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GEST 94 204 Edition 1 (Pneumatically Operated Valves For Use On Storage Tanks For Liquid Chlorine)
GEST 94 204 Edition 1 (Pneumatically Operated Valves For Use On Storage Tanks For Liquid Chlorine)
GEST 94/204
March 1999
First Edition
Euro Chlor
Euro Chlor is the European federation which represents the producers of chlorine
and its primary derivatives.
***********
This document has been produced by the members of Euro Chlor and should not be reproduced in
whole or in part without the prior written consent of Euro Chlor.
It is intended to give only guidelines and recommendations. The information is provided in good
faith and was based on the best information available at the time of publication. The information is
to be relied upon at the user’s own risk. Euro Chlor and its members make no guarantee and
assume no liability whatsoever for the use and the interpretation of or the reliance on any of the
information provided.
This document was originally prepared in English by our technical experts. For our members’
convenience, it may have been translated into other EU languages by translators / Euro Chlor
members. Although every effort was made to ensure that the translations were accurate, Euro Chlor
shall not be liable for any losses of accuracy or information due to the translation process.
Prior to 1990, Euro Chlor’s technical activities took place under the name BITC (Bureau
International Technique du Chlore). References to BITC documents may be assumed to be to Euro
Chlor documents.
Chlorine is essential in the chemical industry and consequently there is a need for
chlorine to be produced, stored, transported and used. The chlorine industry has
co-operated over many years to ensure the well-being of its employees, local
communities and the wider environment. This document is one in a series which
the European producers, acting through Euro Chlor, have drawn up to promote
continuous improvement in the general standards of health, safety and the
environment associated with chlorine manufacture in the spirit of Responsible
Care.
It has been assumed in the preparation of these publications that the users will
ensure that the contents are relevant to the application selected and are correctly
applied by appropriately qualified and experienced people for whose guidance they
have been prepared. The contents are based on the most authoritative information
available at the time of writing and on good engineering, medical or technical
practice but it is essential to take account of appropriate subsequent developments
or legislation. As a result, the text may be modified in the future to incorporate
evolution of these and other factors.
This edition of the document has been drawn up by the Equipment Working Group
to whom all suggestions concerning possible revision should be addressed through
the offices of Euro Chlor.
TABLE OF CONTENTS
1. OBJECTIVE 8
2. DEFINITIONS 8
2.1. Pneumatically Operated Valve 8
2.2. Internal Valve 8
2.3. External Valve 8
2.4. Pneumatic Actuator 8
2.5. Manual Override 9
2.6. Accessories 9
3. VERIFICATION OF THE VALVE 9
4. BASIC FUNCTIONS 9
5. DESIGN PRINCIPLES 10
5.1. Valve Type 10
5.2. Compatibility with the Storage Tank 11
5.3. Inspection and Maintenance 11
6. VALVE OPERATION 11
6.1. Normal Operation 11
6.2. Failure of Pneumatic Pressure 12
6.3. Manual Control 12
6.4. Emergency Closure 12
7. PRESSURE DESIGNATION 12
8. PRESSURE-TEMPERATURE RATINGS 13
9. NOMINAL SIZES 13
10. EXTERNAL VALVE DESIGN 13
10.1. Body 13
10.1.1. General 13
10.1.2. Body Wall Thickness 13
10.1.3. Body End Ports and Seat Bore 14
10.1.4. Drain Tapping 14
10.1.5. End Flanges and the Body to Bonnet/Cover Flange 14
10.1.6. Flange Facing Finish 15
10.1.7. Centre-to-Face Dimensions 15
10.2. Bonnet/Cover 15
10.3. Pneumatic Actuator Mounting 16
10.4. Disc and Disc Nut 16
10.5. Body Seat and Disc Seat 17
10.6. Stem 17
10.7. Bellows Seal 19
10.8. Auxiliary Stuffing Box 19
10.9. Bellows Leakage Detection Tappings 20
10.10. Indicator 20
10.11. Bolting 20
10.12. Soft Seal Ring 21
10.13. Mechanical Strength 21
20. MARKING 38
20.1. Required Marking 38
20.2. Body Marking 38
20.2.1. External Valve Body 38
20.2.2. Internal Valve Body 39
20.3. Identification Plate Marking for External and Internal Valves Details 39
20.4. Identification Plate Marking for Pneumatic Actuator Details 39
20.5. Additional Body Marking and Identification Plate Marking 40
21. PREPARATION FOR DESPATCH 40
21.1. General 40
21.2. Painting 40
21.3. Drying and Blanking 40
21.4. Disc Position 42
22. REFERENCES 42
FOREWORD
Pneumatically operated valves for use on storage tanks for liquid chlorine need to
satisfy a number of basic functions and technical characteristics so different to
other types of valves. The functions and characteristics necessary to satisfy the
Euro Chlor safety criteria for the containment of liquid chlorine are given in this
document which covers design, manufacture, materials, examination, testing and
verification.
