August 2022

「Toughness fine waterproofing and adhesion strength of various sealing materials」

SHOSEKI KAKO Co, Ltd.

1. First of all

The adhesion strength of the sealing material used for the purpose of adhering Toughness Fine
waterproofing and Metal stick etc. is reported below.

2. Adhesion test

Adhesion between toughness fine waterproofing and various sealing materials, and adhesion
between Metal stick and various sealing materials,
We asked for each and confirmed the suitability of the material.

(1) Test items

Adhesive strength to substrate [Complies with 6.12 Adhesive performance of JIS A
6013:1992 (Modified Asphalt Roofing Sheet)]
① Various sealing materials
② Metal stick and various sealing materials
(2) Preparation of specimen
1) Apply a primer to the base ※ Omitted in ②
2) Construction of waterproof layer and sealing material

Table-1.1 Adhesion test process ( ① Toughness fine waterproofing and various sealing materials )

Process Asphalt urethane Modified silicone Urethane sealant

sealant
Toughness fine MS caulking Urethane ace

1st day Primer application TF primer

2nd day 1st layer (1.5kg) + Toughness fine + TF cloth
TF cloth
3rd day TF 2nd layer (1.5kg) Toughness fine upper layer
4th day Various sealing materials Toughness fine MS caulking Urethane ace
5th day Curing ↓ ↓ ↓
6th day Curing/testing ↓ ↓ Test after 2 days
7th day Test implementation Test after 3 days Test after 3 days
 Table-1.2 Adhesion test process ( ② Metal stick and various sealing materials )

Process Asphalt urethane Modified silicone Urethane sealant

sealant
Toughness fine MS caulking Urethane ace

Under Slate Slate base plate

plate
1st Seal material (1.0kg/m2) Toughness fine MS caulking Urethane ace
day
Metal stick Metal stick
2nd Curing/testing Test implementation
day

3) After making the waterproof layer, fix the steel attachment (4 cm x 4 cm) with epoxy
adhesive. ※ Omitted in ②
4) After the adhesive hardens, cut along the edge of the steel attachment to reach
the substrate, The waterproof layer around the attachment was removed to prepare
a test specimen. ※ Omitted in ②
 (3) Specimen
Table 2 shows the outline of the specimen.
Table-2 Outline of the specimen
Composition of the test body① Composition of the test body②
(Toughness fine) (Metal stick)
Under plate: Under plate:
slate plate (approx. 7 cm x 7 cm, t8 mm), etc. slate plate (approx. 7 cm x 7 cm, t8 mm), etc.
1：TF PRIMER 0.2 kg/m2 1：Various sealing
materials
2：Toughness fine 1.5 kg/m2 (1) Toughness fine
3：TF Cloth ― (2) Modified silicone sealing Each 1kg/m2
material
4：Toughness fine 1.5 kg/m2 (3) Urethane seal material
5：Various sealing materials 2：Metal stick (1kg/less than)
(1) Toughness fine Metal stick area≒ 45cm2
(2) Modified silicone sealing material Each 1.0kg/m2
(3) Urethane sealant

Cross-sectional view of test piece ① Cross-sectional view of test piece ②

Steel attachment
Epoxy adhesive Metal stick
Various sealing
Various sealing
【Waterproof layer】 materials
4)Toughness fine
3) TF cloth
2)Toughness fine
Under plate (slate base) 1)TF primer Under plate (slate base)

※The metal stick used in the test weighs less than 1g, and
it is calculated that a load of 0.001kg×9.8≒0.01N is
applied to the bonding surface.
 (4) Test conditions
Test temperature: 20±2℃
Test speed: 0.5mm/min , 500mm/min

(5) Test method

① Attach the jig for adhesion test to the tensile tester, attach the test piece, and
pull until the test piece breaks according to the conditions in Table 2.
② Read the maximum load (N) from the automatically recorded chart.
③ The test result was obtained by dividing the indicated strength (maximum load)
of the tester as the test force (N) by the area of the attachment as the
adhesive strength (N/cm2).

Test force(N)
Adhesion strength(N cm2)＝
16cm2
3. Test
results

The test results are shown in Table-3 and Table-4.

