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Soils and Foundations 61 (2021) 1630–1644
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Technical Paper

Influence of prefabricated vertical drains spacing on


FeCl3-vacuum consolidation of a landfill sludge
Xudong Zhang a, Yajun Wu a,⇑, Yitian Lu a,⇑, Guang Chen b,⇑, Qingyang Deng a,
Yang Xu a, Peng Ye a
a
Department of Civil Engineering, Shanghai University, 99 Shangda Road, Shanghai 200444, PR China
b
Shanghai Chengtou Wastewater Treatment Co., Ltd, Shanghai 201203, PR China

Received 21 December 2020; received in revised form 15 September 2021; accepted 1 October 2021
Available online 29 October 2021

Abstract

The spacing of PVDs is an essential factor affecting the consolidation effect of vacuum preloading. For exploring the influence of spac-
ing of PVDs on the impact of sludge drainage consolidation, FeCl3, a commonly used inorganic coagulant, was used to pretreat the
sludge. In the experiment a vacuum filtration test was carried out to determine the optimal addition amount of FeCl3, and then the land-
fill sludge was pretreated according to the FeCl3 optimal addition amount. And two different spacing of PVDs were used to carry out a
vacuum preloading contrast test. Then, the drainage and settlement were recorded, and water content and vane shear strength (VSS)
were measured after the experiment. Finally, Mercury intrusion porosimetry (MIP) was carried out to explore the pore characteristics
of the sludge further. The main conclusions are as follows: After conditioning by FeCl3, the sludge’s flocculent structure was destroyed,
the intracellular water was released, and the effect of drainage capacity was significantly improved. After the spacing of PVDs is halved,
the average volume reduction ratio and shear strength increases, and the effect of advanced dewatering and volume reduction of sludge
improved significantly, leading to a better consolidation effect. In the progress of vacuum drainage consolidation, halving the spacing of
PVDs results in large pores transformation into small pores, and the range of drainage consolidation is greatly expanded.
Ó 2021 Production and hosting by Elsevier B.V. on behalf of The Japanese Geotechnical Society. This is an open access article under the CC BY-
NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).

Keywords: Landfill sludge; Spacing of PVDs; FeCl3 pretreatment; Vacuum preloading; Vacuum clogging effect

1. Introduction pollution. Thus, the treatment of sludge is necessary.


Sludge disposal methods currently mainly include sanitary
With the continuous growth of population and the landfill, agricultural use, dry incineration, construction
development of urbanization, municipal sludge production material use, soil remediation, etc.(Wang et al., 2015).
is also increasing. High water content, loose structure, a Due to the advantages of low cost and large capacity, the
significant amount of organic matter and microorganisms, sanitary landfill was mainly used to dispose of municipal
and certain harmful heavy metals are present in municipal sludge in China (Lin et al., 2014a). Previously, to better treat
sludge. (Chanaka Udayanga et al., 2018; Dong et al., 2013; sewage sludge, many scholars have carried out many studies
Wang et al., 2015), which may cause serious environmental on sludge and landfill. Sludge is similar to organic soil and
has great compression potential (Disfani et al., 2013). When
a large amount of sludge is poured into a landfill, many geo-
⇑ Corresponding authors. logical, environmental problems will inevitably occur, such
E-mail addresses: xdzhang@shu.edu.cn (X. Zhang), wyjdldz@shu.edu. as compression settlement, local instability, and slope insta-
cn (Y. Wu), luyitianxxxx@163.com (Y. Lu), chenguang@shwwt.com
(G. Chen).
bility of the landfill (Lo et al., 2002). Tuncer B. Edil. et al.

https://doi.org/10.1016/j.sandf.2021.10.001
0038-0806/Ó 2021 Production and hosting by Elsevier B.V. on behalf of The Japanese Geotechnical Society.
This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
X. Zhang et al. Soils and Foundations 61 (2021) 1630–1644

