xperi muns No-1

bautnadiral rom h e
HIM- To ind oud one acidie 4 0nu
vC nosqcvmut Sa.

aderiad 9 Tead lue,C Jdbe Afamd, est tube Kold

bwnn, glass rod.

3o{.
himica)'- dil M,So,, ,
oxalic aud,ulnal Fel?a NabH
mral Fe(a
nocedvra
uliminauy Ted
Colon- whute
Odow- A mmandto
sotid
phdical stal e >
Sodub1lik - 3ouble in M,0
esor acdic vadica.
Obsenvation nounee
Experimnt
Cu,co0 lackaBe)
Sallt & HSO, Colourdes4 vapous
mullin9 k e vinegoun my be presAmd.

which wu probably
vapais o CMCO0H a
evolved

Conkrmador Tut
Vinaqas Smell Cu,(o0 (accdade)
Mixtuw is muxed
wih oxalic azid g rub
wim n0 on he pal m,
produced Conrm
VinAn Smull i3
Ptaluud.
20St rudral fel Rredlish coloun
penr
Divide it indo two pants.
 EXpement No -o1 Blamk Page
Audic Aadi cal
Reachion or dretalt ion
2CH3(00 NH + H2Soy 2 CHs C0OM? + [(NHu)2 S0y
2)Fouc Chloside. tut (Vine ga)
tRed blood colow)
SCHCoONHy Natrad Feds
CCHC0o)3 Fe t NHyd
(CsC00)y Fe +2H20
|(CHstoo) (o),t Fe4 t
2tt(00H
(Reddah 6uoon ppt)
* asic Radital
Reactionopr 2eo gMoup
CH3C6 NHy + NaoH NHs H0
NHs +HC NHc
+ + CH3 C06 Na
2) Nesse's
Xeaent Test (8own pPt)
2k [Hy] + N*3 t3k0H HaN Hab. HI
CNessles Reagert) kI+ 2H20
 hixst pard + dil H Reddish olcun
disappea
CMa Y
CU(od
Cmirm
Second pundt MO Redish brotun
bot
Tes or Bauic Radlical
Enp eu met
Obsetvaion Tntexence
)Salt + dil NodH Ammonica Ammonium may be
Smell obtained
PALent.
Conirmatosuy Test
Bsung glass sod
dipped in Conc Hel Dense white
hea he mouth c tuma Ammonium mabe
test hube Conimed.
(2 Nassede's eagnt
mixed wth Obhain ed
Ammomiom ( NH)
1S Conimed
du Solution.
euk The. givn Salt i CHaC00 NH4
Addic Radical -CsCoo
asic Raclical NH
 tpesi met No 2
AIM- TO find out One. audic s one basic slorolica om he. vtn
inoganic Salt
Matexial Kequived Teut tube , test Jube Stand test tube holdet,
holdew,
buuney
glas Tod spafua
Chemicals- Salt, Conc Sulphuic add,
dil, sulyhwic aid
teSOy dil. Hd, K
HOCeduxe
Pxelimi nas Test-
Colouw wite
Odouw No speiffc. odo u
Physical Stobe- (uystaltine
Test tor Addic Radi cal Solubili y Soluble in wade
Expeiment obsevahion Tntxente
Salt + dilH,Sby No hauottexic Dulde gMup abset
o bs eHvacion
CoSso , No2
Salt 4+ Conc. H2s Rddah Bown Nkdrate (NOg) may be
+ piere. opope
Vapot eVolved
Ond soluhion twaus PAeL entr.
bdbuoh.
(onirmodoy Tut:
Epu ment
Ring tut: Mxtute 0bsetvahion Intetn re
JboiJed with dihUed BsMbwn ung s
fuemed
at the N) Nitrate
water and tiltaved Affen sunction o both
dddingshy pslepaned fexolou iquidk Contt rme
Sulp haré Soluhon conc H2 SOy Js
doded slowly by Hhe side of the
teat tuhef
 Eapeuiment No -02 Blonk Pag2
Acidic Radicol
(4) Pb(NU3)2 4 H$0y PbSou + 2HNO
(2) 4 fark hsto wn gas)
PNO3 t (u
(u(No) + 2No +2 H20
Redlah Bxown ja)
Ring Teut
6FeSot3H2 S+
feSoy
2HN0s 3fe2 Cso) t H20 + 2NO
No +
5H20
fe (No) CHhsSoy
(Bown kig)
*Basical Rodical-
4) PbCNOs)2 + 2H fbd2 +2HNO
whit prt
COntumatouy Test
t2) Pbd +2kI
PbTa v t2kd
(yelow ppt)
Pbd +
kz (T04 Pblr 0 t 2k
yello prt)
 Test tor 8asie Radical
Expes mt
Obseu vahion Tntwente
Salt 4 dil NaOH
Ammo nical Smell
not Obseved
Solt4 uwade ahset
(0.s)+dl
HCI
whit ppt P (Lead mau be
pHLet
(onirmatusy Tut
peumet
Dride whi t ppt
into too pa»ds
fiat past add yellow ppt
kI Soluhon,
Obhained
P Lead)
Conhirme
) Tn Secord past
add k,COu
yellow pp
obtained Pb2 (Lead
Comfirme
Result iven satt i Pb(Nbs)a
aidic Tadicale Nos
Basic ad) ral Pb+2
