BLABSYSEvoROBOT 1A

B/LABSYSEVOROBOT-1A
 EVO
LABSYS
ROBOT OPTION
USER'S MANUAL
Labsys Evo – Robot Option
TABLE OF REVISIONS
B/LABSYSEVORO
B 28/09/12 Power on warning added C. MATHONAT L. PASSELEGUE C. MATHONAT
BOT-1A
A/LABSYSEVORO
A 18/06/10 Creation Y. MEIZONNIER C. MATHONAT
BOT-1A
REASON FOR MANUAL REQUESTED
REV DATE APPLIED BY APPROVED BY
REVISION REF BY
Table of Revisions 2
B/LABSYSEVOROBOT-1A - 28/09/2012
CONTENTS
TABLE OF REVISIONS .....................................................................................................2
CONTENTS ....................................................................................................................4
NOTICE TO USERS ..........................................................................................................7
CHAPTER 1 - PUTTING INTO SERVICE .............................................................................10

1. PRESENTATION ...............................................................................................10
1.1 Description of the Labsys™ Evo Robot ............................................................... 11
2. INSTALLATION .................................................................................................15
2.1 Installing the apparatus ...................................................................................... 15
2.2 Dimensions.......................................................................................................... 16
3. ELECTRICAL AND COMPUTER CONNECTIONS ......................................................17
3.1 Electrical connection .......................................................................................... 17
3.2 Computer connections......................................................................................... 17
4. PUTTING THE APPARATUS INTO SERVICE ...........................................................18
5. TECHNICAL CHARACTERISTICS .........................................................................20
5.1 Labsys™ Evo Robot............................................................................................ 20
5.2 Conformity with standards.................................................................................. 21
CHAPTER 2 - UTILIZATION .............................................................................................22
1. PREPARING THE APPARATUS ............................................................................22
1.1 Positioning the crucibles..................................................................................... 22
1.2 Positioning the rod.............................................................................................. 23
1.3 Balancing the balance......................................................................................... 23
1.4 Installing the protective cover............................................................................. 23
2. USING THE CALISTO ACQUISITION SOFTWARE ....................................................24
2.1 Declaring and connecting the apparatus............................................................ 24
2.2 Utilization with Direct Programming................................................................. 25
2.3 Preparing a series of experiments ...................................................................... 27
2.4 Running a Series ................................................................................................. 31
APPENDIX A – ERROR MESSAGES .................................................................................33
1. ACKNOWLEDGED OF ERROR OR WARNING MESSAGE...........................................33
2. ERROR NO.1...................................................................................................33
3. ERROR NO.2...................................................................................................33
4. ERROR NO.3...................................................................................................34
5. ERROR NO.4...................................................................................................34
6. ERROR NO.5...................................................................................................34
7. ERROR NO.6...................................................................................................35
8. ERROR NO.7...................................................................................................35
9. ERROR NO.8...................................................................................................35
10. ERROR NO.9...................................................................................................35
Contents 4
B/LABSYSEVOROBOT-1A –28/09/2012
11. ERROR NO.10.................................................................................................36

12. ERROR NO.11.................................................................................................36
13. WARNING NO.1...............................................................................................36
14. WARNING NO.2...............................................................................................37
15. WARNING NO.3...............................................................................................37
APPENDIX B - ELECTRICAL DIAGRAMS ...........................................................................38
Contents 5
NOTICE TO USERS
The use of this instrument requires scientific and technical competence in order to
comply with all the laws of chemistry and physics. Our product specifications and
applications are liable to change without notices.
SETARAM shall accept liability for any foreseeable injury directly associated
with defects in its instruments, within the limits of the binding provisions of law
applicable to the victim's claim. SETARAM shall not accept liability for
prejudicial consequences associated with experiments conducted using its
instruments. Failure to comply with the advice and recommendations provided in
the putting into service or users manuals shall always constitute a clause for
exclusion of liability, and in particular if the instrument is modified in a way not
specifically approved by SETARAM.
Before putting the instrument into operation, read the instructions carefully and
comply strictly with them in all respects.
The installation and connection of different instruments demand strict compliance

with the instructions and warnings given in their respective manuals.
When using peripheral equipment with our instruments (such as a computer,

