Preparation and Performance Evaluation of Erosion Resistant Lining of Bimetallic Composite Pipeline

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Proceedings of the ASME 2022

International Mechanical Engineering Congress and Exposition


IMECE2022
September 26-30, 2022, Calgary, AB, Canada

IMECE2022-####

PREPARATION AND PERFORMANCE EVALUATION OF EROSION RESISTANT LINING OF


BIMETALLIC COMPOSITE PIPE

Jianwei Dong1, Deguo Wang1, Yanbao Guo1


1
China University of Petroleum-Beijing, Beijing, China

ABSTRACT bonding quality and no obvious defects. In the same erosion


Erosion widely exists in oil and gas production and environment, the bimetallic composite pipe has stronger erosion
transmission pipelines, which seriously affects the service life of resistance, lower erosion rate and higher service life than carbon
pipelines. Ordinary carbon steel pipe can meet the strength and steel pipe. Therefore, through the exploration of the preparation
pressure of oil and gas transportation, but it has the method of bimetallic composite pipe, this paper improves the
disadvantages of poor erosion resistance, short service life and preparation process of bimetallic composite pipe, improves the
frequent replacement. The cost of using erosion resistant metal comprehensive mechanical properties and erosion resistance of
pipe is high, which is not suitable for comprehensive bimetallic composite pipe, and promotes the application of
popularization and application. Bimetallic composite pipe bimetallic composite pipe in industrial production.
includes outer layer and inner layer. It is formed by two different Keywords: Bimetallic composite pipe; Inner layer; Joint
metals through a variety of processing technologies, which has surface; Erosion; Electromagnetic heating
the advantage that a single material does not have. It not only has
the strength and toughness of the outer pipe, but also has the NOMENCLATURE
erosion resistance of the inner pipe. The service life of bimetallic ε epsilon
composite pipeline can be 4-6 times longer than that of 1. INTRODUCTION
traditional carbon steel pipeline, and the manufacturing cost is When the pipeline is transporting oil and natural gas for a
relatively low, the service time is long, and it has good economy. long distance, the particles and flow field in the pipe will cause
Therefore, it is more and more widely used in oil and gas serious erosion and wear to the pipe, resulting in the failure of
production and transportation. However, the common problem the pipe[1-5]. it is not only related to the safety of industrial
of bimetallic composite pipe is that the bonding interface production, but also related to the safety of life and property.
between outer pipe and inner layer is not fully bonded and there Therefore, wear-resistant pipe have been more and more
has gaps. Or the interface binding force is not enough. When the used in industrial production. high chromium cast steel pipe has
composite pipe is eroded by the fluid in the pipe, the stress high wear resistance due to chromium[6-7]. but it needs to be
concentration at the interface will lead to the separation of the formed by centrifugal casting. due to the limitation of casting
inner layer and the outer pipe, leading to the reduction of the process, the pipe wall thickness is thick and difficult to control,
service life of the pipe. Therefore, how to prepare the bimetallic so it is difficult to form a unified standard for pipe diameter. at
composite pipe with good quality and strong erosion resistance the same time, casting sand holes, pores and other defects often
has become an urgent problem to be solved. In this paper, carbon appear in the casting process[8-10]. and the price is high, so it is
steel cemented carbide bimetallic composite pipe was prepared difficult to popularize and use in large quantities. wear resistant
by electromagnetic heating through the application of centrifugal ceramic lined composite pipe is usually prepared by inlay
force and molten metal fluidity. The joint surface of the prepared method, thermal spraying method and self propagating high
bimetallic composite pipe was observed and analyzed, and the temperature synthesis method[11-12]. it has high corrosion
erosion test of the inner layer was carried out. The micro resistance and wear resistance of ceramics, as well as excellent
morphology of the erosion sample was observed and analyzed characteristics such as heat insulation and high temperature
by shape analysis laser microscope. The erosion rate was resistance[13-14]. however, the strength and toughness of ceramic
accurately calculated according to the mass loss of the sample lining are poor. when subjected to strong impact, cracks and even
before and after erosion. The results show that the bimetallic spalling often occur, resulting in short service life. the self
composite pipe prepared by the above method has good interface propagating high temperature synthesis method has the

1 © 2022 by ASME
advantages of simple process and low cost[15]. in recent years, and the inner layer, and the inner layer has no obvious defects
under the research of many scholars, this technology is becoming such as holes and cracks. This is because during the
more and more mature and widely used [16-18]. this provides a lot transformation from molten state to solid state, the solidification
of reference for the process selection and preparation method of rate of cemented carbide is controlled by slowly reducing the
bimetallic composite pipe in this paper. temperature. At the same time, under the action of centrifugal
This paper intends to adopt the electromagnetic heating force, the molten metals squeeze each other and finally solidify,
method with the characteristics of green, energy saving and high so there are no obvious defects.
efficiency[19-20]. bimetallic composite pipe was prepared by using 2.2 Erosion test of bimetallic composite pipe
carbon steel metal pipe and cemented carbide powder. the The erosion resistance of bimetallic composite pipe is an
bimetallic composite pipe not only has the strength and important index to measure its service performance. In this
toughness of the outer carbon steel metal pipe, but also has the paper, the erosion test of the prepared bimetallic composite pipe
high hardness and high wear resistance of the inner cemented is carried out by using the liquid-solid two-phase flow erosion
carbide. a bimetallic composite pipe preparation process with loop system designed and built by the laboratory (FIGURE 2).
simple preparation process, low cost, energy saving and
environmental protection is formed. it provides a new method for
the preparation of bimetallic composite pipe and promotes the
industrialization process of bimetallic composite pipe.
2. MATERIALS AND METHODS
2.1 Preparation of bimetallic composite pipe

