“This lmteraonal standard was deyeoped in acordance with tne od placpes on standardzadan eablaed in the Dedisen on Pcie fr the rationally regaled Development of Ineratonal Sandards, Guides tnd Recotmendaton Isued by Oe Morld rede Organization Techatcal Barrer to Trade (TT) Comte. Aily Designation: F620 - 20 Standard Specification for Titanium Alloy Forgings for Surgical Implants in the Alpha Plus Beta Condition’ ‘This tna ie sued under the fed dsinatoe F620: he mimker immediately following the designation indicates the year of eriginal option or in he case of vse the Year of lst revision, A number in parentheses indicts the ear of las reappeoval A supercrpt “psilon (e) indicates an editorial change since the last revision ce reapproa 1. Seope* 1.1 This specification covers the requirements for titanium alloy forgings for surgical implants, in the alpha plus beta condition, when the material forged conforms to Specifications F136 (UNS RS6401), F1295 (UNS R56700), F1472 (UNS 56400), or F2066 (UNS R58150). 1.2 The SI units in this standard are the primary units, The values stated in either primary SI units or secondary inch- pound units are to be regarded separately as standard. The values stated in cach system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in noncon- formance with the standard, 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appro- priate safety, health, and environmental practices and deter- imine the applicability of regulatory limitations prior t0 use. L4 This international standard was developed in accor- dance with internationally recognized principles on standard- ization established in the Decision on Principles for the Development of International Standards, Guides and Recom- mendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. 2. Referenced Documents 2.1 ASTM Standards: E8/E8M Test Methods for Tension Testing of Metallic Ma- terials E10 Test Method for Brinell Hardness of Metallic Materials, "Tis specication is under the jurisdiction of ASTM Commies FOS on Mesical and Surpcal Materials and Devicesand i the diect responsiblity of Svbcommitee FO12 on Mealuical Materials ‘Curent eltioe approved Feb. 1, 2020, Published March 2020. Originally sgproved a 1979, Last previous ein spproved in 2018 ws F620 11(2015). DOL: WL 1S207F0620-20, "For referenced ASTM standard, vist dhe ASTM website, wrwastm org or contct ASTM Customer Service a service@asim org. Foc Amal Book of AST ‘Stands volume information, rer wo te standards Docueest Summary page 09 the ASTM website E18 Test Methods for Rockwell Hardness of Metallic Ma- terials 29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications 92 Test Methods for Vickers Hardness and Knoop Hard- ness of Metallic Materials E165 Practice for Liquid Penetrant Testing for General Industry E539 Test Method for Analysis of Titanium Alloys by Wavelength Dispersive X-Ray Fluorescence Spectrometry 1409 Test Method for Determination of Oxygen and Nitro- gen in Titanium and Titanium Alloys by Inert Gas Fusion E1447 Test Method for Determination of Hydrogen in Tita- rium and Titanium Alloys by Inert Gas Fusion Thermal Conductivity/infrared Detection Method 52371 Test Method for Analysis of Titanium and Titanium Alloys by Direct Current Plasma and Inductively Coupled Plasma Atomic Emission Spectrometry (Performance- Based Test Methodology) £2994 Test Method for Analysis of Titanium and Titanium Alloys by Spark Atomic Emission Spectrometry and Glow Discharge Atomic Emission Spectrometry (Performance- Based Method) F67 Specification for Unalloyed Titanium, for Surgical Im- plant Applications (UNS R50250, UNS R50400, UNS 50850, UNS 50700) F136 Specification for Wrought Titanium-6Aluminum- 4Vanadium ELI (Extra Low Interstitial) Alloy for Surgical Implant Applications (UNS R56401) F601 Practice for Fluorescent Penetrant Inspection of Me- tallic Surgical Implants F1295 Specification for Wrought Titanium-GAluminum- Niobium Alloy for Surgical Implant Applications (UNS 56700) F1472 Specification for Wrought Titanium-GAluminum- 4Vanadium Alloy for Surgical Implant Applications (UNS. 56400) 2066 Specification for Wrought Titanium-15 Molybdenum ‘Alloy for Surgical Implant Applications (UNS R58150) "A Summary of Changes seeton appears at the end of this standard ‘coy © AST eran, 00 Bar Har One, PO Bx C70, West Conshohocken, PA 18882960, Untd Sin ceancGuove SRL pattem) MUSSATTONGPECAGUST: OOM,fly F620 - 20 IEEE/ASTM SI 10 American National Standard for the Use ‘of the Intemational System of Units (SI): The Modem Metric System 2.2 180 Standard:? 1SO 9001 Quality management systems requirement 3. Terminology 3.1 Definitions of Terms Specific to This Standard: 3.1.1 lot—the total number of forgings produced from the same heat under the same conditions and heat treated at essentially the same time. 4. Ordering Information 4,1 Inquiries and orders for forgings under this specification shall include the following information: 4.1.1 Quantity, number of pieces; 4.1.2 ASTM designation and date of issue, material grade; 4.13 Condition; 4.1.4 Mechanical properties; 4.1.5 Finish; 4.1.6 Applicable dimensions or drawing number, 4.1.7 Special tests, if any; and 4.1.8 Other requirements. 