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Rochester Institute of Technology

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Theses Thesis/Dissertation Collections

5-1-1985

A study of the effect of ink viscosity on dot gain in


offset lithography
David Dailey

Follow this and additional works at: http://scholarworks.rit.edu/theses

Recommended Citation
Dailey, David, "A study of the effect of ink viscosity on dot gain in offset lithography" (1985). Thesis. Rochester Institute of
Technology. Accessed from

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A STUDY OF THE EFFECT OF INK VISCOSITY ON
DOT GAIN IN OFFSET LITHOGRAPHY

by

DAVID GORDON DAI LEY

A thesis submitted in partial fullfillment of the


requirements for the degree of Master of Science in the
School of Printing in the College of Graphic Arts and Photography
of the Rochester Institute of Technology

May 1985

Thesis Advisors: Dr. Julius Silver


Chester Daniels
I, DAVID GORDON DAILEY, prefer to be contacted each time a request

for reproduction is made. I can be reached at the following address.

910 Gail Avenue


Neenah, WI 54956

/XS"

2/
DATE:
+
ACKNOWLEDGEMENTS

I would like to thank the following for their time, help and

patience:

Mr. Chet Daniels of the Technical and Education Center of the

Graphic Arts and Dr. Julius Silver for technical advice and help in

experimental planning; Mr. William Eisner of the Technical and

Education Center of the Graphic Arts and Mr. Lloyd Swisher of Ron

Ink Company for donation of materials; Mrs. Anne Vogt for typing;

and the Graphic Arts Technical Foundation for assistance during my

studies.

11
TABLE OF CONTENTS

LIST OF TABLES v

LIST OF FIGURES vi

ABSTRACT 1

CHAPTER I
INTRODUCTION 1
PURPOSE 1
BACKGROUND 1
DOT GAIN 1
INK PROPERTIES 7
FOOTNOTES 10

CHAPTER II
STATEMENT OF PROBLEM 12
FOOTNOTES 14

CHAPTER III
LITERATURE REVIEW 15
FOOTNOTES 17

CHAPTER IV
HYPOTHESIS 18

CHAPTER V
METHODOLOGY 19
FOOTNOTES 23

CHAPTER VI
MEANS REQUIRED 24

CHAPTER VII
ANALYSIS OF DATA 25
FOOTNOTES 54

CHAPTER VIII
CONCLUSIONS AND OBSERVATIONS 55

CHAPTER IX
RECOMMENDATIONS FOR FURTHER INVESTIGATION 57

BIBLIOGRAPHY 59

APPENDIX A
DEFINITION OF TERMS 61

m
APPENDIX B
DERIVATION OF MURRAY-DAVIES EQUATION 63

APPENDIX C
INSTRUMENTATION 64

APPENDIX D
PRESS RUN DOCUMENTATION 66

APPENDIX E
YATES TABLE FOR EXPERIMENT 67

APPENDIX F
SUMMARY TABLES OF EXPERIMENT 75

APPENDIX G
TACK VALUES AND RELATION TO VISCOSITY 84

APPENDIX H
TEST FORM FOR EXPERIMENT 85

IV
LIST OF TABLES

Table 1 Correlation of Percent Solvent Ink


and Viscosity

Table 2 Smoothness Values of Papers

Table 3 Porosity of Papers

Table 4 Density of K & N Oil on Papers

Table 5 Absorptivity of Papers

Table 6 Area of Slur Targets of Plates

Table 7 Density of Patches and Ink Viscosity

Table 8 Density of Patches and Paper Absorbency

Table 9 Density of Patches and Ink Level

Table 10 Density of Patches and Screen Ruling

Table 11 Density of Patches at Different Ink/Paper Combinations

Table 12 ANOVA Summary Table for Solid Patch

Table 13 ANOVA Summary Table for Fill-in

Table 14 ANOVA Summary Table for Slur

Table 15 ANOVA Summary Table for Total Dot Gain

Table 16 Duncan Test of Viscosity and Solid

Table 17 Duncan Test of Viscosity and Percent Fill-in

Table 18 Duncan Test of Viscosity and Percent Slur

Table 19 Duncan Test of Viscosity and Percent Total Dot Gain


LIST OF FIGURES

Figure 1 . Enlarged dots showing the effects of


a) no dot gain, b) fill-in only, c) slur around

cylinder, d) side
slur, e) doubling,
f) slur and fill-in 2

Figure 2 . Equal diameter gain 3

Figure 3. Typical dot gain curve for offset printing 3

Figure 4. How a spot of incident light spreads to a patch of

appreciable size before emerging from the paper 4

Figure 5. Absorption of light on entering and emerging


from paper 5

Figure 6. Effect of tack reducer on dot gain 15

Figure 7 . RIT Symmetrical Test Scale 19

Figure 8. Adjusted Density/Dot Gain vs. Ink Viscosity 31

Figure 9. Adjusted Density/Dot Gain vs. Paper Absorbency 32

Figure 10. Adjusted Density/Dot Gain vs. Ink Level 33

Figure 11. Adjusted Density/Dot Gain vs. Screen Ruling 34

Figure 12. Dot Gain for 25 Percent Patch of 100 Line Screen
at Different Ink/Paper Combinations 35

Figure 13. Dot Gain of 25 Percent Patch of 150 Line Screen at

Different Ink/Paper Combinations 36

Figure 14. Percent Dot Gain at 50 Percent Square Dot Target of

100 Line Screen at Different Ink/Paper


Combinations 37

Figure 15. Percent Dot Gain for 50 Percent Square Dot Target of

150 Line Screen at Different Ink/Paper


Combinations 38

Figure 16. Percent Dot Gain at 75 Percent Patch of 100 Line


Screen at Different Ink/Paper Combinations 39

vi
Figure 17. Percent Dot Gain at 75 Percent Patch of 150 Line
Screen at Different Ink/Paper Combinations 40

Figure 18. Adjusted Density/Dot Gain for Different Papers at

High Ink Levels 41

Figure 19- Adjusted Density/Dot Gain for Different Patches for


Papers at Low Ink Levels 42

Figure 20. Adjusted Density/Dot Gain Differences for Uncoated


Paper at Different Ink Levels 43

Figure 21 . Adjusted Density/Dot Gain Differences for Coated


Paper at Different Ink Levels 44

Figure 22 . Standard Order for Experiment 46

VII
ABSTRACT

Dot gain is the enlargement which takes place in a dot from the time

the dot is captured or generated on the film until it is printed. Dot gain

can cause many problems, including color variation and loss of contrast,

and if uncontrolled is one of the main contributors to waste in offset

lithography. Of the many factors influencing dot gain, inks have been

found to be a major contributor. One property recommended for further

investigation is ink viscosity, which is the resistance to flow of an ink.

The purpose of this study was to investigate the effect of ink

viscosity on dot gain in offset lithography. It was found that as ink

viscosity increases, dot gain will decrease, and if ink viscosity is

optimized, dot gain will be optimized. Experimentation was done on a

single color, single impression sheet-fed lithographic press, with five

inks of different viscosities.

Results of this experiment show that ink viscosity is significant in

affecting the amount of dot gain that occurs. Inks with 15 and 20 percent

solvent added, which were less than 1000 poise viscosity, were found cause

the significant difference. Other factors found to be significant were

screen ruling and paper absorbency. The Yates Method of Analysis of

Variance and graphing were used to analyze the data.


CHAPTER I

INTRODUCTION

Purpose

The purpose of this research is to study the effect of ink viscosity

on dot gain in offset lithography. Interest in this topic began after

talking to several people in the quality control department of a large

printing company, and after doing preliminary reading on dot gain. Several

authors stated that inks are one of the main contributors to dot gain and

that one property which should be studied for its effect on dot gain is ink

viscosity.

Background

Dot gain is the enlargement which takes place in the area of a

printed dot during the transfer stages from film to printed sheets, usually

expressed as the percentage increase in printed area relative to film dot

1 ' 2
'

area. For example, if a dot that is a 50 percent dot on film prints as

a 65 percent dot on paper, the dot gain that has occurred is 15 percent.

It is often referred to, when calculated from density measurements, as

apparent dot gain. This is because the calculated values are somewhat

greater than the actual geometric area of the dot, because of light

3
diffusion within the paper.

Change in dot size is inherent to every printing process, and if

controlled, is not bad. However, it is assumed by various authorities that

uncontrolled dot gain is to blame for much of the waste in offset

lithography. When printing black-and-white halftones, dot gain can change

picture contrast and cause a loss of definition and detail.


In four color process printing, dot gain can lead to similar loss of

contrast and depth, plug up the screens, and cause color changes. Color

variation is one of the largest problems in offset lithography, and is a

4
large contributor to the high waste factor in web offset publication.

There are two kinds of dot gain, physical and optical. Physical dot

gain is an enlargement of mechanical dot size. It can occur between film

generations, during the platemaking process, or during printing if there

are changes in ink and paper characteristics or in other printing

conditions. Physical dot gain may be circumferential -


uniform all around

the dot -
or it may be irregular due to printing defects such as slurring

(directional dot increase), doubling (double images of dots out of register

5,6
with each other), or fill-in (radial increase in the size of the dot).

( Figure 1 ) .

A BO

.
?" ^

__gl
^^k >

M
\ m
'
.^M

\^^Hi
W
^^/

D 2 F

Figure 1 . Enlarged dots showing the effects of

a) no dot gain, b) fill-in only,

c) slur around cylinder, d) slide slur,

'
e) doubling, f) fill-in and slur.
Dot gain is believed to be composed of varying proportions of slur

and fill-in. Optical dot gain is present whenever ink is placed on paper,

because when light illuminates and penetrates a printed paper surface, some

of the light is trapped in the paper and lost, some passes through the

particles in the paper, and some gets trapped under the printed dots.

Optical dot gain usually causes a uniform expansion of the diameter in dots

of different sizes, changing the diameter of the dots by the same amount in

highlight, middletone, or shadow dots. However, the area around the dot

9
will increase more when there is a greater circumference around the dot.

( Figure 2. )

&-

10
Figure 2. Equal diameter gain

Therefore, the greatest dot gain occurs in the middletones, around

the 50 percent dot


size.11

(Figure 3.) This is because as the dots get

bigger than 50 the area for the dots to grow gets smaller, and the
percent,

12
gain the dots experience begins to overlap.

0 25 50 75 100
Halftone Dot Area
13
Figure 3. Typical dot gain curve for offset printing
According to Yule and Nielsen, measurements show that light does not

emerge from the paper at exactly the spot where it entered, so that some of

the light which enters through a dot emerges through white paper. This

increases the density of the middletones, and multiple internal reflections

from the paper increase it still more. For example, a 50 percent tint

printed on a perfectly white paper covers exactly 50 percent of the paper

area. The paper should absorb less than 50 percent of the light that reaches

it, since the ink is not perfectly black. However, if measured by optical

1 5
densitometry, it usually absorbs more than 50 percent. While some feel that

this is caused by penetration of ink vehicles into the paper between the dots,

Yule feels that it is more likely that the penetration of light into the paper

may be the chief reason. (Figure 4.)

