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    OVP - OQ Test Protocol: Overall Test Result PASSED

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    Ali Rizvi
    None Resolution [cm-1]: 8 Zero filling: 2 Phase Correction: Pow er Spectrum Velocity: 10 KHz Apodization Function: Blackman-Harris 3-Term Phase Resolution: 64 Low Pass Filter: 10 KHz High Pass Filter: Open ________________ Page 6 of 8 Page Signature OVP - OQ Test Protocol Linearity Test , Spectrum 1.000 0.998 0.996 0.994 0.992 7290 7295 7300 7305 7310 7315 7320 7325 Wavenumber cm-1

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    OVP - OQ Test Protocol: Overall Test Result PASSED

    Uploaded by

    Ali Rizvi
    28 views8 pages
    None Resolution [cm-1]: 8 Zero filling: 2 Phase Correction: Pow er Spectrum Velocity: 10 KHz Apodization Function: Blackman-Harris 3-Term Phase Resolution: 64 Low Pass Filter: 10 KHz High Pass Filter: Open ________________ Page 6 of 8 Page Signature OVP - OQ Test Protocol Linearity Test , Spectrum 1.000 0.998 0.996 0.994 0.992 7290 7295 7300 7305 7310 7315 7320 7325 Wavenumber cm-1

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    Original Title

    OQ_TestProtocol_MPA_Sample_Compartment_20200418_163051

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    None Resolution [cm-1]: 8 Zero filling: 2 Phase Correction: Pow er Spectrum Velocity: 10 KHz Apodization Function: Blackman-Harris 3-Term Phase Resolution: 64 Low Pass Filter: 10 KHz High Pass Filter: Open ________________ Page 6 of 8 Page Signature OVP - OQ Test Protocol Linearity Test , Spectrum 1.000 0.998 0.996 0.994 0.992 7290 7295 7300 7305 7310 7315 7320 7325 Wavenumber cm-1

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    28 views8 pages

    OVP - OQ Test Protocol: Overall Test Result PASSED

    Uploaded by

    Ali Rizvi
    None Resolution [cm-1]: 8 Zero filling: 2 Phase Correction: Pow er Spectrum Velocity: 10 KHz Apodization Function: Blackman-Harris 3-Term Phase Resolution: 64 Low Pass Filter: 10 KHz High Pass Filter: Open ________________ Page 6 of 8 Page Signature OVP - OQ Test Protocol Linearity Test , Spectrum 1.000 0.998 0.996 0.994 0.992 7290 7295 7300 7305 7310 7315 7320 7325 Wavenumber cm-1

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    © All Rights Reserved
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    of 8

    OVP - OQ Test Protocol

    Company: Novartis Pharmaceuticals


    Operator: Administrator
    Instrument Type: MPA Sample Compartment
    Optics Configuration: Sample Compartment w ith: NIR, Quartz, TE-InGaAs [Internal]
    Accessory: None
    Instrument Serial Number: MPA.0325.04
    Instrument Firmw are Version: 1.300 Apr 14 2004
    OPUS/DB Version: OPUS 7.2 Build: 7, 2, 139, 1294 / DB: 7,2,139,1294
    Overall Test Result PASSED
    Test expires: 4/18/2021, 4:30:51 PM (GMT-7)
    Test Date/Time: 4/18/2020, 4:30:51 PM (GMT-7)
    Test Spectra Path: C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051
    Comment:

    Resolution Test

    Water Vapor Band: 7306.74 cm -1


    Maxim um Resolution: 2.00 cm -1 Measured Resolution: 1.67 cm -1

    Sensitivity Test

    Measurem ent Region, Start: 6100.00 cm -1 Measurem ent Region, End: 5600.00 cm -1
    Minim um S/N: 8000 Measured S/N: 12145.38

