Filename Miel 2

Instrument 5343-0070
Operator Julieth García
rundate 2/3/2022
Sample nameMiel 2
Geometry na 40.0mm 1.00972° cone plate, Peltier plate Aluminium, Solvent Trap - 62771
Procedure n Sample
Flow ramp
procedurese Flow ramp
[File Parameters]
Name Miel 2
Instrument t Discovery HR20
Instrument s Offline
Instrument 5343-0070
Instrument loCICAT
Company na REOMETRO-CICAT
Trios version 5.1.0.46403
File name C:\ProgramData\TA Instruments\TRIOS\Data\CICAT\2022\Fenómenos\Miel 2.tri
Instrument f 11.13
Run date ###
Time at start 40.7421
[Geometry Parameters]
Geometry Ty Cone plate
Name 40.0mm 1.00972° cone plate, Peltier plate Aluminium, Solvent Trap - 62771
Diameter 40.0 mm
Cone angle 01:00:35 deg:min:sec
Truncation g 101.0 µm
Loading gap 60000.0 µm
Trim gap offs 51.0 µm
Material Aluminium
EnvironmentaPeltier plate
Serial numbe 2.8596E+10
Notes
[Geometry Extended Parameters]
Expansion coe1.06624 µm/°C
Expansion coeyes
Compliance 1.03 mrad/N.m
Geometry Ine3.04077 µN.m.s²
Friction 0.288447 µN.m/(rad/s)
Friction corr yes
Stress consta 59683.1 Pa/N.m
Strain consta 56.7441 1/rad
Normal Stres 1591.55 Pa/N
Fluid Density 2.36E-11
[Instrument Options]
ETC camera ano
Friction 0.288447 µN.m/(rad/s)
Friction calib ###
Friction corr yes
Rotational m ###
Rotational m 40.0mm 1.00972° cone plate, Peltier plate Aluminium, Solvent Trap - 62771
Rotational ma 2
Rotational m standard
Smart swap eyes
[Temperature Options]
Current temp1.06624 µm/°C
Current temp0.000 °C
Current temp 1
Gap temperat ###
Gap temperatyes
Purge gas onlno
Temperature yes
Temperature Peltier plate
Upper temperno
Temperature 00:00:10 hh:mm:ss
Temperature 0.200000 °C
[Inertia Options]
Instrument in21.0311 µN.m.s²
Instrument in ###
[Gap Options]
Axial force f 1.00000 N
Closure dista 1000.00 µm
Closure profilnone
Closure veloc 100.000 µm/s
Gap velocity 32000.0 µm/s
Gap velocity (3000.00 µm/s
Gap velocity 32000.0 µm/s
Gap zero mo standard (DHR) or deceleration (AR)
Gap handling Falag mismatches between geometry and instrument gap
Gap toleranc 4.00000 µm
Gap wait dur 00:00:02 hh:mm:ss
Override waitno
[Axial Force Control]
Axial force a Return to initial value
Control axial no
Control axial 1000.00 µm
Control axial 1000.00 µm
Control axial 0.100000 N
Control axial no
Control axial Compression
Controlled axi1.00000 N
[Flow Options]
Flow collect ayes
Flow collect yes
Flow inertia yes
Flow non-ste 1.00000e-6 rad/s
Flow torque l 0.0100000 µN.m
Flow velocity 1.00000e-6 rad/s
Flow velocity 5.00%
Flow zero strayes
[Oscillation Options]
Oscillation d 1.00000e-5 rad
Oscillation d 5.00%
Oscillation ra 170.000 °
Oscillation to 0.100000 µN.m
Oscillation t 1.00%
Oscillation ve 5.00%
[Conditioning Options]
Zero axial fo no
Zero speed afLeave as is
Zero velocity 0.100000 rad/s
[Experiment all steps options]
Maximum axial 50.0000 N
Minimum axial 0.100000 N
Temperature 1t .00000 °C
Flow ramp - 1
Stress Shear rate Viscosity Step time Temperature Normal stress
Pa 1/s Pa.s s °C Pa
15.8162 1.23457 12.8111 3.14707 25 -20.5061
24.426 1.94103 12.584 9.50275 25 -4.07318
36.4048 2.9852 12.1951 15.7287 25 -10.8441
54.371 4.61 11.7941 22.0201 25 -8.51927
83.0274 7.0852 11.7184 28.246 25 6.81198
127.176 10.896 11.6717 34.472 25 33.4135
195.418 16.8272 11.6132 40.7634 25 -58.4404
297.955 25.8614 11.5212 46.9893 25 -30.3373
456.198 39.7714 11.4705 53.2153 25 -13.3663
700.465 61.4206 11.4044 59.5067 25 14.0739
1075.25 94.8543 11.3358 65.7982 25 95.3647
1641.3 145.78 11.2587 72.0241 25 6.60258
2503.95 224.191 11.1689 78.25 25 85.9894
3831.17 346.227 11.0655 84.5415 25.01 162.492
5813.63 532.109 10.9256 90.7674 25.02 305.461
8628.36 814.368 10.5952 96.9278 25.04 359.155