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Lab Session Permeability Measurements
Lab Session Permeability Measurements
4
Learning Objectives
• Measure porosity of actual core samples
• Use Dean-Stark distillation to estimate fluid saturations
• Measure contact angle of oil and water on reservoir rock sample
• Measure capillary pressure between oil and water
5
7.1 Measurements of absolute permeability
Methods for Measuring Permeability
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Main Reference for Permeability Measurement
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Steady State Method Using Liquids
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Steady State Method Using Liquids
A core holder
A rubber sleeve
Pressure gauges
Flow lines
10
Steady State Liquid Permeability Measurement
Pressure transducer
Dp
Core
V1 V1
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Steady State Liquid Permeameter, Vinci Technologies
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Steady State Liquid Permeability Measurement
Core sample is cleaned, dried, and saturated with the test liquid
Cylindrical core plugs are inserted into rubber sleeve
Two end caps are pressed against the core sample at the axial ends
End caps are designed with flow distributors
A flow distributor receives the fluid from flowline and distributes it
uniformly at the face of core plug
Flow distributor ensures that flow across core is one dimensional
Rubber sleeve and end caps protect core plug from external fluids
13
Steady State Liquid Permeability Measurement
Annular space between core holder and rubber sleeve and end caps is
filled with a confining liquid
Annular liquid is pressurized
It is of utmost importance that there is no fluid leakage from the core
and there is not any external fluid entry into the core sample
Constant rate pump injects test liquid into core sample
Liquid injection pumps can inject fluid at several different rates
Liquid injection pumps are equipped with a gear box to set the rate
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Steady State Liquid Permeability Measurement
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Steady State Liquid Permeability Measurement
Initially, pressure drop across the core sample increases and varies with
time
After some time transients die out, pressure drop stabilizes and
becomes constant
Permeability is estimated from Darcy’s equation
𝑘 = 𝑞𝜇𝐿/𝐴∆𝑝
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Steady State Liquid Permeameter – Example 9
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Steady State Gas Permeameter
The most common gases used to measure permeability are listed below.
Air
Helium
Nitrogen
Gases are clean, nonreactive, and do not alter the pore structure
Experimental apparatus is simpler
Experiments using gases are much faster
Gas permeameters can measure very low permeabilities (md and hd)
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Steady State Gas Permeameter
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Steady State Gas Permeameter
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Steady State Gas Permeameter – High Pressures
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Steady State Gas Permeameter – High Pressures
Pressure transducer
Dp