    Energy Distribution Test

    Minim um Energy Value: 1.00% Energy at 12000.00 cm -1 3.20%


    Minim um Energy Value: 1.00% Energy at 4000.00 cm -1 54.42%

    Wavenum ber Accuracy Test Water Vapor

    Expected Band: 7306.740 cm -1 Measured Band: 7306.769 cm -1


    Maxim um Deviation: 0.100 cm -1 Measured Deviation: 0.029 cm -1

    Alignm ent Test

    Interferogram Peak Range: 35000 - 28000 Measured Peak Position: 33482


    Peak Am plitude: 9056

    Linearity Test

    Maxim um Energy[%]: 0.30 Measured Energy[%]: 0.28

    Reproducibility Test

    Maxim um Deviation: 2.00 Measured Deviation: 0.13

    Overall Test Result = PASSED

    Date and Signature Date and Signature

    ________________
    Page 1 of 8 Page Signature
    OVP - OQ Test Protocol
    Resolution Test , Spectrum
    1.201.15
    Single channel
    1.10 1.05

    7290 7295 7300 7305 7310 7315 7320 7325


    Wavenumber cm-1
    C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051\OQ_MPA_Sample_Compartment_Resolution.0

    Resolution Test , M easurement Parameters


    Number of Scans: 32 Preamplifier Gain: Ref
    Resolution [cm-1]: 2 Zero filling: 8
    Aperture: Open Phase Correction: Pow er Spectrum
    Acquisition Mode: Double Sided,Forw ard-Backw ard Velocity: 10 KHz
    Apodization Function: Four point Phase Resolution: 32
    Low Pass Filter: 10 KHz High Pass Filter: Open

    ________________
    Page 2 of 8 Page Signature
    OVP - OQ Test Protocol
    Sensitivity Test , Spectra
    102.0101.0
    Transmittance [%]
    99.0 100.098.0

    6100 6000 5900 5800 5700 5600


    Wavenumber cm-1
    C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051\OQ_MPA_Sample_Compartment_SN.0
    C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051\OQ_MPA_Sample_Compartment_SN.1
    C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051\OQ_MPA_Sample_Compartment_SN.2
    C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051\OQ_MPA_Sample_Compartment_SN.3
    C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051\OQ_MPA_Sample_Compartment_SN.4
    C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051\OQ_MPA_Sample_Compartment_SN.5
    C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051\OQ_MPA_Sample_Compartment_SN.6
    C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051\OQ_MPA_Sample_Compartment_SN.7
    C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051\OQ_MPA_Sample_Compartment_SN.8
    C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051\OQ_MPA_Sample_Compartment_SN.9

    Sensitivity Test , M easurement Parameters


    Number of Scans: 10 Preamplifier Gain: Ref
    Resolution [cm-1]: 8 Zero filling: 2
    Aperture: Open Phase Correction: Pow er Spectrum
    Acquisition Mode: Double Sided,Forw ard-Backw ard Velocity: 10 KHz
    Apodization Function: Blackman-Harris 3-Term Phase Resolution: 64
    Low Pass Filter: 10 KHz High Pass Filter: Open

    ________________
    Page 3 of 8 Page Signature
    OVP - OQ Test Protocol
    Energy Distribution Test , Spectrum
    0.14
    0.10
    Single channel
    0.06 0.02

    12000 11000 10000 9000 8000 7000 6000 5000 4000


    Wavenumber cm-1
    C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051\OQ_MPA_Sample_Compartment_SN.9

    Energy Distribution Test , M easurement Parameters


    Number of Scans: 10 Preamplifier Gain: Ref
    Resolution [cm-1]: 8 Zero filling: 2
    Aperture: Open Phase Correction: Pow er Spectrum
    Acquisition Mode: Double Sided,Forw ard-Backw ard Velocity: 10 KHz
    Apodization Function: Blackman-Harris 3-Term Phase Resolution: 64
    Low Pass Filter: 10 KHz High Pass Filter: Open

    ________________
    Page 4 of 8 Page Signature
    OVP - OQ Test Protocol
    Wavenumber Accuracy Test , Spectrum
    0.090
    0.085
    Single channel
    0.080 0.075