M/Kw^

>

Paper
Ma/VntNAA/

Figure 4. How a spot of incident light spreads to a patch

17
of appreciable size before emerging from the paper
Since some of the light is diffused by the paper, it is likely to

spread sideways to the same extent that it penetrates through. Therefore,

some of the light which enters a halftone pattern through a space tries to

1 P>
come out through a dot, and is absorbed instead of reflected. If a 50

percent checkerboard pattern is printed, 50 percent of the incident light

will strike the black dots and be absorbed, and the remaining 50 percent

will be diffused by the paper and lose its dot structure. However, in

extreme cases, half will be absorbed on the way out, resulting in only 25

1 9
percent of the original light escaping from the paper. (Figure 5.)

50?. Absorbed on Entering Paper

" \\"
,
\\X\
Half of Remainder Absorbed on Leaving Paper

A 4 A A A A

-nxxrr
i
Total Absorption 75$
Reflectance 25$

20
Figure 5. Absorption of light on entering and emerging from paper
Dot gain should be measured with a densitometer because the human

eye is not accurate enough. When measuring the dot area of a printed

reproduction, the optical dot area is the total amount of light absorbed

by the halftone pattern printed on a substrate, expressed as the

percentage of the substrate that would have to be covered with halftone

dots to achieve a certain density, provided there was no dot spread and

21
the substrate reflected 100 percent of the light on the surface.

Measurements are based on the premise that if a solid area of ink

absorbs a fraction of the incident light (A ), then the halftone area


s

will absorb a fraction of that (A ) which depends on the area of the

dot. Thus, ' the area of the dot (a) is: A, 22


a = t.

A
s

On prints it is more convenient to measure density rather than

absorption, which makes the equation more complex. Since absorption is

equal to 1 -
1 ,
where D is density, the equation then becomes

io-Dt

1 -

a =

-Ds This equation is known as the Murray-Davies equation.


s -
10

For example, a solid patch (100 percent area) could be measured,

and the densitometer calibrated. Then a tint of, for example, 25 percent

dot could be measured. The density could then be converted to dot


area,

and the percent dot gain found by subtracting the desired dot area
area,

from the dot area found from the print. The optical dot area
(25 percent)

is calculated using the Murray-Davies equation, which is

1
Rt
" 10-Dt

a = 1 -

10"DS

1 -
R = 1 -

s
where a is dot area R. is the reflectance of the halftone tint, R
t s

is the reflectance of the printed D is the the


solid, density of

halftone tint, and D is the density of the solid. It is derived in

Appendix B.

To calculate the physical dot area, the "n"


factor, which takes

into account the effect of paper on light scattering, is used as a

denominator for reflectance and density. This is the Yule-Nielson

equation, and is expressed as: _, ,

10"Dt/n

1 - R .
1 -

a = t/n

10"Ds/n

1 -
R ,
_
1 -

s/n

There are several contributors to dot gain, including ink properties,

blanket type, packing, paper, screen ruling, solid ink denisty, and ink

film thickness. Since the purpose of this paper is to study the effect of

ink viscosity on dot gain, ink viscosity and its relationship to other ink

rheological properties will be explained.

Ink Properties

Ink viscosity is its resistance to flow. An ink with a high

viscosity has a greater resistance to flow than an ink with a low

viscosity. Most sheetfed lithographic inks have a high viscosity.

Viscosity is important because if it is too low, the ink will be poorly

distributed on the inking system. An ink with a viscosity which is too

high can cause poor printing of solids, ink piling on the rollers, tinting,

ink fly, and paper picking.


-X4

One type of viscometer is the Brookfield

Rotational Viscometer. The Brookfield measures viscosity by measuring the

force applied to a spindle which is connected to a spring. The spring

rotates a pointer that is connected to a dial. The spindle is allowed to


rotate for three minutes, and the inks'
viscosity in centipoise is

calculated, using a table based on the size of the spindle and the

revolutions per minute used when measuring the viscosity.

Another important ink property is tack. Tack is the "stickiness", or

force required to split an ink film. If tack is too high, it can cause

paper picking, sticking of the paper to the blanket, curling of lightweight

sheets, and ink distribution problems on the press. If the tack is too

low, it can create piling of the ink on the rollers, tinting, and ink
fly.25

However, tack alone does not control or define ink flow. Two inks may have

the same tack, but their flow or mobility can be completely different

Pfo
depending on their viscosity characteristics. According to various

authorities in the field, tack is a function of viscosity, and for

practical purposes, tack and viscosity will go in parallel directions, and

high and low viscosities are normally accompanied by high and low tack

'
'
values respectively. Also, as long as vehicle chemistry and shortness

are similar, tack and viscosity are roughly proportional and are affected

29 ' 30
in the same way by additions to the ink. Tack can be measured on an

inkometer.

The last condition to be discussed is pigment concentration, which is

the amount of pigment in an ink, expressed as a percent by weight or

volume. Pigment concentration is related to both tack and viscosity in

that as it increases, both tack and viscosity will increase. This is

supported by a study at the National Printing Ink Research Institute, which

found that the inkometer reading (tack), and viscosity increased with

31
increased pigment loading. According to another author, the amount of

pigmentation in the ink affects its viscosity, with viscosity increasing


32 ,33

with increased pigment particle amount.


All of the above conditions are believed to be directly related,

since as one increases, the others will. For example, if any reducer is

added to an ink, the pigment concentration, tack, and viscosity will all

decrease. The only exception to this would be the addition of varnish or

body gum, which would reduce pigment concentration, but increase tack and

viscosity .
10

CHAPTER I

FOOTNOTES

1
Kelvin Tritton, "Dot Gain: Pinpointing the Causes", Printing World 207,
(April 7, 1982), p. 18.

2
"Measuring Dot Gain with a Densitometer", Goss Professional Pressman,
March, 1983, p. 3.
3
Kelvin Tritton, "Dot Gain: Pinpointing the Causes", Printing World 207,
(April 7, 1982), p. 18.
4
Miles Southworth, "Dot Gain: Causes and Cures", Quality Control Scanner 2,
(September, 1982), p. 1. Graphic Arts Publishing Company, Livonia, NY.
5
Ibid.

6
Milton Pearson, Irving Pobboravsky, and Chester Daniels,
"Instrumentation For the Measurement of Slur and Fill-in On A
Lithographic Web Press", 31st TAGA Proceedings, 1979, p. 162.

7
Ibid., p. 164.

8
Ibid., p. 163.

9
Miles Southworth, "Dot Gain: Causes and Cures", Quality Control Scanner 2,
(September, 1982), p. 1. Graphic Arts Publishing Company, Livonia, NY.
10
Ibid.

11
Ibid.

12
Sven Ahrenkilde and Franz Sigg, Private Communications, April 15-17, 1985.

13
Miles Southworth, "Dot Gain: Causes and Cures", Quality Control Scanner 2,
(September, 1982), p. 1. Graphic Arts Publishing Company, Livonia, NY.
14
J.A.C. Yule and W.J. Nielsen, "The Penetration of Light Into Paper and
Its Effect on Halftone Reproduction", Third TAGA Proceedings, 1951, p. 65.

15ibid.
16
Ibid. ,
P- 66

17
Ibid. ,
P- 65
18
Ibid. , p. 67
19
Ibid., p. 69.
11

20
Ibid.

21
Miles Southworth, "Dot Gain: Causes and Curves", Quality Control Scanner
2, (September, 1982), p. 3. Graphic Arts Publishing Company, Livonia, NY

Kelvin Tritton, "Dot Again in Offset Lithography", Ink and Print 1,


(Autumn, 1982) , p. 16.

23
Ian C. White and Barry Daniels, "The Specification of Offset and
Letterpress Printing Inks", 23rd TAGA Proceedings, 1971, p. 30.
24
S.W.P. Wyszkowski, "The Long and Short of the Printing Inks or is
Rheology Really Necessary?", 23rd TAGA Proceedings, 1971, p. 217.
25
Julius Silver, Class Notes, Ink, Color and Substrates, April 2, 1984.

26
Ian C. White Barry Daniels, "The Specification of Offset and
and

Letterpress Printing Inks", 23rd TAGA Proceedings, 1971, p. 29.


27
Y. Pete Jacob, "Ink Physical Property Specifications for Quality
Control Purpose", 22nd TAGA Proceedings, 1970, p. 4
28
Julius Silver, Class Notes, Ink, Color and Substrates, April 2, 1984.

29
T. B. Turner, "Rheology of Ink in Relation to Printing Quality", The
British Ink Maker 18, (February, 1976), p. 57.

30
Robert W. Bassemir, "The Physical Chemistry of
oi Lithographic Inks",
American Ink Maker 59, (February, 1981), p. 44.

31
J.B.M. Coates, "Rheology of Litho Inks", Coates Inklings, No. 103
1978), p. 3.

32J.J.
'.J. Hammel et.
c al .
, "Printing Studies With Black Inks", 12th TAGA
FProceedings, 1960, p. 65.

33
Lane Olinghouse, "Ink Characteristics
Ch Affecting Its Use In
Lithography", In-Plant Printer 17, (November, 1977), p. 29.
12

CHAPTER II

STATEMENT OF PROBLEM

The one feature that sets process inks apart from other inks is the

need for them to form a well-defined dot on the substrate which gives a

faithful reproduction of a continuous tone original. Because of this,

inkmakers and printers must look carefully at the formulations of their

1
process inks, and not worry only about color matching. Since the primary

objective in printing is to produce a quality product in the most efficient

and economical way possible, inks with optimum transfer and water balance

on the press, print on the substrate, drying and dry ink film properties

are required. One property which affects press performance and

reproduction is rheology, which is the physical flow properties of an ink,


2
including viscosity and tack. Attempts are continually being made to

identify the various rheological parameters and relate these to press

3
performance and printability . The adjustment of rheological properties of

an ink has been shown to have a significant influence on the level of dot

4
gain.

A study carried out by PIRA showed that of the variables examined,

which included blankets, inks, number of printing units, paper, and plates,

5
inks had the greatest influence on dot gain in offset lithography. The

study concluded that dot gain is not a fault, but instead an inevitable

part of the lithographic process. The author also stated that more work is

required to examine more fully the influence of ink properties on dot

6
gain.
13

Other work indicates that rheological properties ideal for printing

solids are substantially different from those ideal for printing halftone

and detail, and that sharp dots and low growth are favored by inks with

7
high viscosity. Other inkmakers noted that in general terms, a lower

viscosity ink will give greater dot gain, although the magnitude of any
Q

increase has not yet been able to be predicted. Finally, PIRA and Coates

Brothers inkmakers suggested that viscosity be studied to see its effect on

9, 10
dot gain.

Because of this information, and discussions with people in industry,

it is felt that it would be beneficial to investigate the effect of ink

viscosity on dot gain.


14

CHAPTER II

FOOTNOTES

1
J.B.M. Coates, "Lithographic Process Inks", Coates Inklings, No. 120
(1982), p. 1.

Robert W. Bassemir, "The Physical Chemistry of Lithographic Inks",


American Ink Maker 50 (February, 1981), p. 33.