thermostat-controlled bath, pump, etc.), refer to the specific users manuals
provided with each peripheral item in order to guarantee correct operation and
adequate safety of these items for our applications.
Once the instrument is correctly installed, the customer shall ensure that the
people who use it have the necessary technical and scientific competence. The
customer shall ensure that the products and gaseous atmospheres employed and
the experimental conditions are not liable to cause damage in the event of
noncompliance with the laws of physics and chemistry. The customer shall also,
under its own personal responsibility, ensure that the instrument and its
connections are not accessible to any working or service personnel who are not
familiar with the rules for the use of the instrument.
Contact SETARAM before using the instrument in any way that does not strictly
correspond to its general specifications.
Notice to Users 7
The use of the instrument at the limits of its operating characteristics (maximum
speed, maximum temperature, etc.) can in the long run lead to the aging of certain
components and consumable parts.
Transport the instrument with care.
Bear in mind that vibrations or impacts can damage the interior of the instrument!
Read the safety labels!
Do not remove any labels!
Do not switch on a damaged instrument.
Disconnect the instrument from the mains power supply before performing
servicing or repair work on it
The operating instructions list other safety recommendations signaled by an

exclamation mark placed within a triangle. Read and follow these
recommendations with care. Failure to comply with these recommendations
can have serious consequences, such as failure of the instrument, material
damage, bodily injury or even death.
Indicates a hot surface.
Indicates an electrical hazard.
Indicates a cold surface.
Indicates a risk of pinching or crushing.
Directive on the discarding of waste electrical and electronic equipment

(WEEE): In the European Union this label indicates that the product must not
be discarded with household waste. It must be discarded in a specialized
waste center for appropriate recycling. Please consult us for further
information on the appropriate recycling of this product in your country.
Notice to Users 8
CHAPTER 1 - PUTTING INTO SERVICE
1. Presentation
Labsys™ Evo Robot consists of a structure incorporating:
• a TG balance associated with the DTA and DSC sensors.

• a metallic resistor furnace.
• an automatic sample changer.
• a multi-task software package controlling the modules and the sample changer.
FIGURE 1 : LABSYS EVO ROBOT
The sample changer comprises:
• A manipulator arm (1 - Figure 1).

• A measuring rod blocking arm.
• A tray for holding the Sample and Reference crucibles (2 - Figure 1).
Putting into service 10

• A protective cover.
™
1.1 Description of the Labsys Evo Robot
The automatic sample changer is designed to function with the different Labsys
Evo rods: TG, TG-DTA and TG-DSC.
TG ROD TG-DSC ROD TG-DTA ROD
It is possible to manage 6 Reference crucibles and 30 Sample crucibles of the

following types:
• TG alumina crucible 440µl

• TG platinum crucible 500 µl
• TG-DSC or TG-DTA alumina crucible 90µl
• TG-DSC or TG-DTA platinum crucible 100µl
• TG-DSC or TG-DTA aluminum crucible 80µl
WARNING The Cp rod is not compatible with the sample changer.

1.1.1 Crucible tray
The crucibles are placed on the tray on the left of the apparatus (2 - Figure 1).
The storage tray is removable; it can accommodate crucibles of different

diameters: the small-volume crucibles for the DTA and DSC rods, and the large-
volume crucibles for the TG rods. It has locations for the Reference crucibles (1 -
Figure 2) and the Sample crucibles (2 - Figure 2), and one location for placing the
crucibles not recognized by the sample changer (3 - Figure 2).

FIGURE 2 : CRUCIBLE TRAY
1.1.2 Measuring rod blocking arm
A blocking arm (1 - Figure 3) with a clip (2 - Figure 3) can be used to immobilize

the rod while the sample changer is manipulating the crucibles, and ensures
excellent reproducibility of positioning of the Sample and Reference crucibles.
It can function with the 2 rod protection half-shells (3 - Figure 3).
FIGURE 3 : MEASURING ROD BLOCKING ARM

1.1.3 Manipulator arm
A manipulator arm (2 - Figure 1) enables the Reference and Sample crucibles to

be placed on the TG-DSC or TG-DTA rod and enables the Sample crucible to be
placed on the TG rod by means of 4 gripping fingers (1 - Figure 4).
FIGURE 4 : MANIPULATOR ARM
The crucible manipulator arm can rotate and move in the direction of the two Y
and Z axes as shown in Figure 5
Raising - Lowering
of Arm Movement of
Gripper
Rotation
of Arm
FIGURE 5 : CRUCIBLE MANIPULATOR ARM
WARNING The manipulator arm does not recognize the size of the manipulated crucible.
Care must therefore be taken not to load a large-volume crucible of the TG type
onto a TG-DTA or TG-DSC rod.

