U 926 Muffle Furnace

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Date Entry Sheet for DUC &

Env. Temp. & 25.1 °C Env. Temp. & 26.3


Humidity Before Humidity After
50 %RH 43
DUC Name Digital Thermometer With R-Type T/C Range (0 to 1200) °C
Make Mextech L. Count 0.1 °C
Model DT-9 Sr.No. 170203905

Inst. Location. -----


Temperature (°C)

100 °C 300 °C 500 °C 700


Standard
Calibraiton Standard DUC Standard DUC Standard DUC Standard
Point Readings Reading Readings Reading Readings Reading Readings

°C °C °C °C °C °C °C °C

100.22 100.0 300.41 300.0 500.52 500.0 700.71


100
100.23 100.0 300.42 300.0 500.53 500.0 700.72
100.24 100.0 300.44 300.0 500.54 500.0 700.74
300
100.25 100.0 300.45 300.0 500.55 500.0 700.75

100.26 100.0 300.46 300.0 500.56 500.0 700.76


500
100.27 100.0 300.47 300.0 500.58 500.0 700.77
100.28 100.0 300.48 300.0 500.59 500.0 700.78
700
100.29 100.0 300.51 300.0 500.62 500.0 700.78

100.31 100.0 300.52 300.0 500.63 500.0 700.79


1200
100.32 100.0 300.54 300.0 500.64 500.0 700.81
Average 100.27 100.00 300.47 300.000 500.58 500.000 700.76
te Entry Sheet for DUC & Observation
°C Location At Site
%RH SRF No 52/20
C Calibration Date 26/06/2020
Source Low Temp Bath & 9144
Master SPRT with Indicator
Inst./Tag ID. TH-01

°C 1200 °C
DUC Standard DUC
Reading Readings Reading Error Resolution of Uniformity of Stability of Master
DUC Source Source Uncertainty

°C °C °C °C °C °C °C ±°C

699.9 1200.83 1199.9


-0.267 1 0.1 0.03 0.04
699.9 1200.85 1199.9
699.9 1200.86 1199.9
-0.470 1 0.6 0.05 0.04
699.9 1200.88 1199.9

699.9 1200.89 1199.9 -0.576 1 0.6 0.05 0.04


699.9 1200.92 1199.9
699.9 1200.94 1199.9
-0.861 1 0.6 0.05 0.04
699.9 1200.95 1199.9

699.9 1200.96 1199.9


-1.006 1 0.8 0.05 0.04
699.9 1200.98 1199.9
699.900 1200.91 1199.90
°C

Expanded
Uncertainty

±°C
0.58

0.89

0.89

0.89

1.07
Calibration Certificate
ULR No.: CC309622000000926F
Certificate No.: CCTPL/DB/0116/34 Field: Thermal
SRF No.: 100/22 Date of Receipt: 02/06/2022
SRF Date: 29/05/2022 Date of Calibration: 02/06/2022
Company Name & M/s. ARC Testing Laboratory Recommended Due Date.:
Address 01/06/2023
(As per agreed by customer)
Kh. No.42/9/4, Village-Badli, Near Astha
Hospital, New Delhi-110042 Certificate Issue Date: 05/06/2022

DUC* Details
Digital Temp. Indicator (Thermocouple
Instrument Name: Instrument Sr. No.: -----
Sensor)
Make: PSI Instrument Id No.: ATL/DTI-01
Model No.: ----- Location: Lab
Range: (0 to 1200) °C DUC Condition: OK
Readability: 0.1 °C Calibration Performed at: At Site
Standard Equipments Used(Traceable to National Standard)
Sr. No Instrument Name Cert. No Cal. By Calibration Due Date
1 S-Type Thermocouple 30051509 BELZ 28/03/2023

Temperature Humidity Reference Standard Calibration Procedure No.


Environment Condition
26.8 ºC 55 %RH DKD-R-5-1 CCTPL/TH/CP/03

Calibration Result

Sr. No. Nominal Temperature Standard Reading DUC* Reading Deviation Expanded Uncertainty

(°C) (°C) (°C) (°C) ±(°C)


1 100 100.27 100.0 -0.27
2 300 300.47 300.0 -0.47
3 500 500.58 500.0 -0.58 2.17

4 700 700.76 699.9 -0.86


5 1200 1200.91 1199.9 -1.01
Note : DUC* : Device Under Calibration
Uncertainty of measurment at approx 95% Confidence Level with coverage factor k = 1.96

Calibrated By : Amit Pal Approved By : Sandeep Sharma


Calibration Engineer Director

Note. 1.This Certificate only to the particular instrument submitted for calibration.
2.This Calibration Result reported in this certificate valid at the time of and under the stated condition of measurement.
3.This particular certificate can not be reproduce except in full, without prior permission of CCTPL.

