5E-MF6100K Muffle Furnace

CHANGSHA KAIYUAN INSTRUMENTS CO.
, LTD 5E- MF6100K Muffle Furnace
Contents
Warranty ......................................................................................................... 3
Notice .............................................................................................................. 4
Preface ............................................................................................................ 5
Caution Symbols............................................................................................ 6
1 Brief Introduction..................................................................................... 7
1.1 Safety Attentions ..................................................................................... 7

1.2 Alert Signals ............................................................................................ 8
1.3 Package .................................................................................................. 9
1.4 Features.................................................................................................. 9
1.5 The Main Parameters and Functions .................................................... 10
1.6 Working Environment............................................................................ 11
2 Operation................................................................................................ 12
2.1 Slow Ash Analysis ................................................................................. 14

2.2 Quick Ash Analysis ............................................................................... 16
2.3 Volatile Matter Analysis ......................................................................... 18
2.4 Caking Index Analysis ........................................................................... 20
2.5 Common Analysis ................................................................................. 22
3 Setup....................................................................................................... 23
3.1 View the furnace Temperature .............................................................. 24

3.2 Setup the Calibrated Temperature ........................................................ 24
3.2 View the Calibrated Temperature .......................................................... 24
3.3 View the cooling compensation temperature ........................................ 24
3.5 Setup Common analysis parameters .................................................... 25
3.6 Setup parameters of Caking Index ....................................................... 25
3.7 Setup parameters of Volatile Matter ...................................................... 26
3.8 Setup Parameters of Quick Ash ............................................................ 26
1
CHANGSHA KAIYUAN INSTRUMENTS CO., LTD 5E- MF6100K Muffle Furnace
3.9 Setup parameters of slow Ash .............................................................. 27

3.10 View the Default Parameters .............................................................. 28
4 Troubleshooting..................................................................................... 29
5 Wiring Diagram ...................................................................................... 30
2
Warranty
Changsha Kaiyuan Instruments Co., Ltd. (CKIC) warrants this instrument is free from
defect in material and workmanship for a period of six months from the date of installation.
Equipment not manufactured by CKIC is covered to the extent of warranty provided by the
original manufacturer and this warranty does not cover any equipment, new or used,
purchased from anyone other than CKIC. All replacement parts shall be covered under
warranty for a period of thirty days from date of purchase. CKIC hereby disclaims all other
express or implied warrants for the product including warrants of merchantability and
fitness for a particular purpose with respect to the goods sold hereunder.
Expendable items such as crucibles, combustion tubes, chemicals and items of like nature
are not covered by this warranty.
CKIC's sole obligation under this warranty shall be to repair or replace any part or parts
which, to our satisfaction, prove to be defective upon return prepaid to CKIC. This
obligation does not include labor to install replacement parts, nor does it cover any failure
due to accident, abuse, neglect, or use in disregard of instructions furnished by CKIC. In
no event shall damages for defective goods exceed the purchase price of the goods, and
CKIC shall not be liable for incidental or consequential damages whatsoever.
All claims in regard to the parts or equipment must be made within ten (10) days after
Purchaser learns of the facts upon which the claim is based. Authorization must be
obtained from CKIC prior to returning any other parts. This warranty is voided by failure to
comply with these notice requirements.
3
Notice
The warranty on CKIC equipment remains valid only when genuine CKIC replacement
parts are employed. Since CKIC has no control over the quality or purity of consumable
products not manufactured by CKIC, the specifications for accuracy of results using CKIC
instruments are not guaranteed unless genuine CKIC consumables are employed in
conjunction with CKIC instruments. If purchaser defaults in making payment for any parts
or equipment, this warranty shall be void and shall not apply to such parts and equipment.
No late payment or cure of default in payment shall extend the warranty period provided
herein.
Changsha Kaiyuan Instruments Co., LTD is not responsible for damage to any associated
instruments, equipment or apparatus nor will CKIC be held liable for loss of profit or other
special damages resulting from abuse, neglect, or use in disregard of instructions. The
buyer, their employees, agents and successors in interest assume all risks and liabilities
for the operation, use and/or misuse of the product(s) described herein and agree to
indemnify, hold harmless and defend the seller from any and all claims and actions arising
from any cause whatsoever, including seller's negligence for personal injury incurred in
connection with the use of said product(s) and any and all damages proximately resulting
therefrom.
4
Preface
Thank you for purchasing 5E-MF6100K intelligent Muffle Furnace manufactured by
Changsha Kaiyuan Instruments Co., Ltd.
Before the first assembly and use of the instrument, be sure to read all the attached
documents that will help you better operate and maintain the instrument. Changsha
Kaiyuan Instruments Co., Ltd (CKIC) will not be responsible for damage caused by
neglect of instructions or misuse of this instrument resulting from misunderstanding the
instruction manual. The installation or commissioning operated by our professional
engineers is not included.
In spite of careful check, we are not completely assured that the Manual has no error and
omission. If you have questions about this manual, please contact our technical personnel
for details.
The instrument and its accessories listed in this manual are subject to change. Please
refer to the packing list received with the instruments.
CKIC reserves all the rights for improvement or modification of products, software
programs and instruction manual. It is subject to change without notice.
5
Caution Symbols
This symbol indicates a caution. (Specific instructions are

