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A Capacitive Sensor System For The Analysis of Two-Phase Ows of Oil and Conductive Water
A Capacitive Sensor System For The Analysis of Two-Phase Ows of Oil and Conductive Water
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A capacitive sensor system for the analysis of two-phase flows of oil and
conductive water
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Article history: A sensor system for the study of oil–water flow in pipes is proposed. The purpose is to estimate the area
Received 29 April 2010 fraction occupied by each fluid in a given section of the pipe, taking advantage of the difference in dielectric
Received in revised form 14 July 2010 permittivity between the fluids. The estimation is done by capacitance measurements between electrodes
Accepted 15 August 2010
flush-mounted on the external surface of a nonconductive section of the pipe. A key contribution of the
Available online 20 August 2010
present work is to propose a solution to the problem of capacitive sensing in presence of conductive
water which introduces parasitic coupling to stray elements outside the measurement section of the
Keywords:
pipe. To this purpose it is proposed a novel sensor configuration that employs guard electrodes, coupled
Capacitive sensor
Capacitance probe
to a tailored electronic interface to drive the guard electrodes and amplify the measurement signal at
Two-phase flow 2 MHz. The sensor system has been designed, manufactured and tested in an experimental plant where
Oil–water flow flows of oil–tap water have been generated. The results obtained from the developed sensor system
for different fluid fractions have been compared with those obtained by the Quick Closing Valve (QCV)
technique adopted as a reference. Differences between the two methods below 3% have been found in
the estimations of the normalized oil-area fraction.
© 2010 Elsevier B.V. All rights reserved.
0924-4247/$ – see front matter © 2010 Elsevier B.V. All rights reserved.
doi:10.1016/j.sna.2010.08.018
M. Demori et al. / Sensors and Actuators A 163 (2010) 172–179 173
Fig. 1. Cross-section of the pipe with oil–water flow (a); capacitive technique
schematization with definitions of material properties (b).
(ds − lo )/2 1 lo
Cwp = ε0 εw ; Rwp = ; Co = ε0 εoil .
lo w (ds − lo )/2
(2b)
Eq. (4) shows that the impedance ZS can be expressed as the sum Fig. 3. Computed phase (a) and magnitude (b) of the impedance per unit axial length
of three terms. The first term does not depend on Ho because it is ZS as a function of the oil fraction Ho for different values of frequency.
only related to the capacitance of the pipe wall. The second term
shows a dependence on Ho only in the magnitude, and the third
As mentioned and shown in Figs. 3a and b and 4, the frequency
term is a function of Ho both in the magnitude and in the phase.
directly influences the sensitivity. This is due to the conductive
As a consequence, it is difficult to immediately determine the
water that, for certain flow regimes such as the investigated core-
effect of Ho on ZS from the analytic expression of Eq. (4). However,
annular flow, completely separates the pipe internal wall from the
by inserting into Eq. (4) the material parameters and dimensions for
oil, thereby acting as a shield for the oil inner region. For frequen-
each region, the impedance ZS as a function of the oil fraction Ho can
cies in the order of 1 MHz and higher, the quantities w and ωε0 εw
be calculated for different frequencies. This has been done by using
in Eq. (4) become of the same order of magnitude. In this way
the following values, which account for the physical dimensions of
the dielectric behavior of water becomes comparable to the con-
our pipe and electrical characteristics of pipe and fluids: dp = 2 mm,
ductive behavior, resulting in an increased sensitivity. The analysis
ds = 19.64 mm, εp = 3.4, εw = 80, and w = 0.03 S/m.
shows that to detect hold-up values across a suitably wide range it
The results for the magnitude and phase of ZS as a function of Ho
is necessary to operate with frequencies in the order of 1 MHz or
for different frequencies ranging from 100 kHz to 5 MHz are shown
higher.