`--- End of Certificate --- Page 1 of 1


Calibration Observation Sheet for Thermal
Calyss Calibration & Testing Pvt. Ltd.
CCTPL/QF/6.4/05/T-01
Issue Date:08/07/2019 Amd Date:00
F-40, Sector-9, Noida-201301,UP
Issue No: 01 Amd No: 00

1 S.R.F. No.: 2 Job Order Number:


3 Calibration Date: 26//06//2020 4 Rcoommended Date of Next Calibration : 01//06//2023
5 Instrument Details(DUC) :
Digital Temp. Indicator PSI
Name: Readablity : 0.1 °C Make/Model :
(Thermocouple Sensor) -----

Range : (0 to 1200) °C ID/Sr.No: ATL/DTI-01 / ----- Location: At Site

6 Instrument Details (Standard):


Name: S-Type Thermocouple ID/Sr.No: CCTPL/TH/R-1909 Calibrated By: BELZ
Make/Model : Fluke/5609 Cert. No: 30051509 Cal.Valid upto: 28//03//2023
7 Instrument Details (Source):
Name : ID/Sr No.: Make/Model :
8 Enviromental Condition :
Before: 25.1 Before: 50
Temperature (ºC): Humidity(%RH):
After : 26.3 After: 43

9 Observations:
Set Value: 100 ˚C Set Value: 300 ˚C Set Value: 500 ˚C
Display Value: Display Value: Display Value:
Sr. No.
Reading of Std Reading of DUC Reading of Std Reading of DUC Reading of Std Reading of DUC
(˚C) (˚C) (˚C) (˚C) (˚C) (˚C)

1 100.22 100.0 300.41 300.0 500.52 500.0


2 100.23 100.0 300.42 300.0 500.53 500.0
3 100.24 100.0 300.44 300.0 500.54 500.0
4 100.25 100.0 300.45 300.0 500.55 500.0
5 100.26 100.0 300.46 300.0 500.56 500.0
6 100.27 100.0 300.47 300.0 500.58 500.0
7 100.28 100.0 300.48 300.0 500.59 500.0
8 100.29 100.0 300.51 300.0 500.62 500.0
9 100.31 100.0 300.52 300.0 500.63 500.0
10 100.32 100.0 300.54 300.0 500.64 500.0

Remarks: ..........................................................................................................................................................

Calibrated by: Checked by:

Prepared By: Approved By: Issued By:


Quality Manager Director Quality Manager
Calibration Observation Sheet for Thermal
Calyss Calibration & Testing Pvt. Ltd.
CCTPL/QF/6.4/05/T-01
Issue Date:08/07/2019 Amd Date:00
F-40, Sector-9, Noida-201301,UP
Issue No: 01 Amd No: 00

10 Observations:
Set Value: 700 ˚C Set Value: ### ˚C Set Value: %RH
Display Value: Display Value: Display Value:
Sr. No.
Reading of Std Reading of DUC Reading of Std Reading of DUC Reading of Std Reading of DUC
(˚C) (˚C) (˚C) (˚C) (%RH) (%RH)

1 700.71 699.9 1200.83 1199.9


2 700.72 699.9 1200.85 1199.9
3 700.74 699.9 1200.86 1199.9
4 700.75 699.9 1200.88 1199.9
5 700.76 699.9 1200.89 1199.9
6 700.77 699.9 1200.92 1199.9
7 700.78 699.9 1200.94 1199.9
8 700.78 699.9 1200.95 1199.9
9 700.79 699.9 1200.96 1199.9
10 700.81 699.9 1200.98 1199.9

11 Observations:
Set Value: %RH Set Value: %RH Set Value: %RH Set Value: %RH
Disp. Value: Disp. Value: Disp. Value: Disp. Value:
Sr.No.
Reading of Reading of Reading of Reading of Reading of Reading of Reading of Reading of
Std (%RH) DUC(%RH) Std (%RH) DUC(%RH) Std (%RH) DUC(%RH) Std (%RH) DUC(%RH)
1
2
3
4
5
6
7
8
9
10

Remarks: ….......................................................................................................................................................

Calibrated by: Checked by:

Prepared By: Approved By: Issued By:


Quality Manager Director Quality Manager
Uncertainity Calculation Sheet
1. Laboratory : CCTPL

3. Standard / Equipment Used for Calibration

Details of Standard Used Standard1 Source


Instruments Name : SPRT with Indicator Low temp. Negative Bath
Manufacturer/Model : Fluke/5609 Tempsens
Sr.No./I.D.No: CCTPL/TH/R-1909 CCTPL/TH/R-1915
Range : (-15 to 660 degree C) (-145 to 110 degree C)
Certificate No. FL/CAL/TH/07082019-C001
CalibrationDate&validity 28.08.2019 & 28.08.2020
Traceability: Farelabs Gurugram

4.Environmental Condition During Calibration


Temperature 25±2 0 Humidity 55±10 % RH

5. Evaluation
100 °C 300 °C 500 °C 700
Standard Standard DUC Standard DUC Standard DUC Standard
Calibraiton Readings Reading Readings Reading Readings Reading Readings
Point