5. Materials and Manufacture 5.1. Material for forgings shall be bars or wire fabricated in accordance with Specification F136, F1295, F1472, or F2066. 5.2 The material shall be forged by hammering, pressing, extruding, of upsetting and shall be processed, if practicable, so as to cause metal flow during the hot-working operation in the direction most favorable for resisting stresses encountered in service, as may be indicated to the fabricator by the purchaser, 5.3 Forgings shall be free of splits, scale, eracks, laws, and other imperfections not consistent with good commercial practice (see Note 1). Offset or mismatch allowance, dependent ‘upon part size and configuration, shall be within standard forging tolerances. [Note 1 Compliance to these requirements may be verified by Practice 65 oF Practice F01 or other suitable methods. 54 After all hot-working operations have been completed, the forgings shall receive an annealing treatment consisting of heating the parts to an appropriate elevated temperature for a specified dwell time followed by appropriate cooling to meet the applicable metallurgical requirements specified herein, 5.5 Optional identification marks, including the manufactur- ex's logo, material designation, heat code number, and impres- sion number may be placed upon each forging, the method and location of which shall be specified by the purchaser. 6. Chemical Composition 6.1 When specified by the purchaser, the chemical compo- sition of either the forging bars or the completed forgings shall * available from Americon Naional Standards Insitute (ANSD. 25 W. 44d St, sath Flor, New York, NY 10036, baputwwwanicry. be determined and confirmed by the forger, and shall meet the product check analysis limits of the appropriate material specification. 6.1.1 Hydrogen content shall be determined on annealed forgings. Samples for hydrogen analysis shall be taken after descaling, pickling, or chemical milling, if these operations are performed. 6.2 For referee purposes, Test Methods E539, E1409, 1447, E2371 and E2994 shall be used. 7. Mechanical Requirements 7.1 The mechanical properties of forgings shall be tested by the forger and shall comply with the minimom mechanical properties as specified in Specifications F136, F1295, F1472, or F206. 7.L.1 Test specimens shall be taken from a representative forging if possible, or from a representative forged test bar. A representative test bar may only be used if the configuration is such that a test bar cannot be obtained. Any specially forged test bar must be annealed with the forgings it represents. 7.1.2 Specimens for tension tests shall be machined and tested in accordance with Test Methods ES/E8M. Tensile properties shall be determined using a strain rate of 0.003 0 0.007 mm/mm/min [in/inJ/min} through yield and then the crosshead speed may be increased so as to produce fracture in approximately one additional minute. 7.2. Number of Tests: 7.2.1 Perform at least one tension test from each lot in the longitudinal direction. Should any test specimen not meet the specified requirements, test two additional test pieces represen- tative of the same lot, in the same manner, for each failed west specimen, The lot will be considered in compliance only if all additional test pieces meet the specified requirements. 7.2.2 Tensile tests results for which any specimen fractures outside the gauge length shall be considered valid if both the clongation and reduction of area meet the minimum require- ‘ments specified. If either the elongation or reduction of area is less than the minimum requirement, invalidate the specimen, and retest. Retest one specimen for each invalidated specimen. 7.23 Ifeither the elongation or reduction of area is less than the minimum requirement, discard the test and retest. Retest fone specimen for each specimen that did not meet the ‘minimum requirements. 7.3 When desired, hardness may be specified on the pur- cchase order or drawing and shall be determined in accordance with Test Methods E10, E18, or E92. 8. Microstructure 8.1 The alpha plus beta microstructure shall meet the requirements in Specifications F136, F1295, F1472, of F2066. 9. Significance of Numerical Limits 9.1 The following applies to all specified numerical limits in this specification, To determine conformance to these limits, an ‘observed or calculated value shall be rounded to the nearest unit in the last right hand digit used in expressing the specification limit, in accordance with the rounding method of Practice E29. GIP epaenag.naerongreoasrsconfly F620 - 20 10, Dimensions and Permissible Variations 10.1 Units of Measu 10.1.1 Selection—This specification requires that the pur- chaser selects the units (SI or inch-pound) to be used for product certification. In the absence of a stated selection of units on the purchase order, this selection may be expressed by the purchaser in several alternate forms listed in order of precedence. 10.1.1.1 If the purchaser and supplier have a history of using specific units, these units shall continue to be certified until expressly changed by the purchaser. 