-
 tpeimert ND 3
AIM To ind ou one
dudic g one basic
Jnosganic. Salt sladical om
Stadical rom tht
the given
ivn
Mat
u steg uoed Test tuhe. test 4be stand,tet tubt halde',
bun e glass tod
Chemical cld Ha SOy ,Conc. Sulphic. add,NaOH MH,OH kz(,0
KyCfeCCMg.NHy
Ptoc edut
Paeliminay Teut
Tolow- Bstown
Odoux- Not speui
Physical state- (xgstalline
Solubiliy - Not Soluble in Wate
Tes tr audic dadtcal
Eapimet Obsevahon Tnterente
Salt+ dil HSO No Chavattuihc DiLude sHoup absent
Observation CO3s*,So ,NO2
2 Salt + Conc. H2 SOu Colode as wth Chloside (C)
punget smell m be. puesent
Conttratuy Tut:
Ezpmt Obsenwchion Ienen te
u) Silvo nitra tat:-
while. ppt Chlouide Cu)
0S+Sivor nitale o btaed which
Solution. et disolveNtd4 Con Tmtd
NHyOH Solution.
i) hxomy! thlouide
Salt + Hnge gas
evolved which
dbHoppes COnC as eoHsuuyh
HSOy NaOH Sbluhiðn
 tapuiment No -03 Blomk Pagej
*Audic Radital
2 Feds +3th s0y 6dH fe2 (Sov)a
(2) NH«d + Ha Pungnt smell)
> NH»d H20
(whi le tum
Comirmatosy Tut
Fecls +k2 ChHomy chlaside dest-
(r209 + Ha
Soy fesou + kaS0y + (z02 d2 tHa0
C02da+ 4Na0H (Red vapoun)
Naz (T04 + 2
( Sod. Chuomate)H20 + 2 Na
Na2 (Oy+ (CHt0od2 Pb Ph(rOy t2CH3(00
*Basic Radical (ead chsomabe)(yellow PPt)Na
(4) Fe Cls +
3NHOH
3AH4+FeCaHD
2 Fe Cow)st 3Hd (Reddah Bvoun Ppt)
fets +SH20
Coriumatouy esh
Fexuc femoqanide
)
fedt 3hCNS (pHusnion blue)
3k t Fe Ccns)s
Fexuc sulphscy anide
blood les
ous) Co
Chuomyl hloide Test
T6 Salt odd kz(v209 and
tfw dloPs o (on c H2Soy
ChHomyl tlouide c Conhirmed
CC02C) Hed
Vapo
ass ed dih gas td Na0H
Soluhion. Pale yellow
(NaaCr0u)
T Salt huhili ed by
CHsCOOH and Pb Dak ellow
add'ed. Ppt trb (>0u)
Tut tur Banic Radical,
Epmet ObseAvahions
To add salt and Teente
NaOH heat mmo nical Smel
not obsetved NH abseat
To Salt add
No pp pme rst soup absent.
dil H
To add salt+ No ppt tprmed Serond gHoup a b s e t ,
dd Hd t HaS
1) 0.S Soluh'on + Red ppt obtaned R mou be p tsent
NHyd and NHyDH
Contiratos Tut
Dissolve. sed ppt
n dil Hd and
cdi vide itine two
pal
ut pat -kylfe (cn
blue Colo Fe3 Confirmed.
Setond
pat-fotassiom hloo d sted tolou
Fe CCNS)3
Roult iven SaltfeCd
Audtc Radi cal C0
Sasic Kadical Fes+
 Epeiment - 09
Aim To ind out he audié and basic sadital trom the given
0ganic Salt.
Matedal Reguined 7Test kube ,tst tbe stdnd tet ube holded , bun t,
lass 9A0d Spatula.
Chemitals- Dil H,Soy , (ond H04-
Bala Hasoy Na OH, NHyd ,NH,0
DiJ Ha, Ka720y
PMbcedwe- Pnelimi nasy,
Test
Colou-white
Odou Odouwdes
Physical stade- Pouwder toom
Solubiliky Soluble in dil H2SOy
Test or Adidte Radrcal-
Epeimnt Obseuuahon Teence
Salt + dil mSoy. AlO Hedthion Dilule fuop abset
2 Salt + Cont HaS0y C0S, so, No2
NO Heauion Conc tup ahst
aud
, , I , Nos,
) Bad2 Soluhon is added white pueipitahe
o the mixtme in P4eonte obtained So may be puesrt
o o Hl or HNOg in a
ass test tube.
Conrmatosy Tut
while ppt diusld PPE insoluble
n HNOg- So Confirmed.
 Test or Bauic Aadicd-
Epu'ment
ObservahHon Inexen ce
ASalt t NoH NadH Ammoca Smell
hot ohs eved 2eto oup absent
OS + dil Hcl No while ppt TS Houp ahs ent
toxmed
Abore olution + No black ppt
HaS ga Tdo med
T Hop aset
0:S Soluhion t NHy lo whtle pet
+NHyOH d oup absnt
foomed
5 0.s + NHud
NHy
heat Has ga OH No PPt V Ap absa
toTmed
6 DS+ NHd +NHyOH
t(NH), COs whie ppt vh
v oupà prsen
fdomed
lrale the soltion
and divide it in
twe
htee pads
irst past -