The procedure for Euro Chlor verification of pneumatically operated valves for use
on storage tanks for liquid chlorine is given in GEST 94/201 - Procedure for
Verification of Pneumatically Operated Valves for Use on Rail and Road
Tankers and ISO-Containers for Liquid Chlorine.
NOTE: Where this document uses the term “agreed”, this means “agreed in
writing” between the valve manufacturer and the buyer.
1. OBJECTIVE
2. DEFINITIONS
For the purposes of this Euro Chlor document the following definitions apply:
A spring loaded check valve which protrudes into the storage tank. The
internal valve is opened by the downward movement of the stem of the
external valve when the external valve is opened.
A globe type angle valve which is mounted on top of the internal valve,
external to the storage tank.
A device which is fitted to the body of the pneumatic actuator and which
allows manual operation of the external valve stem.
2.6. Accessories
Devices such as position indicators, micro switches, bellows leakage
detectors, etc.
Note: The procedure for inspection and testing prior to Euro Chlor
verification is given in GEST 86/129 - Procedure for an
Independent Assessment of Valves for Use on Liquid Chlorine,
Prior to Consideration for Euro Chlor Homologation.
4. BASIC FUNCTIONS
a) Allow safe transfer of liquid chlorine into an out of the storage tank;
b) Provide an external valve capable of a tight seal against the passage of
gas or liquid;
c) Close rapidly;
d) Provide, within the storage tank, a tight seal in the event of failure of the
external valve body;
e) Provide remote operation.
1) A valve, called the internal valve, located within the storage tank. It shall
be operable remotely, close rapidly and ensure a tight seal within the
storage tank. In the case of failure of the motive fluid to the pneumatic
actuator, the internal valve shall close automatically, as well as the
external valve.
2) A globe type angle valve, called the external valve, which is located
outside the storage tank and directly mounted on the flange of the internal
valve. The external valve shall be leak free, designed and located in such
a way that, in the event of impact, the internal valve will not be damaged.
This may be achieved by, for example, the inclusion of a breaking zone or
designed failure point.
During the transfer of liquid chlorine it should always be possible to close the
valve rapidly and remotely to ensure safe operation. In the case of
emergency closure, the internal valve should remain gas and liquid tight in
such a manner as to permit suitably trained personnel, using appropriate
protective clothing and equipment (see GEST 91/171 - Personnel Protective
Equipment for Use with Chlorine) to carry out any necessary repairs.
5. DESIGN PRINCIPLES
The external valve shall have a stem and disc which is directly in line with
the internal valve ball/disc.
The design of the pneumatically operated valve shall allow the individual
components to be adequately inspected and readily maintained.
6. VALVE OPERATION
Still further movement of the stem shall move the internal valve ball/disc from
contact with the seat and compress valve spring. Finally at full stroke both
the external valve and the internal valve shall be open and the actuator
spring(s) and internal valve spring subject to compressive forces of such
magnitude as to cause, upon release of pneumatic pressure from the
diaphragm:
The manual override shall permit the manual control of the actuator stem and
the external valve stem.
7. PRESSURE DESIGNATION
8. PRESSURE-TEMPERATURE RATINGS
9. NOMINAL SIZES
10.1. Body
10.1.1. General
The minimum wall thickness of the valve body shall comply with the data of
Table 1.
Nominal size Body & bonnet Body end port inside diameter
thickness min. and seat bore ± 5%
NPS DN Class PN 40
300 (mm) (mm)
(mm)
1 25 6.3 7.0 25
1½ 40 7.9 8.0 40
2 50 9.5 9.0 50
3 80 11.9 10.5 80
4 100 12.7 12.0 100
The branch end port and the seat bore shall be circular and not less than the
dimensions appropriate to the nominal size of the valve.
