Chemical Engineering Department Mass Transfer- I(3340502

Observation:-
1. Room temnperature 3 0c
2 Volume of Acetic acid ml
Volume of Benzene
4. Volume of Water
. Volume of extract layer
96ml
6. Volume of raffinate layer ml
Density of Acetic acid
S gm/cc
8. Density of Benzene
9. Density of water
--87gm/ce
gm/cc
Extract:
Burette: 0.1N NaOH Solution
Pipette:-10 ml dilute solution
Indicator:-Phenolphthalein
End Point: Colorless pink
-

to

Observation Table:-

Initial Final
Sr.
Burette Burette
No. Difference Mean
Reading Reading Difference
H8. H8.2
3. S1O SI O
4.
0.0 9.3 ug. 3
9 5

Raffinate:
Burette: - 0.1N NaOH Solution

Pipette:-1Oml dilute solution (Raffinate +Water)

Indicator:-Phenolphthalein
End Point: - Colorless to pink

Government Polytechnic. Valsad

 Chemical Engineering Department
Mass TransferT-I3340M

Observation Table:

Initial Final
Sr.
Burette Burette Difference Mean
No.
Reading Reading Difference

423
3.
O
14-2
4.4 1413
4.

Calculation:-
For EXTRACT:
1. Normality of Acetic Acid

N V Na V2
N NV2/V
O-1xu.S/!o
O. 9 S
For 10 times dilution,

S
2. Concentration in gm/L =

equivalent weight X Normality

60 X 4. s

294em/L.
1000ml aT gm
5ml
gm of Acre Aud
6.038 m of ccidc Hed
Phu

gm of Acetie Acid.

Government Polytechnic, Valsad

 = Mass/Volume
.Density
Volume = Mass/Density

16.038/1O5
IS.2
ml of Acetic acid.

For RAFFINATE:-

1. Normality of Acetic Acid

NV N V2
N NV2/Vi
oxju2310

For 10 times dilution,

X 10
-1.N
2. Concentration in gm/L equivalent weight X Normality
60XN:q23

&Sgm/L
F5,38 gm
1000 ml
2 ml 792

3 5.38xa/toou
.929
Acetic Acid.
gm of

= Mass/ Volume
3. Density
= Mass/ Density
Volume = 1 7929/1.05

acid.
1.70 nlpf Acetic

9-3m Benzene
a - 1 .?
16.g28m/m
0.&H =

19-3 x
.792 + t692 9.41
A Berzen
Government Polytechnic, Valsad
wttracthon
18- 0 dSS
Chemical Engineering Department
Mass Transfer I (3340502)
Result

Weigh
Fouhon
Xi = 0 0 a s
Perceg
Weight Fractien;
N95%
Y Od43 Y6-3%

Conclusion:

for Exteacu luyu

S6-15.27 Ho.13
o.13x05 u2.76
42.4C+ IS.44 =58.03
1527
S& 03
= 0.363 w hracthoy