(1990) proposed two mathematical models to predict landfill destroy the cell structure of sludge and release interstitial
settlement more accurately to evaluate the residual capacity water and bound water to improve the drainage potential,
of landfill more efficiently and make full use of the valuable which is often used for sludge treatment. After chemical
space of landfill. Lo et al. (2002) estimates the slope stability pretreatment, the sludge dewatering potential is greatly
and potential settlement of CEPT sludge by analyzing CEPT improved. Vacuum preloading is the drainage consolida-
sludge’s geotechnical engineering characteristics and recom- tion of sludge in a landfill under vacuum pressure. Reduc-
mends the maximum allowable slope value of CEPT sludge. ing the sludge volume by reducing the water content of
Asakura et al. (2009) studied the permeability of sludge in a sludge is beneficial to reduce the cost of subsequent sludge
landfill. They analyzed the parameters that had a significant reuse. However, few systematic studies on the vacuum drai-
influence on the oxygen penetration depth by considering the nage reinforcement of landfill sludge. As one of the effec-
diffusion and convection driven by a temperature gradient to tive methods to reduce the volume of landfill sludge,
ensure the allowable proportion of sludge in the landfill’s vacuum preloading is lack of more comprehensive
oxygen-demand area. These studies provide important guid- research. When sludge treated by vacuum preloading, the
ance for sludge treatment. However, with the continuous prefabricated vertical drain (PVD) needs to be connected
increase of sludge production, the storage capacity of many to the drainage pipe and inserted into the sludge at a cer-
sludge reservoirs or sludge pits is insufficient in China. It is tain distance. And use geomembrane seal sludge. Then,
difficult to find new landfill sites because of the shortage of the vacuum pressure was applied to the sludge by vacuum
land resources. Therefore, the drainage volume reduction pump, and the sludge was consolidated under vacuum
and pit reinforcement in the sludge reservoir area have pressure. PVD plays an essential role in draining water
become the problems to be solved in most landfills. There and transferring vacuum load in the vacuum preloading
are two ways to solve the problem of sludge landfill site’s process. It is the core material of vacuum preloading tech-
insufficient storage capacity: ectopic treatment and in-situ nology. Recently, researchers have shown an increased
treatment. Due to the need to dig out the sludge, the off- interest in the effect of PVD in vacuum drainage consolida-
site treatment easily causes secondary pollution such as odor tion. Cai et al. (2017) studied the PVD embedded in
and sewage. It may cause damage to the protective mem- dredged soil and proposed deformed effect PVD on soil
brane and leakage of leachate to pollute the environment. consolidation drainage capacity. Wang et al. (2020b) inves-
In-situ treatment is to directly use vacuum preloading tigated the influence of PVD with varying pore sizes on
method on the sludge pit for in-situ drainage reinforcement, vacuum preloading and suggested the filter membrane opti-
the secondary pollution can be avoided if the filtrate is prop- mal pore size. Wu et al. (2021) studied the effect of different
erly treated, and in-situ treatment has the advantages of low PVD filter membrane sizes on the vacuum drainage consol-
treatment cost and large single treatment capacity (Cai et al., idation of landfill sludge conditioned by Fenton reagent.
2015; Lin et al., 2014a; Zhu et al., 2018). The spacing and arrangement of PVDs are essential fac-
The studies on sludge mainly focuses on improving the tors in vacuum preloading (Sun et al., 2017). At present,
dewatering index sludge and solidifying sludge (Guo only few scholars have conducted studies on the selection
et al., 2020; He et al., 2015; Lang et al., 2020; Rao et al., and optimization of the spacing of PVDs. R.
2019; Wang et al., 2020a; Wu et al., 2020b; Zhang et al., Radhakrishnan (2011) conducted the field test of vacuum
2021a; Zhang et al., 2020; Zhang et al., 2021b). Many preloading for soft clay foundation and suggested that
scholars have explored the dewatering characteristics of the distance of PVDs should be reasonably reduced to
sludge before. Ayol (2005), using high molecular flocculant improve the effect of vacuum preloading. Sun et al.
for enzymatic pretreatment of sludge can significantly (2017) conducted experiments on improving the soft clay
improve sludge dewatering capacity. Ruiz-Hernando by vacuum preloading combined with short prefabricated
et al. (2014) carried out ultrasonic, thermal and alkaline drainage boards. They explored the influence of the spacing
treatment on the sludge to improve its dewatering capacity. of PVDs on vacuum preloading and proposed the optimal
The results showed that heat treatment, high ultrasonic spacing of PVD. Wang et al. (2020d) studied a membrane
intensity and alkaline treatment could improve the sludge connector vacuum preloading method and compared the
dewatering capacity by releasing interstitial water. Fitria efficiency of this new method with that of the traditional
et al. (2013) tested different shapes of mixers (radial, axial, PVD-hose method, investigated the influence of different
wheel, three-blade and magnetic) to evaluate their effects PVD spacing on soil reinforcement, and suggested an opti-
on sludge dewatering test. Lee and Liu (2000) studied the mal PVD spacing.