in Fig. 3a and b, respectively. As it can be seen, at 100 kHz there
The above results of the analysis on the measurement sec-
are no substantial variations of ZS as a function of Ho except for
tion impedance confirm what found in previous works where
Ho very close to 1. Therefore, at this frequency and below, it is not
comparatively high frequencies were used to extract the hold-
possible to obtain the adequate sensitivity to measure Ho across a
up information from the impedance between electrodes. In these
wide range. Increasing the frequency, the sensitivity increases as
works the adoption of AC capacitance meters, RF capacitance
can be seen from the results obtained for 2 and 5 MHz. Analyzing
meters or systems based on phase shift measurements were
the phase trend of Fig. 3a, it can be observed that for the most part of
described [3,10,14–18].
the values assumed by Ho the phase remains near −90◦ . This means
that the behavior of ZS can be mainly considered as dominated by
capacitive effects in spite of the presence of a conductive fluid. The
considered pipe is made by a purely dielectric material (Plexiglas)
with a finite thickness and the pipe walls act as two capacitances
in series to the actual impedance of the fluids. The value of these
capacitances is expressed by the first term of Eq. (4) and, from the
results of Fig. 3a and b, this value is dominant for most part of the
values assumed by Ho .
Further insight in the behavior of ZS can be obtained by analyz-
ing the trend of the admittance per unit axial length YS = (1/ZS ) that
is plotted in Fig. 4 where the real and imaginary components are
separately shown. As expected, the dominant part of YS is the imag-
inary component because of the prevailing capacitive behavior of
ZS . The imaginary part of YS is also monotonically sensitive to Ho .
Therefore, from a measurement viewpoint, it is expected that the
Ho information can be conveniently extracted from the imaginary Fig. 4. Computed real and imaginary parts of the admittance per unit axial length
part of YS or from a quantity directly linked to it. YS = (1/ZS ) for different values of frequency.
M. Demori et al. / Sensors and Actuators A 163 (2010) 172–179 175
simplified model the lumped impedances Z, ZGL and ZGR are divided
into two equal parts in order to introduce the conductive path along
the pipe represented by the impedances ZR and ZL . The impedances
ZLL and ZLR represent the terminal elements where all the external
couplings are assumed to be concentrated.
From this model it is evident that to minimize the effect of exter-
nal couplings it is necessary to limit the leakage currents ILL and
ILR flowing through ZL and ZR . This can be obtained by forcing the
nodes R and L in the model of Fig. 6b at the same potential of node
X. In this way, the measurement section becomes isolated from the
remaining pipe and therefore it is not influenced by the impedances
ZLL and ZLR due to the external couplings. In practice, however,
Fig. 5. Simplified schematization of the coupling between the measurement section nodes R, L and X are not directly accessible and, as such, perfectly
and external elements along the pipe by conductive water paths, and corresponding equal potentials cannot be achieved.
leakage currents.
To approach as much as possible this target condition it is neces-
sary to use the same polarization for the corresponding electrodes
2.2. External couplings in the measurement and the guard sections. This is achieved by
placing the three electrodes represented on the high side of Fig. 6b
The capacitance technique applied to a conductive fluid creates at the potential VP and the corresponding opposite electrodes at
problems not only related to the phenomena that take place in the zero potential. In addition, it is necessary that ZGL and ZGR are
cross-section, but also due to effects that occur along the pipe. The made low enough to allow the current passing through them to
conductive fluid creates conductive paths that may couple the mea- be much higher than the current through ZLL and ZLR . To reduce
surement section with the up-stream and down-stream portions of ZGL and ZGR two ways can be used: (1) to increase the length LG of
the pipe and the surroundings. the guard electrodes, which provides a correspondent reduction of
If, for instance, we consider an insulating pipe filled by water, as ZGL and ZGR ; (2) to increase the working frequency since ZGL and
shown in Fig. 5, the cylinder of fluid inside the pipe can be seen as ZGR are expected to have the same dominantly capacitive behavior
two pieces of conductive wire originating from the measurement described for ZS in Section 2.1.