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Steady State Gas Permeameter
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Steady State Gas Permeameter – Klinkenberg Plot
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Steady State Gas Permeameter – Example 10
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Steady State Gas Permeameter – Example 10
Table 11 – Pressure and rate data from a gas permeameter at low pressures –
Example 9
Test # p1 p2 qsc p~ 1/p~ kag
(1/atm
() (atm) (atm) (cm3/s) (atm) (d)
)
1 1.401 0.982 1.54E-05 1.192 0.839 2.68E-07
2 2.151 0.975 4.48E-05 1.563 0.640 2.11E-07
3 2.605 0.975 6.24E-05 1.790 0.559 1.85E-07
4 3.010 0.975 7.88E-05 1.993 0.502 1.68E-07
5 3.356 0.974 9.26E-05 2.165 0.462 1.55E-07
6 3.750 0.980 1.09E-04 2.365 0.423 1.45E-07
26
Steady State Gas Permeameter – Example 10
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Steady State Gas Permeameter – Example 10
28
Steady State Gas Permeameter – Example 10
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7.2 Estimation of Relative Permeability
Relative Permeability Measurement
Centrifuge methods
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Steady State Methods
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Steady State Methods
Hassler method
Hafford method
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Steady State Methods
34
Steady State Methods – Test Procedure
35
Steady State Methods – Test Procedure
During test, pressure drop, oil injection rate, water injection rate, oil
production rate, and water production rate must be measured
Additionally, fluid saturations in each step of steady state method are
measured
Fluid saturations in core are measured by removing core from test
apparatus and weighting core at the end of each step
36
Steady State Methods – Test Procedure
37
Steady State Methods – Test Procedure
38
Steady State Methods – Test Procedure
𝑘𝑜 𝑆𝑤 = 𝑞𝑜 𝜇𝑜 𝐿/𝐴∆𝑝𝑜 (26)
𝑘𝑤 𝑆𝑤 = 𝑞𝑤 𝜇𝑤 𝐿/𝐴∆𝑝𝑤 (27)
Note that, in Eqs. 26 and 27, pressure drops in oil and water phases are
different
When oil and water flow inside porous rock, there is a pressure
difference between oil and water phases due to capillary pressure pc
Since saturation distribution inside porous rock is uniform so is capillary
pressure
Capillary pressure does not change along core length
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Steady State Methods – Test Procedure
Inlet and outlet pressures are measured in bulk fluids at just outside
both ends of core sample not inside porous rock
There should not be any capillary pressure in bulk fluid phases
Pressure drops in both oil and water phases should be the same
It is reasonable to assume that
∆𝑝𝑜 = ∆𝑝𝑤 = ∆𝑝 (28)
Dp = pressure drop across core
Using Eq. 28 in Eqs. 26 and 27,
40
Steady State Methods – Test Procedure
𝑘𝑜 𝑆𝑤 = 𝑞𝑜 𝜇𝑜 𝐿/𝐴∆𝑝 (29)
𝑘𝑤 𝑆𝑤 = 𝑞𝑤 𝜇𝑤 𝐿/𝐴∆𝑝 (30)
After computing ko and kw, relative permeabilities are calculated using
either Eqs. 20 and 21 or Eqs. 22 and 23
𝐾𝑟𝑜 𝑆𝑤 = 𝑘𝑜 𝑆𝑤 /𝑘1𝜙 (20)
𝐾𝑟𝑤 𝑆𝑤 = 𝑘𝑤 𝑆𝑤 /𝑘1𝜙 (21)
𝑘𝑟𝑜 𝑆𝑤 = 𝑘𝑜 𝑆𝑤 /𝑘𝑜𝑆𝑤𝑐 (22)
𝑘𝑟𝑤 𝑆𝑤 = 𝑘𝑤 𝑆𝑤 /𝑘𝑜𝑆𝑤𝑐 (23)
41
Steady State Method – Example 1
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Steady State Method – Example 1
Table 1 – Basic rock and fluid data, Table 2 – Oil and water rates and wet core
Example 1 weight data for steady state relative
