A eccmmen cone eae: | Rev.# | 00 [Rev. pate] avoan« | pace | 112 _] @OPITL ‘WORK PROCEDURE SAFETY UNIT 1.0 2.0 3.0 4.0 5.0 TITLE: AMMONIA IN AIR SURVEY PROCEDURE | orteIvat ' | WHEN IN RED PURPOSE: This procedure specifies the method and guidelines to carry out Ammonia in air survey to effectively monitor breathable air quality within Plantsite. Though 25 ppm of ammonia is allowed as its Threshold Limit but Pakarab Fertilizers intends to keep it to the lowest side by providing appropriate guidelines and implementation of control measures. SCOPE: This procedure ‘applies on all PFL plant sites and areas in the immediate vi Pakarab Plantsite boundary wall. OBJECTIVES: The objective of this procedure is to: 3.1 Enable the Laboratory and HSE personnel to effectively monitor the ammonia in air within Plantsite and its immediate vicinity. 3.2 To establish guidelines pertaining to ammonia in air survey based on international best practices and Contemporaneous Fertilizers Plant in Pakistan. REQUIREMENTS: Following equipment shall be required to be handy for ammonia in air survey. 4.1 A Drager Pump. 4.2. Drager tubes for ammonia monitoring. 4.3 Trained Laboratory Technician. SAMPLING GUIDELINES 5.1. Typical areas to be monitored may include following; * Ammonia Plant Back-end side © Nitric Acid Plants Ammonia circuits « Urea Plant CAN Plant Ammonia Circuit «NP Plant Ammonia circuit * Effluent Treatment Plant & Dirty Cooling Tower «CAN Bulk and Product Stores ROUTE PREPARED BY REVIEWED BY Kamal Shah, Mati ur Rab Siddiqui | Farrukh Iqbal HSE 4.4.6 Desig/Sign. | Sub Engr. Sa 30 -04-} ees HR UM HSE = [om IMS 64.370 8.0 " DOCUMENT CODE SAY * Disposal Points . | ORIGINAL * Evaporation Ponds | WHEN IN RED 5.2 A typical reliable reading may be obtained by taking a sample at 5 feet height and a sample at 5 feet downwind away from the point of containment and then taking their average reading 5.3 Laboratory Technician shall carry out the survey (HSE personnel will accompany him if necessary). PROCEDURE 6.1. Ensure to calibrate the sampling pump to the recommended flow rate. 6.2 Connect the sampling tube to the pump 6.3. Place the sampling tube in the breathing zone as directed by HSE personnel. 6.4 Take a sample by making the 10 strokes of Drager pump to draw a suitable amount of sampling air. 6.5 Take the reading on the tube and note it down. 6.6 Daily samples of most critical areas of Plantsite shall be taken and recorded by Laboratory and any anomaly shall be immediately notified to Management and HSE. 6.7 A thorough survey of all potentially contaminated areas by Laboratory must be done for all areas on quarterly basis. RELATED DOCUMENTS 7.1 List of ammonia in survey areas DISTRIBUTION: HSE Unit Laboratory PREPARED BY REVIEWED BY APPROYED BY. REFERENCE | Kamal Shah Mati ur Rab Siddiqui_| Farrukh [I] Be-eery teh | HSE446 IM HSE = [emmy eeIN AIR SURVEY AREAS AND RE; ORIGINAL T WHEN IN RED. [NITRIC ACID PLANT Concentration Reason Dated: Time: Concentration Reason [Outside Control Room Howards KIC. [Outside Control Room lrowards Pant INKS Pump Line: towards tine B. imp Line B towards tne A [UTILITIES WEST [Demin Plant Near Anion [Demin Plant Near lOperator Cabin [Near 201A Air Icompressor [AMMONIA PLANT In beween PGRU 134-6] 11-6 towards gallery 118-6 towards galery Near 105-J Oil Console UREA PLANT Upsiars n betwee Spheres 182. stern tank towards sch INH3 Compressor [CAN PLANT Near 15-2002 Towards [ear Be sae Tak Howards NP INP PLANT [Near 40-2113 & 40-2114 [Near 40-2115 & 40-2192, EFFLUENT ITREAI [TREATMENT PLANT Dirty Cooing Tower rds NP. loiny Cooing Tower ltowards Onerator Cabin [Tank No. t Towards NP. NAST AREA [Conipressor 1207 To ie [eapressor OTIS To UT YE [1201-JA towards UTY-E OTHER AREAS: