GeMS No: T6002116

Revision: AH
st
Date: 21 Feb 2014
METALLIC MATERIAL SPECIFICATION Page: 1 of 5

TITLE: AISI 8630 Mod Alloy Steel, 80 KSI Min Yield Strength

1. Scope:

1.1. This specification shall be utilized in procurement of AISI 8630 modified steel (UNS G86300)
in quenched and tempered condition to 22 HRc maximum hardness.

1.2. These materials meet the requirements of NACE MR0175/ISO 15156 for hydrogen sulfide
service.

1.3. This material specification is for components with a requirement of corrosion resistance and is
readily weldable.

1.4. Maximum limiting diameter in the solid heat treated condition shall be 10˝. Material above 10˝
diameter needs to be heat treated in hollow form with maximum wall thickness of 6˝.

2. Reference Documents: (Use latest revision of documents below):

Document Description
Standard Specification for Seamless Ferritic and Austenitic Alloy-Steel Boiler,
ASTM A213
Superheater, and Heat-Exchanger Tubes

Schlumberger Private
ASTM A370 Methods and Def. for Mechanical Testing of Steel Products
ASTM A388 Standard Practice For Ultrasonic Examination Of Heavy Steel Forgings
ASTM E10 Brinell hardness
Test Methods for Rockwell Hardness / Superficial Hardness of Metallic
ASTM E18
Materials
ASTM E23 Charpy Impact Testing of Metallic Materials
Standard Practice for Fabrication and Control of Metal, Other than Aluminum,
ASTM E428
Reference Blocks Used in Ultrasonic Testing
Petroleum and natural gas industries Downhole equipment Subsurface safety
API SPEC 14A
valve equipment.
Design and Operation of Subsea Production Systems-Subsea Wellhead and
API SPEC 17D
Tree Equipment.
API 6A/
Specification for Wellhead and Christmas Tree Equipment
ISO 10423
API 5CT Specification for Casing and Tubing
NACE MR0175/
Materials for use in H2S-containing environments in oil and gas production
ISO15156
MIL-STD-1684 Control of Heat Treatment
SAE AMS- H- 6875 Heat Treatment of Steel Raw Materials
BS 2M 54 Temperature Control in Heat-Treatment of Metals
Schlumberger specification for Quality Assurance Approved Supplier
MT-16
Requirements
NDE-31 SLB specification for Ultrasonic examination of wrought metals
NDE-35 Shear wave Ultrasonic Examination of Metal Pipe/Tubing and Hollow Bars.
QA-31 Schlumberger specification for Quality Assurance Documents and Records

Schlumberger private and proprietary rights are included in the information disclosed herein. Neither this document nor the information
disclosed herein shall be reproduced or transferred to other documents or used or disclosed to others for manufacturing or for any
purpose except as specifically authorized in writing by Schlumberger.  Schlumberger.
 GeMS No: T6002116
Revision: AH
st
Date: 21 Feb 2014
METALLIC MATERIAL SPECIFICATION Page: 2 of 5

TITLE: AISI 8630 Mod Alloy Steel, 80 KSI Min Yield Strength

3. Requirements:

3.1. Melting:

The material shall be electric furnace melted, vacuum degassed, fine grained alloy steel.

3.2. Chemical Composition: The chemical composition shall satisfy the following requirements.

Element Symbol Percent

Carbon C 0.25/0.33 Range

Manganese Mn 0.70/1.10 Range

Phosphorous P 0.025 Max

Sulfur S 0.025 Max

Chromium Cr 0.85/1.00 Range

Schlumberger Private
Molybdenum Mo 0.35/0.45 Range

Nickel Ni 0.75/0.90 Range

Silicon Si 0.15/0.35 Range

Vanadium V 0.060 Max

Copper Cu 0.250 Max

Titanium Ti 0.060 Max

Aluminum Al 0.035 Max

3.3. Heat Treatment:

3.3.1 The material shall be quenched and tempered to meet the mechanical properties of section 3.4

3.3.2 Heat treating equipment qualification and calibration:

Furnaces shall be calibrated no less than once a year or when a furnace is moved, repaired or
rebuilt. The practice for qualification of heat-treating equipment shall be one of the following:

3.3.2.1 API 6A annex for qualification of heat-treating equipment or other equivalent

internationally recognized standard.