3T. B. Turner, "Rheology of Ink in Relation to Printing Quality", The


British Ink Maker 18 (February, 1976), p. 55.

Richard Lamprecht, "The Influence of Inks and Blankets on the Printing


Characteristics of a Sheet-Fed Litho Press", Pack & Print (November,
1982), p. 16. citing Kelvin Tritton, "Dot Gain: Pinpointing the
Causes", Printing World 207 (April 7, 1982), p. 19.

Kelvin Tritton, "Research Project Completed on Modifying Dot Gain


-'

Characteristics on Offset Process", PIRA News, No. 166 (1982), p. 3.

6
Ibid.

7T.B. Turner, "Rhelogy of Ink in Relation to Printing Quality", The


British Ink Maker 18 (February, 1976), p. 56.

J.B.M. Coates, "Lithographic Process Inks", Coates Inklings, No. 120

(1982), p. 2.

9 Kelvin Printing World 207


Tritton, "Dot Gain: Pinpointing the Causes",
(April 7, 1982), p. 19.

10
American Ink Maker 62 (July, 1984), 46, quoting J
p. Coates, "Dot
.B.M.

Gain and the Ink Maker", Coates Inklings, No. 128 (1984), pp. 1-4.
15

CHAPTER III

LITERATURE REVIEW

A review of pertinent literature shows that while there has been a

significant amount of work done on both dot gain and ink properties and

their effect on print quality, there has been little work linking the two.

The only major study linking the two was the previously mentioned PIRA

study by Kelvin Tritton. In it, he concluded that inks were shown to be

the variable with the greatest influence on dot gain. He also found that

the level of gain is significantly increased if any form of reducer, which

decreases tack and viscosity, is added to the ink. Since the reducer

reduces both tack and viscosity, the graph would also apply to viscosity as

well as tack reducer. An addition of five percent gel reducer resulted in

1
seven to ten percent higher gain in the middle tones. (Figure 6.) The

percent increase in gain that occurs is greater than the percentage of

solvent or reducer that is added.

Standard ink x* Ink with 5$ gel reducer

j_ ._. Ink: with 10$ gel reducer

40

0 *-+
Percent Dot Area
100

Figure 6. Effect of tack reducer on dot gain.


16

This is due to the lowering of the ink's viscosity, tack and color

3
strength. Tritton also felt that viscosity played a major part in

4
affecting dot gain.

Other work in this area was conducted by Turner, who concluded that

the rheological properties ideal for printing solids are much different

than those ideal for printing halftone and detail, and that sharp dots and

5
low dot growth are favored by inks with high viscosities.

Work at the Pulp and Paper Research Institute of Canada and McGill

University found that inks with chemically similar vehicles show a

correlation between tack and viscosity, and also a correlation between

6,7
viscosity and paper picking, not tack and paper picking.

De Paoli found that dot gain is primarily related to ink film

8
thickness, ink character, and paper character.
17

CHAPTER III

FOOTNOTES

1 Kelvin "Research Completed


Tritton, on Modifying Dot Gain", Offset
Printer No. 162 (1982), p. 25.

2
Richard Lamprecht, "The Influence of Inks and Blankets on the
Printing
Characteristics of a Sheet-Fed Litho Press", Pack & Print (November,
1982), p. 16, citing Kelvin Tritton, "Dot Gain: Pinpointing the Causes",
Printing World 207 (April 7, 1982), p. 18.

3lbid., p. 19.

4Kelvin Tritton, "Dot Gain: Pinpointing the Causes", Printing World 207
(April 7, 1982), p. 19.

5T.B. Turner, "Rheology of Ink in Relation to Printing Quality", The


British Ink Maker 18 (February, 1976), p. 56.

6j. S. Aspler et. al., "Rheological Properties of News Inks and Surface
Strength Test Liquids", 16th International Conference of Printing
Research Institutes (IARIGAI), 1981, p. 235.

7Ibid., p. 248.

8
Alan DePaoli, "The Effect of Printing Conditions on Dot Gain", 33rd
TAGA Proceedings, 1981, p. 38.
CHAPTER IV

HYPOTHESES

Based on the previously mentioned research, it is believed that ink

viscosity and dot gain are inversely related. Because of this, the

following hypothesis has been formulated:

1) If ink viscosity increases, then dot gain will decrease.

If the ink viscosity is increased to the optimum level, then the dot

gain should be limited to the minimum level possible. Since inks with a

viscosity which is too high can cause problems, the ink viscosity cannot be

maximized, but can be made as high as possible. A planned statistical

experiment was conducted to see if different viscosity levels are

significant in affecting dot gain.


CHAPTER V

METHODOLOGY

For the experiment, a series of heatset web standard lithographic

inks with varying viscosities were used and plotted against dot gain. The

inks used were from the same container, and viscosity reduced by adding a

low vapor pressure solvent. The reason for using inks from the same

container was to insure that they had the same chemical composition so that

any change in dot gain could be attributed to the viscosity, and not to any

1
of the other chemicals in the inks.

The papers used were standard coated and uncoated offset paper, 8 1/2

x 10 1/2 inches. The fountain solution was a standard fountain solution

for the duplicator, which was an ATF Chief 15 sheetfed single impression

lithographic press. The test object for measuring dot gain was the RIT

Symmetrical Test Scale, 100 and 150 lines per inch (Figure 7).

^P^P#i
25% 1 25%

Elliptical J I Square

Scale'

Figure 1 . RIT Symmetrical Test

The solvent added was a low pressure vapor solvent, (Magie Oil) which

does not evaporate quickly, insuring that the ink viscosity decreased

instead of increased. A densitometer was used to measure the density of

100 and slur and fill-in areas of the scale. All


the 25 50, 75, percent,
20

of the above conditions as well as the press speed were kept constant

throughout the experiment, with ink viscosity the only


being variable.

Ink Testing

Five cans were filled with heatset web offset ink, and measured on a

triple beam balance. The ink had no additional solvent mixed with it,

while the remaining inks had five, ten, fifteen, and twenty percent of the

weight of the inks in solvent mixed in. The inks were allowed to rest for

24 hours, and then measured on a Brookfield Rotational the


Viscometer, and

viscosities calculated and recorded.

The inks also were measured on a Thwing-Albert Inkometer, and the

tack values recorded at 20 seconds, and one to ten minutes. (Appendix G).

Paper Testing

Samples of both papers were tested for smoothness, porosity, and

absorptivity. The instrument for measuring smoothness was the Sheffield

Smoothness Tester. Ten samples of each paper were measured in three areas,

and the average smoothness values calculated and recorded in Sheffield

units. The samples were then placed in the Sheffield Porosimeter, measured

in three places, and the average porosity values recorded in Sheffield

units. The K & N Oil Absorptivity test was then performed. The optical

densities of the K & N oil stain were recorded and converted to percent

absorptivity, according to GATF Bulletin Number 60.

Press Run

The coated paper was run to an optimum Solid Ink Density for 100

sheets after ink and water balance was achieved, then the uncoated paper
21

was run to 100 sheets at the same amount of ink. The uncoated paper was

then run to an optimum Solid Ink Density for 100 sheets after ink and water

balance was achieved, and the coated paper was run at the same ink level.

This procedure was followed for each ink and the procedure was replicated.

The ink without the solvent was placed in the ink fountain of the

press. When ink and water balance was achieved, a commercially acceptable

product was run, and the Solid Ink Density measured and maintained for 100

sheets.

The sheets were removed, the ink fountain cleaned, and the ink with

the next lowest viscosity placed on the press and run as noted above. This

was repeated for the remaining three inks. Two press runs were

accomplished to provide a measure of experimental error.


22

ANALYSIS

Two random sheets were sampled from the beginning, middle, and end of

each group of 100 sheets from each run. After measuring the first inks and

checking one sheet from the beginning, middle, and end and comparing it to

the other set from beginning, middle, and end, the sets were found to be

similar. Each of the succeeding groups had one sheet from beginning,

middle, and end pulled. The densitometer was calibrated for the different

"n"
types of paper, to take into account the different values of coated and

uncoated paper. The solid, 25, 50 percent square dot, 75, fill-in, and

slur targets were measured for density and dot area. Two targets of 100

and two targets of 150 lines per inch were measured, and the mean and

standard deviation were calculated. Statistical analysis was used to

determine which factors and interactions were significant in affecting dot

gain.
23

CHAPTER V

FOOTNOTES

1
Chester Daniels, Private Communication, October 11, 1984.

Alan DePaoli, "The Effect of Printing Conditions on Dot Gain",


33rd TAGA Proceeding, 1981, p. 20.
24

CHAPTER VI

MEANS REQUIRED

ATF Chief 15 Sheetfed Single Impression Lithographic Press

Heatset Lithographic Web Ink (From same five different viscosities)


container,

GATF Ladder Target

RIT Symmetrical Test Scale 150 and 100 line

Brookfield Rotational Viscometer

Triple Beam Balance

Lithographic Fountain Solution

2000 Sheets 8 1/2x10 1/2 Coated Offset Paper

2000 Sheets 8 1/2 x 10 1/2 Uncoated Offset Paper

Densitometer

3M Tartan Subtractive Plates

Magie Oil (Low Vapor Pressure Solvent for changing ink viscosity)

Sheffield Smoothness Tester

Sheffield Porosimeter

K & N Oil

Cosar Densitometer

All of the above are available in the RIT School of Printing and

Technical and Education Center of the Graphic Arts.


25

CHAPTER VII

ANALYSIS OF DATA

The analysis techniques utilized in this experiment were chosen

to fulfill five tasks: 1 ) To understand the correlation between the

percentage of solvent in an ink and its effect on viscosity, 2) To

examine the differences in the paper used, 3) To check the area of the

slur targets on the plates to see if any dot gain occurred in

platemaking, 4) To understand the interactions of the variables in

this experiment, and 5) To answer the basic research question in this

experiment, that is, does ink viscosity have an effect on dot gain.

The analysis techniques used in this experiment were analysis of

variance using the Yates Method, the Duncan Multiple Range Test, and

1 2' 3
graphing.

Percentage of Ink Solvent and Ink Viscosity

As noted earlier, containers with a given amount of ink were

weighed on a triple beam balance, and varying percentages of that weight

in solvent from 0 to 20 percent were added. The inks were allowed to

stand for 24 hours, and the viscosity measured. The ink not used on the

press was again measured after the press run, along with the ink used

on the press. The results were entered in a calculator, and the

correlation coefficient found. The correlation coefficient, r, is a

value between -1 and +1 which indicates the relationship between two

4
variables. It is derived using the following equation:
26

covariance (XY)
r =

V (variance X) (variance Y)

As r approaches +1 it means that one variable increases as the

other increases. A value approaching -1 indicates that one variable

decreases as the other increases. An r close to 0 indicates that no

5
relationship exists between the two variables. A table showing the

values was constructed. (Table 1).

