CN108862452A Preparation method of biomass material used for removing heavy metal ions in water

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1.A method for preparing a biomass material for removing heavy metal ions in a water body, comprising: the
following steps:

Step 1: Wash the bayberry, then dry it in an oven, remove the nuclear powder, and obtain the bayberry powder;

Step 2: placing the bayberry powder into an atmosphere furnace for high temperature carbonization;

Step 3: Configuring an activation solution, the activation solution is a 1 mol/L aqueous phosphoric acid solution,
and the arbutus powder is immersed in the activation solution and uniformly mixed to obtain a suspension; the
suspension is placed in a reaction vessel, and the reaction vessel is placed in an oven. Heat treatment inside;

Step 4: The heat-treated suspension is first neutralized with a base, and then the suspension is subjected to
suction filtration washing, followed by washing and drying to obtain a biomass material.

2.The method for preparing a biomass material for removing heavy metal ions in a water body according to
claim 1, wherein the specific method of the high-temperature carbonization treatment is to set the atmosphere
furnace temperature to 800 ° C and the treatment time to 2 h.

3.The method for preparing a biomass material for removing heavy metal ions in a water body according to
claim 1, wherein in the second step, a protective gas is continuously introduced into the atmosphere furnace 10
minutes before the high-temperature carbonization treatment; At the end of the carbonization treatment, the flow
rate of the protective gas was 0.4 L/min.

4.The method for preparing a biomass material for removing heavy metal ions in a water body according to
claim 3, wherein the protective gas is any one of nitrogen gas, argon gas and helium gas.

5.The method for preparing a biomass material for removing heavy metal ions in a water body according to
claim 1, wherein the specific method of mixing uniformly in the third step is mixing and stirring for 5 minutes at
a rotation speed of 200 rad/min.

6.The method for preparing a biomass material for removing heavy metal ions in a water body according to
claim 1, wherein the specific method of heat treatment in the third step is to set the oven temperature to 160-200
° C, and the processing time is 4 -6h.

7.The method for preparing a biomass material for removing heavy metal ions in a water body according to
claim 6, wherein the specific method of neutralizing with a base in the fourth step is to add a 0.1 mol/L KOH
aqueous solution dropwise. Until the pH of the suspension is 7.

8.The method for preparing a biomass material for removing heavy metal ions in a water body according to
claim 7, wherein the specific method of washing in the step 4 is first washing with deionized water and then
washing with anhydrous ethanol. Again.

9.A use of a biomass material, characterized in that the biomass material can be used for sewage treatment.