section and extending outwards. Such conductive paths are cou-
pled with the surroundings in two different ways that we define
as external couplings. The first possible coupling mechanism is by 3. System description
direct contact with the metallic parts of the hydraulic set-up, such
as pumps. The second possible mechanism is the capacitive cou- The sensor can be divided into three principal parts as shown
pling between the conductive water and metallic parts that can in the block diagram of Fig. 7: the measurement head made by
be present nearby, such as mounting fixtures and supports. Exter- the electrodes along the pipe; the interface and signal-conditioning
nal couplings can cause two effects due to signal leakage from the electronic circuit; and the measurement data acquisition and visu-
measurement section, and to interference injection into the mea- alization system.
surement section, respectively. In the practical cases, the latter The measurement head has electrodes that are directly placed
effect can be minimized by a proper system layout and an adequate facing each other on the external surface of a nonconductive sec-
filtering and it will be therefore neglected in the following. The for- tion of the pipe. A Plexiglas tube with inner and outer diameters
mer effect can significantly perturb the measurement process and of 21 and 25 mm respectively has been used for the pipe. Spe-
therefore it will be considered in more detail. cial care has been devoted to the dimensioning of the electrodes,
With reference to Fig. 5, if we measure the impedance between in particular to counteract the effects of the conductive fluid, by
the electrodes by imposing a potential difference and measuring using electromagnetic Finite-Element Method (FEM) simulations
the correspondent current, it is evident that the measurement is and preliminary experimental tests. For the measurement section,
influenced by the external couplings. These external couplings rep- an electrode axial length LM = 10 cm and an arc length e = 90◦ have
resent additional paths from which currents ILL and ILR can leak been chosen in order to obtain the required spatial resolution and
out from the measurement section in the axial direction along the to ensure a good sensitivity to the phenomena at the center of the
pipe. For a given system configuration, this could be considered as pipe. For the guard sections, an electrode axial length LG = 40 cm
a systematic effect that could be virtually corrected for. However, and an arc length e = 90◦ have been chosen.
when oil is also present in the pipe together with water, the sec- The transduction electronic circuit has been developed to mea-
tion of the conductive path varies with Ho , which is the quantity we sure at a given probing frequency fp = ωp /2 the imaginary part of
want to measure, and therefore the estimation of the external cou- the admittance Y = 1/Z of the measurement section, which can be
plings necessary to correct the measurement is not straightforward. directly linked to Ho as described in Section 2. The imaginary part of
From these considerations, it is clear that the external couplings Y at fp can be seen as due to an effective capacitance C = Im(Y)/ωp .
prevent the accurate measurement of the impedance between the In presence of nonconductive fluids only, the overall behavior of
electrodes and the reliable estimation of Ho . the system of materials between the electrodes would be purely
In order to minimize the perturbing action due to external cou- capacitive and the effective capacitance C would be exactly the
plings, a properly designed configuration of the sensor system is capacitance seen between them. The present system could then be
here proposed. The configuration is based on the introduction of compared with capacitance probes developed by other authors, yet
two guard sections placed along the pipe before and after the mea- offering the added capability to operate also in presence of fluids
surement section and having the same electrode opening angle of with nonzero conductivity.
the measurement section, as shown in Fig. 6a. With reference to Fig. 6b, the three high-side electrodes in the
The system can be modeled by denoting with Z the impedance sensor head are connected together to the terminal P. The two
between the electrodes of the measurement section, and with ZGL low-side guard electrodes are connected together to terminal GND,
and ZGR the impedances between the guarding electrodes at the while the low-side measurement electrode is connected to ter-
left and right sides of the measurement section respectively. In this minal M. The circuit excites terminal P with a sinusoidal voltage
176 M. Demori et al. / Sensors and Actuators A 163 (2010) 172–179
Fig. 6. Electrodes of the measurement and guard sections (a); axial section of the pipe with electrode configuration and the lumped impedance simplified model to account
for the external coupling and the guarding action (b).