3.3.2.2 Manufacturers’ written specifications including acceptance criteria, which are not less
stringent than the procedures identified above.

3.3.3 Temperature monitoring

The material temperature shall be measured by use of either a contact surface thermocouple
or a heat sink as described in API 6A, ISO 10423 or equivalent international standard.

Schlumberger private and proprietary rights are included in the information disclosed herein. Neither this document nor the information
disclosed herein shall be reproduced or transferred to other documents or used or disclosed to others for manufacturing or for any
purpose except as specifically authorized in writing by Schlumberger.  Schlumberger.
 GeMS No: T6002116
Revision: AH
st
Date: 21 Feb 2014
METALLIC MATERIAL SPECIFICATION Page: 3 of 5

TITLE: AISI 8630 Mod Alloy Steel, 80 KSI Min Yield Strength

3.3.4 All heat treatment shall be carried out in accordance with written procedures. Temperature,
time at temperature and method of cooling must be reported for each cycle.

3.3.5 The quench media shall be one of the following:

3.3.5.1 Oil
3.3.5.2 Polymer
3.3.5.3 Interrupted water, water or other water equivalent quench

3.3.6 The temperature of the water or the quench media with cooling rate approximately that of water
0 0
shall not exceed 40 C (100 F) at the start of the quench. For bath type quenching, the
0 0
temperature of water or equivalent quench media shall not exceed 50 C (120 F) at the
completion of quench.

3.3.7 The temperature range for other quenching media shall meet manufacturer written
specification.

3.3.8 If the heat treatment is carried by sub-supplier, heat treater shall ensure the compliance of
mechanical properties established in section 3.4.

Schlumberger Private
3.4. Mechanical Properties:

The test sample shall be drawn from longitudinal direction. The mechanical properties shall be
measured in accordance with ASTM A370 and shall conform to the following.

Property Requirement
Tensile Strength, ksi (MPa), Min 95 (655)
Yield Strength, ksi (MPa), Min 80 (552)
Elongation in 4D, %, Min 18
Reduction of Area, %, Min 35
Surface Hardness of Raw Material, BHN, Range 207-237
Surface Hardness of Finish Part, BHN, Range 197-237
0 0
Transverse Chary V-Notch @ -20 F (-29 C) or colder, Avg, J(ft-lbs), Min 42 (31)

3.5. NDE:

Material must be examined by UT after heat treatment as per NDE-31 for solids and as per
NDE-35 for hollows. UT demonstrated by comparable industry standards like ASTM E428,
ASTM A213 (For tubing), ASTM A388 (For solids), API 6A PSL 3, API 5CT, SEP 1921 is
acceptable. Mill UT is acceptable when heat treatment is performed by mill.

3.6. Welding: Welding by the supplying mill is prohibited.

3.7. Material Quality:

3.7.1. The material shall be free of injurious seams, laps, or other visual imperfections, which,
due to their nature, will interfere with the use of the material in machining, or fabrication
of suitable parts.

Schlumberger private and proprietary rights are included in the information disclosed herein. Neither this document nor the information
disclosed herein shall be reproduced or transferred to other documents or used or disclosed to others for manufacturing or for any
purpose except as specifically authorized in writing by Schlumberger.  Schlumberger.
 GeMS No: T6002116
Revision: AH
st
Date: 21 Feb 2014
METALLIC MATERIAL SPECIFICATION Page: 4 of 5

TITLE: AISI 8630 Mod Alloy Steel, 80 KSI Min Yield Strength

3.8. Identification and Packing:

Protection shall be provided to prevent mechanical damage during shipment. Grade, Heat number,
heat treat condition shall be clearly marked on individual tube/forge lengths. Other information shall
be provided or marked as required by the purchase order.