method of sludge dewatering by dual polyelectrolyte regu- All of the above are related studies on soft clay or
lation, and proposed the reaction mechanism of dual poly- dredger fill silt, and there is no in-depth explanation of
electrolyte regulation based on the enhanced flocculation of the influence mechanism of PVDs space. The sludge prop-
sludge particles. erties are quite different from soft clay and silt. Therefore,
In recent years, chemical pretreatment combined with it is necessary to study the influence of PVDs space on
vacuum preloading is considered to be an effective method sludge in-situ reinforcement effect.
for sludge drainage volume reduction. Chemical reagents, Based on the above problems, in this paper, the com-
due to their strong oxygen or coagulation effects, can mon inorganic coagulant FeCl3 is used to precondition
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the sludge. As a sludge coagulant, FeCl3 is often used in pump, vacuum conversion valve, jars, vacuum gauge,
sludge pretreatment by compressing the double electric meter ruler, drainage pipe, valve, sealing film, geotextile,
layer of sludge cells, significantly improving the drainage etc. The vacuum preloading test device is shown in Fig. 2.
and consolidation effect of sludge (Lin et al., 2014b). In this
test, two different spacing of PVDs were set up to carry out 2.3. Test procedure
the vacuum preloading contrast test. After vacuum
preloading, the data of sludge drainage, VSS, water content 2.3.1. Vacuum filtration test
distribution, and pore distribution were compared, the In the research for investigating sludge dewatering per-
influence of the PVDs space on vacuum drainage reinforce- formance, the specific resistance to filtration (SRF) is usu-
ment was analyzed, and the mechanism of spacing between ally used as an essential index to evaluate the sludge
PVDs was preliminarily revealed, which provides a certain dewatering performance. The smaller the SRF, the easier
reference for engineering practice. the sludge is dewatered (Lo et al., 2001). SRF represents
the resistance on the filtration area per unit mass of sludge
2. Materials and methods under a certain pressure.
In this study, FeCl3 was selected as a pretreatment
2.1. Sludge samples and chemical reagents reagent to treat sludge. To explore the relationship between
the addition amount of FeCl3 and the SRF of sludge, we
The landfill sludge was taken from a sludge landfill area in determined the addition amount of FeCl3 according to
Shanghai. The sludge basic geotechnical properties are the percentage of sludge mass after drying. Thus, different
shown in Table 1. It is important to note that the sludge used amounts of FeCl3 were added to the sludge based on the
in this study has been stored in landfills for a long time. Due dry sludge’s proportion in this test. The additional amount
to the high organic matter content of sludge and the exis- is shown in Table 2. Then the vacuum filtration test was
tence of many microorganisms, the sludge in the landfill is carried out after thorough mixing. During the test, record
subject to certain decomposition reactions. It leads to deteri- the test parameters such as vacuum pressure, filtrate vol-
oration of the sludge engineering properties (Klein and ume, etc. The SRF can be calculated as follows:
Sarsby, 2000). Therefore, the measurement of sludge organic
2PA2 b
matter is essential. In this test, the sludge sample was placed r¼ ð1Þ
lC
in a muffle furnace and burned at 550°C for 2h. The organic
matter in the sludge would decompose and carbonize under where A is the filtration area; b is the slope of the line
the action of high temperature. The final mass reduction is t=m ¼ mb þ a, where v represents the filtering volume and t
the organic matter content of the sludge. Besides, due to represents filtering time.; C is the weight of solids per unit
the high organic content of the sludge, the oven temperature volume of filtrate; P is the pressure of filtration; and l is the
cannot be set to 105°C when measuring the water content filtrate viscosity.
because the high temperature will burn the organic particles
in the sludge and make it dry and carbonized (Arulrajah 2.3.2. Vacuum preloading model test
et al., 2013; Arulrajah et al., 2011). Therefore, in this water According to the vacuum filtration test results, the opti-
content measurement test, the drying temperature was mal additive amount of FeCl3 was 20 %. Therefore, 20 %
65°C and the drying time was 48h. FeCl3 was used to pretreatment sludge No. 1 and No. 2,
In the test, FeCl3 is used as conditioning reagent, and and No. 3 was the original sludge. Separated PVD was
the mass fraction is 98%. When treating the sludge, first selected for vacuum preloading model test, the spacing of
weigh the weight of ferric chloride, then prepare the solu- PVDs in No. 1 and No. 3 was 60cm, and No. 2 was
tion, finally fully mixed. As shown in Fig. 1(b), all the 30cm. The detailed test scheme is shown in Table 3. Then
reagents were added according to the mass percentage of the vacuum preloading model test was carried out; the
the sludge dry basis. schematic diagram of this test is shown in Fig 2. During
the vacuum preloading, the data of vacuum degrees, water
2.2. Test apparatus and devices discharge. A ruler is placed on the inner wall of the model
box to record the sludge height during the vacuum preload-
The test equipment and instruments mainly include elec- ing process. Due to the uneven height of the sludge, heights
tronic scale, beaker, PVD, model box (Fig. 1 (d)), vacuum of the sludge at the different positions were measured to

