ya Chic ililThelivil lil ha no G.C.1-5 Limiting Reagent Study 37 G.C. 1-5: LABORATORY REPORT brarde Date!O~0 3-22 Name lexuil Lab partners’ names: Cage ror, TA’s Name: Sae7in@ YOU MUST SHOW ALL YOUR CALCULATIONS TO RECEIVE CREDIT FOR THEM! Proper use of significant figures and units is part of the grading, Part I | ‘Testtube | Testtube | Testtube Test-tube Forcoc, | a | a | 46 Concentration | OID A Volume delivered (mt 2,00 mt_| 2,00) | 4,00 ro). | 6 400 mat. | FO mi |10,00 pi. [ Motes of CoC 9810" ot [40 tas io.) Testtube | Testtube | Testtube | Test-tube Test-tube For Na,COs al a 8 4 46 Concentration — | 0,10 M Volume delivered (mL) 12.20 mot |U1.00 mb [4.00 mi. |7.60 mb |S Come | 1:2 «102/11 13s) 48 10" ter Zs x10 Soe 10" Testtube | Testtube | Testtube | Testtube | Test-tube 2 ® C as #6 patel Posie eta eee 4 #6 _| Moles of NasCO, | Volume Measurements [ise otreinn | = |= tate formed (em) _| Iden ERs. Fan, | 78S em |8O0e, S25 c, Color of supema- | [fanigudorencs | Clear | Clear | Clear | Clear | Clear [Ctean | | Cotor of precipitate letigntty Hace (Ta | Water, cacregPeirite ee ay [en lacie |” Nae | eI, in Cary ont caleaatons for our dt ely38. G.C. 1-5 Limiting Reagent Study sent: This section can be completed while waiting forthe pres pitate to settle 1 Test-tube | Test-tube Testtube | Testtube | Testtube | 2 oy 45 #6 Excess Co™ or 2- on CO?” present? | C05, Weiter | Co | Moles of Co® in 4 a _ — | w& e = | : 2a} Motes of €0;"in i [sao | = excess pa a em) Theoretical yield vel olaeew leew of COCO, (moles) aoe tes [60 teal aoe te IEP ial Part Il: Verification of Limiting Reagent | Wesabe Tee | Toctabe | Teste of precipitate a “4 as #6 formation | | | Reaction of super Pik raanitigaidwin |YR | MR | WR | WR | WR NaPO, | Reaction of super: te [vhrte [unite [white |v | ye “re te (rt fee | 909299992900 0°°0000020000000 eee—E—EK—————————— flexanse, Grante| IGICLILS ; f 7 ee @ Calevlations fr > Test tbbe. 2.00 mb dolla, te) | O10 Md doe ~ 2.0 xc Mrol Colle 1000 mL. te > Tekh te HZ 3.00 mb Colle WU. Ola M Galle = 210 x 'o mol UuCle "o00rt 1G >Tesk tube H3 4.00 nb lly» 61M bodily = Ox tol mol Colle ote ie e Jot tube #4 1.00 mb Colla 1 ot M table, ~ B.0 x tomo! Colle 1000 mL te 7 Teck tube HE P56 wb Coll, | ib |) Ot Lace =| 45 'x| 10 fmol Colle 108 aL 1 yTest tube 4G 1.0m Colle. AL» OM loll = Lxto 1000 mit,Alevander Grande 6.L.| I> Ih @ aie > Test be #1 + 13.00 mb, MaglO3, LL | O.)0 M Wald; =| 123 x 10 MyM Oz 1909 prt! We > Tesh tube #2 43 12.00 mt NadlO, | Ie|_ |. 0.10 MMa, 60, ~ | 2% 107 MyMa,lOz 1000 rt Iu > Test’ bbe 43. Hipo mk Majo, IL | | G10 A Mal > |b xt Pol Ma Dae Ie 7 Test tube 4 ONO | Meg hE, L000 gL Muy Oy WU |, O1O|M Ang L0; 4 4,0» 10° mol Meaz Lz lene Iu oe 7 Test tube! 5" 7-50 mL MalO;, Ie 0.10 MMe L0) + 7.51 x tol) Na CO; 12 my, ri 7 Jest whe we 5.00 ml. Ma, L0,, 1b |, O10 M AapLOz ~ 5.0 x lott dl Az LO; [aod mt re| Ee Klevander Grande GL. 1-5 13 x 10 >ymol Ma60, | — 2.0% 10 Tol COClz = Il x 16 * pol LO, > Tesh tbe U2 “4 zt 2 ato Lal NazlOs — 3-0 x 107" mol Col, = 4:0 ¥ 10 mw! CO; > Test tube #3 34 = Lx 107? mol Ma, C0; — 4.0 x10 ImolGeCle = 7-0 xo" vol COs > Test tube we 4.0 ¢ oO pol Ma, O0, — 6.0% 10 mul LLI,= 3-0 x10 mol 60,2- > Test tebe HS 7.5 x 107" pro] Maz COs - 2-5 # IO mol e.l, 2 O Mo les_of Co in excess > Test tube HO @ Ox 1? pol CoCly = £0 x ome] Ma,C0, = £0 «16 lS 3—————————— Mexunder Grupde 6.0. 