3.9. Deviation From Requirements:

All requests for deviation must be submitted to Schlumberger for review and approval by the
engineering department, or directly to the engineer in charge of the project.

4. Documentation And Retention:

Supplier records involving this specification must be auditable / retrievable for a period of five (5)
years from the date that the raw materials were certified. Supplier should submit the necessary
documents from following list along with the certification package.

4.1. Copy of the original mill certificate from the producing mill.

4.2. Copy of actual chemical composition (check analysis) of the material which lists all of the

Schlumberger Private
elements specified in paragraph 3.2.

4.3. Copy of the final heat treat data including temperature, time at temperature and method of
cooling must be reported for each cycle in accordance with paragraph 3.3

4.4. Copy of mechanical properties including impact test results. Test results must meet the
requirements of paragraphs 3.4

4.5. The statement of compliance to ultrasonic testing requirements per paragraphs 3.5

4.6. Statement of compliance from mill or supplier conforming compliance with this specification (by
number) and the Schlumberger Purchase order (by number and line item number).

4.7. All documentation generated by this specification shall be retained in accordance with procedure
QA-31.

5. Authority

5.1. Amending Authority

This document is controlled by Project MatEng. It shall be revised only with the agreement of
technical representatives of all Schlumberger Segments using it.

5.2. Interpretation Authority

Interpretation authority for this document shall reside with the Materials Engineering or Quality
Manager of each Technical Centers using it. No deviation from this specification is permitted
without a waiver approved by Engineering.

Schlumberger private and proprietary rights are included in the information disclosed herein. Neither this document nor the information
disclosed herein shall be reproduced or transferred to other documents or used or disclosed to others for manufacturing or for any
purpose except as specifically authorized in writing by Schlumberger.  Schlumberger.
 GeMS No: T6002116
Revision: AH
st
Date: 21 Feb 2014
METALLIC MATERIAL SPECIFICATION Page: 5 of 5

TITLE: AISI 8630 Mod Alloy Steel, 80 KSI Min Yield Strength

Quality Check List

P.O. Ln Heat
P/N Rev Job No.
Item No.

Material Grade AISI 8630 Mod Manufacturer

Chemical Composition

Element Symbol Percent Actual

Carbon C 0.25/0.33 Range
Manganese Mn 0.70/1.10 Range
Phosphorous P 0.025 Max
Sulfur S 0.025 Max
Chromium Cr 0.85/1.00 Range
Molybdenum Mo 0.35/0.45 Range

Schlumberger Private
Nickel Ni 0.75/0.90 Range
Silicon Si 0.15/0.35 Range
Vanadium V 0.060 Max
Copper Cu 0.250 Max
Titanium Ti 0.060 Max
Aluminum Al 0.035 Max

Mechanical Properties

Property Requirement Actual

Tensile Strength, ksi (MPa), Min 95 (655)
Yield Strength, ksi (MPa), Min 80 (552)
Elongation in 4D, %, Min 18
Reduction of Area, %, Min 35
Surface Hardness of Raw Material, BHN, Range 207-237
Surface Hardness of Finish Part, BHN, Range 197-237
0 0
Transverse Chary V-Notch @ -20 F (-29 C) or colder, Avg, J(ft-lbs), Min 42 (31)

Certification

Verification of Ultrasonic Inspection of raw material prior to machining ____________

Material Non-Conformance Request (NCR) attached (If applicable) ____________

Schlumberger private and proprietary rights are included in the information disclosed herein. Neither this document nor the information
disclosed herein shall be reproduced or transferred to other documents or used or disclosed to others for manufacturing or for any
purpose except as specifically authorized in writing by Schlumberger.  Schlumberger.