referred to the manual)
This symbol indicates a risk of electric shock. (Specific

instructions are referred to the manual)
This symbol indicates a high temperature surface. (Specific

This symbol indicates being corrosive. (Specific instructions

are referred to the manual)
Note: non-important procedure may be not instructed in this manual,

please read the updated instructions.
6
1 Brief Introduction
1.1 Safety Attentions
Electricity
Make sure the instrument is well grounded.
Do use the original standard power cord.
Always disconnect this instrument during thunderstorm, lest it may cause a risk on your
personal safety.
Do not share the power socket with other high power electrical equipment, lest it may
cause voltage instable.
Do not insert or extract any part of instrument before cutting off the power supply.
Do check the power cords and power plugs periodically, make sure the cables are not
pressed.
Do use special delivering forks with insulated handle while placing sample into the
furnace.
High temperature
The instrument is used for high temperature heating. Do not touch the instrument during
use or for a period of time after use, Make sure the whole instrument is cool before
disassembly.
Gas Source
When operation with chamber atmospheres O2 or N2, make sure the furnace is free of oil
and flammable and explosive substance, lest it may cause a fire or violent explosive.
Do locate the gas source away from heat source, naked flame
Do operate the high pressure gas cylinder in conformance with safety codes, make sure
there is no gas leakage
7
1.2 Alert Signals
Alert signals are highlighted in this instruction manual.
Alert Signals of the instrument and accessory parts are designed to prompt users to safely
operate the instrument. Operators should read the relative chapters carefully and use the
instrument in accordance with the alert signals to ensure the safety of instruments and
operators.
High temperature hazard alert you to a possibility of
personal injure if you come in contact with a
surface during use or for a period of time after use.
Refer to the instruction manual for better operation.
This symbol indicates a risk of electric shock.
(Specific instructions are referred to the manual)
This symbol indicates a pinch point, you should
watch your hands while operating (Specific
8
1.3 Package
When you received your instrument, check to see that you have received everything you
ordered and that it all arrived undamaged. For any doubt, please contact the logistics
center or CKIC
Note: the part list may be subject to change, refer to the received package list
1.4 Features
5E-MF6100K Muffle Furnace is a kind of common heating equipment (As Figure 1). This
Muffle Furnace is newly designed, and has unique upward-opening furnace door structure.
It is equipped with the new heat preservation material and also with an intelligent
temperature-controlling system for easy operation. Compared with the traditional Muffle
Furnace, this instrument has the advantages such as less weight, quick temperature
rising, low power cost and precise temperature controlling. It can be used to analyze the
ash and volatile matter of the coal, and also can be used for heating analysis or heat
treatment of some other objects.
5E-MF6100K can be applied to fuel intelligent control system. With an electronic lock on
the furnace door, analysis shall not be manual suspended until it is finished, when
analysis is forced to suspend, the furnace will sound alarms and the analysis result will be
invalid.
5E-MF6100K muffle furnace is designed to work independently or be controlled by a
computer, when the furnace is controlled by a computer it can record and upload the
analysis information including test temperature, test time interval, status of furnace door,
status of the electronic lock. The analysis result shall be directly showed in a spreadsheet
provided by computer on the screen.
9
1.5 The Main Parameters and Functions
1). Rated Temperature: 1000 ℃

2). Power: 3.5 KW
3). Temperature Range: 300 ℃~999℃

4). Temperature Resolution: 1℃
5). Average Temperature Stability: ±2℃
6). working environment: Ambient Temperature 0 ~40 ℃ ℃