The flow-way area between the body end ports shall be not less than the
branch end port area.
The end flanges and the body to bonnet/cover flange shall be forged or cast
integral with the body except that the branch flange may be attached by
welding. In which case the branch flange shall be a forged welded neck type
attached to the body by a butt weld. Welding shall comply with the
requirements of Clause 16.
End flanges for PN 25 and PN 40 valves shall comply with the requirements
of ISO 7005 and end flanges for Class 300 valves shall comply with the
requirements of ASME B16.5. The branch flange facings shall be one of the
types shown in ISO 7005 for PN 25 and PN 40 flanges and ASME B16.5 for
Class 300. The buyer shall specify the type of facing required for the branch
flange.
The bottom flange shall have male or tongue facings for connection to the
internal valve flange (see 11.3).
In the case of branch flanges with raised faces, the gasket contact surface
shall be either a serrated-concentric or serrated-spiral finish with a surface
roughness between 3.2 and 6.3 µm Ra.
The gasket contact surface finish of other types of facings for branch flanges
shall be specified by the buyer.
The gasket contact surface finish of the body to bonnet/cover flange and the
bottom flange shall be appropriate to the types of flange facing and be
suitable for the gasket materials.
10.2. Bonnet/Cover
Integral bonnet stuffing boxes with no welds directly separating the process
fluid from the atmosphere are preferred.
Welding is permitted in order to assemble the bellows into the bonnet. Weld
quality shall be inspected and demonstrated to be satisfactory.
The minimum wall thickness of the bonnet/cover shall comply with data of
Table 1.
The bonnet/cover flange bolting shall be by studbolts with a nut at each end
except that studs may be used for valve nominal sizes DN 25, DN 40, NPS 1,
NPS 1½. Where agreed studs may be used for larger nominal sizes of
valves. Studbolts/studs shall comply with:
The mounting for the pneumatic actuator shall be in the form of a yoke which
may be integral with, or separate from, the bonnet/cover or in the form of a
bridge/flange mounted on pillars. The pillars shall be through bolted and
securely held in place with hexagonal nuts. The pillars shall not be used for
the body to bonnet/cover flange joint fastenings.
The disc shall have a bevelled seating surface and be securely attached to
the stem, independent of the valve assembly, whilst permitting correct
alignment and proper seating. The disc nut shall be securely locked in place
to prevent loosening in service. The seating surfaces of disc and seat shall
be designed to give either line or very narrow area contact.
The minimum radial clearance between the outside diameter of the disc and
the inside surface of the body shall be as shown in Table 3.
When the disc is in the fully open position, the minimum flow area between
the disc and the seat or disc and body shall be not less than the area of the
branch end port.
Any contact between the bonnet and the disc or disc nut shall not allow the
trapping of fluid within the bonnet.
10.6. Stem
The stem shall be of the rising, non-rotating type which shall be prevented
from rotating by provision of a spline or similar arrangement.
The stem shall be of one piece design, having one end suitable for
connection to the stem of the pneumatic actuator.
The surface of the external valve stem that moves within the packing shall
have a surface finish of 0.4 µm Ra or smoother.
The out of roundness of the external valve stem (the difference between the
maximum diameter and the minimum diameter measured at the same cross
section) that comes into contact with the gland packing, shall not exceed 0.01
mm.
Prior to assembly the external valve stem shall not deviate from straightness
by more than 0.005% of the length of the stem.
The bellows seal arrangement shall prevent leakage past the external valve
stem to atmosphere.
The bellows shall have a minimum of two plies. The bellows shall have a
guaranteed minimum life of 10,000 cycles (fully opened to fully closed) at the
maximum allowable working pressure of the valve at 20°C i.e.:
a) PN 25 25 bar g
b) PN 40 40 bar g
c) Class 300 51 bar g
One end of the bellows shall be welded to the external valve stem and the
other end to the bonnet/cover. Welding shall comply with clause 16.
A number of options for welding the bellows to its supporting rings exist. It is
preferred that the supporting rings and the bellows are of the same material.
The drawing shall clearly identify the materials of the bellows and supporting
ring separately.
The bellows shall not protrude into the main area of flow for top vessel outlets
or except when debris collection is a known problem e.g. for bottom outlet
valves..