Table 1
Basic geotechnical properties of sludge.
Water content Specific gravity Organic matter content Density Permeability coefficient Void ratio
(%) (%) (gcm-3) (10-7cms-1)
76.2 1.8 40.9 1.12 1.9 5.75

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Fig. 1. Flow diagram of this study.

calculate the average height, and the change in the average to capture the colloidal particles of sludge, and the exces-
height is the settlement of the sludge. After vacuum sive hydrolysate is suspended in the liquid, which weakens
preloading, sludge samples were taken for water content its coagulation capacity (Wu et al., 2020a). The additional
test and vane shear test. In order to further explore the amount of 20 % is an obvious inflexion point of the curve.
state of the sludge after vacuum preloading, MIP was con- Thus 20 % FeCl3 is selected as the optimal addition
ducted to investigate the pore characteristics of the sludge. amount.
The flow diagram of this study is shown in Fig. 1.
3.2. Vacuum degree
3. Results and discussion
The variation of vacuum degree with time during the
3.1. Vacuum filtration test results test is shown in Fig. 4. It can be seen from Fig. 4 that
the vacuum degree of the three groups of tests is the same
According to the vacuum filtration test results, the rela- during the test process. In the test process, most of the time
tions between SRF and FeCl3 is shown in Fig. 3. The SRF the vacuum degree is above 60 kPa, the sealing condition is
of the original sludge is about 9.5  1012 m/kg, and when good. However, due to the vertical settlement and radial
FeCl3 addition is less than 20 %, the SRF of sludge shrinkage of the sludge in the test process, it is inevitable
decrease rapidly with the increase of FeCl3 addition, and to lead to air leakage in the model box. The vacuum degree
when FeCl3 addition is 20 %, the SRF reached the mini- reduces to less than 40 kPa. Due to the timely repair, the
mum. The SRF was 0.28  1012 m/kg, which decreased vacuum degree soon returned to about 60 kPa, without
by more than 97% compared with the original sludge. After affecting the test results.
FeCl3 was added more than 20 %, the SRF no longer
reduced but increased. The reason is that when FeCl3 is 3.3. Cumulative water discharge
in an appropriate amount, Fe3+ hydrolyzes to produce
Fe(OH)3 and H+, Fe(OH)3 as coagulant can promote the The curve of water discharge of each model box in the
flocculation of colloidal particles in the sludge through test over time is shown in Fig. 5. When the drainage rate
adsorption and bridging; H+ reduce the PH value of is lower than 0.02 L/h, the vacuum preload test can be
sludge, and destroy the extracellular polymer of sludge, regarded as stable, and it will be stopped. When the consol-
release intracellular water. However, when FeCl3 addition idation drainage reaches stability, No. 1 and No. 3 spend
is more than 20 %, some hydrolytic products are difficult 730 h, while No. 2 only spends 490 h. It can be seen from
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Fig. 2. Schematic diagram of the vacuum preloading test.

Table 2 vacuum degree to rise. Therefore, it can be seen that main-


The addition amount of reagent. taining a high and stable vacuum degree is conducive to
Reagent Addition amount increase the water discharge and shorten the consolidation
Anhydrous FeCl3 0% 10% 20% 30% 40% time of vacuum preloading.
Note: The added amount is the mass ratio of FeCl3 to the sludge dry basis. As shown in Fig. 5, The drainage curve of No. 2 can be
divided into two stages. The stage 1 is 0  90 h, and the
stage 2 is 90  490 h. The 90 h was derived from the inter-
Fig. 5 that the drainage performance of the original sludge section of the slopes of the two tangents in the No. 2. Stage
is abysmal, and the total drainage volume is the smallest, 1 was the fast drainage period, where the sludge was
only 5.65 L. After conditioning with FeCl3, the drainage drained rapidly due to the high vacuum pressure provided
volume of No. 1 and No. 2 increases significantly, and by the double PVDs. The drainage volume of No. 2 in
the finally drainage are 49.86 L and 57.11 L, respectively. stage 1 was 28.7 L, which accounted for 50.3% of the total
The reason for this phenomenon is that the addition of drainage volume. Stage 2 was the stabilization stage, and
FeCl3 destroys the sludge’s stable flocculent structure and there was no significant difference between the drainage
releases intracellular water. rates of No. 1 and No. 2 after 90 h. It can be concluded
The slowdown of the drainage rate of No. 2 after 170 h that decreasing the spacing of PVDs can significantly
is owing to the decrease of vacuum pressure. The sudden improve the consolidation and drainage rate in the early
increase of the drainage curve at 270 h is due to the repair period, while the sludge solidification drainage rate gradu-
of the test device after air leakage, which caused the ally decreases with the test time increase.