Relative Humidity: RH ≤ 80%
7). Power Supply: 210~230 VAC, 50±1Hz
8). Features:
a).Four special analysis programs available: slow ash, quick ash and volatile matter
（
caking index Also can be used as common analysis program ）
b).One common analysis program: seven temperature points and seven time points as
well as the rising temperature rate can be set.
c).It can be used to analysis ash and volatile matter of the biomass fuel.
d).It will alarm if the thermocouple is broken or over-temperature.
e).It can display clearly with backlit display LCD, it has light and sound alarms as well.
f).The furnace door locked automatically during analysis.
g).During an analysis, the furnace temperature, analysis time interval, state of furnace
door, etc. all the parameters shall be recorded and uploaded by a computer. If there is
an abnormal temperature, an alarm will sound.
f).Multiple muffle furnaces can be controlled by one computer.
10
1.6 Working Environment
Environmental temperature: 5 ℃～40℃

Relative humidity: ≤85 ％
Electrical Requirements: AC198~242V, 40~60 Hz, current capacity no less than 15A
，，
Others: No vibration airflow, dust severe electromagnetic interference and corrosive gas
are allowed in this laboratory.
11
2 Operation
WARNING
To avoid electrical shock and scald, do use special sample feeding folk with
insulated handle to place sample into furnace, hold the insulated handle with
your hand.
After thermocouple and chimney installation and power cord connection, an analysis shall
be started.
On the control board, there are five function-choosing keys: slow ash, quick ash, volatile
matter, caking index and common (as Figure 2-1), and four number-setup keys: setup,
hundreds digit, tens digit and digit, and one start key. (Note: When pressing a key, you will
hear an indicating sound of the keyboard.)
There also has an indicator, a buzzer and a power switch on the keyboard, the indicator is
used to display the state of heat, when the furnace is heating, the heating indicator LED
will be lit. The buzzer is a light and sound buzzer, when press any key on the keyboard,
you will hear an indicating sound. When an analysis is on the point of finishing, the buzzer
will successively sound to prompt users. When the power switch is pressed, there will
appear a symbol “FL000” on the temperature display screen and an IP address on the
time display screen, immediately the instrument comes into the initial stage
12
Figure 2-1
The Digit/Reset key is used to reset the instrument and set the unit digit number of
temperature. During an analysis, press the Reset/Digit key to terminate in advance. If you
want to enter another analysis program, briefly press the “Reset/Digit” key (or restart the
instrument), and choose the desired function.
There are five indicators on the control board, when choosing one of the analysis
programs of slow ash, quick ash, volatile matter, caking index or common, the
corresponding LED indicator will be lit. The lit ready LED indicates the furnace has
reached a target temperature. For example: when selecting the volatile matter to do
analysis, once the furnace temperature reaches 920 ℃, the ready LED will be lit ,which
indicates samples can be delivered to the furnace.
In addition, there are two display screens on the board, the bigger one is the analysis
temperature display screen, it is used to display the furnace temperature, and the other
one is the analysis time display screen, the format of displaying time is “hour, minute,
second”, it is used to display the analysis time.
The MF6100K has 4 special analysis programs and one common analysis program, all
these can be selected from the keys on the panel. To set one of the 4 special analysis
programs when the instrument is in setup status , briefly input “118 “to load default values.
（Note: the default values are in conformance with the GB/T212-2008 standard）
4 special test programs: slow ash, quick ash, volatile matter, caking index (test program).
The special test program can be selected as common test program, each test program
13
can be divided into 7 temperatures and 7 time intervals. When the temperature of current
step is greater than the previous step temperature, it means that the temperature will be
rose to the current setup temperature; when the current temperature is identical with the
previous step temperature, which indicates this step is a constant temperature step.
Note: When the furnace door is stuck, it is need to lightly press the door before open it.
Steps Parameters Illustration
Temperature T0 0 ℃ The analysis can be started at any

Initial step
time.
Time interval t0 0
Temperature T1 500 ℃ Ramp from room temperature to

The first step
Time interval t1 30min. 500 ℃ in 30 min.
Temperature T2 500 ℃
The second step Soak at 500 ℃ for 30min.
Time interval t2 30min
Temperature T3 815 ℃ Ramp from 500 ℃ to 815℃ at fast