1-S > Test tube 4 210] wlid=4 adi Koll x |Imol 4.005, |-| 2.O« 10 ~T mal CoCOp Imol Coll, > Tesh by 30 © 107% mol lolly x Imol Ce6O3 ~ 20% 107 rol CLO3 Trl Co Cle. > Test bbe #3 40 ¥to mol Collex Imel dolOz ~ YO x10 mol CoCO3 ] mol Co Clo ? Test bebe BY > Test Whe BS 6.0 x Wi mol Colle ¥ Jee! cotta 2 0x 10% mol Colle mol Codi 4 7S x lOTt mol Colle x Jmol ColOg + 75% 10 mol Colle Vol Co Ely 7 Test tube Ho 6.0 x10 mol Colle x tae Labo, 25.0 < 0 mol CoCle riot Lo CleSP ETRTAEETEEEEENEN TENSEI errr eeerey ere eevee errr Alepander Garde | eo I-6 As the theoreh'cal yield of the CoLO3 fercipt tobe sé $d us| Pho pedudured| bled) Ak bC| the] jpretaie'Hede. | This| was true as observed sn Hest tubes I-Syhowever, fest tube an anomaly, Tat tube @ theoritical yreld decreqged where ab Me hevpnt of the jareciprtale increased, Tre cour Of tHe Preapriate daveened for $4 IF However wus Pink for TT Sard by 2. When a precipbate 1 Formedltsame of the suferrmale weud ard te solution contaniniy barium ions from (Balle) thet We vere able beverly that the carbonate fons were *n exe and the cobaltion Vas the reagent This was witnes sat fA besh tes IM in which a WAL be percrcimate ors hvmred, Howerer teat tye € had a reaction of sumone gut wth Ma3fOy in whith Zw bnessed acolo change te Pink, This verhat that cobalt fons wenn excess and the gobalt ions wereererm vas the loath ag regen he anomaly was besk bbe S mith no rete lion- 4. Colle cagy + WazrlOz tag) > COCOz 13) + 2 NaCl tag) 4, @ Using tne 'salanced epuahdr mine Shi daovete c YeCuuhon \6 used, “Me wolac fakin has an effec Me moles of Ine produc are Cartulated 46 ace ore Clathanks, Ine Celarenswmiv 1s vs-d te Berrenne iL ang 6F tne Cachan bas lnibed Guar, if so knen cd inot possiole +o Pr9OLLE \ne PrPAcr. ME tompovad wit the \ Cast Gwe WMOleS 1S Ae lenihng Ceageah Ballz + KID, —= Galt 2cl7 + K+ Wy” Gallae 2KI0, — Ba (10,), + 2ICCIG.C. 1-5 Limiting Reagent Study 39 G.C. 1-5: DISCUSSION QUESTIONS 1. Compare the theoretical yield of the CoCO, precipitate expected with the heights/volum: What would explain any anomalies you may find? Did any of Were your predictions for which ion was in ex verified by Part Il of the experiment? Expl 4, What reagent would you predict to be in excess for reacting 50 mL of a0.10 M BaC\, solution wit 50 ml. of }0 M KIO, solution? Explain, Hint: Balance the equation first, SHOW YOUR WORK BELOW:Mexancder bande 4b I-% My, 60 my KIO, « bs omrolk = ViTE mmo\ Ks \e qi Grae ale Orie mrel 5 0:1 manor Balle ve ( Wolo l 4, (iz) lentess |. Cro LuncihingAlexander Grande GC. [-5 Limiting Reagent Stuly 10-02 [Purpose] Stoichiomelry is neeled te verrby theed there will be the correct amount of products and reachens. Tt 1s alse ved to correctly balance the eation before it 1S done Combining Cobalt Carbonate Chloride and Sodiver Carbonale will rescit in a insolvable solid, Coballarbonute Predicting the me lar rakio, molarity and volume, meles of selvbion Used, and moles ef formed prodvet are possible if you Use Stoicromely and the formula. Before perfor ing an exprivet of mixing cobalt chloride and Sediver Carbenat€ jn six ditkeentvolumes, Caleviating the amovat of cobalt carbonate ghould be clone. Waste manage mend Soapy water used 40 clean pipet con be washed in the sink. Pipets afler vee are to be thrown away in proper bin. Chemicals after reaction go into nazardovs vaste in Fume hood « Part | — collect Jehvbby test thes and dpipeb = one porter gels Cobalt Chloride and one Sedivm Carbona — Llean a 25OmL Erlenmeyer Flask ancl your Stock Soluhion — Uean pipet and babe | = Finge fifet with needed Solution — Aiseald ¢inse solvtion into waste beaterAlexander Grarde 6.C, 1-8" — Fill piety Laged off of table z — Soul test FU wu nparelii'lon and mix by thverting ~ Allow zo min For preciprkte fo selttle —\werk on distession qvestors ih the meantime — reasupe height of solid (reciprtate = record observation ~ data anys's will le completed here = Calevlate molec of lllz and Ma,COz = fediet Which reagent is | \n_extess - Ce colalt eX. Lge — lalevlate excess CO,” ~ pet Hleorebical yrela of LoCO; Cart ul “lable well ofa 24 vell plate = extract supetnaten} Wquicl Fro bes+ fobe HY) ~ Ada some liquid 40 velle From | pipet land2 Seg or ercess, Co° 7 ~resrfor exces (6.7 at yereat Leetify ig ih my ow work aml vabrstoed tat Te) an Gaunl be iaVidlabion! of hig core, T vill Me subject to He. highest perry Y sea V7