Parameter Value permeability experiment
L, cm = 5.0
d, cm = 3.0 Index qo qw Wwc
f, fraction = 0.15 () (cm3/s) (cm3/s) (g)
mo, cp = 10.0 1 0.05556 0.00000 84.9679
mw, cp = 1.0
2 0.04547 0.00434 85.0209
k, d = 0.15
ro, g/cm3 = 0.85 3 0.03608 0.01736 85.0739
rw, g/cm3 = 1.05 4 0.02745 0.03906 85.1270
Dp, atm = 3.275 5 0.01964 0.06944 85.1800
A, cm =2 7.0686
3
6 0.01276 0.10851 85.2330
Vb, cm = 35.3429
7 0.00694 0.15625 85.2860
Vp, cm3 = 5.3014
Vm, cm3 = 30.0415 8 0.00246 0.21268 85.3390
WDc, g = 80.0906 9 0.00000 0.27778 85.3920
43
Steady State Method – Example 1
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Steady State Method – Example 1
45
Steady State Method – Example 1
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Steady State Method – Example 1 – Figure 6
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Unsteady State Methods to Measure Relative Permeabilities
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Unsteady State Methods to Measure Relative Permeabilities
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Unsteady State Methods – Test Procedure
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Unsteady State Methods – Test Procedure
core is ready for unsteady state experiment when water and oil
saturations in te core are Sw = Swc and So = 1-Swc
At the end of core preparation stage, effective oil permeability at
connate water saturation, koSwc, is measured
Test is started by injecting water at inlet face of core sample
Water injection rate is kept constant; qwI = constant
Injected water displaces movable oil under dynamic (time-dependent)
flow conditions
During test, pressure drop across core varies with time
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Unsteady State Methods – Test Procedure
52
Apparatus for Unsteady State Experiments – Figure 7
Pressure transducer
Dp
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Unsteady State Methods – Test Procedure – Figure 8
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Unsteady State Methods – Test Procedure – Figure 9
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Unsteady State Methods – Test Procedure
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Unsteady State Methods – Test Procedure
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Unsteady State Methods – JBN Method
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Unsteady State Methods – JBN Method
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Unsteady State Methods – JBN Method
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Unsteady State Methods – JBN Method
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Unsteady State Methods – JBN Method
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Unsteady State Methods – JBN Method
It can be shown that foL is the derivative of NpD with respect to WID
𝑓𝑜𝐿 = 𝑑𝑁𝑝𝐷 /𝑑𝑊𝐼𝐷 (35)
Next, we compute water saturation at core outlet
Using a mass balance, it can be shown that water saturation at core
outlet can be expressed as below
𝑆𝑤𝐿 = 𝑆𝑤𝑐 + 𝑁𝑝𝐷 − 𝑓𝑜𝐿 𝑊𝐼𝐷 (36)
Now, we compute a derivative that is somewhat complicated and used
in calculation of oil relative permeability
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Unsteady State Methods – JBN Method
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Unsteady State Methods – JBN Method
