Scribd Logo
Upload

Welcome to Scribd!

  • 11 views

    1H NMR Standard - TriPhenylPhospheneOxide

    Uploaded by

    daniel sihyun
    This document contains the NMR spectrum and associated experimental parameters for a sample containing triphenylphosphine oxide. The NMR spectrum shows peaks between 7.68 and 7.26 ppm. The document provides details on the instrument used, acquisition parameters, processing details and experimental conditions.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Flag for inappropriate content

    You might also like

    1H NMR Standard - TriPhenylPhospheneOxide

    Uploaded by

    daniel sihyun
    11 views2 pages
    This document contains the NMR spectrum and associated experimental parameters for a sample containing triphenylphosphine oxide. The NMR spectrum shows peaks between 7.68 and 7.26 ppm. The document provides details on the instrument used, acquisition parameters, processing details and experimental conditions.

    Original Description:

    Original Title

    1H NMR Standard_TriPhenylPhospheneOxide

    Copyright

    © © All Rights Reserved

    Available Formats

    PDF, TXT or read online from Scribd

    Did you find this document useful?

    Is this content inappropriate?

    Report this Document
    This document contains the NMR spectrum and associated experimental parameters for a sample containing triphenylphosphine oxide. The NMR spectrum shows peaks between 7.68 and 7.26 ppm. The document provides details on the instrument used, acquisition parameters, processing details and experimental conditions.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Flag for inappropriate content
    Download as pdf or txt
    11 views2 pages

    1H NMR Standard - TriPhenylPhospheneOxide

    Uploaded by

    daniel sihyun
    This document contains the NMR spectrum and associated experimental parameters for a sample containing triphenylphosphine oxide. The NMR spectrum shows peaks between 7.68 and 7.26 ppm. The document provides details on the instrument used, acquisition parameters, processing details and experimental conditions.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Flag for inappropriate content
    Download as pdf or txt
    of 2

    7.

    68
    7.66
    7.65
    7.63
    7.56
    7.54
    7.52
    7.47
    7.47
    7.45
    7.45
    7.44
    7.43
    7.26
    Triphenylphosphine Oxide Current Data Parameters
    NAME SP19-226-E6_Wittig_STD_Ylide_02_2
    EXPNO 1
    PROCNO 1

    F2 - Acquisition Parameters
    Date_ 20190314
    Time 22.17 h
    INSTRUM spect
    PROBHD Z108618_0422 (
    PULPROG zg30
    TD 65536
    SOLVENT CDCl3
    NS 8
    DS 2
    SWH 6410.256 Hz
    FIDRES 0.195625 Hz
    AQ 5.1118078 sec
    RG 139.37
    DW 78.000 usec
    DE 6.50 usec
    TE 298.1 K
    D1 2.00000000 sec
    TD0 1
    SFO1 400.2224013 MHz
    NUC1 1H
    P1 15.00 usec
    PLW1 14.25000000 W

    F2 - Processing parameters
    SI 65536
    SF 400.2200093 MHz
    WDW EM
    SSB 0
    LB 0.30 Hz
    GB 0
    PC 1.00

    10 9 8 7 6 5 4 3 2 1 ppm
    -0.00

    -0.00
    0.03
    5.94
    3.00
    5.97
    0.01
    0.00

    0.00

    0.01
    0.25
    0.25

    0.10
    7.68
    7.66
    7.65
    7.63
    7.56
    7.54
    7.52
    7.47
    7.47
    7.45
    7.45
    7.44
    7.43
    7.26
    Current Data Parameters
    NAME SP19-226-E6_Wittig_STD_Ylide_02_2
    EXPNO 1
    PROCNO 1

    F2 - Acquisition Parameters
    Date_ 20190314
    Time 22.17 h
    INSTRUM spect
    PROBHD Z108618_0422 (
    PULPROG zg30
    TD 65536
    SOLVENT CDCl3
    NS 8
    DS 2
    SWH 6410.256 Hz
    FIDRES 0.195625 Hz
    AQ 5.1118078 sec
    RG 139.37
    DW 78.000 usec
    DE 6.50 usec
    TE 298.1 K
    D1 2.00000000 sec
    TD0 1
    SFO1 400.2224013 MHz
    NUC1 1H
    P1 15.00 usec
    PLW1 14.25000000 W

    F2 - Processing parameters
    SI 65536
    SF 400.2200093 MHz
    WDW EM
    SSB 0
    LB 0.30 Hz
    GB 0
    PC 1.00

    8.4 8.2 8.0 7.8 7.6 7.4 7.2 7.0 6.8 6.6 6.4 6.2 6.0 5.8 ppm

    -0.00
    0.03

    5.94

    3.00

    5.97

    0.01

    0.00

    0.00

    You might also like