FIGURE 2: SOLID-LIQUID TWO-PHASE FLOW EROSION


LOOP SYSTEM
The system mainly includes the following modules: water
and sand mixing box and mixing device, corrosion-resistant and
wear-resistant pump, variable frequency speed regulator, flow
acquisition module, flow velocity acquisition module and visual
1-Power supply; 2-Cemented carbide powder; 3-Temperature erosion box. Use electromagnetic flowmeter to measure liquid
measuring instrument; 4-Electromagnetic coil; 5-Carbon steel flow. The pipeline between the corrosion-resistant and wear-
pipe resistant pump and the visual erosion box is equipped with a
FIGURE 1: SCHEMATIC DIAGRAM OF BIMETALLIC check valve and an anti-seismic pressure gauge. The check valve
COMPOSITE PIPE SAMPLE PREPARATION is used to prevent the reverse flow of fluid at the moment of start
The schematic diagram of preparing bimetallic composite and stop of the device, and the pressure gauge is used to measure
pipe sample is shown in FIGURE 1. The outer layer of the the pressure in the pipeline. The erosion rate is adjusted by the
composite pipe adopts carbon steel pipe to ensure its high frequency conversion speed regulator, the sand and water are
strength and mechanical properties. Cemented carbide powder is mixed and proportioned by the agitator, and then enter the visual
selected as the material for making the inner layer, so that the erosion box from the sand outlet through the corrosion-resistant
prepared inner layer has good properties of high temperature and wear-resistant pump for erosion. The mixture of sand and
resistance, corrosion resistance, wear resistance and so on. Place water after erosion flows into the sand mixing device through the
the carbon steel pipe with cemented carbide powder in the sand outlet to realize the circulation effect. The erosion angle and
electromagnetic coil and power on the equipment. The heat distance are controlled and adjusted by the fixture in the visual
generated by electromagnetic heating melts the cemented erosion box.
carbide powder placed in the carbon steel pipe. The molten The test methods used in this erosion test mainly include
cemented carbide is subjected to centrifugal force in the weight loss method and microscopic technology. Due to the
circumferentially rotating carbon steel pipe and the fluidity of small surface area of the sample. Therefore, the average erosion
the molten metal itself, so that it can be evenly distributed on the rate calculated by the weight loss method can be used as the final
inner wall of the outer pipe. After slow cooling, a certain erosion rate at this position. The calculation formula of erosion
thickness of inner layer is formed in the carbon steel outer pipe. rate is:
After the preparation of bimetallic composite pipe, the m  m1 (1)
= 0
combination of outer pipe and inner layer is observed and msand
analyzed. A large number of studies have shown that the Where: ε is the erosion rate of the sample, g/kg; m0 and m1 are
interface between the outer layer and the inner layer of bimetallic the mass of the sample before and after erosion, g; msand is the
composite pipe and the surface forming quality of the inner layer total mass of sand particles impacting the target, kg.
play a key role in the performance of bimetallic composite In the two-phase flow used in the test, the liquid medium is
pipe[21-22]. After inspection, the prepared bimetallic composite deionized water and the solid medium is quartz sand, which the
pipe sample has achieved a good combination of the outer pipe particle size range is 200~300 um, with edges and corners. The