TABLE 1 : Correlation of Percent Solvent and Ink Viscosity

Percent Viscosity (In Poise)


Ink Number Solvent Unused Ink Used Ink

Before Run After Run

1 0 3600 4240 2940


2 5 2000 2380 1700
3 10 1120 1480 1000
4 15 840 1160 660
5 20 600 760 480

Correlation -.93 -.93 -.94

Paper Analysis

The two papers used in this experiment, a dull coated and an

uncoated stock, were measured for smoothness, porosity, density, and

absorptivity. The smoothness was measured on a Sheffield Smoothness

of each stock were pulled, and measured


Tester. Ten random sheets

on each side. A low Sheffield value indicates


in three different places

A table of the mean values and standard deviations


increased smoothness.

both papers was constructed. (Table 2). The mean is


of both sides of

the data values, while the standard deviation is a


the average of all

6,7
of the spread of data.
measure
27

TABLE 2: Smoothness Values of Papers

Paper Type Side Mean Standard Deviation

Dull Coated 1 26.3 2.21


2 34.67 2.57
Uncoated 1 135.3 19.87
2 138.5 17.13

Porosity measurements were carried out on a Sheffield

Porosimeter, and the procedure for computing values the same as

smoothness, with the results below. (Table 3). A higher value

indicates a higher porosity, meaning more air passes through the

given sample.

TABLE 3: Porosity of Papers

Paper Type Side Mean Standard Deviation

Dull Coated 1 4.867 .562

2 4.867 .499

Uncoated 1 209.5 32.26


2 198.5 30.47

Oil absorptivity was determined by using the K & N Oil Test.

A given amount of oil is placed on the stock and allowed to stand on

the paper for two minutes, then wiped off. When dry, it is measured

on a densitometer with a neutral density filter, and the optical density

measured and recorded. Three random sheets were pulled, the

densitometer zeroed on the paper, the density of the oil measured,

and the mean and standard deviations calculated. (Table 4).


28

TABLE 4:
Density of K & N Oil on Papers

Paper Type Side Mean Standard Deviation

Dull Coated 1 .1587 .0146

2 .1613 .0181

Uncoated 1 .5080
.0227

2 .4153 .0250

After measuring the density, the results were converted to

percent absorptivity, using a Paper Factors Conversion Chart. A

percent absorptivity table was constructed.

TABLE 5: Absorptivity of Papers

Paper Type Side Mean Standard Deviation

Dull Coated 1 40.75 3.13


2 41.317 3.79
Uncoated 1 92.017 2.20
2 82.15 2.76

Plate Analysis

The slur targets of both the 100 and 150 line targets on

both plates were measured using a microscope equipped with a filar

eyepiece to see if any dot gain had occurred during the platemaking

process. As noted in the table, no gain occurred. (Table 6).

TABLE 6: Area of Slur Targets of Plates

Screen Ruling Desired Area Measured Area Standard

( Lines/Inches) (In Inches) (In Inches) Deviation

100 .0050 .0050 .000087

150 .0033 .0033 .00011


29

Analysis of Press Run for Interaction of Factors and Main Effects

Two random sheets from the


were sampled beginning, middle, and end of

each ink level/paper absorbency combination, for all five inks in both

press runs, for a total of 40 combinations. Because of the time involved

in measuring two sheets from the beginning, middle, and end of the first

ink, only one sheet from beginning, middle, and end of each combination was

analyzed, for a total of 120 press sheets analyzed. Prior to the single

sheet, sampling procedures, the sheets from the first ink analyzed were

divided into two groups, with one sheet from beginning, middle, and end,

and the mean of the solid, 25 percent, 50 percent square, 75 percent, slur,

and fill-in targets analyzed and compared. Since the results were both

within one standard deviation of each other, they were considered to not be

significantly different, allowing one sheet from the remaining combinations

to be analyzed. The targets were measured with a smart densitometer, which

converts density to equivalent dot percent area for tint, after measuring

the solid (100 percent) patch. After all measurements were recorded, the

mean and standard deviations of all areas were recorded.

A computer program in the Ink and Paper Testing Laboratory of the

Technical and Education Center of the Graphic Arts at RIT was used to

calculate fill-in, and total dot gain. The densities of the solid
slur,

"n"
the fill-in, and slur targets were entered, along with the value
patch,

of the paper and the line width in microns. The width of a line for a 100

line per inch screen is 254 microns, and 169-33 microns for a 150 line per

inch screen. After the densities were input, the width of a line for both

and fill-in targets were then added in the calculator, unless the slur
slur

in which case the area of only the fill-in target was


result was negative,
30

used. If slur was not negative, the amount was added to fill-in to find

total gain. The percent area for slur, fill-in, and total gain were

calculated by dividing the calculated responses expressed in microns by the

width of a 50 percent line for the patch at a particular ruling. (Appendix

F).

After all the preceding data was recorded, the mean density of the 25

percent, 50 percent square dot, 75 percent, and solid patch were divided by

the solid ink densities to give adjusted densities. This normalized the

curves to a Solid Ink Density of 1.0. The adjusted densities and dot area

for each of the patches were plotted on PC Graph Paper, supplied by the RIT

Technical and Education Center of the Graphic Arts. (Figures 8-11). The

actual densities are in Tables 7-10 and Appendix F.

In addition, graphs of percent dot gain of each area on 100 and 150

line screens versus ink viscosity were plotted for each of the four ink

level/paper absorbency combinations. (Figures 12-17). The adjusted

density/dot gain for each ink level on each paper, and each paper at both

ink levels were also plotted. (Figures 18-21). The actual densities are

given in Table 1 1 .

TABLE 7: Density of Patches and Ink Viscosity

Percent 25 50 Percent 75
Solvent Solid Percent So uare Percent
Ink Number

1 1
1 0 .28 .36 .70 .00

2 5 1 .17 .35 .65


.91

10 1 .37 .70 .98

3 .17

1 1
4 15 .19
.46 .85 .07

1 1 .10

5 20 .17 .53 .91


31

CD
CL
CC
0_
CD
>
o

<

in
c
CD
Q

10 20 30 40 50 60 70 80 90 100

Halftone Dot Area % (Positive)


*-*7
Ink 1(No added solvent) Ink 2(5% added solvent) Ink4(15% added solvent!

0 0 ink 3 (10% added solvent) ----Ink 5 (20% added solvent!

FIGURE 8: Adjusted Density/Dot Gain vs. Ink Viscosity


32

CD
Q.
CO
Q_
CD
>
O

<

O
>,

c
CD
Q

10 20 30 40 50 60 70 80 90 100

Halftone Dot Area % (Positive)


-Uncoated Paper Coated Paper

FIGURE 9: Adjusted Density/Dot Gain vs. Paper Absorbency


33

CD
Q.
CO
0_
CD
>
O

<

-4*

c
CD
Q

10 20 30 40 50 60 70 80 90 100

Halftone Dot Area % (Positive)


-High Ink Level Low Ink Level

FIGURE 10: Adjusted Density/Dot Gain vs. Ink Level


34

10 20 30 40 50 60 70 80 90 100

Halftone Dot Area % (Positive)


100 Line Screen 150 Line Screen

FIGURE 11: Adjusted Density/Dot Gain vs. Screen Ruling


35

Dot
Grain
Percent

40

35

30

25

20 *"-^-
k=w==9 +T A k A A

15

10

600 840 1120 2000 3600


Ink Viscosity( poise)

Optimum (Low) Ink Level Uncoated Paper, same (Low) Ink Level
Coated paper,

Optimum (Hi) Ink Level Coated Paper, same (Hi) Ink Level
Uncoafed paper,

12: Dot Gain for 25 Percent Patch of 100 Line Screen at


FIGURE

Different Ink/Paper Combinations


36

Dot
Sain
Percent

50

45 *v\

40

i A, J-L
u A
A
A
_
*"
35 \ ^^-1^^
_ _k

w b ijv m p
vL-^^*

30
___
__

25

20

15

10

CI 600 840 1120 2000 3600


Ink Viscosity(poise)

Coated paper, (Low) Ink Level Uncoated Paper (Low) Ink Level

Uncoated paper, (Hi) Ink Level Coated Paper (Hi) Ink Level

FIGURE 13: Dot Gain Percent of 25 Percent Patch of 150 Line Screen at

Different Ink/Paper Levels


37

Dot
Gain
Percent

40

35

30

25

20

15

10

_j i_

600 840 1120 2000 3600


Ink Viscosity( poise)

Coated paper, Optimum Ink Level Uncoated paper, (Low) Ink Level

Optimum Ink Level Coated paper, same (Hi) Ink Level


Uncoated paper,

50 Percent Square Dot Target of 100 Line


FIGURE 14: Percent Dot Gain at

Screen at Different Ink/Paper Combinations


38

Dot
Sain
Percent

45

40
-* * kr

35
i*~iM

30

25

20

15

10

600 840 1120 2000 3600


Ink Vlscosity( poise)

Coated paper, Optimum Ink Level Uncoated paper, (Low) Ink Level

Uncoated paper, Optimum Ink Level Coated paper, (Hi) Ink Level

FIGURE 15: Percent Dot Gain for 50 Percent Square Dot Target of 150 Line

Screen Target at Different Ink/Paper Combinations


39

Dot
(Jain
Percent

25

20

15

10

600 840 1120 2000 ,-3600

Ink Viscosity(poise)

Coated paper, Optimum (Low) Ink Level Uncoated paper, same (Low) Ink Level

Uncoated paper, Optimum (Hi) Ink Level Coated paper, same (Hi) Ink Level

FIGURE 16: Percent Dot Gain at 75 Percent Patch of 100 Line Screen

Target at Different Ink/Paper Combinations


40

Dot
Sain
Percent

25

20 h

15

10 *

5 -

0 600 840 1120 2000 3600


Ink Viscosity( poise)

Coated paper, Optimum (Low) Ink Level Uncoated paper, same (Low) Ink Level

Uncoated paper, Optimum (Hi) Ink Level Coated paper, same (Hi) Ink Level

FIGURE 17: Percent Dot Gain at 75 Percent Patch of 150 Line Screen

Target at Different Ink/Paper Combinations


41

CD
Q.
CO
Q_
CD
>
O
_Q

<

Q_

c
CD
Q

10 20 30 40 50 60 70 80 90 100

Halftone Dot Area % (Positive)


Uncoated Paper Coated Paper

FIGURE 18: Adjusted Density/Dot Gain for Different Papers at High Ink Levels
42

CD
Q_
CO
0_
CD
>
O
_Q

<

O
>^

CO
c
CD
Q

10 20 30 40 50 60 70 80 90 100

Halftone Dot Area % (Positive)


Uncoated Paper Coated Paper

19: Adjusted Density/Dot Gain for Different Patches for Papers


FIGURE

at Low Ink Levels


43

CD
d
CO
0_
CD
>
O
__

<

o
>4

w
c
CD
Q

0 10 20 30 40 50 60 70 90 100

Halftone Dot Area % (Positive)


---Low Ink Level
'
High Ink Level

Adjusted Density/Dot Gain Differences for Uncoated Paper at


FIGURE 20:

Different Ink Levels


44

10 20 30 40 50 60 70 80

Halftone Dot Area % (Positive)

Low Ink Level High Ink Level

FIGURE 21: Adjusted Density/Dot Gain Differences for Coated Paper at

Different Ink Levels


45

TABLE 8: Density of Patches and Paper Absorbency

25 50 Percent 75
Paper Type Solid Percent Square Percent

Coated 1 .38 .42 .84 1.15


Uncoated 1 .01 .41
.69

TABLE 9: Density of Patches and Ink Level

25 50 Percent 75
Ink Level Solid Percent Square Percent

High 1 .22 .43 .79 1 .05

Low 1 .17 .40 .73 .97

TABLE 10: Density of Patches and Screen Ruling

Screen Ruling 25 50 Percent 75


(Lines Per Inch) Solid Percent Square Percent

100 1.19 .36 .69 .96

150 1 .20 .47 .84 1 .06

TABLE 11: Density of Patches at Different Ink/Paper Combinations

25 50 75
Paper Type Ink Level Solid Percent Percent Percent

Uncoated Optimum (High) 1.03 .42 .70 .89

Coated Same (High) 1.42 .44 .88 1 .20

Uncoated Same (Low .99 .40 .67 .86

Optimum (Low) 1.34 1


Coated .40 .80 .09

to graphing, the Yates Method of Analysis of


In addition

(ANOVA) was performed, since there were four variables at two


Variance

'
levels in the experiment. The analysis breaks down each
to five

from low to high. The results are arranged in


variable by levels,
46

a standard order, with the lowest levels assigned 0, and all higher

levels assigned a 1 or
higher.11
An example is given. (Figure 22!