    7290 7295 7300 7305 7310 7315 7320 7325


    Wavenumber cm-1
    C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051\OQ_MPA_Sample_Compartment_WvnAccuracy.0

    Wavenumber Accuracy Test , M easurement Parameters


    Number of Scans: 32 Preamplifier Gain: Ref
    Resolution [cm-1]: 2 Zero filling: 8
    Aperture: Open Phase Correction: Pow er Spectrum
    Acquisition Mode: Double Sided,Forw ard-Backw ard Velocity: 10 KHz
    Apodization Function: Blackman-Harris 3-Term Phase Resolution: 16
    Low Pass Filter: 10 KHz High Pass Filter: Open

    ________________
    Page 5 of 8 Page Signature
    OVP - OQ Test Protocol
    Alignment Test , Spectrum
    0.2
    0.1
    0.0
    -0.1
    -0.2

    3750 3800 3850 3900


    Points
    C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051\OQ_MPA_Sample_Compartment_SN.9

    Alignment Test , M easurement Parameters


    Number of Scans: 10 Preamplifier Gain: Ref
    Resolution [cm-1]: 8 Zero filling: 2
    Aperture: Open Phase Correction: Pow er Spectrum
    Acquisition Mode: Double Sided,Forw ard-Backw ard Velocity: 10 KHz
    Apodization Function: Blackman-Harris 3-Term Phase Resolution: 64
    Low Pass Filter: 10 KHz High Pass Filter: Open

    ________________
    Page 6 of 8 Page Signature
    OVP - OQ Test Protocol
    Linearity Test , Spectrum
    0.0006
    Single channel
    0.0004 0.0002

    4000 3500 3000 2500 2000 1500 1000


    Wavenumber cm-1
    C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051\OQ_MPA_Sample_Compartment_SN.9

    Linearity Test , M easurement Parameters


    Number of Scans: 10 Preamplifier Gain: Ref
    Resolution [cm-1]: 8 Zero filling: 2
    Aperture: Open Phase Correction: Pow er Spectrum
    Acquisition Mode: Double Sided,Forw ard-Backw ard Velocity: 10 KHz
    Apodization Function: Blackman-Harris 3-Term Phase Resolution: 64
    Low Pass Filter: 10 KHz High Pass Filter: Open

    ________________
    Page 7 of 8 Page Signature
    OVP - OQ Test Protocol
    Reproducibility Test , Spectra
    101.0100.5
    Transmittance [%]
    99.5 100.099.0

    10000 9500 9000 8500 8000 7500 7000 6500


    Wavenumber cm-1
    C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051\OQ_MPA_Sample_Compartment_Reproduce.0
    C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051\OQ_MPA_Sample_Compartment_Reproduce.1
    C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051\OQ_MPA_Sample_Compartment_Reproduce.2
    C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051\OQ_MPA_Sample_Compartment_Reproduce.3
    C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051\OQ_MPA_Sample_Compartment_Reproduce.4
    C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051\OQ_MPA_Sample_Compartment_Reproduce.5
    C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051\OQ_MPA_Sample_Compartment_Reproduce.6
    C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051\OQ_MPA_Sample_Compartment_Reproduce.7
    C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051\OQ_MPA_Sample_Compartment_Reproduce.8
    C:\OPUS_7.2.139.1294\Validation\Data\20200418\163051\OQ_MPA_Sample_Compartment_Reproduce.9

    Reproducibility Test , M easurement Parameters


    Number of Scans: 10 Preamplifier Gain: Ref
    Resolution [cm-1]: 64 Zero filling: 16
    Aperture: Open Phase Correction: Pow er Spectrum
    Acquisition Mode: Double Sided,Forw ard-Backw ard Velocity: 10 KHz
    Apodization Function: Blackman-Harris 3-Term Phase Resolution: 64
    Low Pass Filter: 10 KHz High Pass Filter: Open

    ________________
    Page 8 of 8 Page Signature

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