Vp (t) = Ap cos(ωp t), while terminal GND is grounded. The terminal 656, which allows the use of a RF large enough to have ωp CF RF 1
M is connected to the virtual ground of a transimpedance amplifier, (CF = 50 pF, RF = 10 M). Under this condition the amplifier transfer
which senses the current collected by the low-side measurement function is given by:
electrode while holding it at the same null potential of the neigh-
boring guard electrodes. Vo (1/jωp CF ) Y
=− =− . (5)
The transimpedance amplifier is composed of an inverting- Vp Z jωp CF
configuration operational amplifier where the feedback impedance ωp CF RF 1
Fig. 7. Block diagram of the complete sensor system where the connections to the measurement and guard sections of the sensor head, represented by terminal pairs (P, M)
and (P, GND) respectively, are schematized.
M. Demori et al. / Sensors and Actuators A 163 (2010) 172–179 177
Eq. (6) shows that, with respect to the excitation signal Vp (t), the
output voltage Vo (t) can be divided into an in-phase part propor-
tional to the imaginary part of Y, and a quadrature part proportional
to the real part of Y. To perform phase-sensitive demodulation,
the signal Vo is multiplied by Vp by an analog multiplier circuit
based on the AD835, and the resulting output is low-pass filtered
by a 2nd-order filter with a cut-off frequency of 20 Hz. In this
way, a narrow-band filtering effect around fp is obtained, which
rejects wideband noise and the electromagnetic interference pos-
sibly picked-up by the sensor electrodes. The filter output signal is
level-shifted by the adjustable DC voltage Vref and then amplified
by a gain G to adapt the signal level for the following acquisition.
The overall output Vmeas of the transduction circuit is a DC volt-
age given by: Fig. 8. Output voltage and RCD for a sequence of flows with three different values
of oil hold-up HO . The inset pictures shows a section of the correspondent flow are
A2p /1V Im(Y (ωp )) A2p /1V taken by a lateral position along the transparent pipe.
Vmeas = G − + Vref = −G C + GVref , (7)
2CF ωp 2CF
establish the minimum signal variation that can be related to the oil
where the term 1 V accounts for the dimensional gain introduced by
fraction variation. These parameters in turn quantify the short-term
the analog multiplier. The role of the adjustable offset voltage Vref is
and medium-term measurement resolution, respectively. In the
to adapt the circuit to the most common case where the variations
condition of pipe completely filled with water, noise levels of about
of C due to the oil fraction variations are much smaller than the
1.5 mVrms , and 2.5 mVrms have been measured over an integration
absolute value of C. For this reason, it is necessary to have high sen-
time of 10 s in no flow and steady flow conditions, respectively.
sitivity while at the same time it is important to center the dynamics
The slight increase in the noise level in the flow condition is due to
of Vmeas around a given absolute value of C. For instance, it can be
the increased electromagnetic noise generated from the electrical
easily possible to adjust at zero the signal Vmeas for a fixed condi-
pumps actuation. On a long term operation, a base-line drift in the
tion, e.g. pipe filled with water, and then evaluate the Ho variations
signal Vmeas lower than 15 mV per hour has been measured for the
from such preset value.
water-filled pipe in either no flow and steady flow conditions.