The external valve shall have an auxiliary packed gland external to the
bellows to prevent leakage to atmosphere should the bellows fail. The gland
shall be externally adjustable.
The stuffing box shall be integral with the bonnet/cover except as permitted
by 10.2. It shall be flat bottomed and have a minimum depth suitable for at
least five rings of packing.
The inner surface of the stuffing box shall have a surface finish of 3.2 µm or
smoother.
Tappings to the interspace between the bellows seal and the auxiliary packed
gland shall not be provided unless specifically requested on the order.
10.10. Indicator
Each valve shall be fitted with an indicator which clearly indicates the fully
open and fully closed positions of the valve.
10.11. Bolting
b) Hinged bolts (eyebolts) with integral forged eyes, providing that they are
effectively secured and their attachment is an integral part of the
bonnet/cover.
Where a soft seal ring is fitted, it shall be designed to compress down to the
level of the metal seat when the disc is in the fully closed position and to give
a metal seal even if the soft seal ring is damaged or displaced.
During manual operation the maximum load shall be taken as 300 N applied
by each hand. The equivalent torque is therefore (300 × d) Nm, where "d" is
the handwheel diameter in metres. Valves shall be designed to withstand
three times this load without the material of any part yielding and without the
operability of the pneumatic actuator, the external valve, the internal valve
and the leak tightness of the external valve gland being affected.
11.1. General
The internal valve shall have a spring loaded disc/ball which seals against the
internal valve seat. It shall have a flange suitable for both connection to the
storage tank and for the direct mounting of the external valve. The other end
shall be threaded or preferably prepared for welding.
The normal opening of the internal valve shall be carried out by the
application of pneumatic pressure to the pneumatic actuator and the closing
by the internal valve spring after the release of the pneumatic pressure.
11.2. Body
The minimum wall thickness of the valve body shall comply with the valve
manufacturer's standard, appropriate to the pressure designation, body
material and the nominal size of the flange.
The internal valve shall have a flanged end suitable for connecting to both the
storage tank and the external valve with the other end suitable for the
attachment of a dip pipe.
The flange shall be of a nominal size and dimensions compatible with the
flange of the external valve and be capable of meeting the pressure-
temperature rating appropriate to the pressure designation and material. For
PN designated valves the flange and facings should be based on the
requirements of ISO 7005 and for class designated valves on ASME B16.5.
The flange should have a female or groove on the front of the flange for
connection to the external valve and a male or tongue on the back of the
flange for connection to the storage tank.
The other end shall have an internal thread or be prepared for butt welding or
socket welding so that, for valves used for the transfer of liquid chlorine, a dip
pipe may be attached.
The ball/disc shall be held on the seat by the internal valve spring, which shall
maintain a tight shut-off until the downward movement of the external valve
stem pushes the ball/disc from the seat. The seat may be of a hard facing
material deposited directly on the body or a soft seating material securely
attached to the body (only on special request).
Both ends of the spring shall be closed and ground, properly located and
guided.
12.1. General
The pneumatic actuator shall be either a single acting diaphragm type with
spring return or a single acting piston type with spring return. Pneumatic
pressure when applied to one side of the diaphragm/piston shall compress
the spring(s) and cause linear movement of the pneumatic actuator stem.
The spring(s) shall give a positive return action of the stem when pressure on
the diaphragm/piston is released.
The design of the pneumatic actuator shall be such that the stem will operate
with a motive fluid minimum pressure of 3 barg against a storage tank
pressure of 14.5 barg unless otherwise agreed by the buyer.
The actuator body shall have a minimum ingress protection level of IP55 as
defined in EN 60529 (protection against dust and water jets).
The actuator housing shall not be vented directly to atmosphere. Any vent
hole shall be either plugged or vented via a moisture removing device. The
non-pressure side of the actuator diaphragm shall be designed in such a way
that any trapped gas shall not affect the valve operation adversely.
A manual override shall be fitted to the actuator body (see Clause 13).
The securing of the diaphragm by the actuator body and cover shall ensure
that the joint does not leak when subjected to:
13.1. General
Each valve shall be provided with a manual override in order to operate the
valve in the case of lack of or failure of the motive fluid to the pneumatic
actuator.