ka7,04
Second pat (NH)2$0
elkbuw prt 8as Congirned
NO whik prt
4hnd pot - S2
ST2t
abstt
(NH,)2 (204 No whie Pet
Ca absut
Conis matosy Tet
)Potassiom Chxomakt. tut
abore soluhion a
ew
yello ppt
Cta (rou)
dbiops klron Solution
Tame Test
salt + Flame
Meon glass
lame
 -
Rsalt niven Sat Basoy
Acdic Radical So
Basic Radical -
8
: ii
0 S +NHyd+ No pet
NHuDH heat 1Mup up abstrt
for med
Has8as
5) Ds + NH NHOu
Not h e v u0 up ab seT
+ (NH)(Os
t m
9)Salt + Disodium hiC ppt
tn
Hydw og (hosphade Magntaium v 10up
No O Ammohi um PMoent
Phasphate
COmair matusuy Tat
mmcnium hosphak, Tut
Os Soid Nd NHuOH
whie pet Mt
hiu
m morium smel obstrutd (onbim d
d.+ mmontum
'hcy haCaintsolahion
side a he oub test
as od. tubt

niven SaltMaCo,
AGRadital (oa
asic adiralal- H+
 Date

Expt. No. ,
(olowe o - eporr rr Page No.

Cx PE RIM ENT No,6

EPUAT IO AIM To p3t0pax Sal Solwion

1MTCAL
Qvhmonium SulDhak 250ml ol
Wakk Ui is Calculake molasit

2 (o) 2 (NI
N
kMnOy SAuh
O1-6H20t o]
OuN
+13 Ha O Appa unn,Weighd 6ox
chencal
Molwwmtiic

omotia
2KMnOu Chownical flak
wadch las le
K2 SO + 2m SD4 tez(CO),
0 (NH2S Oy ol'sUaol waler,
CHENICALS = Moh sall
dil. H2 SOy n R o n K Mn OySol
e

M seo paratoa Sal Mo Sal Eecoy (NH4) SO

F
as mo lecula Ma 392ame i i e
' O
e t Mn pouima Stondad
3 92 G2Caue
fe2t F 39 tacto is L

e.wt Mwi
=1
2O
250392

The oy oags lwnpemag@nale is astuorg

xid ho huosemte sulphwic

Teacher's Signature
 Date
Expt. No.. 6
Page No. S
O6sesyationg

Vat
irhial wosk iral ooo 2 K MnOy
S . N o N ,9 F A S
Ss ip1) 6usMe
04 bHe M n Ou 3Hztoy K Soy 2 Mu Soy 3 He O
cOm Ued o e
96 9.6 23ttmaiou M o haT
20 Sal Ox ld e sorouy Sa
Sa Qudic
3I 5
me m
20m 6