65
Computation of Derivatives in JBN Method
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Computation of Derivatives in JBN Method
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Algorithm for JBN Method
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Algorithm for JBN Method
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Algorithm for JBN Method
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Estimating Relative Permeabilities - JBN Method – Example 2
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Estimating Relative Permeabilities - JBN Method – Example 2
WI, Np, and Dp sandpack recorded at discrete times are all tabulated in
Table 5
Np and WI are plotted in Figure 10
Figure 11 display Dp as a function of time
Using JBN method, analyze unsteady state experimental data
Estimate SwL, kro, and krw at core outlet
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Estimating Relative Permeabilities - JBN Method – Example 2
Table 4 – Basic data for the unsteady
state experiment, Example 2
Parameter Value
L, cm = 54.7
d, cm = 4.8
f, fraction = 0.306
mo, cp = 108.4
mw, cp = 1.0
k, d = 3.42
qwI, cc/s = 0.0278
Swc, fraction = 0.119
koSwc, d = 3.16
A, cm2 = 18.0956
Vb, cm3 = 989.83
Vp, cm3 = 302.69
Vm, cm3 = 687.14
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Estimating Relative Permeabilities - JBN Method – Example 2
Table 5 – Test data recorded during unsteady Table 5 – Test data recorded during unsteady
state water-oil displacement experiment state water-oil displacement experiment
t WI Np Dp t WI Np Dp
(h) (cc) (cc) (atm) (h) (cc) (cc) (atm)
0.000 0.0 0.0 0.0000 7.943 794.3 133.5 0.1647
1.026 102.6 102.0 0.6138 9.762 976.2 135.3 0.1565
1.062 106.2 103.5 0.5648 13.155 1,315.5 138.0 0.1449
1.196 119.6 106.8 0.4702 17.311 1,731.1 140.4 0.1354
1.329 132.9 109.0 0.4130 21.467 2,146.7 142.0 0.1293
1.520 152.0 111.7 0.3688 25.620 2,562.0 143.2 0.1245
1.777 177.7 114.4 0.3314 31.831 3,183.1 144.4 0.1218
2.028 202.8 116.8 0.3096 33.910 3,391.0 145.0 0.1191
2.543 254.3 120.2 0.2722 38.072 3,807.2 145.6 0.1184
3.442 344.2 124.1 0.2259 40.170 4,017.0 145.9 0.1157
4.855 485.5 128.0 0.1892 44.326 4,432.6 146.2 0.1157
6.142 614.2 130.5 0.1715 48.479 4,847.9 146.5 0.1157
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Estimating Relative Permeabilities - Example 2 – Figure 10
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Estimating Relative Permeabilities - Example 2 – Figure 11
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Estimating Relative Permeabilities - JBN Method – Example 2
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Estimating Relative Permeabilities - JBN Method – Example 2
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Estimating Relative Permeabilities - Example 2
Table 6 – Calculations for the interpretation of the unsteady state water-oil displacement experiment, Example 2
WID NpD Dp Ir ln(WID) ln(1/WID) 1/WIDIr ln(1/WIDIr) foL SwL y kro krw
() () (atm) () () () () () () (fraction) () (fraction) (fraction)
0.1190 0.9240 0.0000
0.339 0.337 0.6138 4.3350 -1.0818 1.0818 0.6805 -0.3850 0.1830 0.3940 0.3681 0.4971 0.0207
0.351 0.342 0.5648 4.7110 -1.0470 1.0470 0.6048 -0.5029 0.1754 0.3994 0.3562 0.4924 0.0216
0.395 0.353 0.4702 5.6587 -0.9289 0.9289 0.4474 -0.8043 0.1519 0.4120 0.3192 0.4758 0.0248