°C °C °C °C °C °C °C °C
100.220 100.000 300.410 300.000 500.520 500.0 700.71
100 100.230 100.000 300.420 300.000 500.530 500.0 700.72
100.240 100.000 300.440 300.000 500.540 500.0 700.74
300 100.250 100.000 300.450 300.000 500.550 500.0 700.75
100.260 100.000 300.460 300.000 500.560 500.0 700.76
500 100.270 100.000 300.470 300.000 500.580 500.0 700.77
100.280 100.000 300.480 300.000 500.590 500.0 700.78
700 100.290 100.000 300.510 300.000 500.620 500.0 700.78
100.310 100.000 300.520 300.000 500.630 500.0 700.79
1200 100.320 100.000 300.540 300.000 500.640 500.0 700.81
Average 100.267 100.000 300.470 300.000 500.576 500.000 700.761
Standard 0.03 °C 0.04 °C 0.042999 °C 0.0314
Deviation

TYPE B UNCERTAINTY EVALUATION

Ub1: Source: Uncertainty of Reference Instruments SPRT with Indicator


(Taken from the calibration certificate)

b1 = num ˚C Diviser-k: 2
Assuming Normal Distribution,Ub1= b1/k=
Degree of freedom V1 = infinite

Ub2: Source: Uncertainty due to Uniformity of Bath (Source)


(Taken from Manufacturer's Specification of Bath)

b2 = num ˚C Diviser-k: 1.7320508


Assuming Rectangular Distribution,Ub2= b2/k=
Degree of freedom V1 = infinite
Ub3: Source: Uncertainty due to Stability of Bath (Source)
(Taken from Manufacturer's Specification of Bath)

b3 = num #REF! Diviser-k: 1.7320508


Assuming Rectangular Distribution,Ub3= b3/k=
Degree of freedom V1 = infinite

Ub4: Source: Uncertainty due to Reolution of DUC)


Since the limits given are half the count, and assuming Rectangular Distribution

Resolution Multiplier b4 Diviser Ub5


o
C Sqrt(3)
0.01 0.5 0.005 1.732051 0.0028868

Uncertainty,Ub5 = b4 / √3

Combined Uncertainty Range


Ua
𝑼𝒄=√(∑129_(𝒊 Ub1
=𝟏)^𝑵▒𝑼_𝒊^𝟐
) Ub2
Ub3
Ub4
Uc = √ [(Ua)2+(U1)2+(U2)2+…+(Un)2] Uc
Coverage
Factor
Expanded
Expanded Uncertainty at 95% Confidence level :- Uncertainity
Expanded Uncertainty U = k x Uc

Effective degree of freedom :- Range


Veff
Veff = Uc4(Y)
[Σ{(ui4(Y / Vi)}] Range
Final Result= 100
300
500
700
1200
Uc=√(∑1
𝑼𝒄=√(∑129_(𝒊 With Coverage Factor K=2 at 95 %Confidence Level
29_(i=1)^
=𝟏)^𝑵▒𝑼_𝒊^𝟐
N▒U_i^2
) )
˚C

°C 1200 °C
DUC Standard DUC Standard Type A Uncertainty
Reading Readings Reading Deviation Uncertainty of Standard
Error Instrument Uniformity
(±)

°C °C °C °C °C °C °C °C
699.9 1200.83 1199.9
-0.267 0.03 0.0105462 0.04 0.1
699.9 1200.85 1199.9
699.9 1200.86 1199.9
-0.470 0.04 0.0135810 0.04 0.6
699.9 1200.88 1199.9
699.9 1200.89 1199.9
2.000 0.04 0.0135974 0.04 0.6
699.9 1200.92 1199.9
699.9 1200.94 1199.9
-0.861 0.03 0.0099387 0.04 0.6
699.9 1200.95 1199.9
699.9 1200.96 1199.9
-1.006 0.05 0.0162070 0.04 0.8
699.9 1200.98 1199.9
699.900 1200.906 1199.900
°C 0.051 °C

T with Indicator

Range
100 300 500 700 1200
0.04 0.04 0.04 0.04 0.04
0.02000 0.02000 0.02000 0.02000 0.02000

Range
100 300 500 700 1200
0.1 0.6 0.6 0.6 0.8
0.05774 0.34641 0.34641 0.34641 0.46188

Range
100 300 500 700 1200
0.03 0.05 0.05 0.05 0.05
0.017321 0.028868 0.028868 0.028868 0.028868

ar Distribution

Range
100 300 500 700 1200
1 1 1 1 1
0.28868 0.28868 0.28868 0.28868 0.28868

100 300 500 700 1200


0.010546 0.013581 0.013597 0.009939 0.016207
0.020000 0.020000 0.020000 0.020000 0.020000
0.057735 0.346410 0.346410 0.346410 0.461880
0.017321 0.028868 0.028868 0.028868 0.028868
0.288675 0.288675 0.288675 0.288675 0.288675
0.295767 0.452494 0.452495 0.452400 0.546043

1.96 1.96 1.96 1.96 1.96

0.5797026 0.8868889 0.8868898 0.8867033 1.07024376

100 300 500 700 1200


5.57E+06 1.11E+07 1.10E+07 3.86E+07 1.16E+07

100.000 ± 0.58
300.000 ± 0.89
500.000 ± 0.89
699.900 ± 0.89
1199.900 ± 1.07
Stability Resolution

°C °C
0.03 1

0.05 1

0.05 1

0.05 1

0.05 1

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