10.1.1.2 In the absence of historic precedence, if the units used to define the product on the purchaser's purchase order (PO), specification, and engineering drawing are consistent, these units shall be used by the supplier for product certifica- tion. 10.1.1. If the purchaser's selection of units is unclear, the ‘units of measure shall be agreed upon between the purchaser and the supplier, 10.1.2 Conversion of Units—If the supplier's test equipment does not normally report in the selected units, the test equip- iment units may be converted to the selected units for certifi cation purposes. Accurate arithmetic conversion and proper use of significant digits should be observed when performing this conversion. ASTM IEEE/ASTM SI 10 provides guidelines for the use of SI units. Annex A provides conversion tables and ‘Annex B provides rules for conversion and significant digits 11, Certification Requirements 11.1 The supplier shall provide a certification that the material was tested in accordance with this specification and ‘met all requirements. A report of the test results shall be furnished to the purchaser at the time of shipment. 11.2 Gauge length must be reported with elongation. 12. Quality Program Requirements 12.1 The supplier shall maintain a quality program such as defined in ISO 9001 or similar quality program. 13. Keywords 13.1 forgings—surgical implants; metals (for surgical implants)—titanium alloys; onthopaedic medical devices— titaniunvtianium alloy; ttaniumitanium alloys (For surgical implants) APPENDIXES (Nonmandatory Information) XI. RATIONALE X1.1 The purpose of this specification is to characterize the ‘chemical, mechanical, and metallurgical properties of wrought annealed titanium alloy forgings in the alpha plus beta condi- tion for surgical implants, X12 The microstructural requirements contained in this specification represent current general consensus with respect to optimization of meckanical properties for implant applica- tions. 1X2. BIOCOMPATIBILITY X2.1 No known surgical implant material has ever been shown to be completely free of adverse reactions in the human body. The alloy compositions covered by this specification, however, have been subjected to testing in laboratory animals, ‘and have been used clinically for more than a decade. The results of these studies indicate a well-characterized level of local biological response that is equal to or less than that produced by the reference material unalloyed titanium (sce ‘Specification F67) that has a long history of successful clinical application in soft tissue and bone implants in humans. SECRET amy ancronarenou ceAil F620 - 20 SUMMARY OF CHANGES Committee FO4 has identified the location of selected changes to this standard since the last issue (F620 —11@015)) that may impact the use of this standard. (Approved Feb. 1, 2020.) (J) Revised 1.2 10 confirm that SI units are the primary units (4) Added “check” to product analysis limits in 6.1 and added 1.3 and to match the latest requirements established (5) Added ‘Test Methods E539 and E2994 to Section 2 and 6.2. by Subcommittee FO4.12 on Metallurgical Materials. (6) Spelled out “purchase order” (PO) in 10.1.1.2. (2) Corrected titles for SI 10, ISO 9001, and Test Methods E92. (7) Microstructure requirements were changed to coincide with (3) Changed Test Method E165 to Practice E165 in Note 1. individual forging specifications. ASTM Interatonal takes no posion respecting the vay of any pater rights asserted in connscion with any tam mensoned In iis standara Users ofthis standard are express advsad that determination ote vali of any such pent rigs, andthe isk ‘of iningement of such nights, are ently thar cwn responsi, ‘Tri standardie subject to reiion a ary time by te responsible technica committee and must bo eviewod evry fv years anc ‘tpotrevse, eter reapproved or aitarawn. Your comments are invited athe fr evo o this stand or or action tandaros ‘and should be adcrossed fo ASTM Intemtona! Headqvarars. Your comments wil rcoive crail consideration at a meeting ofthe ‘espansble tecnica conte, which you may altand If you fe thal your commonts have net receved af heaving you shoud ‘make your ows known tothe ASTM Commitee on Standars, atte adcrss shown below. 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CININWLOROSY ONIN v ‘SvOad apes. 2161S‘This international standard was developed in accordance with ineratonally recone praipes em standarltion stabs Inthe Dean on Principles forthe Development of nternatonal Standards, Guides and Recommendations tase Hythe World Trade Organisation Technical Darsier te Trade (TT) Commer, fly Designation: B381 - 13 (Reapproved 2019) Standard Specification for Titanium and Titanium Alloy Forgings’ “This stata isued under the fed designation B38; the number um following the desigation indicates the year of ‘xg aoption orn the cave of vision, he year of lst revison, A number in parentheses odes the year of lst eepproval A ‘ipescript epson (e) indicates an eit change since the last revision o approval. 