2 © 2022 by ASME
specific gravity of quartz sand is about 15%. The liquid-solid
two-phase flow erosion test was carried out under the condition
of water temperature of 25℃ and liquid flow rate of 30 m/s. Each
test shall be carried out continuously for 5.5 h. In order to reduce
the test error, parallel experiments shall be carried out, and the
average value of the two results shall be taken as the final erosion
rate. After each test, replace the solution and quartz sand.
In order to control a single variable, the erosion rate, erosion
angle, sand weight ratio, time and other parameters of each group (a) The first group of carbon steel pipe erosion samples (b) The
are adjusted to be unified, and only the erosion sample is taken first group of bimetallic composite pipe erosion samples (c)
as the only variable. Two sets of erosion tests were performed on The second group of carbon steel pipe erosion samples (d) The
each sample. The test parameters are shown in Table 1. second group of bimetallic composite pipe erosion samples
Table 1: EROSION TEST PARAMETERS FIGURE 3: MACRO MORPHOLOGY OF EROSION SAMPLE
Sand The micro morphology of the erosion sample is shown in
Velocity Angle specific Time FIGURE 4 and FIGURE 5. From the microscopic morphology
Sample Group
(m/s) (°) weight (h) magnified by 200 times (FIGURE 4), pits caused by two-phase
(%) flow erosion appear on the surfaces of bimetallic composite pipe
Carbon 1 30 30 15 5.5 erosion samples and carbon steel pipe erosion samples, and the
steel pipe 2 30 30 15 5.5 distribution is relatively uniform. It shows that the prepared
Bimetallic 1 30 30 15 5.5 bimetallic composite pipe has uniform texture. However, in the
composite same visual field, the number of pits in the bimetallic composite
2 30 30 15 5.5 pipe erosion sample is significantly less than that in the carbon
pipe
In order to more clearly observe and analyze the erosion steel pipe erosion sample. It shows that the erosion resistance of
results, the working surface of the sample shall be polished bimetallic composite pipe is stronger. At the same time, it is
successively with 240#~1500# water sandpaper before the observed that there are obvious corrosion traces around the pits
erosion test. After cleaning and drying, weigh the mass of the in the carbon steel pipe erosion sample, indicating that the
sample before the experiment with an electronic balance corrosion phenomenon occurs at the same time under the action
(Accuracy: 0.01 g), measure it for 3 times and take the average of two-phase flow erosion. Under the combined action of erosion
value. Then, the erosion test shall be carried out according to the and corrosion, the damage of the sample will be accelerated.
above parameter settings. After the test, clean and dry the Under the action of erosion, fatigue cracks appear on the surfaces
sample, weigh the mass with a balance, measure it for 3 times of both samples. The growth, expansion and falling off of fatigue
and take the average value. Then, the 3D erosion morphology of cracks on the surface will cause quality loss. The crack length in
the erosion sample was observed and analyzed by using VK- the erosion sample of bimetallic composite pipe is about one fifth
X250K shape analysis laser microscope. of that of carbon steel pipe, which shows that bimetallic
3. RESULTS AND DISCUSSION composite pipe has stronger resistance to fatigue damage and
The macro morphology of bimetallic composite pipe and higher fatigue life in the erosion environment.
carbon steel pipe samples of the same specification after erosion
test is shown in FIGURE 3. In the erosion test, under the same
test parameters, the average width of erosion wear of carbon steel
sample is 15 mm and that of bimetallic composite pipe sample is
11 mm. After erosion, the damage area of bimetallic composite
pipe is smaller.

FIGURE 4: MICROSTRUCTURE OF EROSION SAMPLE


(200X): (A) CARBON STEEL PIPE (B) BIMETALLIC COMPOSITE
PIPE
As can be seen from the microscopic morphology magnified
by 1000 times (FIGURE 5), furrows formed by the plastic
extrusion of quartz sand appear on the surfaces of both samples
under the action of low angle erosion of two-phase flow. At a
lower impact angle, the cutting wear trace of quartz sand on the
surface of the erosion sample is obvious, and the metal falls off
on the surface. When the cutting wear occurs in the actual
industrial oil and gas pipeline, the surface metal will fall off and
the internal metal will be exposed again. The long-term erosion

3 © 2022 by ASME
will lead to the thinning of the wall thickness of the eroded part provides a new low-cost, green and energy-saving method for
and reduce the service life of the oil and gas pipeline. At the same the preparation of bimetallic composite pipe.
time, it is observed that there are few furrows and cutting marks (2) Compared with carbon steel pipe, the strength and
on the surface of bimetallic composite pipe, while there are many erosion resistance of the bimetallic composite pipe are greatly
furrows and cutting marks on the surface of carbon steel pipe. improved, the probability of corrosion in the erosion
This is because with the progress of erosion, the original environment is smaller, and the bimetallic composite pipe has
microstructure, properties and mechanical state of the first higher fatigue life and strong erosion resistance.
damaged position on the sample surface have changed. The ACKNOWLEDGEMENTS
strength and erosion resistance of the material are affected, We gratefully acknowledge the kind cooperation of Dr. Bin
which makes the damage further develop and accumulate Wang in the preparation of this application note.
gradually. Finally, the furrow and cutting marks in the figure are REFERENCES
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FIGURE 5: MICROSTRUCTURE OF EROSION SAMPLE Quarterly, 2021.
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In this paper, the forming quality and erosion resistance of [22] Gao H T, Wang L, Liu S L, et al. Journal of Materials
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are tested and analyzed. The erosion resistance of bimetallic
composite pipe is studied. Through the erosion test, the
observation and analysis of the macro and micro structure
morphology of the erosion sample and the analysis of the test
data, the following conclusions are mainly drawn:
(1) Due to the centrifugal force, the inner layer of the
bimetallic composite pipe prepared by electromagnetic heating
has uniform forming texture, no obvious defects, and the
bonding quality of the outer pipe and the inner layer is good. It

4 © 2022 by ASME

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