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Macroetch Testing of Tool Steel Bars: Standard Practice For
Macroetch Testing of Tool Steel Bars: Standard Practice For
Macroetch Testing of Tool Steel Bars: Standard Practice For
This standard has been approved for use by agencies of the Department of Defense.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1
A 561 – 71 (1999)
times under 10 min or over 40 min are avoided with tool steels. 7.1.1.4 Concentrations of nonmetallic inclusions,
The time of etching is best adjusted by trial to develop the 7.1.1.5 Porosity, and
degree of etching desired. Where recovery of temperature of 7.1.1.6 Internal cracks or thermal flakes.
the solution is slow after immersion of cold specimens, NOTE 1—Carbide segregation is better determined by examination of a
reproducibility is enhanced by preheating the specimens in hot polished surface after etching in 4 % nital solution.
water prior to immersing in the etchant.
6.3 Macroetching Technique: 7.1.2 Surface and Subsurface:
6.3.1 After preparation as described above, clean the speci- 7.1.2.1 Seams, laps, cracks, etc.,
men of dirt and grease with a solvent, if necessary. Then place 7.1.2.2 Ingot corner segregation or cracks, and
directly into the etching solution already heated to the proper 7.1.2.3 Pinholes,
temperature, or preheat in water as in 6.2 and then transfer to 7.1.3 Miscellaneous:
the hot etching bath. The purpose of preheating the specimen is 7.1.3.1 Entrapped metallic or nonmetallic material, and
to obtain better control of the etching conditions where close 7.1.3.2 Ingot pattern (dendritic segregation, columnar grain
reproducibility of degree of development is desired. The structure, etc.).
specimen must be completely immersed. 7.2 Twelve photomacrographs2 provide a numerical rating
6.3.2 Moderate agitation (stirring) of the solution during of severity levels of porosity (7.1.1.5) and ingot pattern
macroetching promotes uniform development by eliminating (7.1.3.2) that may be present in tool steel bars.
temperature and composition gradients. Provision for agitating 7.2.1 These conditions identified in general as porosity and
the etchant may be desirable where the volume of solution is ingot pattern are described as follows:
relatively small. 7.2.1.1 Center Porosity—A center concentration of minute
6.3.3 At the end of the etching period, remove the specimen voids related to etched out carbides, or nonmetallic inclusions,
from the hot acid and rinse immediately in a stream of water. etc.
Flush off the sludge which forms on the surfaces of the 7.2.1.2 Ring Ingot Pattern—One or more concentric rings
specimen during etching with the aid of a stiff brush. Then dry characterized by differential etching associated with a minor
the specimen with alcohol, a clean air blast, or live steam. gradient in chemical composition or ingot solidification.
6.3.4 After drying, protect the etched surface from rusting 7.2.2 Ratings for the conditions can be determined by
by an application of oil, grease, glycerine, or transparent comparing macroetched disks with these photographs.
lacquer. 7.2.3 The photographs are not intended as standards for
acceptance or rejection. The numerical identity listed with each
7. Interpretation of Results figure only refers to a degree of severity. The extent that each
7.1 Examine the etched surface visually or at up to 103 condition is permissible for a given application should be
magnification to determine its structure. Note the presence, stated by the tool steel specification covering the application or
absence, and severity of the following conditions: as negotiated between the supplier and purchaser.
7.1.1 Internal:
7.1.1.1 Pipe, 2
The set of 12 photomacrographs may be obtained from ASTM Headquarters,
7.1.1.2 Bursts, 100 Barr Harbor Drive, W. Conshohocken, PA 19428, at a nominal cost. Request
7.1.1.3 Carbide (see Note 1) or alloy segregation, Adjunct ADJA0561.
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