0.439 0.360 0.4130 6.4418 -0.8233 0.8233 0.3536 -1.0395 0.1334 0.4204 0.2901 0.4599 0.0278
0.502 0.369 0.3688 7.2143 -0.6892 0.6892 0.2761 -1.2869 0.1131 0.4312 0.2578 0.4388 0.0321
0.587 0.378 0.3314 8.0291 -0.5327 0.5327 0.2122 -1.5503 0.0932 0.4423 0.2258 0.4128 0.0374
0.670 0.386 0.3096 8.5938 -0.4005 0.4005 0.1737 -1.7506 0.0790 0.4521 0.2026 0.3901 0.0424
0.840 0.397 0.2722 9.7754 -0.1744 0.1744 0.1218 -2.1055 0.0594 0.4661 0.1697 0.3502 0.0516
1.137 0.410 0.2259 11.7776 0.1284 -0.1284 0.0747 -2.5946 0.0404 0.4831 0.1362 0.2964 0.0657
1.604 0.423 0.1892 14.0653 0.4725 -0.4725 0.0443 -3.1162 0.0257 0.5007 0.1085 0.2374 0.0837
2.029 0.431 0.1715 15.5165 0.7075 -0.7075 0.0318 -3.4494 0.0188 0.5118 0.0941 0.1998 0.0971
2.624 0.441 0.1647 16.1577 0.9647 -0.9647 0.0236 -3.7471 0.0132 0.5253 0.0816 0.1621 0.1126
3.225 0.447 0.1565 17.0007 1.1709 -1.1709 0.0182 -4.0042 0.0099 0.5340 0.0735 0.1348 0.1255
4.346 0.456 0.1449 18.3576 1.4693 -1.4693 0.0125 -4.3793 0.0064 0.5470 0.0641 0.1004 0.1444
5.719 0.464 0.1354 19.6490 1.7438 -1.7438 0.0089 -4.7218 0.0043 0.5587 0.0574 0.0741 0.1616
7.092 0.469 0.1293 20.5798 1.9590 -1.9590 0.0069 -4.9833 0.0030 0.5665 0.0532 0.0569 0.1747
8.464 0.473 0.1245 21.3670 2.1358 -2.1358 0.0055 -5.1977 0.0023 0.5729 0.0503 0.0449 0.1850
10.516 0.477 0.1218 21.8445 2.3529 -2.3529 0.0044 -5.4368 0.0015 0.5798 0.0473 0.0326 0.1968
11.203 0.479 0.1191 22.3438 2.4162 -2.4162 0.0040 -5.5227 0.0014 0.5826 0.0465 0.0295 0.2001
12.578 0.481 0.1184 22.4722 2.5319 -2.5319 0.0035 -5.6442 0.0011 0.5862 0.0452 0.0243 0.2059
13.271 0.482 0.1157 23.0009 2.5856 -2.5856 0.0033 -5.7211 0.0010 0.5879 0.0447 0.0221 0.2084
14.644 0.483 0.1157 23.0009 2.6840 -2.6840 0.0030 -5.8196 0.0008 0.5902 0.0437 0.0184 0.2129
16.016 0.484 0.1157 23.0009 2.7736 -2.7736 0.0027 -5.9091 0.0007 0.5924 0.0430 0.0154 0.2167
79
Estimating Relative Permeabilities - JBN Method – Example 2
80
Estimating Relative Permeabilities - Example 2 – Figure 12
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Estimating Relative Permeabilities - JBN Method – Example 2
82
Estimating Relative Permeabilities - Example 2 – Figure 13
83
Estimating Relative Permeabilities - JBN Method – Example 2
84
Estimating Relative Permeabilities - JBN Method – Example 2
85
Estimating Relative Permeabilities - JBN Method – Example 2
86
Estimating Relative Permeabilities - JBN Method – Example 2
Step 10; we repeat calculation algorithm for all recorded data points
All calculations are presented in Table 6
Finally we plot kro and krw as a function of SwL
Figure 14 displays kro and krw estimated from unsteady state water-oil
displacement experiment
Note that, in unsteady state method, we cannot estimate kro and krw in
water saturation range of Swc = 0.119 < Sw < 0.394
In Swc = 0.119 < Sw < 0.394 interval, we simply do a linear interpolation
87
Estimating Relative Permeabilities - Example 2
Table 6 – Calculations for the interpretation of the unsteady state water-oil displacement experiment, Example 2
WID NpD Dp Ir ln(WID) ln(1/WID) 1/WIDIr ln(1/WIDIr) foL SwL y kro krw
() () (atm) () () () () () () (fraction) () (fraction) (fraction)
0.1190 0.9240 0.0000
0.339 0.337 0.6138 4.3350 -1.0818 1.0818 0.6805 -0.3850 0.1830 0.3940 0.3681 0.4971 0.0207
0.351 0.342 0.5648 4.7110 -1.0470 1.0470 0.6048 -0.5029 0.1754 0.3994 0.3562 0.4924 0.0216