1, Scope 1.1 This specification? covers 39 grades of annealed tita- nium and titanium alloy forgings as follows: 1.1.1 Grade F-1—UNS R50250. Unalloyed titanium, 1.1.2 Grade F-2—UNS R50400. Unalloyed titanium, 1.1.2.1 Grade F-2H—UNS 50400. Unalloyed titanium (Grade 2 with 58 ksi (400 MPa) minimum UTS), 1.1.3 Grade F-3—UNS R50550. Unalloyed titanium, 1.14 Grade F-4—UNS R50700. Unalloyed titanium, LLS Grade F-5S—UNS RS6400. Titanium alloy (6 % aluminum, 4 % vanadium), 1.1.6 Grade F-6—UNS 54520. Titanium alloy (5% aluminum, 2.5 % tin), 1.1.7 Grade F-7—UNS R52400, Unalloyed titanium plus 0.12 t0 0.25 % palladium, LL7.1 Grade F-7H—UNS R52400. Unalloyed titanium plus 0.12 to 0.25 % palladium (Grade 7 with 58 ksi (400 MP2) ‘minimum UTS), 1.1.8 Grade F-9—UNS R56320. Titanium alloy (3% aluminum, 2.5 % vanadium), 1.1.9 Grade F-I1—UNS R52250. Unalloyed titsnium plus, 0.12 to 0.25 % palladium, 1.1.10 Grade F-12—UNS R53400. Titanium alloy 0.3 % ‘molybdenum, 0.8 % nickel), LLM Grade F-13—UNS R53413. Titanium alloy (0.5 % nickel, 0.05 % ruthenium), 1.1.12 Grade F-14—UNS R53414. Titanium alloy (0.5 % nickel, 0.05 4% ruthenium), 1.1.13 Grade F-15—UNS RS3415. Titanium alloy (0.5 % nickel, 0.05 % ruthenium), 1.1.14 Grade F-16—UNS RS2402. Unalloyed titanium plus, 0.04 to 0.08 % palladium, 1.1.14.1 Grade F-16H—UNS R52402. Unalloyed titanium plus 0.04 to 0.08 % palladium (Grade 16 with 58 ksi (400 MP) minimum UTS), "This spcitcaton is under the jurado of ASTM Commitee B10 on Reactive and Refractory Meas and Alloys and isthe dicet responsibility of Sabcommitse 810.01 on Tani, (Crete sppove July 1 2018. Pb uly 2019, riially approved 4 1891. Last previous edition approved in 2013 as B38! ~13, DOL 1015201 ‘s8-13R19. * For ASME Boiler and Pressure Vessel Code appictions, see relied Spei- cation SE°381 in Section TI ofthat Code 1.1.15 Grade F-17—UNS R52252, Unalloyed titanium plus, 0.04 to 0.08 % palladium, 1.1.16 Grade F-8—UNS R56322. Titanium alloy 3% aluminum, 2.5 % vanadium) plus 0.04 % to 0.08 % palladium, 1.1.17 Grade F-19—UNS R58640. Titanium alloy (G3 % aluminum, 8 % vanadium, 6 % chromium, 4 % zirconium, 4 % ‘molybdenum, 1.1.18 Grade F-20—UNS 58645. Titanium alloy 3% aluminum, 8 % vanadium, 6 “ chromium, 4 % zirconium, 4 % molybdenum) plus 0.04 to 0.08 % palladium, L119 Grade F-2I-UNS R58210, Titanium alloy (3 % aluminum, 2.7% niobium, 15% molybdenum, 0.25 % silicon), 1.1.20 Grade F-23—UNS R56407. Titanium alloy (6% aluminum, 4% vanadium, extra low interstitials, ELD, 1.1.21 Grade F-24—UNS R56405, Titanium alloy (6% aluminum, 4% vanadium) plus 0204 to 0.08 % palladium, 1.1.22 Grade F-25—UNS R56403. Titanium alloy 6% aluminum, 4 % vanadium) plus 0.3 to 0.8 % nickel and 0.04 to 0.08 % palladium, 1.1.23 Grade F-26—UNS RS2404, Unalloyed titanium plus 0.08 to 0.14 % ruthenium, 1.1.23.1 Grade F-26H—UNS R52404. Unalloyed titanium plus 0.08 to 0.14% ruthenium (Grade 26 with 58 ksi (400 MPa) minimum UTS), 1.1.24 Grade F-27—UNS R52254. Unalloyed titanium plus, 0.08 to 0.14 % ruthenium, 1.1.25 Grade F-28—UNS R56323. Titanium alloy (3% aluminum, 2.5 % vanadium plus 0.08 to 0.14 % ruthenium), 1.1.26 Grade F-29-UNS RS6404. Titanium alloy (6% aluminum, 4% vanadium, extra low interstitial, ELI plus 0.08 t0 0.14 % ruthenium), 1.1.27 Grade F-30—UNS R53530. Titanium alloy (0.3 % cobalt, 0.05 % palladium), 1.1.28 Grade F-31—UNS RS3532. Titanium alloy (0.3 % ‘cobalt, 0.05 % palladium), 1.1.29 Grade F-32—UNS RSSUL. Titanium alloy (5% aluminum, 1% vanadium, 1% tin, 1% zirconium, 0.8 % molybdenum), 1.1.30 Grade F-33—-UNS R53442. Titanium alloy (0.4 % nickel, 0.015 % palladium, 0.025 % ruthenium, 0.15% chromium), (ony @ASTH neat 108 Ba Har Divo, PO Box C700, West Conshohocken, Ph 1928-2568, Ure Sates SCRE er pegn sronrciscan4Gy 8381 - 13 (2019) 1.1.31 Grade F-34—UNS RS3445. Titanium alloy (0.4 % nickel, 0.015 % palladium, 0.025% ruthenium, 0.15 % chromium), 1.1.32 Grade F-35—UNS R56340. Titanium alloy (4.5 % aluminum, 2% molybdenum, 1.6 % vanadium, 0.5 % iron, 0.3 % silicon), 1.1.33 Grade F-36-—UNS R58450. Titanium alloy (45 % niobium), 1.1.34 Grade F-37—UNS R52815. Titanium alloy (1.5 % aluminum), and 1.1.35 Grade F-38—UNS 54250. Titanium alloy (4 % aluminum, 2.5 % vanadium, 1.5 % iron). ‘Nore I—H grade material js identical tothe comesponding numeric anade (that is, Grade 2H = Grade 2) except forthe higher guaranteed ‘minimum UTS, and may always be certiied as mecting the requirements of its coresponding numeri grade. Grades 2H, 7H, 16H, and 26H are {mended primarily for pressure vessel use. 1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard. 3 This international standard was developed in accor- dance with internationally recognized principles on standard- ization established in the Decision on Principles for the Development of International Standards, Guides and Recom- ‘mendations issued by the World Trade Organization Technical Barriers to Trade (BT) Committee. 