Organic Chemistry Lab1

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Names Oxwey Auran / 9-5 Latoe® qualitative elemental ant functional onalyis of organic compounal | Recpose Chemical tests are tests done is labs using to find out unknown organic substonces by observi identify cartein chemical Celemants / compound or certain out different results / observations after the fest. The oder, color, precipetate and change of stote Experiments: => Detection of Carbon ond Hydrogen ( CxHy Oa ) in a test Lube and add 500-1000 © Ada the untnown substance Of powdered copper (IT) oxide ( oxidisingagent) in a test tube and mix bby “Shating intended for turing. eqipment, ont Unasin svtasfance the dest resules. Chemical tert Functional groups by giving observations con be * Ada extension tobe to another dube intended for cottecting the gasemitting Coutlet tube) © Hold tube with Observation © + Formation of ulater droplets on the walls of 4ube, * Release of gos 5 COs wich is deiected by turning the Ba (OH), solution 4urbia | * White precipetate Formule» [02 CxHyO2 —> COa+ Hao. COs * Ba (oH). —> Bacos clamp and heat test tube over fire — Betecting Sulfur (Skeps! Remove totum fiom ol © Cut sodium into small peices © Dry sodium osing 3 fier paper horaughig » then asd to — a test t © Heat the Lube by hobing HX horitantaly an flame ae The bot red tube 6 qicly lowered ino 0 ghss of weter to lesicoy HX snd 47ASAF dhe reontion produts Inte solution Ads ach of soaium nt opemds Naa [Fe (oni), (NO)] Observation: Bright Violet color, (SHES! Remove —soaium From # Cut sodivem into smal peices. + Bry sodium ing 9 Liter paper oroughty , then acs to O teat dite * Heot the tube by helding i¢ horiaortaly on flame ©The hot ced tube is quietly lowered inte a gaat of water to denioay: ik and Aransfer the readion products into solution © The Resulting mixture is filtered hrough a funnet with filter ino- a new test tube. © Ads mixture of iron (TZ) and iron (IT) ions ant bai! for SO seconds © Col ander evening wader «Add concentrates HC| dropwise ond shobe the mixture: ObseNotion Y Bue color sppeore, = Detection of heloges © Burn 2 kip of copper wire untill Lhe flame color stops being qrees * Wet the tip of copper wire ons dip into Ahe uninoun sestance + Put the tip of copper wit an the flome and notice — flame color Orange color observes is CI is * ‘a presat, + Betection oF Melty! Ketone Grup (Een) # Puc solotion of iodine in potasivm iodide ant sad hydroe Solution with the unkown Substance © Add feu drops of Acetone Solution * Turbidity and preeipetote + Any change > Detection of phenolic Group Doo SRP lock snare fume hens + Pour smoll amount of pheral soutien into 2 test Lubes 2 Ads feu drops of iron (ST) cloride be the first tice + Add few drogs of bromine water to the stamd 4est tute, * Bromine water is discolores, * Vives / purple color observed. a. 9 se &, on a 1*. 9 + Fes —> V2 & © Adki lop of onitne hydrochkrse sation 40 fille” paper. © Add dep of sodium qirite saiution do the resulting siain + Adsl deep of N,N- dimethotine om observe resulta + Orange celor precipeiete * Smet —™ Detection of Aldehyses Steps: * Ads drops of aqueous ammonia 0 silver nitrate sowion © Heep ontsing ammonia undil the precipetote formes did ves © Ada sodium hy drowide # Ads giveare sottion bo Ave restng sation of arnonia oP she axe, Gnd SHE ond cue io Kt woler Lor Seteral minstes + Mierer lay = emad en the wath OR + Block grecipiiote of aher with fon. — Detection of Nyirocorton ( Pare 3) Sips inQ Prepare 3 eet Jules yp mix of atoms in @, put bensene in(Q), a pinine in © Test 4- Add bromine 40 the 3 test Lubes au stove wait © Test2- Ada Kurd, sotstion to 8 test tubes © Test8 - Adel nitrosing mixture into 2 aly teA bike) odd arcps of Petro in one fest babe ond then bensene £0 nother and Shake carefily ~ Nitroting mixture + 1,90, + NNO, Test 4- Decolarised ; react utith oL- pinine © Test 2- Bloch proipetete win om pine © Ter 3-2 loyer soesn'4 mix with atane ge color , bubheg » reacds. Conclusion Oduley Aurore O4- 9D

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