0.395 0.353 0.4702 5.6587 -0.9289 0.9289 0.4474 -0.8043 0.1519 0.4120 0.3192 0.4758 0.0248
0.439 0.360 0.4130 6.4418 -0.8233 0.8233 0.3536 -1.0395 0.1334 0.4204 0.2901 0.4599 0.0278
0.502 0.369 0.3688 7.2143 -0.6892 0.6892 0.2761 -1.2869 0.1131 0.4312 0.2578 0.4388 0.0321
0.587 0.378 0.3314 8.0291 -0.5327 0.5327 0.2122 -1.5503 0.0932 0.4423 0.2258 0.4128 0.0374
0.670 0.386 0.3096 8.5938 -0.4005 0.4005 0.1737 -1.7506 0.0790 0.4521 0.2026 0.3901 0.0424
0.840 0.397 0.2722 9.7754 -0.1744 0.1744 0.1218 -2.1055 0.0594 0.4661 0.1697 0.3502 0.0516
1.137 0.410 0.2259 11.7776 0.1284 -0.1284 0.0747 -2.5946 0.0404 0.4831 0.1362 0.2964 0.0657
1.604 0.423 0.1892 14.0653 0.4725 -0.4725 0.0443 -3.1162 0.0257 0.5007 0.1085 0.2374 0.0837
2.029 0.431 0.1715 15.5165 0.7075 -0.7075 0.0318 -3.4494 0.0188 0.5118 0.0941 0.1998 0.0971
2.624 0.441 0.1647 16.1577 0.9647 -0.9647 0.0236 -3.7471 0.0132 0.5253 0.0816 0.1621 0.1126
3.225 0.447 0.1565 17.0007 1.1709 -1.1709 0.0182 -4.0042 0.0099 0.5340 0.0735 0.1348 0.1255
4.346 0.456 0.1449 18.3576 1.4693 -1.4693 0.0125 -4.3793 0.0064 0.5470 0.0641 0.1004 0.1444
5.719 0.464 0.1354 19.6490 1.7438 -1.7438 0.0089 -4.7218 0.0043 0.5587 0.0574 0.0741 0.1616
7.092 0.469 0.1293 20.5798 1.9590 -1.9590 0.0069 -4.9833 0.0030 0.5665 0.0532 0.0569 0.1747
8.464 0.473 0.1245 21.3670 2.1358 -2.1358 0.0055 -5.1977 0.0023 0.5729 0.0503 0.0449 0.1850
10.516 0.477 0.1218 21.8445 2.3529 -2.3529 0.0044 -5.4368 0.0015 0.5798 0.0473 0.0326 0.1968
11.203 0.479 0.1191 22.3438 2.4162 -2.4162 0.0040 -5.5227 0.0014 0.5826 0.0465 0.0295 0.2001
12.578 0.481 0.1184 22.4722 2.5319 -2.5319 0.0035 -5.6442 0.0011 0.5862 0.0452 0.0243 0.2059
13.271 0.482 0.1157 23.0009 2.5856 -2.5856 0.0033 -5.7211 0.0010 0.5879 0.0447 0.0221 0.2084
14.644 0.483 0.1157 23.0009 2.6840 -2.6840 0.0030 -5.8196 0.0008 0.5902 0.0437 0.0184 0.2129
16.016 0.484 0.1157 23.0009 2.7736 -2.7736 0.0027 -5.9091 0.0007 0.5924 0.0430 0.0154 0.2167
88
Estimating Relative Permeabilities - Example 2 – Figure 14
89
Empirical Methods for Two-Phase Relative Permeabilities
90
Empirical Methods for Two-Phase Relative Permeabilities
91
Empirical Methods for Two-Phase Relative Permeabilities
92
Empirical Methods for Two-Phase Relative Permeabilities
𝑆𝑔 −𝑆𝑔𝑐 𝑆𝑔 −𝑆𝑔𝑐
𝑘𝑟𝑔 = 𝑘𝑟𝑔𝑆𝑜𝑟𝑔 1.1072 + 2.7794 𝑆𝑜𝑟𝑔 (49)
1−𝑆𝑤𝑐 1−𝑆𝑤𝑐
93
Empirical Methods for Two-Phase Relative Permeabilities
94
Empirical Methods for Two-Phase Relative Permeabilities
95
References
96
References
97
Useful Links
http://petrowiki.org/Relative_permeability
http://petrowiki.org/PEH:Relative_Permeability_and_Capillary_Pressur
e
http://wiki.aapg.org/Relative_permeability
http://wiki.aapg.org/Relative_permeability_and_pore_type
https://en.wikipedia.org/wiki/Relative_permeability
http://perminc.com/resources/fundamentals-of-fluid-flow-in-porous-
media/chapter-2-the-porous-medium/relative-permeability/relative-
permeability-curves/
98
Useful Links
http://homepages.see.leeds.ac.uk/~earpwjg/PG_EN/CD%20Contents/F
ormation%20Evaluation%20English/Chapter%2010.PDF
https://www.youtube.com/watch?v=fKEw0e1QwHg
https://www.youtube.com/watch?v=ZgO1G3JUHFY
https://www.youtube.com/watch?v=GIORNcSUbD4
https://www.youtube.com/watch?v=fs9cgR8oK2Q
https://www.youtube.com/watch?v=E3lAbwLz5-4
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