Table 3
Vacuum preloading test scheme.
Model box number Sludge consumption (kg) Reagents Add ratio (%) Distance(cm)
1 150 FeCl3 20 60 (Single PVD)
2 FeCl3 20 30 (Double PVDs)
3 — — 60 (Single PVD)

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3.4. Cumulative settlement and the volume reduction ratio

3.4.1. Cumulated settlement


During the test, the change of sludge height with time
was recorded by the scale. Due to the uneven height of
the sludge, the sludge height in this article is the average
height. The average settlement of sludge can be calculated
by the variation of sludge height. Besides, due to the
decrease of sludge volume during vacuum preloading, the
sealing membrane around the sludge is separated from
the model box’s inner wall, resulting in gaps, as shown in
Fig. 6 (b). After the test, the width of the gaps is measured
by a ruler, which is the radial shrinkage. The curves of each
model box’s cumulative settlement over time are shown in
Fig. 3. Sludge SRF variations with different additive amounts of FeCl3. Fig. 6 (a). The cumulative settlement curve of No. 3 (orig-
inal sludge) is very slow, and the final settlement is only 2.4
cm. After pretreatment with FeCl3, the cumulative settle-
ment of sludge increased obviously. At 490 h, the sludge
of No. 2 was stable. At this time, the settlement of No. 1
was 14.80 cm, the settlement of No. 2 was 11.43 cm, and
the settlement of No. 3 without chemical treatment was
only 2.01 cm. Similar to the drainage curves, the settlement
curve of No. 2 can also be roughly divided into two stages.
The first stage is the rapid settlement stage. The settlement
in the early 90 hours is 6.92 cm, accounting for 60.5% of
the total settlement. The second stage is 90492 h, which
is a slow settlement stage, and the settlement is only
4.51 cm.
It can be seen from the previous description that the
cumulative drainage of No. 2 is more than that of No. 1,
while the settlement of No. 2 in Fig. 6 (a) is less than that
of No. 1. The reason is shown in Fig. 6 (b) that No. 1 and
No. 2 pretreated by FeCl3 have not only vertical settlement
but also have radial shrinkage during the vacuum preload-
ing, but the radial shrinkage of No. 2 is much larger than
that of No. 1. The sludge after the test is shown in Fig. 7
(c). After the end of the test, the maximum radial shrinkage
Fig. 4. variation curves of vacuum degree over time.
of No. 2 is 9 cm, much larger than that of No. 1 at 4.5 cm.

3.4.2. Variation in the height of sludge surface


Six observation points along the radial direction are
selected to monitor the sludge surface’s height after vac-
uum preloading. The schematic diagram of observation
points is shown in Fig. 8. The monitoring results are shown
in Fig. 9. It can be seen from Fig. 9 that in the process of
vacuum drainage consolidation, the settlement of the
sludge surface is uneven. In model box No. 1, the settle-
ment on both sides of PVD is large, but the settlement near
PVD is small, which is shown in Fig. 8(a); The final height
of the sludge surface is M-shaped in No. 2, the settlement
of soil near the two PVDs is small, and the settlement in
the middle of the two PVDs is large. The common feature
of No. 1 and No. 2 is that there is less settlement near the
PVD and more settlement on both sides. As shown in
Fig. 8, the sludge near the PVD is higher than elsewhere,
like a rising ‘‘soil pile”, which may be related to the
Fig. 5. Variation curves of water discharge with time. clogging effect around the PVD (Zhang et al., 2020). A
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Fig. 6. (a) Variation curves of cumulative settlement with time; (b) Schematic diagram of settlement and radial shrinkage.

schematic diagram is drawn to better explain the clogging gradually increase, and the ‘‘soil pile” will correspondingly
mechanism around the PVD, as shown in Fig. 7(c). In rise, as shown in Fig. 7 (a).
the vacuum drainage consolidation process, the small par-
ticles in the sludge move horizontally and gather around 3.4.3. The volume reduction ratio
the drainage plate under the action of horizontal seepage The volume reduction ratio of each group was calcu-
force and gradually form a clogging zone with high lated according to the volume change before and after
strength and low permeability through seepage compres- the vacuum preloading, as shown in Table 4.
sion and vertical consolidation. (Wang et al., 2020c; Xu According to Table 4, the volume reduction ratio of No.
et al., 2020). Because the density and strength of ‘‘soil pile” 3 is the smallest, only 4.6%. Compared with the pretreat-
are higher than in other places, the compression settlement ment sludge, the volume reduction ratio of No. 2 is
of ‘‘soil pile” is small. As consolidation proceeds, the settle- 50.7%, and that of No. 1 is 36.2%; compared with the orig-
ment difference between near and far from the PVD will inal sludge, the volume reduction ratio of No. 2 is 45.0%,
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Fig. 7. (a), (b) Sludge at the end of the experiment; and (c) Schematic diagram of the clogging effect.