WARNING When using Platinum crucibles with a TG-DSC rod, check carefully before
running the series that the Alumina pellets are present on the rod to prevent
crucibles adhering to it.
1.1.4 Protective cover
A protective cover (1 - Figure 6) is used to protect the sample changer and the
measuring rod during the sample changer's manipulations. This cover must be in
place during each of the sample changer operations.
FIGURE 6 : LABSYS EVO ROBOT WITH PROTECTIVE COVER
A hinged section (2 - Figure 6) opens to give access to the crucible storage tray.
1.1.5 Rod safety and recognition device
An electronic device:
• Manages the raising of the column automatically,

• Recognizes the type of measuring rod - TG, TG-DTA or TG-DSC - in order to
correctly position the crucibles,
WARNING The rod recognition device cannot distinguish the rod temperature range. The
measuring range of the rod must therefore be verified to declare the right type
of apparatus when it is connected.
Remark If the type of rod detected does not correspond to the type of apparatus
connected, the sample changer will not be activated.
• Manages the safety devices associated with the protective cover and automatic
opening of the furnace.
Remark A sensor detects the presence of the protective cover.

Remark Another sensor verifies that the column is in the raised position before
authorizing the sample changer to manipulate the crucibles and position them
on the rod.
Remark Opening the hinged section at the front of the protective cover disables the
movement of the sample changer.
Remark An additional safety device prevents the column from being raised until the
furnace temperature has cooled down sufficiently. This is to prevent the risk of
manipulating crucibles while they are still hot.
2. Installation
The Labsys™ Evo Robot is supplied with:
• The various connection cables for the water and gases

• Two Ethernet cables
• One Ethernet switch
• One mains power cable
• The software
The different sections of the ordered Labsys™ Evo Robot have been
carefully inspected and tested before shipping. Check the conformity of the
delivery with the order.
On reception of the apparatus, carefully check the condition of the different
sections. Make the usual reservations with the carrier if any damage is found.
2.1 Installing the apparatus
Avoid installing the instrument in a room with a floor that transmits vibrations
(floorboards), or where there are drafts, or near machines that cause vibrations.
Level the apparatus on the table by adjusting the height of its legs (see Figure 7).
Adjustable
legs
FIGURE 7 : ADJUSTMENT OF THE LEGS

WARNING To obtain the best performance from the Labsys™ Evo Robot, it is
recommended to install it on a stable table (such as a laboratory table or
suitable surface plate) away from direct sunlight.
2.2 Dimensions
Weight: 68 kgs
TM
FIGURE 8 : DIMENSIONS OF LABSYS EVO
The apparatus must be carried by two people and lifted by placing the hands
on the either side of it under the structure. To do this, remove the metal strip
under the apparatus (cf. Figure 9).
Metal strip
Position
of hands
FIGURE 9 : HANDLING THE APPARATUS

3. Electrical and computer connections
3.1 Electrical connection
Controller Robot
Ethernet Ethernet
Port Port
The mains power cable must be

connected to a grounded 230V / 6A
socket
230 V
mains
FIGURE 10 : ELECTRICAL CONNECTION
3.2 Computer connections
Remark The connection indications for the computer itself are subject to change. The
Labsys Evo apparatus is connected to the PC via a crossover Ethernet cable
(Ref: S06/57046) and the sample changer via a straight-through Ethernet cable
(Ref: S06/57082)
1
Ethernet
switch
3
4 5 6
FIGURE 11 : COMPUTER CONNECTIONS

• Connect the Crossover Ethernet cable (S06/57046) No.1 between the

controller and the Ethernet switch.
• Connect the Straight-through Ethernet cable (S06/57082) No.2 between the
sample changer and the Ethernet switch.
• Connect the Straight-through Ethernet cable (S06/57082) No.3 between the
central processor unit (CPU) and the Ethernet switch.
• Connect the monitor cable between the CPU and the monitor.
• Connect the printer cable between the CPU and the printer.
• Connect the mouse cable.
• Connect the keyboard cable.
• Connect the Ethernet switch power cable No.4.
• Connect the monitor power cable No.5.
• Connect the CPU power cable No.6.
• Connect the printer power cable.
Remark If the PC used with the apparatus does not have 2 network boards, it is possible
to use the Ethernet switch to connect to the internal network. Contact your
network administrator for this.
4. Putting the apparatus into service
The manipulator arm of the sample changer is calibrated in the factory. In the
event of a problem, contact SETARAM Instrumentation After-Sales.
The apparatus is switched on by actuating the switch on the back panel. The green
diode on the front left-hand side of the apparatus should light up.
FIGURE 12 : POWER-ON LIGHT

Raise the furnace by simultaneously actuating the safety switch and the raise-
lower switch on either side of the apparatus (Figure 13).
Raise-
Safety Switch Lower
Switch
FIGURE 13 : SWITCHES FOR RAISING THE FURNACE