2, Referenced Documents 2.1 ASTM Standards:* B348 Specification for Titanium and Titanium Alloy Bars ‘and Billets E8 Test Methods for ‘Tension Testing of Metallic Materials [Metric] E0008_E0008M £29 Practice for Using Significant Digit Determine Conformance with Specifications E539 Test Method for Analysis of Titanium Alloys by Wavelength Dispersive X-Ray Fluorescence Spectrometry E1409 Test Method for Determination of Oxygen and Nitro- ‘gen in Titanium and Titanium Alloys by Inert Gas Fusion E1447 Test Method for Determination of Hydrogen in Tita- nium and Titanium Alloys by Inert Gas Fusion Thermal ‘Coniluctivity/Infrared Detection Method E1941 Test Method for Determination of Carbon in Refrac~ tory and Reaetive Metals and Their Alloys by Combustion Analysis E2371 Test Method for Analysis of Titanium and Titanium Alloys by Direct Current Plasma and Inductively Coupled Plasma Atomic Emission Spectrometry (Performance- Based Test Methodology) 2626 Guide for Spectrometric Analysis of Reactive and Refractory Metals (Withdrawn 2017)* Test Data 10 ° For referenced ASTM standards, vist the ASTM website, wavwastm.or. of comsct ASTM Chstamer Servi at srvce@asim.ory For Annual Hook of ASTM ‘Standards volume information, rete t the sandars Document Summary page on {eASTM website “The lst approved Yerslon of tls historical standard is referenced on swat. 3. Terminology 3.1 Definitions of Terms Specific 10 This Standard: 3.1.1 bar, n—a hot rolled, forged or cold worked semifin- ished solid section produet whose cross sectional area is less than 16 in.? (10323 mm”). 3.12 billet, n—a solid semifinished section, hot rolled or forged from a igo dha crss etna ae reser tan 16 (10323 mm). 3.13 forging, n—any product of work on metal formed to a desired shape by impact or pressure in hammers, forging machines, upsetters presses or related forming equipment. 4. Ordering Information 4.1. Onders for forgings under this specification shall include the following information, as applicable: 4.1.1 Grade number (Section 1), 4.1.2 Tensile properties (Table 1), 4.1.3 Dimensions and tolerances (Section 10), 4.14 Sampling, mechanical properties (Section 8), 4.1.5 Methods for chemical analysis (Section 6), 4.1.6 Marking (Section 17), 4.1.7 Packaging (Section 17), 4.1.8 Certification (Section 16), 4.1.9 Disposition of rejected material (Section 14), and 4.1.10 Supplementary requirements (S1). 5. Materials and Manufacture 5.1. Material conforming to the latest revision of Specifica- tion B348 shall be used when producing forgings to this specification. 6. Chemical Composition 6.1. The grades of titanium and titanium alloy metal covered by this specification shall conform to the requirements as to chemical composition prescribed in Table 2. 6.1.1 The elements listed in Table 2 are intentional alloy additions or elements which are inherent to the manufacturer of titanium sponge, ingot or mill product. 6.L1.1 Elements other than those listed in Table 2 are deemed to be capable of occurring in the grades listed in Table 2 by and only by way of unregulated or unanalyzed scrap additions to the ingot melt. Therefore, product analysis for elements not listed in Table 2 shall not be required unless specified and shall be considered to be in excess of the intent of this specification, 6.1.2 Elements intentionally added to the melt must be identified, analyzed, and reported in the chemical analysis. 6.2 When agreed upon by the producer and purchaser and requested by the purchaser in his written purchase order, chemical analysis shall be completed for specific residual elements not listed in this specification, 6.3 Product Analysis—Product analysis tolerances do not broaden the specified heat analysis requirements, but cover variations between laboratories in the measurement of chemi- cal content. The manufacturer shall not ship material which is ‘outside the limits specified in Table 2 for the applicable grade. Product analysis limits shall be as specified in Table 3. inka eno. tsar rongPrASiscOKAf 8381 - 13 (2019) TABLE 1 Tensile Requirements Vit Senin (02% Ofset rin or Renae Gongatonin 40, Radon of Awa, Sate e ri “Pay nin mn, 36 ma 35 (20) 20 98) 2 = Fa 50 es) ry 25) 2 2% Faneo 58 (400) « 5) 20 20 Fs 65 (450) 55 (380) 18 30 a 8 (650) 7 (ass) 15 2 Fs 130 (235) 120 (es) 10 2 Fe 120 (a2) 15 (735) 10 2 7 50 () 40 (275) 20 2 emo 58 (400) 40 es) 20 x Fe 20 (220) 10 (750) 10 2 Fo? 80 (620) 7 483) 6 2% et 3% (20) 2 (38) 2 ee 7 (420) 50 (45) 2 Fis “0 (es) 2 (7) 2 2 ta 60 (eo) 0 (27s) 20 3 AS 7 (G29) 55 (300) 18 2 6 50 es) “0 275) 2 2 FtgHee 58 (400) ” (27s) 20 2 BIT 35 (20) 20 (ise) 24 2 8 0 (, 0 (aes) 1s 2s F192 90 (620) 7 (383) 2 2 Fg 15 (733) 110 50) 15 2s Fo 135 (G20) 90 10 150 (007) t (1096) 10 2 Fg? 1s (38), 160 1 185, (100 19 (1276) 5 2 415 (22) 110 (759) 5 2 135 (900) 13010159 (097) t (10836) 10 2 165 (38) 160 10185 (108) (1276) 5 2 ne 733) 0 i) 15 3 140 (068) 1300 159 {687 10 (1086) 10 2 70 aie 180 0 185 (1104) (1276), 8 2 129 (e28) 0 7) 0 2 120 (sas) 0 59) 75",60) 25 130 (095) 20 (2) 10 28 190 (035) 20 (320) 10 25 50 os) 40 er) 2 30 58 (400) 0 @5) 20 30 3 (20) 2 (038) 24 3% 0 (620) n (aes) 15 2% 90 (620) 70 (ass) 2 2 20 (e25) 110 (759) 10 2% 20 (@5) 110 (50) 75" .60° e 0 (4s) #0 275) 20 2 & (40) 55 (G20) 8 Eo 100 (ces) 85 (586) 10 2 23 50 os) “0 (275) 2 % F6 6s (450) 55 (20) 18 0 Fas 130 =) 120 (ozs) 3 2 Fs, 65 (450) 601095 (410% 655) 0 Far 50 (8) 31 15) 2 30 a8 130 (325) 15 94) 10 Fa ‘These properties aply to forgings having a ease secon no greater han 9 (195 