and that of No. 1 is 28.8%. After the spacing of PVDs is and different distances from the PVD. The sampling points
halved, the volume reduction ratio of No. 2 is increased and test points are shown in Fig. 10, and the results are
by 48.2% on average compared to No. 1. It can be seen shown in Fig. 11.
from the results that the reagent combined vacuum It can be seen from Fig. 11 that within the depth of
preloading method has dramatically improved the sludge 20cm, the water content of No. 3 original sludge is more
dewatering ability. Moreover, with the decrease of PVDs than 72%. The water content of the original sludge is still
spacing, the volume reduction rate of sludge further high after vacuum preloading because the original sludge
increased. The volume reduction rate in No. 2 (double has poor drainage capacity. Within the 20cm depth, the
PVDs) reached 50.7 %, and the volume of sludge was water content of No. 1 and No. 2 are both significantly
reduced by half. The volume reduction effect was excellent. lower than before vacuum preloading. At 1cm from the
surface PVD, the water content of No. 1 and No. 2
3.5. Water content distribution decreases the most, which drops to 57%, 56.8%, decreases
by 18.8%, and 19%, respectively. In other locations, with
After the vacuum preloading model test, the water con- the increase of the distance from the PVD and the increase
tent of each model box was measured at different depths of the depth, the water content gradually increases. In the
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Fig. 8. Schematic diagram of observation points and ‘‘soil pile”.

(a) No. 1 (b) No. 2


Fig. 9. Sludge height variation curves.

completely lower than 60 %, which meets the requirements


Table 4 of advanced dewatering. Therefore, increasing the number
Volume reduced ratio. of PVDs or reducing the PVDs spacing will promote the
Model box Volume reduced ratio Volume reduced ratio vacuum preloading consolidation of sludge, and signifi-
number (compared with (compared with original cantly reduce the water content.
pretreatment sludge) sludge)
(%) (%)
At 1 cm away from the PVD, the water content of No. 2
at depth of 0 cm and 20 cm increased by 1.2 %, and No. 1 is
1 36.2 28.8
2 50.7 45.0
3.2 %. At 13 cm away from the board, the water content of
3 — 4.6 No. 2 at depth of 0cm and 20cm increased by 1.5 %, and
that of No. 1 is 6.2 %. This phenomenon shown that reduc-
ing the PVDs spacing can make the water content distribu-
surface layer, the water content distribution is more even tion more even. Increasing the number of PVDs or
than in the deep layer. Compared with Fig. 11(a) and (b), decreasing the spacing of PVDs to make full use of the
it easy to found that the water content curves of No. 1 effective influence range of PVDs, and form a broader
and No. 2 has a significant change at a depth of 10 cm, range of vacuum seepage field between the two PVDs
which indicates that the water content in the depth of 10 (Song et al., 2004), which can enhance the effect of vacuum
cm is more even than that of 20 cm. The distribution prop- preloading combined action and improve the effect of
erties of water content in three groups can be obtained: the ‘‘infiltrating-concretion” in vacuum seepage field.
deeper the depth, the higher the water content; under the
same depth, the farther away from the PVD, the higher 3.6. Vane shear strength
the water content, which may be affected by the dissipation
of vacuum pressure (Zhu et al., 2010). As shown in Fig. 11, As shown in Fig. 1(f), after the vacuum preloading model
after vacuum preloading, only the water content in No. 2 is test, the vane shear test was carried out on the sludge at 3cm,
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Fig. 10. Schematic diagram of sampling points and test points.

13cm, and 23cm away from the PVD. The test points are 3.7. Mercury intrusion porosimetry
shown in Fig. 10. Firstly, the vane shear test was carried
out on the sludge in the model box, and then the sludge be MIP has been used to study the pore distribution of soft
remoulded, and the vane shear test was carried out on the clay, but it is rare to study the pore distribution of sludge
remoulded sludge. The results are shown in Table 5. after vacuum preloading. The mechanism of MIP is to
It can be seen from Table 5 that the average VSS of assume that the pores in the soil are cylindrical. By apply-
No. 3 after vacuum preloading at a depth of 20cm is only ing a certain mercury pressure, a certain amount of mer-
1 kPa, which is very low. The VSS of No. 1 and No. 2 cury is pushed into the pores in the soil, the mercury
conditioned by reagent has been dramatically improved volume is equal to pore volume, and the pore size can be
after vacuum preloading. The VSSmax of No. 2 reached calculated according to the mercury pressure. In order to
24.9 kPa, with an average of 17.4 kPa, and the VSSmax explore the pore size and pore distribution properties after
of No. 1 reached 18.6 kPa, with an average of 11.7 vacuum preloading, sludge samples were taken at the sur-
kPa, which increased more than 10 times compared with face, and the positions were 1cm and 13cm away from
No. 3. Compared with No. 1, the VSSmax of No. 2 has the PVD. The test device is shown in Fig. 1 (g), and the test
increased by 33.8 %. The average VSS has increased by points are shown in Fig. 10. Due to the water content of
48.7 %, which indicates that reducing PVDs spacing is No. 3 is too high and the strength is too low, it is impossi-
conducive to sludge drainage consolidation. As the pore ble to take out stable samples, thus the pore distribution
water pressure continues to dissipate, the effective stress characteristics of No. 1 and No. 2 are only studied.
increases, then the VSS of sludge is further improved. It
can be seen from Table 5 that the distribution of VSS is
uneven. The farther away from the PVD along the radial 3.7.1. Macroscopic analysis of pores
direction, the lower the VSS is, and the strength close to It can be seen from Table 6 that within 1cm13cm away
the PVD is the highest, which is consistent with the distri- from the PVD, the void ratio of No. 1 is 0.52 and the void
bution properties of water content. ratio is 0.93; the void ratio of No. 2 is 0.56, and the void
It can be seen from Table 5 that the VSS of No. 3 ratio is 0.64. It can be seen that in the area close to the
remoulded sludge is the same as the in-situ strength, and PVD, the difference of the porosity in two model boxes is
the strength of No. 1 and No. 2 remoulded sludge is not significant. However, the farther away from the drai-
reduced compared with the in-situ strength. No. 1 drop nage plate, the larger the porosity difference will be.
by 13.1 kPa at most, and No. 2 drops by at most. The After FeCl3 pretreatment and combined vacuum
sludge’s strength decreased significantly after being dis- preloading, the average pore ratio of No. 1 and No. 2
turbed, which indicated that the structure of the sludge decreased more than 87 %, indicating that in the vacuum
treated by the reagent was improved considerably after preloading process, with the continuous discharge of pore
vacuum preloading. The sensitivity of No. 2 is more than water, the pore volume decreased significantly, which also
3.0, belonging to medium sensitivity soil, and the sensitivity explained the reason why the drainage rate slowed down
of No. 1 is also more than 1.6, close to medium sensitivity in the middle and later period of vacuum preloading. From
soil. the distance of 1cm13cm to the PVD, the porosity of