5. Technical characteristics
5.1 Labsys™ Evo Robot
• Single-phase mains power supply 230 V ± 10 % 50/60 HZ

• Total input power 820 VA
• Safety equipment Furnace and sample safety temperature
programmable by software.
Water circulation safety device.
Furnace opening safety device: the furnace cannot
be opened when the pressure in the analysis
chamber is less than 680 mbar or when the
temperature is higher than 70°C.
• Gas inlet pressure 3 bars max.
• Water inlet pressure 3 bars max.
• Ambient operating temperature 15°C to 30°C
• Relative humidity Max. 80% for ambient T° up to 31°C, then

decreasing to 50% for T° equal to 40°C.
• Dimensions: LxHxD
Working position 530 x 560 x 580 mm
Raised position 530 x 760 x 580 mm
• Weight 68 kg
• Operating temperature range Ambient to 1400°C (Standard Utilization)
1600°C (Exceptional Utilization)
These values can vary according to the sensors,
crucibles, sweeping gases used. It is therefore vital
to refer to the manual.
• Scanning rate 0.001 to 100°C/min.
Note: the furnace risks aging if used intensively at
scanning rates exceeding 50°C/min.
• Sample volume (according to Alumina crucible: 80, 90 and 440ml
sensor used) Platinum crucible: 80, 100, 380 and 500ml
Aluminum crucible: 80 and 100 ml
WARNING Prolonged utilization of the apparatus above 1400°C accelerates aging of the
furnace. It is recommended to limit the duration of the isothermal holding
periods above 1400°C to 30 minutes. It is recommended to heat at rates
exceeding 2°C/min above 1400°C

5.2 Conformity with standards
• Low Voltage Directive (LVD)

• European Directive 2004/108/CE
• European Directive 2006/95/CE
• EN 61326-1
• EN 61326/A1
• EN 61326/A2
• EN 55022 Class B

CHAPTER 2 - UTILIZATION
Utilization of Labsys™ Evo Robot is no different from the standard Labsys™ Evo.
The measuring rods, their installation, the electronic microbalance and the furnace
are identical in all respects. Refer to Chapter 2 of the Labsys™ Evo manual.
1. Preparing the apparatus
1.1 Positioning the crucibles
• Position the crucible tray on the appliance.

• The tray is positioned by 2 ball and spring plungers (Figure 14) to have
optimum ease and reproducibility of positioning.
Ball and Spring

Plungers
FIGURE 14 : BALL AND SPRING PLUNGER FOR THE POSITIONING OF THE STORAGE TRAY
• Position the Sample and Reference crucibles on the tray. The storage tray can
hold up to 30 Sample crucibles and 6 Reference crucibles. The crucible
locations are numbered from 1 to 30 for the Samples and 1 to 6 for the
References (see Figure 15).
WARNING The manipulator arm does not recognize the size of the manipulated crucible,
therefore care must be taken not to load a large-volume crucible designed for a
TG rod onto a TG-DTA or TG-DSC rod.
Utilization 22
Reference Reject
Crucibles Tray
Sample
Crucibles
11
1 21
FIGURE 15 : STORAGE TRAY
1.2 Positioning the rod
Refer top the Labsys™ Evo manual, Chapter 1, § 5.1.
• Balance the Reference crucible by adding a thermally inert substance (e.g.

alumina) to keep the rod centered in the furnace, whatever the type of Sample
crucible.
1.3 Balancing the balance
Refer to the Labsys™ Evo manual, Chapter 1, § 5.2.
• Balance the balance

• Use a crucible whose weight is representative of all the crucibles to study.
Take into account the potential variation in weight of the sample when
choosing this crucible to avoid being outside the measuring range during an
experiment.
1.4 Installing the protective cover
• Install the protective cover to guarantee risk-free operation of the apparatus.

• Put the cover in place when the furnace is in the closed position.
The protective cover governs the following functions:
• Starting of a series with the acquisition software.

• Starting of the movements of the sample changer.
• Automatic and manual lowering of the telescopic column.
Utilization 23
It is now possible to prepare a series of experiments with the apparatus.
2. Using the Calisto acquisition software
In addition to the standard functions, the Calisto acquisition software integrates

all the functions for operating the sample changer and creating, managing and
processing series of experiments.
2.1 Declaring and connecting the apparatus
2.1.1 Declaring the apparatus and defining the IP address
• Declare the apparatus via the "Declare Apparatus" menu