2te SOq t 3 H S o [o1 ,(SOt O

3 6 8.6
2O m
kM Oy Htuaion MO y terna in diCaho
5 ml
el inolicad
onco d adRonolivg is 9 The
binkish Haa w h The dop
o
s

W4. o

Vo' o's ppen pasasl 2 Scm

Molai obrSa Sol O.O5
Tndicoto k Ou s oel
dicoo,
2

Vaf 1'ok
9
2 0w Enol oi - Colouslay mavet b'nk
Colou

Poocedu
s0pa Z50 m 9 m/20 m os SaUF
soluhom sy du'ssYolulg Mohs'g_
Sat o lukion pod_pih u
mor' sol Souton 4 Pihette
2 0. 0 m in aUaahud HtatH0n
Ouwtte the
KHu Ou Solutio
Teacher's Signature.
 Date
xpt. No. 6
Page No.

alculationt

ocia N) loho
es(2O Suphuwuc

o (neily Slu) ton i Raion Ptosk

19.5vm No le ho ntia
Volum k4 O
Cll 20m
in uo

Mo h Nous ado kM Oy 3outio

MV,N Va mhasuted
hinR colow is
MKMnO VKMdy o So lutOn in
TO 2mo le kvOy flak0n adol tion Jot
MOkr's Slt VMeh's KHn Oy SolutioM
Sal
N (9. 5
Nole he
.5
Ropeat tho obo gp -5 r)t9a
O0 wolA

k M Oy

Mol as Mola Ma-> 0.0 /5R

The moloou ty KHv Oy o i
.Ou 9// Stngth is
 EXpt. No
Page N0.

nemmiCa l eqtafiong
CXpesimen N o -
Molela
A 2An SOy H20 Atm To Das M/O Ox al'C a co
K2 SO
5( Solution
H? SOu 250 nd
Soluton
60 2co 3 x 5
(00.2120 o
batus adh qlosj analti ca a an
ihd_box 2do ma a ke as od,
KMO 2 H2 y 250
CO OH measuSng las k
(HEMTCALS - xal' acdo C9Sa' Omnd d's a
wale

cO2 5 PREPERA TION Mole a

OX all
Ho
2 M2
2 Mr Oy +6 T 4 5 (z04 CoO H_
Heme
au ol
OXalc ac 9 ueo 126-
ing 250m O.1M S lwlona
OKalic a id Osta'
26s 250 O
OOO

3.1501

Teachers Signature.
 N t , No.
Pge N . 8

heo Potoni
20)enlo

peeai Vo 1 2 KMvM Oq
a t 3H2 SOy KaSo1t2Mn SoY 3 6 t 0
inifi.alLendi Solul on
Ne
Voltp

6reco)
50]
Cam Jse yed
(P ) C
09stimakon oxa0i
m Ox idi zes Oxa ljc ao
2 . 5
2 Om

2 6 m CooH H26
2C 6
2 0v cooH
2 5 marcotor
(.5m 7.6m T kMnOq 2a Hon. Mo x 3nal
2 0
is 9e09 9ao_o ge ino'cato.
0intis
25 m
Ange i h he ot 3inae
on ro drcjua
KMuO Soln.
Indcahion KMn Oy e in ol'catos
point Colourle to e monut hik
Colow

Weah n 2609 Oxalic Ociol Csta's_

di'ssou than ak to paepa 2 s0 m
OX aluc Soluttou 2 5v
To
flak Rintt ia Ho w h
he Qx alc aud Solutton i h a d oud
Teacher's Signature
 Date
lExpt. No.
Page No. 9

MO 2 O n
A)Mo(2ie y 1 Uahoo 0ion flask
MV M2 V
Mn Oy inse (uslte
Mo la kMn O Solullon
Veume kM Oy
Ove est ube (~2om) fu otlwle
Molasu
V2 Votun 8x alic
Selhunic atio N) 9o Soluon in
ralion ftak

OuseH e
Maie a Voxabck
aNole heiwltal

(S)Heat ho tak to 6 0 7 0C Goloadolkto

Soluto o Swote
pes m amo ihtink Colout3 impautecd
O. 32 M Soluton he aton l 3R
tA OvM
KMnOu
adoluHon
SolutHon.
lo 8inqla dos
Mola
he tnal
O.32 126
61Nole he owote

0.32,/R Ropeat he Qbou 8te y-5 Rme

Con codont_eo 9Aeaolias
Result
Sol. s
The Mola
O 32 M sa k Oy

Teacher's Signature