INK VISCOSITY

Ink Ink Ink Ink Ink


Screen Paper Level Level Level Level Level
Ruling Absorbency Low High Low High Low High Low High Low High

Low Low 0000 1000 2000 3000 4000


0100 1100 2100 3100 4100
(1) 1
V1 V V2 V V3 V V4 V

High 0010 1010 2010 3010 4010


0110 1110 2110 3110 4110
a la v la v2a v?la v3a v3la V4a v, la
V 4

High Low 0001 1001 2001 3001 4001


0101 1101 2101 3101 4101
s 1 v Is v2s v Is Xs v3ls v. Is
s V V 4

High 0011 1011 2011 3011 4011


0111 1111 2111 3111 4111
as las v as v las v as vlas v3as v3las v. as v, las
4 4

FIGURE 22: Standard Order for Experimental Design

A similar table was drawn for the solid ink density, slur,

fill-in, and total dot gain components. Since the experiment, a

5x2x2x2 level experiment, was twice replicated, the results were

12,13
added to get the total response. (Appendix E) . The results for the

two-factor interactions, three-factor interactions, and


main effects,

four-factor interactions are shown in an ANOVA summary table. This

tabulation provides an indication of the significant factors at a


47

five percent level of significance. The five percent level was chosen

because it is a commonly used level in industry, since a one percent

level is too tight, and a 10 percent level too loose. Results for

the response of solid ink film density, fill-in, slur, and total gain

are shown. (Tables 12-15). Based on the Yates ANOVA, the only

interactions found to be significant were viscosity/ink level, and

viscosity/absorbency, and only for fill-in. (Table 13).

Concerning the basic research question in this experiment,

ink viscosity was found to have a significant effect on solid ink

density (SID), fill-in, slur, and total dot gain. In addition, the

ink level was found to be significant in affecting SID and fill-in,

while paper absorbency was a significant factor in SID, fill-in, and

total gain, and screen ruling significantly affected fill-in, slur,

and total gain.

After determining which factors were significant, the Duncan

Multiple Range Test was performed to determine which levels of the

15
"

variables caused the factors to be significant. With SID, the ink

viscosity, ink level, and paper absorbency were found to be significant.

After performing the Multiple Range Test on the ink viscosities, Ink 1

(with no additional solvent) was found to be significantly different

than the inks with solvent added, thus causing the viscosity factor

(Table 16). Since the other factors had only two


to be significant.

Duncan Test was not performed, but absorbency and ink level
levels, the

were found to be significant in affecting SID.

With regard to fill-in, the inks with 10 to 20 percent solvent

found to be significantly different than the inks with no


added were
48

added solvent and 5 percent (Table 17).


solvent added. The screen

ruling was also found to be a significant factor, along with the

viscosity/ink level and viscosity/absorbency interactions. However,

because several groups of the interactions were significantly different

among some of the groups but not others, no conclusions on

significance of individual interactions groups could be determined.

When the Multiple Range Test was applied to slur, the order

of the variables was not in any order from lowest to highest, as one

might have expected, and the only significant difference was between

the two extreme values. (Table 18). The screen ruling also was

found to be significant in effecting slur.

Finally, when the test was applied to Total Dot Gain, the inks

with 15 and 20 percent added solvent were found to be significantly

different than the inks with 10 percent or less added solvent.

(Table 19) .

The following symbols are used in the following tables:

v is the ink with 15% solvent.

v is the ink with 10% solvent.

v is the ink with 5% solvent.

is the ink with no added solvents.


v,
4

are all viscosities.


v -
v,

1 is ink level.

s is screen ruling.

a is absorbency.
49

TABLE 12: ANOVA Summary Table for Solid Patch

Sum of Degrees of Mean Calc Crit Sign at


Source Squares F reedora Square F_ F_ 5 Percent

Main
Effects

11 2.6144 *
v1 .069 .036 .1421

v2 .0*3 .146

.034 -
4

'd
I
.002

.059 .059
18.2013
4.0934 *

a 2.72 2.72 827.8956 4.0934


s .003 .003 .9113 4.0934

Two-Factor
Interactions

V
"21
.003

.003
-
-.016 -4 .0039 1 .1920 2.6144
.005

v,4 1 .003
~

V .664

.008 -.015
.002 -4 .0038 1.1723 2.6144
a
v, .0006

la .012 .011 3.5707 4.0934


v1s .008
^H
V2S .0009 -.013 ,L .0033 1 .0307 2.6144
1
V .0015

.0027
_jj

Is .0009 .0009 .2767 4.0934


as .0012 .0012 .3647 4.0934

Three-Factor
Interactions

v la .0001

v la .0038
-
.0074 -4
.0019 .5822 2.6144
v,la .0033

v,la .0002

v,ls .0009 T
1 .

V-lS .0004 -.0016 -4 .0004


.1287 2.1644
v Is .0003

v. Is .0000

4
v as .002

v,as .002 -r0043 -4 .0014


.4415 2.6144
v as .ooooe

v,4 as .oooo;

,
las .00001
.00001 .00343 4.0934

Four-Factor
Interactions

v las .0003
T
v-las .00005
1

Vas .ooooe -.00042 i -4 .00013 .0395 2.6144


las .0000
i
v
4

TOTAL: 3.0006.i :9 Error Term = .0032938


50

TABLE 13: ANOVA Summary Table for Fill-in

Sura of Degrees of Mean Calc 3rit Sign at


Source Squares Fr eedom Square F F 5 Percent

Main Effects

v1 3748.09 1015.73
163.88
v2 -4
137.9275
19.006 -4062.9
v3
144.18 *
2.61
?
1 97.68 97.68 *
13.2689 4.0934
a 144.18 144.18 19.5857 4.0934 *
s 2070.61 2070.61 281.2673 4.0934 *

Two-Factor
Interactions
21
V
V2X
.60

.025

43.16 87.73 -
4 21
V3| 22.94
.93 2.9795 2.6144 #

V
Vla 158.80
vpa 18.40 200.95 -4 50.23 6.8242 2.6144 X
v a 15.19
V 8.55
la 1 .058
1.05 .1437 4.0934
T
V .240

12.16 -4

38.12 50.80 12.70 1 .7252 2.6144

y
.273

Is 1 .68
1.68 .2285 4.0934
as 23.98 23.98 3.2575 4.0934

Three-Factor
Interactions

v la 2.75
v la .000
-38.69 -4
9.67 1 .3141 2.6144
v la 26.81

v,4 la 9.12
v Is 24.18
v Is -754 -66.72 -4
16.59 2.2540 2.6144
v Is 37.92
v,4 Is 3.51
v as 1.29
v as .345 -4
2.25 .0368 2.6144
v,as 6.28 -9.03

v, as 1.11
.4
las 7.93 7.93 1.0783 4.0934

Four-Factor
Interactions

v las 6.4 T
v,las 0.00 -
17.27 i -4 4.31 .5867 2.6144
v las 9.75 l
v. las 1.12 _L

TOTAL; 6881 .238 39 Error Te rm = 7.36 725


51

TABLE 14: ANOVA Table for Slur

Sum of Degrees of Mean Calc Crlt Sign at


Source Squares Freedom Square F F 5 Percent

Main
Effects

7.31 2.7471 2.6144


16.72 -25.59 6.39
.027

1 .53

.045 .041
.01937 4.0934
.055 .055 .0237 4.0934
21 .32 21.32 9.1532 4.0934

Two-Factor
Interactions

9.90
5.28 |-20.34 5.08 2.1832 2.6144
v,l 3.27
1 .88

2.20
1
v a 1.05 3.59 .3858 2.6144
V3a .095

231
la 1 .03 1 .03 .4444 4.0934
2
V
.30

V
.051

v3s .517 6.22 1.55 .6684 2.6144


3 .35

y
Is .946 .946 .4062 4.0934
as 1 .32 1.32 .5693 4.0934

Three-Factor
Interactions

v la .729

v la 1 .96
-
5.99 1.49 .6436 2.6144
Oa 3.27
v, la .021

4.
v. Is 3.02
v Is 1 .61 1.61 .6945 6.6144
v Is 1 .50 6.47
v, Is .332

4
v. as .090

v as .577 .2477 2.6144


v,as .023

v as 1.55
las .036
.036 .0155 4.0934

Four-Factor
Interactions

1 .12

vlas 1 .51
1.23 .5287 2.6144
.033 -4.92

v ,
las 2 25

TOTAL: 101 .442


34 Error Term = 2.329375
52

TABLE 15: ANOVA Summary Table for Total Dot Gain

Sum of Degrees of Mean Calc Crit Sign at


Source Squares Freedom Square F F 5 Percent

Main
Effects

3971.05 51.6481 2.6144


284.85
134.68 -4412.72 103.18
22-1*
73.34 73.34 3.4338 4.0934
176.41 176.41 8.2593 4.0934
1791.72 1791.72 83.8836 4.0934
Two-Factor
Interactions

56.05
4.68
V2
25.20 98.21 24.55 1.1496 2.6144
V3
12.28
V
86.53 Tl
V
v2a 17.83
v a 24.96 -136.23 34.06 1.5947 2.6144
6.86
y
la 6 84 6.84 .3204 4.0934
105
V
v2s 1 1 88 10.06 .4711 2.6144
V s 26 08 40.24
2 17
y
Is 4.32 4.32 .2025 4.0934
as 36.18 36.18 1.6030 4.0934

Three-Factor
Interactions

v la 17 .75

v la .094
-
32.83 8.21 .3845 2.6144
v la 7 .52

v,4 la 7 .47

v Is 7 43
v Is 0044 42.99 10.75 .5034 2.6144
v Is 33 39
v,4 Is 2 17
v as 1 12
v as 54 -
-9.31 2.33 .1091 2.6144
v,as 7 65
v, as 003
,
4
las 2.1 2.88 .1352 4.0934

Four-Factor
Interactions

v las 2.28
v las 1.14 -13.64 3.41 .1597 2.6144
v las 7.35
v, las 2.87
4

TOTAL: 6871 .02 39


53

TABLE 16: Duncan Test of Viscosity and Solid Patch

X1 X2 X3 X4 X5
1 .27 1.17 1.17 1 .19 1 .17

The ink with no added solvent (Ink 1) was found to be significantly


different from the others.