The manual override shall be securely fastened to the cover of the pneumatic
actuator and connected to the pneumatic actuator stem.
13.3. Handwheel
The handwheel shall be of the spoke and rim or closed disc design. Pressed
steel handwheels are not permitted.
The handwheel shall be fitted such that it may be replaced, when necessary,
but secured so as to preclude loosening in service.
The valve shall be designed to be operated without the use of a wheel key;
therefore, the handwheel diameters shall be not less than those given in
Table 4.
14.1. General
Materials shall be suitable for use with liquid chlorine (see GEST 79/82 -
Materials of Construction for Use in Contact with Chlorine) over the
temperature range minus 40°C to plus 120°C and for the drying procedure
(see 21.3)
2) 640 N/mm2.
14.4. Castings
Body and bonnet/cover castings shall comply with the requirements of ASTM
A352 grade LCB or LCC, or equivalent national standard. The casting
manufacturer's quality assurance procedures shall ensure that any
discontinuities in the castings meet the acceptance levels given in Table 5.
14.5. Forgings
Body and bonnet/cover forgings shall comply with the requirements of ASTM
A350 grade LF2 or equivalent national standard.
There shall be a difference in hardness between the disc seating material and
the body seat material. The body seat shall have a minimum hardness value
of 300 HB.
Note : Hard seats (stellite) have been chosen due to their greater longevity
and the fact that they do not develop leaks with time.
Material for the soft seal ring shall be suitable for continuous use on chlorine
at the pressure designation (PN 25, PN 40 or ANSI Class 300) over the
temperature range minus 40°C to plus 120°C.
14.7. Bellows
The bellows specification and supplier shall be agreed between the valve
manufacturer and the buyer. Each ply shall be made preferably from
Hastelloy C276. The material selection shall be agreed between the valve
manufacturer and the buyer.
Material for auxiliary gland packings and for gaskets shall be suitable for
continuous use on chlorine at the pressure designation (PN 40 or
ASME Class 300) over the temperature range minus 40°C to plus 120°C.
The gasket between the valve body and the valve bonnet shall be of bonded
asbestos, a PTFE based material that minimises cold flow or PTFE with a
metal insert of a type suitable for use with chlorine. Other non-asbestos
gasket materials already used with satisfactory results on similar applications
by Euro Chlor members are also accepted.
14.9. Actuators
The use of aluminium parts should be avoided. Otherwise, these parts shall
be anodised and coated. The minimum coating and painting requirement is a
2 component epoxy coating with a total dry film thickness of minimum 75 µm
and maximum 150 µm.
Aluminium shall not be used for any other part of the valve.
16. WELDING
b) The requirements for preheating and for heat treatment shall have been
established by the approved welding procedures.
c) The impact properties shall have been met in qualifying the welding
procedures.
17. EXAMINATION
17.1. General
The hydrostatic test pressure shall be maintained for at least two minutes.
All tested parts shall be dried prior to assembly and new gaskets shall be
used.
18.2.1. General
a) The body ends shall be blanked so that the body is not constrained.
b) The valve shall be in the partly open position.
c) The pneumatic test pressure shall be 1.1 times the maximum allowable
working pressure of the valve at 20°C, appropriate to the pressure
designation.
d) The pneumatic test pressure shall be maintained for at least two minutes.
Visible leakage when using a bubble forming solution shall be cause for
rejection.
a) The body ends shall be blanked so that the body is not constrained;
b) The disc/ball shall be in the partly open position;
c) As 18.2.2c);
d) As 18.2.2d).
Visible leakage when using a bubble forming solution shall be cause for
rejection.
a) The body ends shall be blanked so that the body is not constrained.
c) The test pressure shall be applied to the underside of the disc/ball from
the dip pipe end of the body, with the flanged end blanked and having a
connecting pipe to a bubble test rig.
When a soft seal is fitted, following the high pressure test the seat shall be
checked for damage.
a) The body flanges shall be blanked so that the body is not constrained.
b) The valve shall be closed by the pneumatic actuator spring force (fail
close position).
c) The two blanking flanges shall have connecting pipes to a bubble test rig.