• In the "Server Bootp" menu, define the IP addresses for the controller and the
sample changer.
To do this:
• Select the address of the sub-network corresponding to the network board

connected to the instrument (1 - Figure 16).
• Insert two IP addresses (2 - Figure 16).
• Click on the "Start" button (3 - Figure 16). The light changes from red to
green.
• Wait for the MAC addresses to appear on the screen to be sure of being able to
connect the apparatus.
• Check the box in the bottom left-hand corner (4 - Figure 16).
• Quit the Bootp Server window by clicking on "Close".
FIGURE 16 : BOOTP SERVER
Utilization 24
2.1.2 Connecting the apparatus
WARNING At power on, it takes about 40 seconds for the Labsys™ Evo Robot to initialise.
It is necessary to wait this duration before trying to connect with CALISTO
• Connect the Labsys™ Evo Robot and choose the type of rod in the "Apparatus
Connection" window of Calisto.
• Use the pull-down arrows (1 - Figure 17) to assign the IP addresses to the right
apparatus.
FIGURE 17 : CONNECTION OF THE LABSYS™ EVO ROBOT
Remark Connect the right type of apparatus according to the measuring rod installed on
the balance. If there is a connection error, a message appears at startup.
Remark Take care to connect the controller and the sample changer to their respective
IPs.
2.2 Utilization with Direct Programming
The Robot Labsys Evo tab defines (Figure 18):
• the version of the embedded software,

• the type of rod used
• the numbers of the crucibles loaded on the rod,
• the status of the sample changer,
• a “Advanced” button for special Robot command,
• the buttons for loading or unloading the Sample and Reference crucibles.
Utilization 25
FIGURE 18 : DIRECT PROGRAMMING TAB
Remark Open the furnace before any direct programming commands. If the furnace is
closed, a warning appears. After opening the furnace, the ongoing command
can be restarted or abandoned.
2.2.1 “Advanced” Button
The “Advanced” Button enables two special Robot command: the “Reset” and the
“Recover Idle Position” commands.
Their commands have to be used exceptionally. Their commands have to be used

if the Robot lost its position after a power supply shutdown or after a critical error.
If after the utilization of their commands, the Robot does not work correctly,
contact the SETARAM Instrumentation After-Sales Service
2.2.1.1 “Reset” Button
The “Reset” button resetting the Robot. This button enables the “Recover Idle
Position” command.
Utilization 26
FIGURE 19 : “RESET” BUTTON
2.2.1.2 “Recover Idle Position” Button
The “Recover Idle Position” button is a command which recover the idle position
automatically. After a main power supply shutdown or a critical error, the Robot
can not recover the idle position. This command permits to recover the idle
position to return on standard utilization.
FIGURE 20 : “RECOVER IDLE POSITION” BUTTON
2.3 Preparing a series of experiments
Calisto integrates all the functions for programming a series of experiments

requiring the use of Labsys™ Evo Robot.
• Create a new series

• Access the Series Creation Assistant by right clicking on the name of the
series.
FIGURE 21 : ACCESSING THE SERIES CREATION ASSISTANT
• Enter of the parameters for the series in the "Series Creation Assistant" table.
Utilization 27
Series Parameters
Series
Treeview
Experiment Parameters
FIGURE 22 : SERIES CREATION ASSISTANT
• Enter general information concerning the series in the upper zone of the
window.
• In the lower zone of the window enter the information relative to each
experiment in the series (name, sample weight, molar mass, reference crucible
number, sample crucible number, type of crucible, procedure, blank, macro).
2.3.1 Series Parameters
This part of the window is used to define (Figure 23):
• the type of rod used.

• the name of the Experiment Series. This can serve as a prefix for the name of
each experiment: check the box "Use series name in experiment's name".
• The generic name of the experiments. This will be the same for all the
experiments in the series. Confirm with the button situated to the right of the
data entry box.
• Specify the number of experiments in the series.
• Press the "Add experiment" button. The name of each experiment is
incremented automatically.
Utilization 28
FIGURE 23 : SERIES CREATION ASSISTANT - UPPER SECTION
2.3.2 Experiment Parameters
• The experiments appear in the table (Figure 24).

• Enter the information specific to each experiment, either directly in the table
or in the boxes in the right-hand section of the window.
• Enter the weight and molar mass expressed in milligrams and milligrams per
mole respectively.
• Indicate the number of the Reference crucible and the Sample crucible and the
type of crucible use for the experiment.
Remark It is possible not to put any crucible - Reference or Sample - on the measuring
rod. In this case, specify crucible No.0.
• It is possible to call up an existing saved procedure. Otherwise the procedure
will be created after creating the series.
• It is possible to define the blank and the macro for each experiment, allowing
subsequent automated processing of the data.
A procedure contains:
• the number and type of phases.