TABLE 17: Duncan Test of Viscosity and Percent Fill-in

x1 x2 X3 X4 X5
19.38 19.56 24.06 32.88 36.92

Inks 3 to 5 were significantly different from Inks 1 and 2.

TABLE 18: Duncan Test of Viscosity and Percent Slur

x_
x3 x2 x4 x1
.11 .575 .944 .969 1.83

The only significant difference was between Inks 3 and 5.

TABLE 19: Duncan Test of Viscosity and Percent Total Dot Gain

x1 x2 x3 x4 x5
20.36 21.16 24.18 33.79 38.53

found to be significantly different from


Inks 4 and 5 were

Inks 1 and 3.
54

CHAPTER VII

FOOTNOTES

1
Albert D. Rickmers and Hollis N. Todd, Statistics: An Introduction,
McGraw-Hill, Inc. 1967, p. 154.

Ibid., p. 323.

3Ibid., p. 223.

^Ibid., p. 266.

5Ibid., p. 255.

6Ibid., p. 19.

7Ibid., p. 22.
o

Frank M. Preucil, A New Method of Rating the Efficiency of Paper for Color
Reproductions, (Pittsburgh: Graphic Arts Technical Foundation Research
Progress), No. 60, p. 4.
9
Albert D. Rickmers and Hollis N. Todd, Statistics: An Introduction,
"

McGraw-Hill, Inc., 1967, p. 353.

10
Ibid. ,
p. 323.

11Ibid., p. 312.

1 2
M. Carolyn Hughes, "A Systematic Method of Obtaining Predicted Values in
Experiments,"
Mixed-Level Factorial Industrial Quality Control, (January

1966), p. 353.

1 3
Albert D. Rickmers and Hollis N. Todd, Statistics: An Introduction,
McGraw-Hill, Inc., 1967-

Chester J. Daniels, Private Communication, March 28, 1985.

1 '-i
Albert D. Rickmers and Hollis N. Todd, Statistics: An Introduction,
McGraw-Hill, Inc., 1967, p. 223.
55

CHAPTER VIII

CONCLUSIONS AND OBSERVATIONS

The hypothesis tested in this experiment was that ink viscosity has

an effect on dot gain in offset lithography. By using the Yates Method of

Analysis of Variance to analyze the data, ink viscosity was found to be

significant in affecting the amount of dot gain that occurs in the offset

lithographic process. The viscosity was significant in affecting the

density of the solid patch, fill-in, slur, and total gain. The analysis

also found that ink level, paper absorbency, and screen ruling are

significant in affecting slur, fill-in, and total gain. Ink level was

found to have a significant effect on solid ink density and fill-in, while

paper was significant in affecting SID, fill-in, and total dot


absorbency

gain. The screen ruling was significant in affecting the fill-in, slur,

and total dot gain.

The graphs showed that the inks with 15 and 20 percent solvent showed

dot that inks with less than 1000


a sharp rise in percent gains indicating

have a significant effect on increase in percent dot gain.


poise viscosity

the statistical analysis.


This is also supported by

drawn from this experiment include:


Other observations

of the 50 percent area, where the most dot gain


1 ) The configuration

the amount of dot gain that occurs. For example,


occurs, seems to affect

dot areas of the slur and fill-in targets were usually


the densities and

the 50 percent square dot.


less than that of
56

2) The ink level, paper absorbency, and screen ruling all had an

effect on various components in the experiment, with absorbency and screen

ruling significant in affecting three of the four components.

3) Ink viscosity and screen ruling were found to be significant in

affecting the amount of slur. However, "negative", or side, slur was

observed in some samples, but no cause was found for it.

4) Two of the two factor interactions, viscosity/ink level, and

viscosity/paper absorbency were found to have a significant effect on

fill-in.

5) Viscosity and tack do go in parallel directions, that is, there

is a positive correlation between the two. The high correlation indicates

almost complete dependence of one upon the other.

6) In general, the 50 percent dot area showed the most dot gain.

However, in extreme cases, as with the ink with 20 percent added solvent,

the 25 percent patch exhibited the greatest amount of gain.


57

CHAPTER IX

RECOMMENDATIONS FOR FURTHER INVESTIGATION

1 ) What effect does configuration have on dot gain? Several

different configurations with square, elliptical, round, laser, and other

dots, along with slur and fill-in targets could be tested.

2) Of all the factors studied, which is most significant in

affecting total dot gain? An experiment with as many absorbency, ink film,

solid ink density, and screen ruling levels as possible should be tested.

3) What are the causes of slur, especially negative or side slur?

In this experiment, viscosity and screen ruling affected slur, but the

cause is still not known. It is believed that press problems cause around

the cylinder (directional) slur, but are other factors the cause? Possible

causes of side slur may be blanket movement, or paper fanning in sheet-fed

lithography, and web weaving in web printing.

4) Different interactions, such as viscosity/ink level,

viscosity/absorbency, and viscosity/screen ruling, and others should be

studied to determine which ones are the most significant in affecting dot

gain.

5) What effect do different additives have on ink viscosity, and

ultimately, dot gain. Work with decreasing ink viscosity, such as with

could be carried out.


varnish,
58

6) At what viscosity does gain for the 25 percent patch exceed gain

for the 50 percent patch? More than the five viscosities tested in this

experiment would have to be studied.

7) What effect does screen angle have on dot gain? Angles in 15

degree increments from zero to 90 could be tested.


59

BIBLIOGRAPHY

Ahrenkilde, Sven, and Sigg, Franz. Private Communications, 1985.

Aspler, J.S.; Lyne, M.B.; Dealy, J.M.; and Pangalos, G.C. "Rheological
Liquids"
Properties of News Inks and Surface Strength Test . 16th
International Conference of Printing Research Institutes (IARIGAI).
(1981): 235-252.

Bassemir, Robert W. "The Physical Chemistry of Lithographic Inks".


American Ink Maker, February, 1981, pp. 33, 36, 41-2, 44, 46, 98.

Coates, J.B.M. "Lithographic Process Inks". Coates Inklings, No. 120,


pp. 1-4.

Litho Inks". Coates Inklings, No. 103, pp.


Coates, J.B.M. "Rheology of

2-4.

Private Communications, 1984-85.


Daniels, Chester J.

Printing Conditions on Dot Gain: An


De Paoli, Alan. "The Effect of

Offset Newspaper Study". 33rd TAGA Proceedings. (1981): 17-39.

"Dot Gain and the


Inkmaker"
. American Ink Maker, July, 1984, pp. 30-31,
46 .

and Zettlemoyer, A.C.


Hammel, J.J.; Fetsko, J.M.; Schaeffer, W.D.;
TAGA Proceedings, (1960):
"Printing Studies with Black Inks". 12th
63-79.

"A Systematic Method for Obtaining Predicted Values in


Hughes, M. Carolyn.
Mixed-Level Factorial Experiments", Industrial Quality Control, January,

1966, pp. 348-354.

"Ink Physical Property Specifications for Quality


Jacob, Y. Pete.
Purpose". 22nd TAGA Proceedings. (1970): 1-10.
Control

Inks and Blankets on the Printing


Lamprecht Richard. "The Influence of

Characteristics of a Sheet-Fed Litho


Press."
Pack & Print, November,
25-29.
1982, pp. 16-19, 22-23,

Densitometer". Goss Professional Pressman,


"Measuring Dot Gain with a

March 1983, p. 3.

Lane, "Ink Characteristics Affecting its Use on


Olinghouse,
29-30.
Lithography". In-Plant Printer, November, 1977,, pp.

Daniels, Chester.
Pearson Milton; Pobboravsky, Irving; and

the Measurement of Slur and Fill-in on a


"Instrumentation for
TAGA Proceedings. (1979), 162-175.
Lithographic Press". 31st
60

Preucil, Frank M. A New Method of Rating the Efficiency of Paper for


Color Reproductions, (Pittsburgh: Graphic Arts Technical Foundation
Research Progress), pp. 1-8.

Rickmers, Albert D., and Todd, Hollis N. Statistics: An Introduction,


McGraw-Hill, Inc., 1967.

Silver, Julius L. Private Communications, 1984-1985.

Southworth, Miles. "Dot Gain: Causes and Cures". Quality Control


Scanner, September 1982, pp. 1-4, Graphic Arts Publishing Company,
Livonia, N.Y. .

Tritton, Kelvin. "Dot Again in Offset Lithography". Ink and Print 1


(Autumn, 1982), pp. 16-18.

Tritton Kelvin. "Dot Gain: Pinpointing the Causes". Printing World,


April 7, 1982, pp. 18-19.

Tritton, Kelvin. "Research Completed on Modifying Dot Gain". Offset


Printer, July 1982, p. 25.

Tritton, Kelvin. "Research Project Completed on Modifying Dot Gain

Characteristics on Offset Presses". PIRA News, May, 1982, p. 3.

Turner, T.B. "Rheology of Ink in Relation to Printing Quality". The


British Ink Maker, February, 1976, pp. 55-57.

White, Ian C, and Daniels, Barry. "The Specification of Offset &


Letterpress Printing Inks". 23rd TAGA Proceedings (1971): 26-39.

"The Long Short the Printing Inks or Is


Wyszkowski, S.W.P. and of

23rd TAGA Proceedings, (1971): 205-223.


Rheology Really Necessary?".

Nielsen, W.J. "The Penetration of Light Into Paper


Yule, J. A.C, and

and its Effect on Halftone Reproduction". Third TAGA Proceedings,


(1951): 65-76.
61

APPENDIX A

DEFINITION OF TERMS

Dot Gain: The enlargement which takes place in a dot

from film to print.

Viscosity: The resistance to flow of a liquid,

Tack: The force required to split a film.

Pigment Concentration: The percentage of pigment in an ink, expressed

in terms of weight or volume.

Reducer: A substance which lowers the tack or viscosity

of an ink.

A solvent is an example of a reducer.

SWOP: Standards for Web Offset Publication

Densities established to provide consistency

in Web Offset Printing.

Rheology: Physical flow properties of a liquid

It includes but it not limited to,

tack and viscosity.

Other rheological properties include

thixotropy, viscoelasticity, and tack stability,


62

Solid Ink Density: The density of a solid, or 100 percent patch,

as measured with a densitometer.