mn), Mechanical properies of forangs having greater Coss eactons shall be negotiated between fhe manufacturer end the puchaser Hate wentica fo tne corresponding momar grado (hat , Grade F-2H = Grade F.2) excep forthe higher guaranteed minimum UTS, and may be dual cerned with soveaponding numee race. Grade FH, F-7H, Fo, and F28H aro intended primal lr pressio vessel usa. ‘The Ht grades were adaod response fuser asctaton request Oagod ont sty f over 5200 commercial Grade 2,7, 18, and 26 tat reports where over 99% ‘mothe 58 ks anima UTS. Peepers for marl n trarstormed:bela condion. © proper for materi nthe slution vealed corton "Properes ‘or sliton Weaod end aged condlion Moderate stongi (deterined by aging temperate) ‘ropersee fr soUutontreaied and aged cendton-righ engi (aoletmanod by aging tomparatur) "For product section of wal rckress values <1. "For product secon or wal hckness valine 10 in. 6.4 Sampling—Samples for chemical analysis shall be rep- obtained from the forgings on a test basis and a frequency as resentative of material being tested, Except for hydrogen and agreed upon between the forger and the purchaser. The utmost unless otherwise specified, chemical analysis of ingot or billet care must be used in sampling titanium for chemical analysis shall be reported. Samples for hydrogen determination shall be because of its great affinity for elements such as oxygen, eis Pee reneip 8381 - 13 (2019) ome ee me = HD 80 S100 sD SEO BO MESO Ie wo wo 0 700 = oro so seo 800 ses Oba * : Sb St ozo coo cro 000 toroad es wf fe $2 cee coo S10 B00 serosa ozo si00 c90 BO OO Hse wey wea a ss co 5100 coo seo sw toned "ed «0 wo fy ee 3 fo $00 SE Sore sto so eo wo omens seu 0 sy seo a woo St Se ore soo soo ceo wo Soros vey 5 E = Se S$ seo seioo wo sro wo somos wey ze = : 2 = -- $2 oro too so 0 Soo clea eye sy 59 rT errs & a oo St Se oo wo aro aro avo sree a Fy 30 sor a oo SS Si Soro a0 soo a0 S00 once a woo oot) zd - eo Se Se seo sto eo sro ao eam Bas wo #00 -- oro 5100 oo so 0 ase Bi moo 2H Ro «we a uy a so 0 POO ee Dw oo ctv 00 S000 tHe so woo FOO SOD 0 St 0D SHO 0 Ye zo aoe ee Re Cy v0 eo Re oe eC so wow Fw ee eC : es FO KO 8 $B seo S100 cD SHO ww ceo oa oo wea FOO sea i009 000 50800 ress Hes oe ro vo + Se 050 S190 90020 90 oa os s ayo S100 900020 90 oomEH Su So Sioa soo oro. 00 oom a : fo Sio8 900 S60 00 Oss Ea wea oo siso $90 seo 0 ons ‘es oo Sica foo 10 foo omnes ‘ta Ra eee oS ULES wRREOR RD HMRAD UnOaPH PEN GnUBITU wreReA UNPR UTouNY Tew mew Fe Sar isan 9p oS “unr -wonsivedonn Bue oar Shin ‘sioner ve “oo on zozeyW00ted no) voRBeCICD “Siuewanbou 1eoqWIOUD Z STAVEAG 8381 - 13 (2019) ro 0 _ 0 seo oo Slory ues ow vo ro oe ~ - 0 S10 WO osresH ge ovo sz vo 60 “O20 a su - 90 Seo BO OreeE se zo sso yo wos +0 se0 0 60 ap SHESH rea z0 sso yoo ro 520 eo seo apo ehesy cou no vi en zu vo v0 90-90 = 90 + - $0 “DSP GD SI00 cD LISS ze o| Wee) UcayS UL UNG aNNENNE —TeROD UREN UneRATON REN —UReGTE UAPeTeD UnpHA UToURY UTS —wew aU WELD Wa YeQUMNY epEID ‘ou es ‘over “vebomfy'vesonN e6uB“uoReD Stn ‘suoworgsvawe om v8 840. 22.10 aooyrtieoreg whys Uonsec09 penumuog 7 S18ly 8381 - 13 (2019) TABLE 3 Permissible Variations In Product Analysis Product Anahes —_ Parmissbis Eloment Limits, Variation in Product maxorRange.‘% Anais Ronaam 525 7020 Aluminum 250675 i040 Carbon | O10) 0.02 ‘Ghvomum 0102 soe Shvomin 5565 050 Cobalt 02008 2008 Fayoropen 00 ce on 6.0 10:18 ion 12w18 020 Molyosenum o2t04 2008 Motedenurn Osi 12 sors Moloderum 15t045 3020 Mo 140% 160 2080 Nowe! a3t08 2005 Niobium 22622 rary ‘Nobiam 230 3050 iron 0.05 10.02 Oxygen 0.0 1000 Oxygen 031 woeo 008 Palagum 20% toe 002 Palagum 8.04 1 0.08 so00s Palau 01210025, 20.02 unis oat 001 20.005 uenium 8.041 00 20.05 une Dos toots soot siicon 8.08 19040 02 Tm 08130 215 Vanadium debs 8 Vanaaum 751035 2040 2rconium bn ta is Zrconiim, 3545 2020 Fesiduais* (cach) ois. soo * fresiualis an elorent presen na mia or anally nena auanites and inherent the manuastun prose but nt add nlontonay In tanur te ‘lent ince saminum,venacum, thon, envoml, maedsnum, Nobu, Zeon, hafnum, bismuth ruthenium, palalum, ym, copper, cen, cabal ‘Smalum miko boron manganese, and tungten nitrogen, and hydrogen. Therefore, the cutting and handling of samples should include practices that will prevent contamina- tion. Samples shall be collected from clean metal 6.5 At least two samples for chemical analysis shall be tested to determine chemical composition. Samples shall be taken from opposite extremes of the product to be analyzed. 7. Methods of Chemical Analysis 7.1 The chemical analysis shall normally be conducted using the ASTM standard test methods referenced in 2.1. Other industry standard methods may be used where the ASTM test methods in 2.1 do not adequately cover the elements in the ‘material or by agreement between the producer and purchaser. ‘Altemate techniques are discussed in Guide £2626, 8. Mechanical Properties 8.1 Forgings supplied under this specification shall conform to the requirements as to mechanical properties specified in Table 1, a8 applicable. 