• the temperature profile.
• the signals to record.
• the regulation parameters.
• the end-of-test conditions.
Remark If a saved procedure is modified, its name will be followed by the suffix
"Modified".
• To create or update the Series, press the "Generate Series" or "Update Series"
button if the Series has been modified since its creation.
Utilization 29
FIGURE 24 : SERIES CREATION ASSISTANT - LOWER SECTION
2.3.3 Structure of the Series
The structure of the Series appears directly in the display frame of the Experiment
Programming window. It takes into account the number of experiments and
associated procedures.
FIGURE 25 : SERIES DISPLAY TREE STRUCTURE
The modifications of each experiment can be applied directly in the structure of

the Series. The method of modifying the Series is the same as for modifying an
Experiment.
In the Experiment parameters:
• Define the introduction temperature (it is set to 70°C by default). This

temperature governs the change of crucibles between two experiments. The
Utilization 30
furnace cannot be opened if the temperature exceeds this introduction

temperature.
Remark If the furnace temperature is higher than the introduction temperature at the end
of the experiment, Calisto will not save the signals during cooling of the
apparatus down to the introduction temperature.
WARNING The introduction temperature must always be higher than the water temperature
or the ambient temperature of the room or the last furnace regulation
temperature, because if it is too low it will be impossible to go from one
experiment to another during a series.
2.4 Running a Series
• Press the button and select the Series to run with the pull-down menu.
FIGURE 26 : RUNNING A SERIES
• The sample changer always checks the loading and unloading positions before
loading or unloading a crucible.
• If a crucible is present on a location that is normally vacant, the sample
changer stops and the software asks the user to remove the crucibles from the
locations that must remain vacant.
Remark If the crucible is not present on the storage tray, Calisto proceeds to the next
experiment.
Remark If the crucible is not present on the rod during crucible changes between two
experiments, Calisto displays a user message and pause the series.
• When performing a Series of experiments, the ongoing Experiment or Series
can be placed on pause or stopped.
Experiment Series Emergency
Pause Pause Stop
Experiment Series
Stop Stop
FIGURE 27 : SERIES MANAGEMENT BUTTONS
Utilization 31
2.4.1 Managing the running of a Series
• The "Series Pause" button enables the running of the ongoing Series to be
stopped temporarily. If an experiment is in progress, it will run to term and
then the Series will set to pause.
• The Series can be resumed or stopped. This information is recorded in the
Audit Trail.
• The "Series Stop" button enables running of the ongoing Series to be stopped.
Once the furnace has reached the introduction temperature, the crucibles can
be unloaded. A message will inform the user that the apparatus is "Waiting for
Crucible Unloading".
• The "Emergency Stop" button enables the sample changer to be stopped if
there is a manipulation problem. After returning the apparatus to normal
operating condition, the ongoing manipulation can be resumed or abandoned.
FIGURE 28 : EMERGENCY STOP BUTTON WINDOW
2.4.2 Managing an Experiment
In the same way as for the Series, it is possible to place an ongoing experiment on
pause or stop (Blue Button on Figure 27).
• The "Experiment Pause" button enables the execution of the ongoing

experiment to be interrupted temporarily, by regulating the furnace to the last
setpoint temperature value. The experiment can then be resumed or stopped.
• The "Experiment Stop" button enables execution of the ongoing Experiment to
be stopped. The Series continues and proceeds to the next experiment. The
crucibles will be unloaded once the introduction temperature is reached. A
message "Waiting for Next Experiment" is displayed.
Utilization 32
Labsys Evo - Option Robot - Appendix A
APPENDIX A – ERROR MESSAGES

These error messages are described for the 2.4 firmware version of the sample
changer controller.
1. Acknowledged of error or warning message
When a critical error or warning described below arises, it must be acknowledged

to reuse the sample changer.
• Disconnect the apparatus from Calisto using the apparatus connections

window.
• Close Calisto.
• Switch Off the Labsys™ Evo Robot.
• Switch On the apparatus after waiting a couple of seconds.
• Launch Calisto and connect the apparatus using the apparatus connections
window.
• Contact the SETARAM Instrumentation After-Sales Service if the error
appears another time.
If a critical error or warning appears during a series, the series will be stopped and
the Robot will be frozen on its position when the error or the warning appears.
2. Error No.1
• ERR_CMD_NOT_RECOGNIZED: <string>: The command sent to the
sample changer is not recognized by it (Information detailed in <string>).
This error can appear when there is a communication fault between the sample
changer and Calisto. The connection cable may be incorrectly connected or the
sample changer's CPU board has failed, at least at communication level. It can
also result from an execution fault in Calisto.
This error message only appears when the command sent does not match the
communication protocol between Calisto and the sample changer.
3. Error No.2
• ERR_ILLEGAL_CMD: <string>: The command cannot be executed in the
current sample changer configuration (Detailed information in <string>).
Appendix A 33
sample changer's CPU board has failed, at least at communication level.
This error can only occur:
• when the apparatus is in TG rod version and Calisto wants to load or unload a
Reference crucible, which is not possible with this type of rod
• if Calisto wants to define the type of rod on the sample changer and it is
already running.
• it can also result from an execution fault in Calisto.
4. Error No.3
• ERR_INPUT_PARAMETERS: <string>: The arguments (Reference and/or
Sample Crucible No.) of the order or their numbers are incorrect.
sample changer's CPU board has failed, at least at communication level. It can
also result from an execution fault in Calisto.
This error only appears:
• if the number of arguments is incorrect.