63

APPENDIX B

DERIVATION OF MURRAY-DAVIES EQUATION

1 Log R
Density -
D -

Lo

Reflectance = R =

A -
Area

Solid Dot

R, . ,
= R x A + R^dot , x A^dot
tint paper paper
t

Since the area of the paper is the whole area (or one),
less the area of the dot,

R, . ,
= R x 1-A , . + R , , x A. ,

tint paper dot dot dot

Since the reflectance of the paper is assumed to be one,

R. .
= 1 x 1-A, ,
+ R , , x A, .

tint dot dot dot

R_tint ,
= 1-A , .
+ R ,
,_
x A , ,

dot dot dot

R,. . ,
=1 -A . . ( 1 -R . . v

tint dot dot)

tint
, +A.
dot
.,
(1-R^dot) J-N
=
-l
1

W M_Rdot) = 1_Rtint

A, .
1-R, . ,

dot = tint

1-R
dot

Since the reflectance of the dot equals the


reflectance of the solid,

1 -
R,
dot
1 -
R
64

APPENDIX C

INSTRUMENTATION

Viscosity:

Instrument: Brookfield Rotational Viscometer


Procedure: After leveling the base and indicator dial,
the spindle is lowered 1/4 inch into the ink,
and the machine turned on and allowed to
rotate for three minutes. The dial reading
is then converted to viscosity in centipoise

by using a table for spindle size and revolutions

per minute included with the instruction manual

for the instrument.

Tack:

Instrument: Thwing-Albert Inkometer


Procedure: After the desired temperature (90 degrees
Fahrenheit) isattained, the machine is
calibrated for the desired speed, depending
on the type of ink, 1 .32 cubic centimeters

of ink are placed on the roller, and readings

taken at 20 seconds, one minute, and at one

minute intervals up to and including ten


minutes.

Smoothness:

Instrument: Sheffield Smoothness Tester


Procedure: After calibration, a paper sample is placed

on the glass bed of the instrument and the


head lowered to the paper under its
testing
own weight. The smoothness value is read
"Sheffield"
from the guage and expressed as

smoothness.

Porosity:

Instrument: Sheffield Porosimeter

Procedure: After calibration, the sample is placed on a

rubber bed orifice, and the


with a given

lowered pneumatically. The porosity is


head
from the guage, and expressed as
read
"Sheffield"
porosity.
65

Absorptivity:

Instrument: K & N Oil Test


Procedure: The paper is folded so that both sides can be
coated with K & N Oil. The oil is allowed to
stand for two minutes, then wiped off. When dry,
the density is measured and converted to percent

absorptivity by using a Paper Factors Conversion


Chart.

Measurement of Plate Areas:

Instrument: Microscope (Equipped with Filar Eyepiece)


Procedure: After calibration, the desired lines are
measured, then divided by 100 to find the
width in inches.

Density of Patches on Press Sheet:

Instrument: Cosar Smart Densitometer


Procedure: After calibration on the reference standard,
then densitometer is calibrated on the paper

sample. The solid (100 percent) patch is


measured for density. The desired tints
are then read for density, and converted to
percent equivalent dot area, always using the
solid as a reference.

Calculations:

Deviation:
Correlation, Mean, Standard

Instrument: Texas Instrument TI-55-H Programmable Calculator

Procedure: The values are entered according to directions


in the Owner's Manual for each function in the
statistical mode.

Total Dot Gain:


Slur, Fill-in, and

Packard 9100-A Programmable Calculator


Instrument: Hewlett
Slur, and Fill-in
Procedure: The Solid Ink Density,
and calculations
densities are entered,
performed to determine the amount of

and total gain in microns.


slur, fill-in,
The microns are then divided by the microns

to find the percent gain.


of the desired patch

in of the line of a 1 00 line


The width microns

is for one line of a 1 50


per inch screen 254,
line per inch screen, 169-33.
66

APPENDIX D

PRESS RUN DOCUMENTATION

Run Speed: 5000 impressions per hour.

Run Length: 100 sheets, after ink and water balance obtained.
Both papers were run to two ink levels.

Ink Setting: Four from off (Maximum)

Fountain Solution Setting: Two or three notches from off.

PH: 4.50 at start and end of both runs

Number of Press Runs: Two


67

APPENDIX E

YATES TABLES FOR EXPERIMENT

YATES TABLE FOR DENSITY OF SOLID PATCH

Replicates Resp Total Effect


Treatment Combination 1 2 (1) (2) (3) (4) (5)

(1) 0000 1.19 1 .41


2.60 13 .25 27.35 47.47 95.43
1000 1 1 2.72 14 20.12 47.96 3.33
v,
.32 .40 .10

2000 1 1 2.67 9 27.25 1 3.13


V2
.36 .31 .87 .09

3000 1 1 2.50 10 20.21 2.24 2.34


V3
.24 .26 .25

4000 1 1 2.76 13 1.33 .48

I*
.30 .46 .51 .59

0100 1.32 1.47 2.79 14 .24 .50 1.80 2.19


1100 1.25 1 2.78 9 1 1
V .43

10
.99 .49 .42 .75

2100 1 .40 1 .32 2.72 .22 .75 .92 .91

3100 1 .40 1 .37 2.77 .10 .83 1.12 -.90

V3i
v4: 4100 1 .47 1 .57 3.04 .49 .50 -.64 -1 .96

a 0010 .95 1 .00 1.95 .16 1 .43


1 .23 -14.77

v1a 1010 .98 .99 1 .97 .34 .37 .96 -.83

v2a 2010 1 .01 .98


1.99 .71 .87 .57 -1 .39

v3a 3010 .94 .95 1.89 .78 .55 .18 -.54

v, a 4010 1 .02 1.05 2.07 .32 .57 .61 .88

la 0110 1 .01 .99 2.00 .43 .35 .30 -.97

v, la 1110 .99 1.05 2.04 .16 .45 -.34 -.17


1 .

vla 2110 1 .01 1 .01 2.02 .67 .67 -.56 -.93

2,
v_,la 3110 1 .03 .97 2.00 .20 -.65 -.92 .74

3.
v, la 4110 1.10 1 .09 2.19 .30 .01 -1 .04 .48

4
s 0001 1.19 1 .39 2.58 .51 .85 -7.23 .49

V s 1001 1.37 1 .33 2.70 .92 .38 -7.54 1.15


1
v.s 2001 1.36 1 .27 2.63 .24 .73 -.09 .47

2
3001 1 .26 1 .37 2.63 .13 .23 -.74 -.50

3
4001 1 1.52 2.97 .60 .39 -.33 -1 .76

V, s .45

is 0101 1 .36 1 .45 2.81 .27 .18 -1 .06 -.27

v. Is 1101 1 .38 1 .37 2.75 .28 .07 -.32 -.39

1
v.ls
.

2101 1.38 1 .28 2.66 .27 .11 -.22 -.31

2.
v^ls 3101 1 .48 1 .41 2.89 .53 .51 .22 -.22

3. 1.51 3.13
4101 1.62 -.12
v, Is
.04 .10 .66

4
as 0011 .94 1 .01 1.95 .21 .41 -.47 -.31

101 1 1 .98 1.98 .14 -.11 -.50 -.65


v as .00

1 1 1 -.21 -.73
v 'as 2011 .02 .96 .98 .50 -.33

2 1 1 -
-.01
v^as 3011 .95
.01 .96 .05 .04 .10

3 1 1 2.12 -.41

v , as 4011 .06 .06


.52 -.49 .44

4 1 -.52 -.03
las 011 1 .98 .98 .96 .15 -.07

v las 1111 1.02 1 .10 2.03 .01 -.55 .32 .25

1 2.01 -
-.37 -.1 1
v. las 2111 .02 .99
.66 .42

2, 3111 1 .99
2.06 .19 -.67 .18 .10

v^las .07

411 1 1 1 2.16 -
.18 -.37 .30 .12

v,4 las
.08 .08

TOTAL: 95.43
68

APPENDIX E

(CONTINUED)

Sum of Calc F Sig


Divisor Squares Ratio At 5 Percent

80 113.84
160 21 *
.069 .0413 Total Sum of Squares
224 X
.044 13.2784 of Replicates = 116.98
160 X
.034 10.3900
1120 .0002 .0624 Sum of Sum of Squares
80 X
.060 18.2013 = 116.85
160 .0035 1.0675
224 .0037 1.1224 116.98 -
116.85 = .1318

160 .0051 1.5370


1120 .0034 1 .0414 .1318/40
= .00329

X
80 2.73 827.8956 [Error Term for 40 Degrees
160 .0043 1.3072 of Freedom)

224 .0086 2.6187


160 .0018 .5533 Critical F = 4.0848
1120 .0007 .2099

80 .012 3.5708
160 .0002 .0548

224 .0039 1.1722


160 .0034 1 .0391

1120 .0002 .0625

80 .0030 .9113

160 .0083 2.5094


224 .0010 .2994

160 .0016 .4743

1120 .0027 .8397

80 .0009 .2766

16C .0010 .2886

224 .0004 .1302

160 .0003 .0918

1120 .00001 .0039

30 .0012 .3647

i60 .0026 .8017

224 .0024 .7225

160 .00006 .0189

1120 .0002
.0524

80 .00001 .0034

160 .0004 .1186

224 .00005
.0164

160 .00006 .0189

1120 .00001 .0039

116.85
69

APPENDIX E (CONTINUED!