The variation of the output Vmeas with respect to C defines the
Thereafter, the system has been experimentally tested in the
system sensitivity SC given by:
core-annular flow configuration. An example of the typical mea-
2
Ap /1V sured output signal is illustrated in Fig. 8, where the voltage Vmeas
∂Vmeas
SC = = −G . (8) is plotted as a function of time during a sequence of three subse-
∂C 2CF
quent flow conditions corresponding to three different increasing
Assuming a positive gain G, SC is negative. This conveniently deter- oil fractions. As expected, the system detects the different oil quan-
mines that an increase of Ho produces an increase in Vmeas . tities by providing different mean values of Vmeas . In addition, the
The circuit has been designed by choosing a probing frequency system is also sensitive to the flow fluctuations as can it be seen by
fp = 2 MHz which is adequately high according to what discussed in the oscillations around the mean value, which are well beyond the
Section 2, Ap = 1 V, and G = 200. These values result in a sensitivity resolution threshold set by background noise level.
|SC | = 2 V/pF which is high enough to estimate Ho even in the worst Fig. 8 reports on the right axis the Relative Capacitance Differ-
case when conductive water acts as a shield. ence RCD [3]:
The DC voltage Vmeas is then fed to the data acquisition and
visualization system which is based on a 16-bit A/D data acquisi- C − Coil Vmeas − Vwater
RCD = =1− . (9)
tion board, National Instruments PCI-6259, connected to a personal Cwater − Coil Voil − Vwater
computer. A dedicated program written in LabVIEW allows the con- The RCD is a dimensionless quantity that represents the relative
tinuous visualization over time of the measured values in order to variations of the effective capacitance C with respect to the end-
estimate C, the associated fluid fractions and their fluctuations. point conditions obtained with the pipe filled of either oil (Coil , Voil )
or water (Cwater , Vwater ).
4. Experimental results Fig. 9a shows the relationship between RCD and Ho derived by
FEM simulations obtained for the annular flow under the hypoth-
The developed sensor system has been mounted on an experi- esis of a perfectly symmetrical fluid configuration with a centered
mental set-up that simulates an oil pipeline. The experimental loop disc oil core. The curve obtained by interpolating the simulation
consists of a 9 m Plexiglas pipe composed of 6 pieces of 1.5 m each. results has been thereafter used as the calibration curve, which
The two fluids are pumped and jointly injected into the pipe by relates the measured data of RCD and the values of Ho to be esti-
an appropriate injection device. Water is supplied by a centrifu- mated.
gal pump connected to a frequency inverter that provides control The hold-up values estimated by the sensor have been com-
of the injected flow rate. Oil is pumped by a screw-type oil pump pared with the values obtained by the Quick Closing Valve (QCV)
and its flow rate is controlled by a mechanical gear reducer con- technique used as a reference [14–20]. To this purpose, a series of
nected to the pump. The two flow rates are separately measured annular flows with different oil hold-up values has been generated
by two turbine flow-meters. At the end of the pipe, oil and water and for each of them the RCD has been measured with our system.
are ejected into a storing vessel where they separate by gravity and At the same time, the oil fraction has been determined by the QCV
further re-circulated into the plant [1]. The measurement head of technique.
the sensor system is placed 5 m down-stream the injection device The RCD for the different flows has been obtained from Eq. (9) by
and a Quick Closing Valve device is placed at the edges of the tract averaging the corresponding Vmeas signal over an integration time
of pipe which includes the sensor. of 10 s; in this way the real-time information on the oil hold-up Ho
Preliminary tests have been conducted to characterize the out- in the measurement section is turned into a time-averaged value.
put signal Vmeas in terms of noise level and base-line drift in order to It can be reasonably assumed that the measured time-averaged Ho
178 M. Demori et al. / Sensors and Actuators A 163 (2010) 172–179
Fig. 10. Output voltage Vmeas measured for a sequence of two different dispersed
flows and the corresponding pictures in the insets. The flow 1 has a very small
amount of oil, while oil quantity is increased in flow 2 which results in an increased
average dimension of the oil drops that is consistently detected by the sensor system.