The third step
Time interval t3 0 rate
The forth step Soak at 815 ℃ for 2h
Time interval t4 2h
Temperature T5 900 ℃ Ramp from 815 ℃ to 900℃ in

The fifth step
Time interval t5 20min 20min.
The sixth step Soak at 900 ℃for 1.5h
Time interval t6 1.5h
2.1 Slow Ash Analysis
In the initial stage of the instrument (the screen displays the symbol “FL000”),when
～
desired, set the temperature T0 T6 and time interval t0 ～t6 refer to the 3.9 Parameters
of Slow Ash(if the test parameters are the same with the previous one, it is not necessary
to set it).then place the sample in the furnace, pull out the bracket on the left side of
furnace and close the furnace door, keep a space of 15 mm. Successively press the “Slow
Ash” key, the “Slow Ash” LED will be on, and then press “Start” key to confirm, and the
14
instrument will control the analysis automatically under the below steps (see table 2-2):
Table 2-2
Steps Parameters Illustrations
Temperature T0 0 ℃ The analysis can be started at any

Initial step
time
Time interval t0 0
Temperature T1 500 ℃ Ramp from room temperature to

The first step
Time interval t1 30min. 500 ℃ in 30 min
The second step Soak at 500 ℃ for 30min
Temperature T3 815 ℃ Ramp from 500 ℃ to 815℃ at fast

The third step
Time interval t3 0 rate
The forth step Soak at 815 ℃ for 60min
Temperature T5 815 ℃ The time interval should be set
The fifth step enough great to prevent it from

Time interval t5 10h
entering the sixth step
Temperature T6 815 ℃ Soak again at 815 ℃ for 20min, then

The sixth step
Time interval t6 20min back to the fifth step
The electronic lock shall be locked 3 seconds after the test begins and unlocked 2
seconds before the test finishes. If the electronic lock is forced to unlock during an
analysis, which may cause the lock getting stuck, thus, you should gently press the
furnace door before unlock it.
15 seconds before the test finishes, the alarm sounds successively to prompt users when
it is need to end an analysis, briefly press the Digit/Reset key.
Refer to related test parameters of standard to test the ash of biomass fuel (see 3.9 test
parameters of slow ash and table 3-2 on the 21th page)
15
2.2 Quick Ash Analysis
In the initial stage of the instrument (the screen displays the symbol “FL000”),when
desired, firstly set the temperature T0 ～T6 and time interval t0～t6 refer to the 3.8
Parameters of quick ash(if the test parameters are the same with the previous one, it is
not necessary to set it).then place the sample in the furnace, pull out the bracket on the
left side of furnace and close the furnace door, keep a space of 15 mm. Successively
press the “Quick Ash” key, the “Quick Ash” LED will be on, and then press “Start” key to
confirm, and the instrument will control the analysis automatically under the below steps
(see table 2-3): table 2-3
Steps Parameters Illustrations
Temperature T0 850 ℃ Ramp to 850 ℃ , the ready LED will

Initial step be on, put sample into furnace, press
Time interval t0 0
Start key
Temperature T1 815 ℃ Quickly ramp to 815 ℃ (the furnace

The first step temperature is lower than 815℃ after
Time interval t1 0min.
sample login)
The second step Skip this step
The third step Skip this step
Time interval t3 0
The forth step Soak at 815 ℃ for 40min
Temperature T5 815 ℃ The time interval should be set
The fifth step enough great to prevent it from

Time interval t5 10h
entering the sixth step
Temperature T6 815 ℃ Soak again at 815 ℃ for 20min, then

The sixth step
Time interval t6 20min return to the fifth step
16
analysis, which may cause a risk of getting the lock stuck, thus, you should lightly press
the furnace door before opening it when the electronic lock is unlocked.
15 seconds before the test finishes, there will be a light and sound buzzer sound
successively to prompt users.
If it is need to end an analysis, press the Digit/Reset key.
17
2.3 Volatile Matter Analysis
In the initial stage of the instrument (the screen displays the symbol “FL000”), when
Parameters of Slow Ash(if the test parameters are the same with the previous one, it is not
necessary to set it). Successively press the “Volatile Matter” key, the “Volatile Matter” LED
will be on, and then press “Start” key to confirm, and the instrument will control the
analysis automatically under the below steps (see table 2-4):
Table 2-4
Temperature T0 920 ℃ Ramp to 920 ℃, the ready LED will be

