Date

Expt. No. Page No. 1

PREPARAT1ON OF POTASH ALUMLka5oy Al[sy)a1 Hz0)

AIM F THE EX PERIMENT

lo prepoRe tnySialline Sali 04
poA asn alum

CHEMICDLS RE OUIRE D
)Po assumn Sulph.ak.
ALumiDzum sulphak

DPP AROTOS REG OI RE D

Two beakens a50 mi 2) China basin
) unnel 4) Fudr ahenS.and sCalasSx.n 6) ash botLe
) Tru pod Slane- ) the qauZe.

PROCEDURE
) The poass um sulphak cnySials oene ekenin
L aso m beaken aod oene_dissdlved 0t mintmum quanh
Shnig29 Simarly he iumintum Su]phat|
cnyb-alS Oeneaken tn_aDDher be.akgn and o ene dissoly ed
w mn rmum quanhhes of ookn hen a b 5nl d i l E ,
LOOS adde q to he Bluminum sulphak solunnn to ch etk
by drolysb(3 unbiiH PensSh he Soluhon oini hl ened
0tnenO1Se hene is no neceSsit oi hih ahon) Haen both he
501u on> ane mtx eq togdhen and ethe aken i a chna qsk
O Q . s he a ed to Con erDnak up n he cay a l k sChon K a n t

LOL conytam shnao s

5 oon as the CAYGANLSOton Poini

O &S ne ach e meheahng U0a9 }o Pp eq and he SoD oas

a ll.ood o t o o l Ohout dilutban ce

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Expt. No. 1 PageNo.

23) 3en
93-1en cool tng otHaheq ral tny biols o poiash alum SePanakeq
ou e an hen ltguOn O . qec ameq oui and the tny>>eil
Cne collet e to a tu ert pap en

CHEMLCHL REC STO1CHIoMETRy

Ka5y Pl y) 16 Da0 +6a0 /10 2.5

t10 q5
Kay Blz ) 2 Ha0
SERyAT1ON
)LO elghi oi the_day 5ample
oloun o he dhu S ampe = ohtk
) Shope oi #oe cny Sta) OLHa hediaj

20dyananda Tara tdan

UC 3 Seme sty
Kol No bS19 O&1

1 6 1 1 4

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Expt. No. Page No. 4

AIMOF THE E XPERIMEINT

Ded ermine henat tonstcin nte qnca

n a k ion Soni) icn audcad alys eq hydrcty sis or m ths

ad nsom km usin.a hycnpthleniL auq

PR I PLE
ESens eD e atmeni wth a minkLal ac[caBal451
alcohal.
undenaD hyatlusi to iarm azL ons an

MAh Acehi au) (Meth alLoboi

akia k
Aoilcn acua minanal ai octs as a casly51 onc
soDLenin ohon does Doi_chang e_durin.q he tounSt a1
neathen n his n eataon thR 1Qe OA neai on deperqs

Laia XCess 15 caled ps ecudoupLo0lecculan

acn drelu Sis i5finS On qe uH eSPed to he esStr

Rat neatHon Lon hydroySs )=Kekn)

Loheru ki raR consen
n eqnadeq mak te.nS an ortha Necichon is qtven by
>0 lo9 a
h ne C n t a l contenaHon O he E 9eh

(T1 aretak)
C Lonenatton o eStn alRA tme

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Ept. No. Page No. 6

HSheachon prro Ce ed45 he mclan centennation 0 onqanic auc

conuously in n eases on he etnminaton oi r a t cenSHen1 O1 l
neahon O KnooD rol ame 04 heeoldopn mix tine is cnaon
a negulan in-lenvals and hen hnarq gain5iSHanq and Sodum
hycnoiqe clution

REQUREMENTS
Mo aceLe ) 2I m) o NaOH
bune lk San v)PLplk v ) phenopth ulne v)Raathtom
boles

PROCE E DUR E
Ca) Rade ons n om expetimenal yalues he
d e enm1nOhon r a t e tonStani nY olves h Åol oLoing leps
) c urQ}ely measune d i00 ml 04 N2 HC1 ts taken n G aD ml

ne athon boHle and 5 m0fmehl aetak cs addenJo HCI

i m e z e n o hme) is noied coh en aboul aml01 mtthhl Qtt fa

ino he eanon bo t1e

IS hans-Jened

") AAen dhhough mix

oDte_plpeHe in Ane tonual Alaskcotanng zIe-cold
LOaten 1S heo HmQLc wth StandaLq ( u ) NaoH oluton
usingphenop-tnal1 cs tndLeaoNBH
uSina e end Poin a pale
P enmonen t_Piok COloun appecInS