8.2 Specimens for tension tests shall be machined and tested in accordance with Test Methods E8. Tensile properties shall be determined using a strain rate of 0.003 to 0.007 in/in-min through the specified yield strength. After the specified yield strength has been reached, the crosshead speed shail be increased to a rate sufficient to produce fracture in approxi- mately one additional minute. 8.3 Sampling—Tension test specimens shall be machined from material as agreed upon by the manufacturer and the purchaser. 9. Nondestructive Tests 9.1 Nondestructive test requirements such as ultrasonic test, X-ray, or surface inspection shall be specified by the purchaser, if required. The standard for acceptance or rejection shall be agreed upon between the forger and the purchaser. 10, Dimensions and Permissible Variations 10.1 Dimensions and tolerances of titanium and titanium alloy forgings covered by this specification shall be as shown ‘on the applicable forging drawing or otherwise agreed upon by the manufacturer and the purchaser. 11. Workmanship, Finish, and Appearance 11.1 Titanium alloy forgings shall be free of injurious external and internal imperfections of a nature that will interfere with the purpose for which they are intended. An- nealed forgings may be furnished as descaled, sandblasted, or ‘ground, The manufacturer shall be permitted to remove minor surface imperfections by spot grinding if such grinding does not reduce the thickness of the forging below the minimum permitted by the tolerance for the forging at the applicable location, 12, Retests 12.1 If the results of any chemical or mechanical property, test lot are not in conformance with the requirements of this specification, the lot may be retested at the option of the manufacturer. The frequency of the retest will double the initial umber of tests. If the results of the retest conform to the specification, then the retest values will become the test values for certification. Only original conforming test results or the conforming retest results shall be reported to the purchaser. If the results for the retest fail to conform to the specification, the ‘material will be rejected in accordance with Section 14, 13, Rounding-Off Procedure 13.1 For purposes of determining conformance with this specification, an observed or a calculated value shall be rounded off to the nearest “unit” in the last right-hand signifi- ‘cant digit used in expressing the limiting value. This is in accordance with the round-off method of Practice E29 14, Rejection 14.1 Forgings not conforming to this specification or to authorized modifications shall be subject to rejection. Unless otherwise specified, rejected forgings may be retumed to the ‘manufacturer at the manufacturer's expense, unless the pur- chaser receives, within three weeks of notice of rejection, other instructions for disposition. 15, Referee Test and Analysis 15.1 In the event of disagreement between the manufacturer and the purchaser on the conformance of the material to the ‘Senin Seenaus $e pez skrrongreCnsuetscomly 8381 - 13 (2019) requirements of this specification, a mutually acceptable ref- cree shall perform the tests in question using the ASTM standard methods in 2.1. The referee's testing shall be used in determining conformance of the material to this specification, 16, Certification 16.1 The manufacturer shall supply atleast one copy ofthe report certifying that the material supplied has been manufactured, inspected, sampled, and tested in accordance With the requirements of this specification and that the results cof chemical analysis, tensile, and other tests meet the require- ments of the specification for the grade specified. The report shall include results of all chemical analysis, tensile tests, and all other tests required by the specification, 17, Packaging and Package Marking 17.1 Packaging—Unless otherwise specified, forgings pur- chased under this specification shall be packaged in accordance with the manufacturer's standard practice. 17.2 Marking—Forgings shall be marked for identification as agreed upon by the manufacturer and the purchaser. 18. Keywords 18.1 forgings; titanium; titanium alloys SUPPLEMENTARY REQUIREMENTS SUPPLEMENTARY REQUIREMENTS COVERING GRADE F3 TITANIUM FORGINGS ‘The following supplementary requirements are primarily intended for U.S. military applications and shall apply only when specified by the purchaser in the inguiry, contract, or order. S1. US. Military Requirements SI.1 Referenced Documents section follows. S12 Unless otherwise specified in the contract or purchase order, the seller is responsible for the performance of all inspection and test requirements in this specification, and the seller may use his or other suitable facilities for the perfor- ‘mance of the inspection and testing. S13. Grade F-3 composition shall be modified as follows: yerogen 0.0125 max iron 020max Ongen 0.26 max S14 Two tensile specimens shall be taken from each lot of forgings up to and 125 pounds, and two tensile specimens shall be taken from each forging greater than 125 pounds for verification of compliance with Grade F-3 mechanical proper- ties of Table 3. Alot shall constitute all forgings from the same heat, of the same design and size and heat treated