Initial step on, put sample into furnace, press
Time interval t0 0
Start key
The first step Skip this step
Time interval t1 0min.
Temperature T2 900 ℃ Rise T2 to (900 ±10)℃ in 3 min, soak

The second step in this temperature for accurately 7
min ( including the 3 min)
Temperature T3 920 ℃ Ramp to 920 ℃ quickly after the

The third step
Time interval t3 0 sample is taken out from the furnace
The forth step Skip this step
The fifth step Skip this step
The sixth step Skip this step
18
the furnace door in advance, open the furnace door until the electronic lock is unlocked.
successively to prompt users.
If it is necessary to end an analysis, press the Digit/Reset key.
19
2.4 Caking Index Analysis
Parameters of Caking Index(if the test parameters are the same with the previous one, it
is not necessary to set it). Successively press the “Caking Index” key, the “Caking Index”
LED will be on, and then press “Start” key to confirm, and the instrument will control the
analysis automatically under the below steps (see table 2-5):
Table 2-5
Temperature T0 850 ℃ Ramp to 850 ℃, the ready LED is on,

Initial step the instrument is ready, put sample
Time interval t0 0
into furnace, press Start key
Temperature T1 850 ℃ Skip this step, directly enter the

The first step
Time interval t1 0 second step
Temperature T2 850 ℃ Rise T2 to (850 ±10)℃ in 6min, and

soak in this temperature for
The second step
Time interval t2 15 min accurately 15 min (including the
6min)
Temperature T3 850 ℃ back to 850℃ quickly after take the

The third step
Time interval t3 0 sample out
The forth step Skip this step
Time interval t4 0
The fifth step Skip this step
Time interval t5 0
The sixth step Skip this step
Time interval t6 0
20
the furnace door before opening it.
successively to prompt users the test will finish soon.
If it is necessary to terminate an analysis, press the Digit/Reset key.
21
2.5 Common Analysis
Parameters of common test parameters by pressing the setup key (if parameters are the
same with the previous one, this step is unnecessary) Press the “Common” key, the
common LED will be lit, Then press “Start” to confirm. The instrument will be heated in
accordance with initial temperature T0, when the furnace temperature reaches the
temperature T0, the ready LED will be on, instrument will be controlled automatically
under the following steps.
The instrument is heated in accordance with setup parameters, after one step is finished
instrument will alarm and reset to zero until the entire program finishes.
Finally press “Digit/Reset” key to exit the common analysis program.
22
3 Setup
Do not set the temperature beyond 990 ℃in order to prolong the using life
An Example Program
The GB method for slow ash analysis of coal and coke (GB/T212-2008) specifies the
following steps:
The initial step: set T0=0 t0=0, this is the initial requirement for ash analysis, once the
temperature reaches 0, the corresponding LED will be on, Briefly press start to proceed
an analysis. T0=0 indicates the analysis can be proceeded at any time.
The first step: ramp from room temperature to 500 ℃ in no less than 30 min
The second step: soak in this temperature for 30 min
The third step: continue ramping from 500 ℃ to（815±10）℃

The forth step: soak at （815±10）℃ for 1 h
To set up and run this program, perform the following procedures (refer to 2.1 the slow ash
analysis).
With different parameters, the analysis processes are different. When performing the slow
ash analysis or the quick ash analysis, press the start key at the fifth step, the analysis will
directly enter the sixth step and loop between the fifth and the sixth steps due to the
inspection ignition. While performing the volatile matter and caking index analysis, the first
step will be skipped (except read the temperature parameter), and after the last step (the
sixth step) is finished, it will return to the initial step. But in common analysis program,
once the last step is finished, the instrument will be cool automatically.
MF6100K can be connected with a computer through the internet interface, with which,
the analysis parameters shall be modified by the computer. When using a computer to
23
control the analysis, briefly click the Start Analysis on computer, a dialog with analysis
parameters will pop out, click Confirm to save and transmit the parameters to the
connected instrument, the instrument will perform an analysis in accordance with the
parameters.
3.1 View the furnace Temperature
Switch on the instrument, the instrument is in the initial stage (show symbol “FL000”).
Press start key to view the current temperature of muffle furnace.
3.2 Setup the Calibrated Temperature
Press “Setup” key twice, when displaying “000”, enter the password “618” and press
“Start” key to confirm
The screen displays “000”
Input the calibrated temperature using the hundreds digit, tens digit, digit(where the
hundreds digit indicates the symbol of calibrated temperature, if the hundreds digit is 1 ,it
indicates the negative calibrated temperature, such as calibrated temperature is 11 ℃,you

