Jotun Adhesion Test Report

Pull-Off Test Method

01-ATR-PERT-NK-
Date: 29 May 2022 Report No:
AMM-2022

Project Name: Pembangunan Dermaga Terminal LPG Pressurized Kupang – (Piping)

Contractor / Phone
Nindya Karya n/a Email n/a
Applicator No.
Phone 0813351265 Abdul.kodir@jotun.
Jotun CA Abdul Kodir Email
No. 98 com
Phone 0852512233
Applicator Supervisor Rahmanu Email -
No. 48
Site / Work Location Workshop NK – Plant ID Number: Test Pipe (Mock up)
Tenau, Kupang
Drawing No. / Paint System :
Specification Penguard HB Grey 1 x 150 µm
Reference: Futura Classic RAL 9003/3023 2 x 80 µm

Coating System:
Average
Ave. DFT Temperature
(10 Readings) Time Cured During Cure
Date Coating
Coating Before
Product Name Applied to µm mils °C °F
Sequence Overcoating
Substrate
(H:M)

Primer Unidentified n/a n/a n/a

Intermediate
Penguard HB grey n/a n/a N/A
1
Intermediate Futura Classic
n/a N/A N/A
2 9003/3020
Futura Classic
Topcoat n/a n/a N/A
9003/3020

Adhesive used to Fix Dolly

Adhesive Average
Mix Cure Time Temperature
Brand Batch No. °C °F
Ratio (Days or during cure
Hours) of adhesive

Araldite N/A 1:1 1 Day 30 deg C

Surface Temperature of Substrate and RH%

Surface Temperature & RH
Deg C° 31 Deg F° - RH% 68
when dolly placed
Surface Temperature & RH
Deg C° 30 Deg F° - RH% 61
when dolly pulled

Test conducted on Structure or Test Plate Test Plate Structure

Test Plate No. /
Test Pipe (Mock-up) N/A
Structure ID No.

Page 1 of 7
Jotun Performance Coatings Inspection Form I Adhesion Pull Off Rev 3 January 2016
 Jotun Adhesion Test Report
Pull-Off Test Method

International Standards special conditions of adhesion test:

Lightly
Abrade & Cut around Number of Load Pull
Ambient
Test Clean the the dolly Adhesion Rate and
surface Conditions
Standard before Tests per Maximum
before fixing During Test
testing? Sample Pull Time
dolly?
Apply a tensile
stress,
Yes, all increasing at a
6, calculate Carry out test
thickness at 23°C ±2°C rate not
the average of
ISO 4624: unless the 6 tests and at 50% ± greater than 1
Yes.
2003 otherwise and record as 5% RH or as MPa/second
specified or the result agreed. and complete
agreed the test within
90 seconds.

Follows ISO
4624 but
NORSOK specifies an
Follows ISO automatic Follows ISO Follows ISO Follows ISO
M-501 Rev
4624 4624 4624 4624
6 pulling device
with centred
pulling force
Generally No.
Only sand or 3 per test site.
clean the Report can be Apply a tensile
No as per the stress less
surface in a for individual
standard. If than 150 psi /
manner that test, omit
agreed, then second (1
will not affect lowest and
ASTM D cutting must MPa/ Second )
integrity of the highest and Not specified
4541 be reported as and complete
coating or average the
a variation to the test in less
leave a remainder or
the standard than 100
residue. Only average all as
test. seconds.
sand with 400 specified or as
grit abrasive agreed.
paper or finer.