Fig. 9. (a) Calibration curve for annular flow regime: Relative Capacitance Difference
versus oil fraction Ho ; (b) comparison between Ho predictions by the sensor system
(applying the calibration curve) and the QCV estimation technique.
impedance has been proposed. In particular, it has been shown that [14] K.J. Elkow, K.S. Rezkallah, Void fraction measurements in gas–liquid flows
it is necessary to chose a measurement frequency high enough to under 1−g and −g conditions using capacitance sensors, Int. J. Multiphase
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posed systems. In addition, the presented analysis of the external
Marco Demori was born in Bovolone (Verona) Italy, on October 24th 1979. In 2008
couplings in presence of a conductive fluid can be extended to the he received the Laurea degree in Electronic Engineering at the University of Brescia.
design of capacitance tomography sensor systems. From 2008 he is a PhD student in “Electronic Instrumentation” at the University of
Brescia, Department of Information Engineering. His main research deals with the
development of electronic systems for the study of multiphase flows in pipes and
References microfluidic channels; this activity is performed in collaboration with the Thermo-
dynamics Laboratory, Department of Mechanical and Industrial Engineering of the
same university.
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in two-phase high-viscosity-ratio liquid–liquid flows in horizontal and slightly Vittorio Ferrari was born in Milan, Italy, in 1962. In 1988, he obtained the Lau-
inclined pipes, Int. J. Multiphase Flow 34 (2008) 950–965. rea degree cum laude in Physics at the University of Milan. In 1993 he received
[2] N. Reinecke, D. Mewes, Recent developments and industrial/research applica- the Research Doctorate degree in Electronic Instrumentation at the University of
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[5] W.Q. Yang, L. Peng, Image reconstruction algorithms for electrical capacitance and frequency-output interface circuits. He is involved in national and international
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[6] A. Martínez Olmosù, M.A. Carvajal, D.P. Morales, A. García, A.J. Palma, Devel-
opment of an Electrical Capacitance Tomography system using four rotating Domenico Strazza graduated in May 2006 in Mechanical Engineering at University
electrodes, Sens. Actuators A 148 (2008) 366–375. of Brescia. In November 2006, he was appointed as a PhD student at University
[7] E. dos Reis, L.J. Goldstein, A non-intrusive probe for bubble profile and velocity of Brescia in the course “Technologies and Energetic Systems for the Mechanical
measurement in horizontal slug flows, Flow Meas. Instrum. 16 (2005) 229–239. Industry”. From November 2006 to October 2009, he worked on liquid–liquid two-
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tomography to gas–solid flows, Chem. Eng. Sci. 52 (1997) 2099–2110. annular flow. In April 2010 Domenico successfully defended his PhD thesis titled
[9] A.J. Jaworski, G.T. Bolton, The design of an electrical capacitance tomography “Two-phase and three-phase core-annular flow in horizontal and slightly inclined
sensor for use with media of high dielectric permittivity, Meas. Sci. Technol. 11 pipes”. He is currently doing research on two-phase and three-phase flows. He is
(2000) 743–757. also working with other researchers on capacitance measurements in multiphase
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Pietro Poesio holds a MSc (Università di Brescia, Italy, 2000) and a PhD (Delft Uni-
[11] H. Canière, C. T’Joen, A. Willockx, M. De Paepe, Capacitance signal analysis of
versity of Technology, The Netherlands, 2004), both awarded with honors. Since
horizontal two-phase flow in a small diameter tube, Exp. Therm. Fluid Sci. 32
October 2004, he works as assistant professor at the Università di Brescia (Italy)
(2008) 892–904.
where he is in charge of the laboratory for Thermal and Fluid Sciences; his fields
[12] M. Demori, V. Ferrari, D. Strazza, A sensor system for oil-fraction estimation in
of interest cover fluid mechanics, microfluidics, and multiphase flows. Pietro has
a two-phase oil–water flow, Proc. Chem. 1 (2009) 1247–1250.
authored more than 60 publications on international journals and national and
[13] S.M. Huang, R.G. Green, A.B. Plaskowski, M.S. Beck, Conductivity effects on
internationals congresses.
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method, J. Phys. E: Sci. Instrum. 21 (1988) 539–548.