) Noo u negulan Tderrals L5 mn eSame olume 0

he neQcHon mxune 1s OLHndhQLon anq Htaed t o NaoH Ib
he Same mcanin. he vol 0 NaOR UKe d wfh_HMe ako as k_

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Expt.No. PageNo.

iv) fon Hhe tnal tidn ak valueli e a e com Pl thtor of eathon)5

m l D H eachon tS mixtune S aken in h e nound bo omed

lask 4ene wih an Londenson 1 houte d tOatn

bath a 0-10 on an houn he ton ents 0J he AlaSk c re
uanhiaAvely hanSp eneq ino a tenical 1aSk ond hen Hinak

h t n a k ralue Jound 15 Y
QgainS Senqarq NaOR

ObSE RYDTION AND CALCULDT1ON

zeno ime Vo
Yolume 0 N/10 NaH usecol
Vol of NaOHuseq a SdLonds
Yolume DN/LO NoDHuseq Loben nec? Lomplek V

o n e mole 04 Oa tno n
nom he chemical neatton Oe Seen O
bydnolusis qves one mole01 ongarn aLc e Say ha1,
nia
ConC () is phoponhonal tu(Y» Vo)
h e ombun4 0ngan uq
een neaCteq
40med is equal o h e amouni OJ

hs ( a - ) on Y , ) Y ) o a-) a(VaX)
}enLe
k 3 0) o8 7a

a.03
Vio Y
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t. No. PageNo. 1 b

REORD

ame o Vol o i
VipV
e Von: Y4
AlaDH t
ml
-
O0 O.004
O. o2
3 660
1 .O03 D
qOO -0.9 10.3 o.6341
5 aoD 0.5 10.3 0.31

O
6
Canaph 6 no shoD qnaphitally hai neciS 0i haj nsi ondan plo
be values o O Ca-)e o V) as ordin at 0qanS
e onnes pon ding valtues 04
i m t n mn o cunve mus b e S J1ne

CDNCLD51ON
he ira tonG Aon bydnolySiS 01eSty 1 o u n c
00 30) O,00O
be-0.

atyananda Tauidan
DG 3 Semestn
Rol No b5 19 S
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Expt. No. Page No. I L

AiM OF THE EXPERIMENT

hepanaton o : d o ttnoloenzene.

CHEMICALS REQURED
)Ntnobenzene 1.5 m
2tuming_ HNO sepLELgnaviy LS mn

PROCEDURE
Mx Aml: umin DttnucacLGand 16m. ton. taSOu4
inaA50 m Ound bolton t)ed cu heiax cond en>Dh

hen oqd nAnolo en zene ip Hsialmen- of aoou Im hom

o coD qensa and hake dhe \abktonmixingha
neocHon pioducs

) Due lo ex DAo eimLc nquneAq ealDD he mx tue btone boj

and Ccqunes a deep bj opncoLour

)Ber he addihon d all the ptAnoloeDzenePlate e tla sk

0ak bah and hea fo about9 mig-

) his laqe a i e m d ops n eacon mx ue era paePanea

w Lol o a A an Lo a hand PMak yello tD Solcq
SepaateS hen e h eCthny (SdiSL0D Ho ueq

h e necn m u une ls ooleq Inq the ContnS pounec unfy

vtg ouneq h o0Inoy InD uou 500
) oar tomdainng
eto pLeeS of e Lohen m d i n tinp aenzene &CRaak

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Expt. No. PageNo.13

a barc yell ow 5olzd

t h e eld o1 mdinitmoo enzene 1s aprsm RengShaltne

0 cuae produu inom nech ied Srit LOen pcle 9etoo
Cnus QlS of m-qiD ttoo en zene methng foin AD ane obliI

REACT1dN
N2
NO2

HHO tHa
NO
m- Cdinthobenze ne

Satananda jaatea
Ut b Semesitn
Kol no BS-P -19-oj

pret
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