400/S30403 or UNS
current and voltages. Other models have the capability of S31600/S31603 stainless steel) that will not form a heavy
providing one or two dimensional analysis of soil resistivity at oxide film or otherwise add significant resistance. The body of
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and temperature. The effect of variations in compaction and
commercial conductivity meter, itself calibrated to standard moisture content can be reduced by fully saturating the sample
solutions at 20 °C (68 °F).4 before placing it in the box. This can be done by preparing a
stiff slurry of the sample, adding only sufficient water to
9. Field Procedures produce a slight amount of surface water, which should be
9.1 At-Grade Measurements: allowed to evaporate before the slurry is remixed and placed in
9.1.1 Select the alignment of the measurement to include the box. Where available, use ground water from the sample
uniform topography over the limits of the electrode span. Do excavation for saturation. Otherwise, use ASTM Specification
not include large nonconductive bodies such as frozen soil, D1193 reagent water. If the soil resistivity is expected to be
boulders, concrete foundations, and so forth, which are not below 10 000 Ω·cm, local tap water can be used without
representative of the soil of interest, in the electrode span. introducing serious error.
Conductive structures such as pipes and cables should not be
NOTE 3—Some soils absorb moisture slowly and contain constituents
within 1⁄2 a of the electrode span unless they are at right angles that dissolve slowly, and the resistivity may not stabilize for as much as 24
to the span. h after saturation.
9.1.2 Select electrode spacings with regard to the structure
of interest. Since most pipelines are installed at depths of from The saturated measurement will provide an approaching
1.5 m to 4.5 m (5 ft to 15 ft), electrode spacings of 1.5 m, minimum resistivity, and can be usefully compared with
3.0 m, and 4.5 m (5 ft, 10 ft, and 15 ft) are commonly used. The “as-received” resistivity measurements. Surplus water should
a spacing should equal the maximum depth of interest. To not be poured off as this will remove soluble constituents.
facilitate field calculation of resistivities, spacings of 1.58 m, 9.2.3 Temperature—Soils shall not be frozen at the time of
3.16 m, and 4.75 m (5.2 ft, 10.4 ft, and 15.6 ft), which result in measurement. Temperature correction will not be required if
measurement is made in-the-ditch or immediately after the
sample is taken. If samples are retained for subsequent
4
Handbook of Chemistry and Physics, 41st ed., The Chemical Rubber Co., p. measurement, correct the resistivity if the measurement tem-
2606. perature is substantially different from the ground temperature.
FIG. 3 Nomogram or Conversion Chart for Reducing Soil Paste Resistance in ohms at a Particular Temperature as Measured in the
Bureau of Soils Cup, to Resistance at 15.6 °C (60 °F)
Correction to 15.5 °C (60 °F) is recommended if the sample the determination of the probability of the presence of a soil
temperature exceeds 21 °C (70 °F). with a resistivity equal to or greater than a particular value.6
Where random resistivities are measured over a plant site,
R 15.5 5 R T S 24.51T
40 D (5) these can best be displayed on a plot plan or similar layout. In
either case, use pedological surveys in the planning and
where: interpretation of any extensive survey. Measurements could be
T = soil temperature, °C, and made in each soil classification under a variety of drainage
RT = resistivity at T °C. conditions to simplify survey planning.
A nomograph for this correction is shown in Fig. 3.5 10.1.2 If the random interval (that is, statistical) method is
utilized to assess the requirement for corrosion control
10. Planning and Interpretation measures, it is recommended that the tests be made on a true
10.1 Planning: random basis. Since the number of soil sections that could be
10.1.1 Surveys may be conducted at regular or random inspected is essentially unlimited, infinite population charac-
intervals. The former method is suited to graphical presentation teristics can be used to simplify statistical treatment. Risk and
and plotting resistivity versus distance and will identify gradi- error must be arbitrarily selected to allow determination of the
ents and abrupt changes in soil condition. In addition to regular number of measurements. A risk of 5 % of an error greater than
intervals, resistivity measurements should be conducted at any 100 Ω·cm should be suitable for most situations. The error limit
areas with geographical changes, which may result in abnor- should be about 10 % of the anticipated mean resistivity.
mally high or low soil resistivities. The latter random interval Where mean or median values cannot be estimated with
method permits precise mathematical statistical treatment, such reasonable accuracy, sequential sampling techniques can be
as cumulative probability analysis. This test method permits employed.
6
Scott, G. N., “Corrosion,” National Association of Corrosion Engineers, Vol
5
National Institute of Standards and Technology Circular No. 579, p. 157. 14, No. 8, August 1958.
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used to facilitate interpretation.
11. General
11.1 It should be recognized that subsurface conditions can multi-participant evaluation with each participant using a
vary greatly in a short distance, particularly where other buried different meter. The data from this evaluation are available
structures have been installed. Surface contamination tends to from ASTM in Research Report RR:G01-1012. A summary of
concentrate in existing ditches with surface run-off, apprecia- these data is given in Table 1.
bly lowering the resistivity below the natural level. Since a 12.1.1 Repeatability—Repeatability refers to the variation
pipeline ditch cannot be included in the span of at-grade in results obtained by the same operator with the same
measurements, soil box samples should be obtained where the equipment and same operating conditions in successive runs.
opportunity exists. To evaluate contamination effects when a In the case of soil resistivity measurements, the repeatability
new route is being evaluated, soil samples can be obtained at
may be characterized by a coefficient of variation, Cv, repre-
crossings of existing pipelines, cables, etc., or by intentional
senting the repeatability standard deviation divided by the
sampling using soil augers.
average result and expressed in percent. The multi-participant
11.2 Other field resistivity measurement techniques and test program results indicate a repeatability Cv of 6.7 %. The
equipment are available. These commonly use two electrodes 95 % confidence interval is 2.8 Cv or 18.8 %.
mounted on a probe that is inserted in the soil-at-grade in an
12.1.2 Reproducibility—Reproducibility refers to the varia-
excavation or a driven or bored hole. The two-electrode
tion in results that occurs when different operators measure the
technique is inherently less accurate than the four-electrode
method because of polarization effects, but useful information same soil. In the case of soil resistivity measurements repro-
can be obtained concerning the characteristics of particular ducibility may be characterized by a coefficient of variation,
strata. More precise procedures may be employed in laboratory Cv, representing the reproducibility standard deviation divided
investigations and these should be defined in reporting the by the average result and expressed in percent. The multi-
results. Where resistivity information is included in published participant test program results indicate a reproducibility Cv of
information, the measurement techniques used should be 16.6 %. The 95 % confidence interval is 2.8 Cv or 46.5 %.
defined. 12.2 Bias—The procedure in Test Method G57 for measur-
12. Precision and Bias 7 ing soil resistivity by the Wenner Four Pin Method has no bias
because the value of Wenner Four Pin soil resistivity is defined
12.1 Precision (see Practice E691)—The precision of this only in terms of this test method.
test method was determined by a statistical evaluation of a
13. Keywords
7
Supporting data have been filed at ASTM International Headquarters and may
be obtained by requesting Research Report RR:G01-1012. Contact ASTM Customer 13.1 four electrode method; soil box; soil resistance meter;
Service at service@astm.org. soil resistivity
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