Table 3 Tensile adhesion test results when adhering Toughness Fine

and various sealing materials
Specification name Test speed Test results Criterion
0.5mm/min 48.3 N/cm2
Toughness Fine Criteria for Open Recruitment
500mm/min 75.6 N/cm2
Technical Examination and
Modified silicone 0.5mm/min 20.3 N/cm2 Certification
sealing material
500mm/min 42.3 N/cm2
「MS caulking」 Adhesion 2.5N/cm2 or more
Insulation 12N/cm2 or more
Urethane sealing 0.5mm/min 25.5 N/cm2
material
500mm/min 26.2 N/cm2
「Urethane Ace」

Table 4 Tensile adhesion test results when bonding Metal stick and the sealing
material

Specification name Test speed Test results Criterion

0.5mm/min 17.2 N/cm2
Toughness Fine
500mm/min 42.7 N/cm2
Criteria for Open Recruitment
Modified silicone 0.5mm/min 14.1 N/cm2 Technical Examination and
sealing material 500mm/min 22.3 N/cm2 Certification
「MS caulking」
Adhesion 2.5N/cm2 or more
Urethane sealing 0.5mm/min 17.6 N/cm2 Insulation 12N/cm2 or more
material 500mm/min 37.0 N/cm2
「Urethane Ace」
4. Summary

From the above results, it was confirmed that there was no problem in adhesiveness in all of
the three types of sealing materials used in this experiment.
The judgment criterion is the judgment criterion of base adhesive strength, which is a high
level used for exposure waterproofing, and it was confirmed that any sealing material exceeded
the judgment criterion.

Toughness Fine waterproofing has the best adhesiveness of the same quality, and is the most
recommended.

The adhesion to the material of the Metal stick (it is thought that most of the products on
the market are made of aluminum) is not particularly inferior, but the application timing,
especially after the progress of hardening, it is conceivable that the register marks cannot
be held in the initial state of low viscosity.

Therefore, it is considered desirable to have marks attached at the timing in the middle of curing
near the end of the pot life.
 T E S T R E S U L T

№
SHOSEKIKAKO CO.,LTD.
Teigeki Building F7
1-1,Marunouchi 3 chome Chiyoda-ku, Tokyo,
100-005, Japan

PRODUCT ： TF PRIMER (Aqueous)

ITEM RESULT TEST METHOD

Condition in container *1 Pass
Workability *2 Pass JIS K 5600
Drying time (23℃) (minute) 25

NOTE
*１：After stirred ,there will be uniform and no hard lumps.
*２：There is no hindrance to roller and trowel work..
 T E S T R E S U L T

№
SHOSEKIKAKO CO.,LTD.
Teigeki Building F7
1-1,Marunouchi 3 chome Chiyoda-ku, Tokyo,
100-005, Japan

PRODUCT ： TOUGHNESS FINE

ITEM RESULT TEST METHOD

Tensile Tensile strength (N/mm2) 2.4
performance Elongation at break (%) 460
(23℃) Tensile product (N/mm) 220
Tear JIS A 6021
performance Tear strength (N/mm) 20
Solid content (%) 75.1
Density at cured product ( Mg/m3) 1.15

NOTE
 T E S T R E S U L T

№
SHOSEKIKAKO CO.,LTD.
Teigeki Building F7
1-1,Marunouchi 3 chome Chiyoda-ku, Tokyo,
100-005, Japan

PRODUCT ： TF CLOTH

ITEM RESULT TEST METHOD

Width (mm) 1025
Thickness (mm) 0.59
Mass per unit area (g／m2) 87
Longitudinal
direction
239
Tensile strength (N)
Cross direction 132 JIS L 1096
Longitudinal
direction
35
Elongation (%)
Cross direction 56
Longitudinal
direction
25
Tear strength (N)
Cross direction 42

NOTE
 T E S T R E S U L T

№
SHOSEKIKAKO CO.,LTD.
Teigeki Building F7
1-1,Marunouchi 3 chome Chiyoda-ku, Tokyo,
100-005, Japan

PRODUCT ： FINE BOND

ITEM RESULT TEST METHOD

Condition in container*1 Pass JIS K 5600
Nonvolatile content (%) 56.5 JIS K5601
Viscosity (mPa･s／23℃) 3000 JIS AK6833

NOTE
＊1 ：After lightly stirred ,there will be uniform and no hard lumps.
 T E S T R E S U L T

№
SHOSEKIKAKO CO.,LTD.
Teigeki Building F7
1-1,Marunouchi 3 chome Chiyoda-ku, Tokyo,
100-005, Japan

PRODUCT ： TF COAT

ITEM RESULT TEST METHOD

Appearance *1 Pass Visual observation
Viscosity (mPa･s／23℃) 12600
JIS K 5600
Density (g／cm3) 1.55
Nonvolatile content (%) 77.0 JIS K 5601

NOTE
*１：No contamination.