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X. Zhang et al. Soils and Foundations 61 (2021) 1630–1644

influence of double PVDs on the porosity is greater than


that of single PVD, which indicates that increasing the
number of PVDs or reducing the spacing of PVDs is con-
ducive to strengthening the effect of vacuum consolidation
between PVDs, expanding the influence range of vacuum
pressure (Chen et al., 2012), making the soil more compact
and consolidating.

3.7.2. Microscopic analysis of pores


The pore size distribution density obtained from the
MIP is shown in Fig. 12. The distance from the PVD is
113 cm, and the maximum pore density does not
change significantly. The distribution density of No. 2 is
the highest when the pore size is about 50  1000 nm,
and the maximum distribution density is 0.32 mL/g. In
No. 2 model box, the maximum pore density at 13 cm is
slightly higher than 1 cm. No. 1 has the highest distribution
density when the pore size is 6000 nm, and that of No. 2 is
800 nm. The corresponding pore size of No. 2 distribution
density is much lower than that of No.1. The results show
that with the increase of the number of PVDs or the
decrease of the spacing of PVDs, the influence range of vac-
uum pressure also increases. Thus, the large pores trans-
form into small pores. The macropores and mesopores
decrease obviously, and consolidation is improved.
It can be seen from Fig. 12 that, in the No. 1, the farther
away from the PVD, the wider the range of pore size distri-
bution, and the more small pores and micropores in the
range of 10500 nm; In the pore size range of 10  40
nm, the pore size distribution density of 2-1 is larger than
2-2; in the pore size range of 40  1000 nm, 2-2 is larger
than 2-1; there is no significant difference in the distribution
density of 2-1 and 2-2 more than 1000 nm, which indicates
that as sludge is drained and consolidated, large pores are
compressed into small pores; In addition, reducing the
spacing between drainage plates will lead to the increase
of small pore density and the decrease of large pore density.
The closer to the PVDs, the conversion rate of large pores
to small pores is improved, the small pores and micropores
increase, the degree of sludge consolidation is higher, and
the effect of vacuum preloading consolidation is better.
Besides, due to the high content of organic matter in land-
fill sludge and long storage time in landfill, long-term
biodegradation will lead to the change of pore network in
sludge, thereby improving the potential of sludge consoli-
dation. The consolidation efficiency of sludge was
enhanced by the action of biodegradation and vacuum
pressure. (Disfani et al., 2013; Tuncer B. Edil. et al., 1990)
In order to study the properties of pore distribution and
accurately describe the change of relative content of differ-
ent size pores, it is necessary to classify the pores. However,
there is no unified standard for the boundary value of pore
Fig. 11. Water content distribution curves. size division of soft clay and sludge (Delage and Lefebvre,
1984; Griffths and Joshi, 1989; Hua yang et al., 2009;
model box No. 1 increased by 0.14, and that of model box Lapierre et al., 1990). Shear et al. (1992) conducted a large
No. 2 increased by 0.03. It can be seen that the pore ratio number of experiments based on undisturbed and reconsti-
and porosity increase along the radial direction, and the tuted specimens of soft gray Pleistocene clay, and classified
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Table 5
Shear strength of sludge.
Depth (cm) Distance from PVD (cm) Sludge strength (kPa) Reshaped sludge strength (kPa) Sensitivity (St)
No.1 No.2 No.3 No.1 No.2 No.3 No.1 No.2 No.3
20 3 18.6 14.8 1.2 5.5 4.5 1.1 3.7 3.3 1.1
13 9.9 24.9 1 5.0 5.6 1 1.8 4.5 1
23 6.5 12.4 0.8 4.1 4.1 0.8 1.6 3.0 1