should input “011”, if the calibrated temperature is “-11”, you should input “111”.
After the data login is finished, press start to confirm.
3.2 View the Calibrated Temperature
Press “Setup” key twice, when displaying “000”, enter the password “207” and press
“Start” key to confirm, and then the screen will display the calibrated temperature.
Press start to reset after viewing
3.3 View the Cooling Compensation Temperature
Press “Setup” key twice, when displaying “000”, enter the password “208”, and press
“Start” key to confirm, the screen will display the cold end compensation temperature.
24
Press start to reset after viewing
3.5 Setup Common Analysis Parameters
A program with three rising temperature steps and three constant temperature steps or 6
rising temperature steps can be set in a common analysis program (Also called 7
temperature parameters and 7 time interval temperatures), each temperature can be set
up to 999℃ and each time can be set up to 24 h. These parameters are set as follows:
a. Press “Setup” key twice, enter the password “111” when “000” is displayed. Press
“Start” to confirm.
b. When T0 which was set previously displays and flashes, we can use “Hundreds digit”,
“Tens digit”, and “digit” to set up temperatures, then press “Start” to confirm.
c. Enter the next parameter setting, previous t0 will be displayed. Press “Hundreds” and
twinkling position will change from the position hours, minutes and seconds (twinkling
position means you can enter the value here). Press “Tens digit”, “digit” to set constant
temperature, then press “Start” to confirm.

d. The order of parameters setting is: T1-t1-T2-t2-T3-t3 (T0,T1,T2,T3,T4,T5,T6 are
temperatures and t0, t1, t2, t3, t4, t5, t6 are time interval parameters).
If some parameters are not need to setup, you can directly skip.
e. After all the parameters are setup, press start to confirm and reset.
3.6 Setup Parameters of Caking Index
Two temperature parameters and one time parameters need to be set in caking index
℃
analysis, each temperature can be set up to 999 and each time can be set up to 24 h.
These parameters are set as follows:
a. Press “Setup” key twice, enter the password “112” when “000” is displayed. Press
25

temperatures and t0, t1, t2,t3,t4,t5,t6 are time interval parameters).
e. After all the parameters are setup, press start to confirm and reset.
3.7 Setup Parameters of Volatile Matter
Two temperature parameters and one time parameter need to be set in volatile matter
analysis, each temperature can be set up to 999 ℃ and each time can be set up to 24 h.
a. Press “Setup” key twice, enter the password “113” when “000” is displayed. Then press

temperatures and t0, t1, t2,t3,t4,t5,t6 are time interval parameters).
e. After all the parameters are setup, press start to confirm and reset
3.8 Setup Parameters of Quick Ash
Two temperature parameters and one time interval parameters need to be set in quick ash
analysis, each temperature can be set up to 999 ℃ and each time can be set up to 24 h.
26

temperatures and t0, t1, t2, t3, t4, t5, t6 are time interval parameters).
3.9 Setup Parameters of Slow Ash
Two temperature parameters and two time parameters need to be set in slow ash analysis,
each temperature can be set up to 999 ℃ and each time can be set up to 24 h. These
parameters are set as follows:
b. When T0 which was set previously displays and flashes, use “Hundreds digit”, “Tens
digit”, and “digit” to set up temperatures, then press “Start” to confirm.
c. Enter the next setting of parameters, previous t0 will be displayed. Press “Hundreds”
and twinkling position will change from the position hours, minutes and seconds
(twinkling position means you can enter the value here). Press “Tens digit”, “digit” to set
constant temperature, then press “Start” to confirm.