Use acetone Yes, if the

coating is Gradually
solvent to
elastomeric or increase the
clean the
greater than load on the
surface then Record the
500µm use a dolly with a
lightly abrade 3 per test site surface
hand drill and rate of
AS 3894.9 with P220 grit saw to cut to and record temperature
increase force
Method C abrasive paper substrate. May each individual and RH% at
of 0.1 MPa
to de-gloss be omitted for result the time of
/second.
and clean rigid coatings test Complete test
again with less than 500 within 90
acetone µm seconds.
solvent

This Test Conducted according to:-

ISO 4624
NORSOK M501 Rev 6
ASTM D 4541
AS 3894.9 Method C

Page 2 of 7
Jotun Performance Coatings Inspection Form I Adhesion Pull Off Rev 3 January 2016
 Jotun Adhesion Test Report
Pull-Off Test Method

Coating Adhesion Range as per Project Coating Specification:

From MPa To MPa From psi To psi

3 MPa 3 MPa N/A N/A

Fixed- Self-Aligning Self-Aligning Self-Aligning

Adhesion Tester Used as Alignment Type 111 Type 1V Type 1V
described in ASTM D4541 Type 11 (push off) (Manual (automatic)
)
 Which type used - - -

Elcometer Elcometer Elcometer

Elcometer 108 506 510
Typical Model Name
106 Elcometer PosiTest PosiTest AT-A
508 AT-M ATA20A

Serial Number - - - AT15342

Result of Test:
DFT Was
Before DFT After cutting tool Result
Abrasion Abrasion used? Failure
Test Date Dolly Date Dolly Mode as
No Microns Mic Placed Pulled MPa psi per chart
ron Yes No below
s

May 28,
1 284 May 29, 2022 Yes 11.00
2022
May 28,
2 270 May 29, 2022 Yes 5.27
2022
3

6
Average MPa/psi
3 Samples 8.13

Adhesion Test Meets or

Yes No
Exceeds Specification

Page 3 of 7
Jotun Performance Coatings Inspection Form I Adhesion Pull Off Rev 3 January 2016
 Jotun Adhesion Test Report
Pull-Off Test Method

Description of failure mode to ISO 4624: 2003

Y/Z = Adhesive failure between

Z = dolly adhesive and dolly

Y = Cohesive failure of adhesive

Y = adhesive

-/Y = Adhesive failure between

F = 5th coat final coat and adhesive

n /m = adhesive failure between

the nth coat and the nth coat of a
multi coat system
E = 4th coat
n = cohesive failure of the nth coat
of a multi coat system
D = 3rd coat

B/C = Adhesive failure between

first coat and second coat

C = 2nd coat
B = Cohesive failure of 1st coat

B = 1st coat
A/B = Adhesive failure between
substrate and first coat

A = Cohesive failure of the

A = substrate
substrate (e.g. concrete or wood)

Page 4 of 7
Jotun Performance Coatings Inspection Form I Adhesion Pull Off Rev 3 January 2016
 Jotun Adhesion Test Report
Pull-Off Test Method

Dolly #1

Reading: 11.00 MPa

70 % Cohesion C
30 % Cohesion B

Dolly #2

Reading: 5.27 MPa

60 % Cohesion B
25 % Adhesion B/C
15 % Cohesion D

Page 5 of 7
Jotun Performance Coatings Inspection Form I Adhesion Pull Off Rev 3 January 2016
 Jotun Adhesion Test Report
Pull-Off Test Method

Jotun CA Notes:

This Pull Off test carried out for trial to find out adhesion value of paint on mock-up (pipe) that have
conducted by applicator self as per actual treatment and application on field.
Average value Pull-Off test is 8.13 MPa from two points & more than minimum requirement
3.00 MPa

Name Date Signature Print Name

Applicator Rep.

Manufacturer Rep.

Contractor Rep.

Client Rep.

Jotun CA Abdul Kodir Sign Name:

Date: 01 June 2022

Page 6 of 7
Jotun Performance Coatings Inspection Form I Adhesion Pull Off Rev 3 January 2016
 Jotun Adhesion Test Report
Pull-Off Test Method
PHOTOGRAPH REPORT

Mock up pipe DFT check in progress Use “Araldite” as adhesive

Install dolly in progress and it result Cut around the dolly was done

Pull-Off test on progress and start from zero 0.00 Mpa Dolly 1 reading 11.00 MPa

Dolly 1 reading 11.00 MPa Average Pull-Off result 8.13 MPa and witnessed by all parties

Page 7 of 7
Jotun Performance Coatings Inspection Form I Adhesion Pull Off Rev 3 January 2016