Table 6
Macroscopic index of porosity of surface sludge.
Depth Distance Porosity Void ratio
(cm) Origin No. 1 (Single PVD) No. 2 (Double PVDs) Origin No. 1 (Single PVD) No. 2 (Double PVDs)
sludge sludge
Within 5 cm 1 0.80 0.34 0.36 4.11 0.52 0.56
13 0.48 0.39 0.93 0.64

the pores in the clay. Therefore, based on Shear’s standard According to the pore division standard above, the vol-
and considering the micro-pore size distribution character- ume percentage content of each pore’ type was calculated,
istics of sludge, the pore diameter was divided into the fol- as shown in Fig. 13.
lowing four categories: ① macropores (d > 100000 nm); ② The pore size distributions of sludge at different sam-
mesopores (10000 < d < 100000 nm); ③ small pores (200 < pling positions are shown in Fig. 13. In the No. 1 model
d  10000 nm); ④ micropores (d  200nm). box, small pores and micropores’ content is 67.71 % at 1
cm away from the PVD and 61.82 % at 13cm. In the No.
2 model box, the content of small pores and micropores
at 1cm is 86.91 %, and that at 13 cm is 83.43 %.

Fig. 12. Pore size distribution density curves. Fig. 13. Changes in pore size distribution.
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X. Zhang et al. Soils and Foundations 61 (2021) 1630–1644

It can be seen that in the two model boxes, the spacing (4) As the distance from the PVD increases, the porosity
of PVD is reduced, the content of small pores and microp- and void ratio increase; the average pore ratio of No.
ores increased, the content of micropores and small pores 2 is smaller than that of No. 1, a contented the change
at 1cm was 5.89 % and 3.48 % more than that at 13 cm, rate of pore content and pore size is also lower, and
respectively. In the vacuum drainage consolidation process, the pore distribution is even than that of No. 1. After
the pores are compressed and filled with small particles, vacuum preloading, the contents of small pores and
resulting in a reduction in macropores and mesopores’ con- micropores are higher, which shows that reducing
tent. Therefore, the degree of consolidation near PVD is the PVD spacing can increase the influence range of
higher than that in other places, which also proves the rea- vacuum consolidation and transform the macropores
son for the occurrence of ‘‘soil piles” near PVD. As shown and mesopores into small pores and micropore,
in Fig. 13, the micropore content of No. 2 at 1cm is signif- improve the effect of drainage consolidation.
icantly higher than that at 13 cm. However, the micropore (5) With the progress of vacuum drainage consolidation,
content of No. 1 at 1 cm is less than that at 13 cm, which is pore water is discharged through PVD. Under the
maybe due to the small particles discharged through the fil- action of pore water, small particles gradually move
ter membrane pores during vacuum consolidation, result- towards PVD and aggregate, forming a vacuum clog-
ing in the pore size at 1cm becoming larger. ging zone. The clogging area has high strength, few
Compared with No. 1 and No. 2, the content of micro- pores, and low water content, which result in less set-
pores at 1 cm of No. 1 is 5.89 % more than that at 13 cm in tlement around PVD, just like a ‘‘soil pile”.
12 cm, while that of No. 2 is only 3.48 %, the pore size dis-
tribution of No. 2 is more even along the radial direction. It
can be seen that the pore size of No. 1 changes more obvi- 5. Data Availability Statement
ously, because in the process of vacuum drainage consoli-
dation, PVD is mainly used to transfer vacuum load, and All data, models, and code generated or used during the
there will be some loss of vacuum pressure along the radial study appear in the submitted article.
direction (Zhu et al., 2010). The closer to PVD, the higher
the vacuum pressure and the better the consolidation effect.
Acknowledgements
It is shown that increasing the number of PVD or reducing
the spacing of PVDs can reduce the dissipation of vacuum
The authors are grateful for the financial support for the
pressure, which is conducive to increase the influence range
study presented in this paper from the Shanghai Sailing
of vacuum consolidation.
Program (Grant No. 19YF1415500), the National Natural
Science Foundation of China (Grant No. 41772303) and
4. Conclusion
Shanghai Municipal Science and Technology Commission
(Grant No. 20DZ2250800).
(1) After conditioning by FeCl3, the SRF of No. 1 and
No. 2 is significantly reduced, the intracellular water
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