d. The sequence of parameters setting is: T1-t1-T2-t2-T3-t3 (T0,T1,T2,T3,T4,T5,T6
indicate temperatures and t0, t1, t2, t3, t4, t5, t6 indicate time interval parameters).
27
Both the slow ash program and the quick ash program can be applied to analysis the ash
in biomass, set the parameters in accordance with the stable 3-2, (Note: all the
parameters in stable are in conformance with GB/T28731-2012 the proximate analysis
method for solid biomass fuel)
3.10 View the Default Parameters
There are default parameters of slow ash, quick ash, volatile matter which are in
conformance with GB/T212-2008, as well as default parameters of caking index in
conformance with GB/T5447-1997 in the instrument memory. View the default parameters
under the following steps:
Press “Setup” key twice, enter the password “118” when “000” is displayed. Then press
All the parameters will be assigned with default value (refer to the corresponding test
program 2.1-2.5)
28
4 Troubleshooting
WARNING
Always disconnect power cord from power supply and Allow furnace
to cool to ambient temperature before servicing instrument.
instrument.
1). There is no display after switching on the instrument, and the indicator of the
electricity power is off: Check if the electricity power wire is in good condition, or the switch
on the backside of the instrument is on and the fuse is damaged or not. Identify the
causes and solve the problem.
2). Continuous alarming after switching on the instrument: Press “Start” key in the initial
stage, if the temperature is more than 1000 ℃, it indicates that the thermocouple is open
circuit, check if the thermocouple and the connection of thermocouple is in good condition.
3).After entering the analysis, the “heat” indicator is on, but the temperature not rises:
Check If the voltage between the third and the forth ends of the solid relay (SSR)
GTJ4-60A is larger than 3.5VDC, if it is larger than 3.5VDC, it indicates the SSR is broken
and replace it.
4). After switching on the instrument, if the instrument is not in the analysis and the “heat”
indicator is off, but the furnace temperature continues to rise: Check the voltage of the two
ends of the heating elements (Be careful with the 220 VAC), if there exists the 220 VAC,
that it means that the solid relay SSR is broken and replace the solid relay.
5). If there is still breakdown not solved, please contact the authorized agent or the
manufacturer.
29
5 Wiring Diagram
30

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CHANGSHA KAIYUAN INSTRUMENTS CO.

, LTD 5E- MF6100K Muffle Furnace

1.1 Safety Attentions ..................................................................................... 7

2.1 Slow Ash Analysis ................................................................................. 14

3.1 View the furnace Temperature .............................................................. 24

3.9 Setup parameters of slow Ash .............................................................. 27

5 Wiring Diagram ...................................................................................... 30

are not covered by this warranty.

due to accident, abuse, neglect, or use in disregard of instructions furnished by CKIC. In

CKIC shall not be liable for incidental or consequential damages whatsoever.

comply with these notice requirements.

Changsha Kaiyuan Instruments Co., Ltd.

neglect of instructions or misuse of this instrument resulting from misunderstanding the

instruction manual. The installation or commissioning operated by our professional

engineers is not included.

refer to the packing list received with the instruments.

programs and instruction manual. It is subject to change without notice.

This symbol indicates a caution. (Specific instructions are

This symbol indicates a risk of electric shock. (Specific

This symbol indicates a high temperature surface. (Specific

This symbol indicates being corrosive. (Specific instructions

Note: non-important procedure may be not instructed in this manual,

Do use the original standard power cord.

cause voltage instable.

there is no gas leakage

1.2 Alert Signals

Alert signals are highlighted in this instruction manual.

High temperature hazard alert you to a possibility of

personal injure if you come in contact with a

surface during use or for a period of time after use.

Refer to the instruction manual for better operation.

This symbol indicates a risk of electric shock.

(Specific instructions are referred to the manual)

This symbol indicates a pinch point, you should

watch your hands while operating (Specific

instructions are referred to the manual)

treatment of some other objects.

5E-MF6100K muffle furnace is designed to work independently or be controlled by a

provided by computer on the screen.

1.5 The Main Parameters and Functions

1). Rated Temperature: 1000 ℃

3). Temperature Range: 300 ℃~999℃

5). Average Temperature Stability: ±2℃

6). working environment: Ambient Temperature 0 ~40 ℃ ℃

7). Power Supply: 210~230 VAC, 50±1Hz

well as the rising temperature rate can be set.

d).It will alarm if the thermocouple is broken or over-temperature.

f).The furnace door locked automatically during analysis.

an abnormal temperature, an alarm will sound.

f).Multiple muffle furnaces can be controlled by one computer.

1.6 Working Environment

Environmental temperature: 5 ℃～40℃

are allowed in this laboratory.

hear an indicating sound of the keyboard.)

instrument), and choose the desired function.

second”, it is used to display the analysis time.

Steps Parameters Illustration

Temperature T0 0 ℃ The analysis can be started at any