Each external valve, assembled with the pneumatic actuator and the manual
override, shall be pneumatically seat tested as follows:
b) the test pressure shall be applied to the underside of the disc with the
branch blanked and having a connecting pipe to a bubble test rig;
c) the test pressure shall be 1.1 times the maximum allowable working
pressure;
The following test shall be conducted to determine the lowest motive fluid
pressure which allows the full stroke of the valve.
c) A progressive motive fluid pressure shall be applied, until the valve starts
leaking.
This pressure shall be lower than the minimum motive fluid value by at
least 20%.
With no pressure being applied to the underside of the internal valve disc/ball,
the valve shall be subjected to a minimum of 5 full strokes (opening and
closing), by using the nominal motive fluid pressure.
The actual stroke of the pneumatic actuator stem shall be recorded and
compared with the calculated nominal stroke.
The test described in 18.3.4.1 shall be repeated but using the maximum
allowable working pressure under the disc/ball of the internal valve.
Note: During the tests conducted under 18.3.4.1 and 18.3.4.2, any
accessories shall be controlled and adjusted.
The manual override shall be fitted and the test described in 18.3.4.2 shall be
repeated by using only the manual override to operate the internal valve.
Dimension “A” is the distance between the end of the external valve stem and
the internal valve disc/ball.
Dimension "B" is the distance between the end of the internal valve ball/disk
and the internal valve face.
Dimensions "A" and "B" are critical for a good performance in operation (see
sketch) and therefore each valve shall be subjected to a specific, individual,
measurement of these dimensions.
d) Using the manual override the valve shall be opened slowly and carefully;
This stroke corresponds to the dimension "A" and shall be compared with the
calculated nominal dimensions (based on drawings) and with the calculated
value based on actual measurements during manufacturing.
18.3.5. Cv Measurement
At the request of the buyer, a flow test shall be carried out and the actual Cv
of the valve determined.
The valve manufacturer shall provide with each order a certificate confirming
that each pneumatically operated valve has been manufactured and tested in
accordance with the requirements of the valve manufacturer's specification
relevant to the Euro Chlor verification, and the purchase order. The test
certificate shall state the test pressures and fluids used in the testing.
It shall also list the references of the material certificates provided with the
raw materials used in the manufacture of the bodies, bonnet/cover, valve
stem, bellows, discs and seats.
20. MARKING
Each valve shall be legibly marked with the body marking and identification
plate marking given in 20.2, 20.3 and 20.4.
The external valve body marking shall be integral with the valve body. The
marking shall include the following:
The internal valve body marking shall be integral with the valve body. The
marking shall include the following:
c) The number of this Euro Chlor Recommendation, i.e. GEST 94/204, 1st
edition, 1997;
e) Valve manufacturer's serial number (the number that identifies the valve
in all respects);
a) Safety position;
21.1. General
Each valve shall be clean, dry and free from all hydrocarbon grease, oil or
solvents. Components which require to be lubricated shall be treated with
chlorine-compatible chloro-fluorinated grease.
Machined and threaded surfaces shall be coated with a chlorine compatible
chloro-fluorinated rust preventive and the ends of the valve blanked.
21.2. Painting
Prior to priming, all external surfaces shall be suitably cleaned to remove all
traces of grease or dirt. This may be by mechanical or chemical means. In
the case of cast or forged materials this shall ensure the complete removal of
sand or rust scale.
One coat of anti-rust primer and an agreed top coat system shall be applied
to all external surfaces that are likely to become rusty.
Each external valve and internal valve shall be dried. The preferred
procedure is in an oven at a minimum of, unless otherwise agreed, 120°C for
at least three hours. After drying, but before blanking, the valves shall be
stored in a way which prevents moisture condensation (e.g. in the oven or
other chamber, with a dry gas purge, or under sealed vacuum).
After the valves are removed from the oven and before the temperature of the
valve bodies falls below 35°C the end connections shall be sealed. Flanges
shall be fitted with suitable gaskets and metal blank flanges having silica gel
sachets or an agreed alternative attached to their inner faces.
The external valve and the internal valve may be packaged separately.
Valves, except those with soft seal rings, shall be in the closed position. In
the case of a soft seal ring external valve the ball/disc shall be backed off the
seat.
22. REFERENCES
Manual override
Pneumatic actuator
External valve
Internal valve
B.1 State that the pneumatically operated valves should comply with GEST
94/204 * Edition.
Euro Chlor
Avenue E Van Nieuwenhuyse 4
Box 2
B-1160 Brussels
Belgium