in the same heat treat furnace load. The test specimens shall be taken from integral prolongations or extra forgings may be provided by the forger. Forgings under 314 in, (90 mm) in cross section may use separately forged test bars provided the wall thickness and amount of working are equivalent to the forgings being supplied. Extra forgings may be provided for samples when forgings are over 31 in, (90 mm) in cross section provided samples cannot be taken from prolongations or by trepanning. ‘Samples shall be taken from the section of forging having the largest cross section. The longitudinal axis of the tensile specimens shall be parallel to the major direction of metal low in the forging SLS_ Repair welding is not permitted. S16 Each forging shall be ultrasonically inspected in accordance with MIL-STD-2154 throughout 100% of their volume. Inspection shall be performed after heat treating when the forging is machined to the configuration for ultrasonic inspection as shown on the forging sketch or drawing. Inspec- tion shall be performed prior to drilling holes, cutting key ways, tapers, grooves, or machining section to final contour. Forgings shall be scanned using a straight beam technique such that all major planes are covered, Disc type forgings shall be scanned using a straight beam from at least one flat face and radially from the circumference when possible. Cylindrical, ring, and hollow forgings shall be scanned from the entire external surface using the straight beam technique, and in the axial direction to the maximum extent possible. Acceptance criteria shall be to class A of MIL-STD-2154, SI.7_ All surfaces of each forging shall be liquid penetrant inspected in accordance with NAVSEA T9074-AS-GIB-010/ 271. Acceptance criteria shall be in accordance with NAVSEA '$9074-AR-GIB-O10/278 as specified in the order. S18 Forgings shall be free of foreign material and con- taminants such as sulfur, lead, marking paints or machining or forming lubricants. Forgings shall be cleaned prior to any heat treatment operations, Forgings shall be free of any oxygen rich layer, such as alpha case 'S1.9. The first forging of each type and design submitted for inspection shall be the first article sample. Mechanical properties for first article inspections shall be determined ‘throughout the forging as specified in the order (which should also include specific instructions regarding arrangements for ‘examinations, approval of test results, and disposition of the first article samples), and the number and location of the test specimens and the acceptance criteria shall be as specified or as ‘agreed upon between the contracting activity and the manu- facturer. In addition, A full cross-section shall be macroetched in accordance with ASTM E340 and examined at 10x magni- fication for uniformity, soundness, grain size and grain flow. ‘The macro etch cross section shall evidence uniformity of quality, soundness and freedom from cracks and porosity. A TIES een xenonGy 8381 - 13 (2019) fully wrought structure shall be evident and variation in grain size shall be such that it will not interfere with ultrasonic examination. The manufacturer shall maintain a record of production practices used for the first article forging. In the event of change in the production practice in the same or subsequent order, the manufacturer shall notify the contracting activity and ‘obtain approval of the changes. The manufacturer may be required to perform specific first article tests and examinations to verify that the change will not or has not degraded forging quality S110. The material shall be electron beam and/or plasma melted or shall be multiple melted with at least one of the melting cycles under vacuum. 82. Referenced Documents S21 ASTM Standard: E340 Test Method for Macroetching Metals and Alloys $2.2. Military Standards T9074-AS-GIB-010/271 Requirements for Nondestructive ‘Testing Methods $9074-AR-GIB-010/278 Requirements for Fabrication Weldingand Inspection, and Casting Inspeetion and Repair for Machinery, Piping, and Pressure Vessels MIL-STD-2154 Inspection, Ultrasonic, Wrought Metals, Processing for ASTM Intemational takes re poston respecting the val of any patent rights asserted in conection wih ary item mentioned inti standars. Users of tis standard are expressly advised Pat determination othe vay of any such patent rts andthe isk Otintangamert of such rigs, are ently thav own reopens ‘This stand subject o revision at ay tine bythe responsive technica cmmitee and must be reviewed evayfve years and than ‘toot ris, eter wagoroved or "Your comment re inited athe for tvisono te standard orfredeltona standards and should be adcressed to ASTM interatonal Headquarters Your comments wil ecave cart consideration a a meeting of te ‘response tesnical commitee, which you may attend. you fel tat your commens have not ecaved a fa hearing you should ‘make your vows krown fo te ASTM Convmtee on Standard, a he actrees chown below. ‘Thi standart is copyrighted by AST ntematioal, 100 Bar Harbor Dive, PO Box C700, West Cnshhocken PA 19426-2959, United State. 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