• if the value of the argument is too high with respect to the type of argument to
use (Argument > Max Nbr Sample (30) or Argument > Max Nbr Reference
(6)).
5. Error No.4
• ERR_EEPROM_EMPTY: The EEprom contains no values.
This error can appear at any time during the use of the sample changer. In this case
the sample changer CPU has lost all its parameters therefore it can no longer
function correctly.
6. Error No.5
• ERR_EEPROM_CRC_FAILED: The CRC command has failed because the
data contained in the EEprom are not valid.
This error can appear at any time during the use of the sample changer. In this case
the sample changer CPU has lost all its parameters therefore it can no longer
function correctly.
Appendix A 34
7. Error No.6
• ERR_RUN_ATTEMPT_FAILED:<string>: The command sent cannot be
executed (Detailed information in <string>).
sample changer's CPU board has failed, at least at communication level. This error
can also result come from an execution fault in Calisto.
• if the sample changer is already running and that Calisto try to send a
command.
• if the sample changer is stopped by a critical error and that Calisto try to send
a command.
• If the sensor type is not defined and that Calisto try to send a command.
8. Error No.7
• ERR_SYSTEM_INITIALISATION: <string>: The system cannot initialize
itself (Detailed information in <string>).
This error appears when the sample changer is switched on. The system initializes
itself each time at each powering on and can encounter this type of error if the
CPU is faulty or failed.
9. Error No.8
• ERR_HARDWARE:<string>: Fault or internal failure of the sample changer
(Detailed information in <string>).
• if the main power supply of the sample changer have a default

• if the room temperature is too hot.
• if one of the movement command wires of one of the sample changer arms is
too hot or cut.
WARNING For this last case, wait a couple of minutes before to switch on the apparatus.
10. Error No.9

• ERR_ARM_BLOCKED:<Motor_No.>: The blocking arm or the manipulator
arm has blocked during a movement (0 = Blocking Arm, 1 = Rotation of
Appendix A 35
Manipulator Arm, 2 = Raising/Lowering of Arm, 3 = Forward/Backward

Movement of Clip).
This error appears if an object prevents the movement of one of the motors during
its movement. It can also appear if the sample changer has impacted an object
during a previous manipulation. Indeed, the slightest impact, even if the sample
changer is stopped, can alter the mechanical settings and cause the motors to force
during a movement.
11. Error No.10

• ERR_ARM_ARRESTED:<MotorNumber><String>: Arm arrested in turn
direction while trying to recover from previous arrest (Detailed information in
<string>).
This error appears if an object prevents the movement of one of the motors during
its movement.
WARNING Before to start a new experiment, check that the calibration is still correct.
Make Load and Unload with the Direct Programming Tab on Calisto. If
there is a problem, use the special Robot commands to recover the idle position
(See § 2.2.1). Contact the SETARAM Instrumentation After-Sales Service if
the error remains.
12. Error No.11

• ERR_POSITION_OUT_OF_RANGE:<MotorNumber><String>: The block
arm or manipulator arm is in an out-of-limit position (0 = Blocking Arm, 1 =
Rotation of Manipulator Arm, 2 = Raising/Lowering of Arm, 3 =
Forward/Backward movement of Clip).
This error appears when the sample changer is moving and one of the motors has
gone beyond its normal travel range. This warning indicates a fault or failure of
the end-of-travel sensors of one of the sample changer motors.
13. Warning No.1

• WAR_WATCHDOG_RESET: An internal error obliges the system to reset
itself to 0.
This can occur at any time when using the sample changer. In this case the sample
changer CPU has experienced an execution fault and must reinitialize itself.
Appendix A 36
14. Warning No.2

• WAR_ARM_ARRESTED:<MotorNumber><String>: Arm motion in turn
direction arrested (Detailed information in <string>).
This warning appears if an object prevents the movement of one of the motors
during its movement.
WARNING Before starting a new experiment, check that the calibration is still correct to
avoid any other problems on the apparatus. Make Load and Unload with the
Direct Programming Tab on Calisto. If there is a problem, use the special
Robot commands to recover the idle position (See § 2.2.1). Contact the
SETARAM Instrumentation After-Sales Service if the error appears another
time.
15. Warning No.3

