PH 212) EXPERIMENTS IN CONDENSED

MATTER PHYSICS
EXPERIMENT: X-RAY INVESTIGATION OF CRYSTLE STRUCTURE /

LAUE METHOD

SURESH CHANDRA JOSHI (Integrated Ph.D.)

Email: sureshjc@iisc.ac.in
SR Number: 10-07-00-10-31-21-1-19435
 # Table for calculation of glancing angle theoretically and experimentally &
corresponding [h k l] values and interplanar spacing and corresponding wavelength
of incident X-Ray
#Note: by taking D = 18mm, the lattice parameter of LiF = 402.6 pm, and n= 1 (first-order)

Spot y Z L Theta h k l Theta y/z k/l d Wavelength

No (Glancing (Glancing
angle) angle)
(exp.) (cal.)
mm mm mm degree degree pm pm
1 5 12.5 13.46291 18.3971339 4 4 10 20.38486 0.4 0.4 35.04183 22.118515

2 0 24 24 26.5650512 2 0 4 26.57853 0 0 90.0241 80.52

3 19 9.5 21.24265 24.8618285 2 4 2 24.10706 2 2 82.18038 69.10243

4 7 6.5 9.552487 13.9773053 1 3 3 13.2694 1.076923 1 92.36277 44.618156

5 10.5 11 15.20691 20.0960321 2 4 4 19.4811 0.954545 1 67.1 46.110403

#TABLE - 1
# Table for calculation of error corresponding to the experimental &
calculated glancing angle

Error theta (exp.) theta (cal.)

degree degree
0.09750998 18.397134 20.38486144
0
0.00050696 26.565051 26.57852536
0
0.03130886 24.861828 24.10706381
0
0.05334846 13.977305 13.26940303
0
0.03156575 20.096032 19.48109672

#TABLE –2

#Table for a spot no. and corresponding [h k l]

Spot number Corresponding [h k l]

1 4 4 10

2 204

3 242

4 133

5 244

#TABLE - 3