• WAR_HARDWARE:<string>: Internal fault or failure of the sample
changer.
This warning appears when verifying certain components of the sample changer. It
is caused by a fault affecting the end-of-travel sensors or the main power supply of
the sample changer.
Appendix A 37
Labsys Evo - Option Robot - Appendix B
APPENDIX B - ELECTRICAL DIAGRAMS
Appendix B 38
Labsys Evo - Option Robot - Appendix B
Appendix B 39
OUR PRODUCT LINES
DSC131 evo
An-easy-to-use Differential Scanning Calorimeter DSC (-170 to 700 °C)
LABSYS evo
Highly automated thermal analyzers: DTA, DSC, TGA, STA (ambient to 1600 °C)
SETSYS Evolution
High-performance modular thermal analyzers: DTA, DSC, TGA, STA, TMA
(ambient / 2400 °C)
SENSYS evo
An innovative line of Thermal Analyzers (-120 / 830 °C) with Calvet 3D technology:
DSC, High Pressure DSC, Robot DSC, TG - DSC coupling to gas analyzer
PCT
A fully automated Sieverts instrument for measuring gas sorption properties of
materials
96 LINE
Large volume thermal analyzers (ambient / 2100 °C): Calorimeter, DTA, DSC, TGA,
STA, TMA
MicroDSC
High-sensitivity DSC and microcalorimeters (-45 to 120 °C)
Calvet 3D CALORIMETERS
Mixing, reaction and isothermal calorimetry systems (-196 to 1600 °C)
TAG
High performance symmetrical TGA and STA system (ambient / 1750 °
SETARAM INSTRUMENTATION
7 rue de l’Oratoire
69300 Caluire - France
Phone +33(0)4 72 10 25 25
Fax +33(0)4 78 28 63 55
SETARAM Inc.
5880 W. Las Positas Blvd., Suite 50
Pleasanton, CA 94588 - USA
Phone +1 (925) 847 9500
Fax +1 (925) 847 9400
Offices in United Kingdom, SETARAM China

Germany, Italy, Switzerland Rm.201, Building D, Block 7,
No.128 Huayuan Rd,
www.setaram.com Shanghai, 200083 - PR China
Phone +86 21 36368319
sales@setaram.com Fax +86 21 36368094

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B/LABSYSEVOROBOT-1A

TABLE OF REVISIONS .....................................................................................................2

NOTICE TO USERS ..........................................................................................................7

CHAPTER 1 - PUTTING INTO SERVICE .............................................................................10

11. ERROR NO.10.................................................................................................36

The installation and connection of different instruments demand strict compliance

When using peripheral equipment with our instruments (such as a computer,

Transport the instrument with care.

Read the safety labels!

Do not remove any labels!

Do not switch on a damaged instrument.

The operating instructions list other safety recommendations signaled by an

Indicates a hot surface.

Indicates an electrical hazard.

Indicates a cold surface.

Indicates a risk of pinching or crushing.

Directive on the discarding of waste electrical and electronic equipment

CHAPTER 1 - PUTTING INTO SERVICE

Labsys™ Evo Robot consists of a structure incorporating:

• a TG balance associated with the DTA and DSC sensors.

FIGURE 1 : LABSYS EVO ROBOT

The sample changer comprises:

• A manipulator arm (1 - Figure 1).

Putting into service 10

TG ROD TG-DSC ROD TG-DTA ROD

It is possible to manage 6 Reference crucibles and 30 Sample crucibles of the

• TG alumina crucible 440µl

WARNING The Cp rod is not compatible with the sample changer.

The storage tray is removable; it can accommodate crucibles of different

Putting into service 11

FIGURE 2 : CRUCIBLE TRAY

1.1.2 Measuring rod blocking arm

A blocking arm (1 - Figure 3) with a clip (2 - Figure 3) can be used to immobilize

It can function with the 2 rod protection half-shells (3 - Figure 3).

FIGURE 3 : MEASURING ROD BLOCKING ARM

Putting into service 12

1.1.3 Manipulator arm

A manipulator arm (2 - Figure 1) enables the Reference and Sample crucibles to

FIGURE 4 : MANIPULATOR ARM

FIGURE 5 : CRUCIBLE MANIPULATOR ARM

Putting into service 13

FIGURE 6 : LABSYS EVO ROBOT WITH PROTECTIVE COVER

1.1.5 Rod safety and recognition device

• Manages the raising of the column automatically,

Putting into service 14

The Labsys™ Evo Robot is supplied with:

• The various connection cables for the water and gases

2.1 Installing the apparatus

FIGURE 7 : ADJUSTMENT OF THE LEGS

Putting into service 15

FIGURE 9 : HANDLING THE APPARATUS

Putting into service 16

3. Electrical and computer connections

3.1 Electrical connection

The mains power cable must be

FIGURE 10 : ELECTRICAL CONNECTION

3.2 Computer connections

FIGURE 11 : COMPUTER CONNECTIONS