YATES TABLE FOR PERCENT AREA FOR FILL-IN TARGET

Replicates Resp Total Effect


Treatment Combination 1 2 (1) (2) (3) (4) (5)

(11 0000 27.7 37.2 64.9 188.2 391.6 358.8 2124.6


1000 27.7 22.6 50.3 203.4 467.2 1265.8
vl -774.4

2000 21.7 9.5 31 229.6 617.0 191


v2 .2 -390.3 .6

3000 11 9.2 21.0 237.6 648.8 145.3


V3 .8 -384.1

4000 10.6 10.2 20.8 291.7 121.9


1* -238.6 -145.9

0100 31 .4 38.0 69.4 325.3 -151.7 69.7 88.4


1100 28.7 25.5 54.2 316.2 33.6 58.8
V 2100 30.2
-228.3

2.4
19.6 10.6 332.6 -155.8 111.7
3100 18.3 9.0 27.3 -117.5 79.2 -64.2 -83.1

V4X 4100 11.5 10.8 22.3 -121 .1 42.7 -81 .7 -160.3

a 0010 29.4 34.5 63.9 -76.8 48.7 38.4 107.4


v1a 1010 26.6 26.0 52.6 -74.9 21.0 50.0 159.4
v2a 2010 25.7 17.7 43.6 -135.9 21 .2 -1.7 -64.2

v3a 3010 18.9 16.9 35.8 -92.4 12.4 60.5 -49.3

4010 17.0 16.9 33.9 -86.4 76.1 7.7 97.9


y
la 0110 29.9 35.0 64.9 -69.4 35.6 -5.3 -9.2

v.la 1110 28.3 27.0 55.3 37.7 -65.4 -2.6 -21 .0

i .

v.la 2110 26.7 17.2 43.9 41.5 1.2 -80.5 .2

v la 3110 20.5 16.3 36.8 19.4 -56.5 -48.8 65.5


4110 21 15.7 36.7 23.3 101
v,4 la .0 -25.2 -111.5 .1

s 0001 40.8 41.5 82.3 25.7 15.2 75.6 407.0


v.s 1001 41 .9 41.5 83.4 23.0 23.2 31 .8 6.2
1
v_s 2001 37.5 18.6 56.1 11 .8 33.6 86.9 -52.2

2
v3s 3001 19.0 8.7 27.7 9.2 16.4 72.5 78.1

v.s 4001 24.0 18.2 42.2 14.5 -3.6 -36.5 -17.5

is 0101 41.3 44.0 85.3 6.7 1.9 -27.7 11 .6

1101 42.9 34.9 77.8 3.6 43.5 62.2


v. Is
-8.8

1
v_ls
,
2101 31.8 23.7 55.5 8.8 17.0 -40.5 -13.0

v^ls
2, 3101 36.1 21.3 57.4 71.3 3.8 66.6 -77.9

3,Is 4101 26.5 22.8 49.3 4.8 3.9 31 .3 -62.7


v,4
as 0011 39.8 39.9 79-7 24.8 -2.7 8.0 -43.8

v,as 1011 38.6 37.5 76.1 10.8 -2.6 -17.2 -14.4

1 61 3.8
v_as 2011 35.3 26.1 .4 -12.3 -7.8 5.5
2 5.2
v,as 3011 25.2 23.7 48.9 -53.1 -26.5 -31 .7

v, as 4011 24.8 25.3 50.1 4.6 -66.5 .1 -35.3

,4

las 0111 38.0 42.3 80.3 -3.4 -14.0 .1 -25.2

v.las 1111 39.9 36.4 76.3 16.7 -40.8 13.0 -32. C


1 63.2 0.0
v_las
,
2111 37.0 26.2 -73.2 -8.0 52.5
2. 58.1 32.8 39.5
v^las 3111 32.2 25.9 -1.8 -89.9

4111 30.0 24.7 54.7 -23.4 -21.6 68.3 35.5


v, las
4
2124.6
70

APPENDIX E (CONTINUED!

Sum of Calc F Sign


Divisor Squares Ratio at 5 Percent

80 56424.07
X Squares
160 3748.10 509.1329 Total sum of
X Replicates
224 163.88 22.2620 of =

X 63,599.48
160 131.95 17-9234
1120 19.01 2.5817
X Sum Sum Squares
30 97.68 13.2689 of of

16C 21 .60 2.9353 = 63,305.01


224 .0257 .0035

160 43.16 5.8628 * 63,599.48 -


63,305.01
1120 22.94 3.1165
-

294.47
X
80 144.18 19.5857 7.36 (error
294.47/40 =
X
160 158.80 21.5713
term for 40 deg. of
224 18.40 2.4994
Freed. )
160 15.19 2.0635
1120 8.56 1 .1624

Critical F = 4.0848
80 1 .06 .1437

160 2.75 .3744

224 .0002 .00002

160 26.81 3.6424


1120 9.126 1 .2397

X
80 2070.61 281 .2673

160 .2403 .0326

224 12.164 1.6524


160 38.123 5.1785
1120 .273
.0371

80 1.682 .2285

160 24.18 3.2846

224 .745 .1025

160 37.928 5.1520


1120 3.51 .4768

80 23.98 3.2575
160 1.296 .1760

224 .345
.0470

160 6.28 .8531

1120 1.11 .1511

80 7.938 1 .0783

160 9.75 1 .3246

1120 1.125 .1528

63,305.01
71

APPENDIX E (CONTINUED!

ANOVA TABLE FOR AREA OF SLUR TARGET

Replicates Resp Total Effect


Treatment Combination 1 2 (1) (2) (3) (4) (5)

(1) 0000 3.9 1.6 5.5 10.7 25.9 55.9 70.5


1000 2.7 2.1 15.2 30.0 14.6 -34.2

v. -.6

2000 2.0 1 14.6 10.4 61.2


V2 -1.0 .0 -7.5

3000 15.4 4.2 -26.7 -2.1

V3
.8 .1 .9

4000 .7 .5 1 .2 4.7 1.9 28.9 -41.5

0100 1.5 .8 2.3 5.7 -9.4 32.3 1.9


1100 1 4.3 3.5 39.8
V -.2 .1

2.8
.9 -9.6

34.4
2100 -.1 2.9 -.1 -17.1 -5.6

3100 -.8 2.0 1.2 -9.8 21 .3 9.9 22.9


4100 7.8 8.0 11.7 7.6 45.9
y .2 -51 .4

a 0010 3.9 1.0 4.9 -9.4 17.0 5.3 -2.1

v.a 1010 1 .1 3.1 4.2 0.0 15.3 -3.4 -18.8

i
va 2010 0.0 2.4 2.4 -6.7 3.2 30.9 -15.4

2
v3a 3010 1 .6 0.0 1.6 -2.9 .3 8.9 -3.9

4010 .9 .6 1.5 -11.1 -2.3 7.7 -16.1

y
la 0110 3.0 .9 3.9 -6.0 -3.3 26.7 -9.1

v. la 1110 .8 2.0 2.8 8.4 19.4 3.7 -10.8

1
v_la
.

2110 .1 1.6 1.7 12.9 -9.5 19.2 -21 .0

2,
v_,la 3110 1 .0 2.4 3.4 2.2 -32.1 13.3 -22.9
3.
v. la 41 10 2.6 1.0 3.6 5.4 -19.3 32.6 4.9
4
s 0001 1 .1 1 .4 2.5 -3.1 4.5 4.1 -41 .3

v.s 1001 1 .0 0.0 1 .0 20.1 .8 -6.2 -19.2

1 3.4
v.s 2001 0.0 -.1 .-.1
5.9 1 .0 -11 .3

2
VT3 3001 1.3 2.0 3.3 9.4 -4.4 -7.5 -9-1

3 21.5
v.s 4001 .3 -2.3 -2.0 -1-9 -13.7 -61 .3

1- 0101 2.4 1.3 3.7 5.1 9.4 -1 .7 -8.7

1101 2.0 2.2 1 3.8 -2.9 -22. C


v, Is .2 .8

1 5.1 19.0
v_ls
,
2101 -1 .4 -1 .6 -3.0 -1 .5 -1 .0

2. 15.5
v Is 3101 -.7 -.4 -1 .1 -9.1 4.5 -28.9

vTls 4101 4.6 -.7 3.9 6.8 3.2 12.8 19.3


4 23.2
as 0011 2.3 1.6 3.9 -3.3 -3.7 -10.3

1011 1.6 2.3 0.0 3.5 -5.4 3.8


v.as .7

1 7.0 12.0
v_as 2011 -1 .8 -.3 -2.1 .7 -12.1

2 1 18.7 1.3 1.9


v.. as 3011 .5 .9
.4 -3.3

3 15.9 41.7
4011 -.4 -.8 -1.2 -2.4 -1 .3

v, as
,4

las 0111 2.5 .1 2.6 -7.1 3.3 -19.7 -1.7

1111 -.4 -17.3 18.0 -19.3 13.4


v. las -.1 -.3

2111 -.9 0.0 -.9 14.8 -4.7 -12.6 -18.4


v.las

v^las 3111 -.6 -1.0 -1 .6 -24.7 2.5 -22.7 -2.3

3 0.0 5.4 30.1 27.6 50.3


v,4 las 4111 .2 .2

TOTAL: 70.5
72

APPENDIX E (CONTINUED;

Sum of Calc F Sig


Divisor Squares Ratio at 5 Percent

80 62.12
160 7.31 3.1383
X
Total Sum of Squares
224 16.72 7.1782
of Replicates =
160 .027 .0118

255.53
1120 1.54 .6601

8C .045 .0193

Sura of Sum of Squares


X
160 9.90 4.502
= 162.35
224 5.28 2.2679
160 3.28 1.4071
255.53 162.35
-

1120 1 .88 .8075


= 93.18
80 .055 .0237

160 2.209 .9483


93.18/40 = 2.329
224 1.059 .4545
( Error Term for
160 .095 .0408

40 Degrees of
1120 .231 .0994

Freedom)
80 1 .035 .4444

160 .729
.3130

Critical F = 4.0848
224 1.969 .8452

160 3.28 1 .4071

1120 .021 .0092

X
80 21.32 9.1532
160 2.304 .9891

224 .052 .0222

160 .518 .2222

1120 3.355 1 .4403

80 .946 .4062

160 3.025 1 .2986

224 1 .612 .6919

160 1.50 .6446

1120 .333 .1428

80 1.326 .5693

160 .090 .0387

224 .643
.2760

160 .0225 .0097

1120 1.55 .6665

30 .036 .0155

160 1.12 .4818

224 1.51 .6489

160 .033
.0142

1120 2.26
162.35
73

APPENDIX E (CONTINUED;

YATES TABLE FOR TOTAL DOT GAIN

Replicates Resp Total Effect


Treatment Combination 1 2 (1) (2) (3) (4) (5)

(1) 0000 31.6 38.7 70.3 198.7 414.2 914.7 2207.4


1000 27.1 25.3 52.4 215.5 500.5 1292.7
v! -797.1

2000 20.7 11.5 32.2 243.9 630.1 252.6


V2 -396.5

3000 12.7 9.2 21 256.6 662.6 146.8


V3 4000 11.1
.9 -400.6

152.1
10.8 21.9 298.2 -231 .0 -157.5

0100 32.9 25.9 68.8 331.9 -165.5 100.5 77.6


1100 28.5 26.6 55.1 324.1 41 94.7
V 2100
-226.4 .1

32.4
19.5 13.4 32.9 338.5 -174.2 105.7
vk 3100 17.5 10.9 28.4 -127.3 94.6 -53.8 -63.5

v3l
V41 4100 19-3 11.0 30.3 -103.7 57.5 -103.7 -117.3

a 0010 33.3 35.3 68.6 -86.0 63.3 29.5 118.8


v1a 1010 27.7 29.1 56.8 -79.5 37.2 48.1 117.7
v2a 2010 25.7 20.1 45.8 -138.4 27.5 30.1 -63.2

v a 3010 20.5 16.9 37.4 -88.0 13.6 64.6 -62.8

4010 17.9 17.4 35.3 -94.2 77.3 16.7 87.7


la 0110 32.9 38.8 71.7 -80.0 28.4 15.7 -23.4

v,la 1 1 10 29.1 29.0 58.1 45.7 -49.3 4.9 -53.3


i ,

v la 2110 26.9 18.8 45.7 48.9 -4.5 -68.2 4.6


v la 3110 21 .5 18.7 40.2 22.0 -73.3 -34.0 34.7
v, la 4110 24.2 16.7 40.9 35.5 -30.4 -83.3 91.5
4
s 0001 41.8 42.9 84.7 26.4 16.8 86.3 378.6
v s 1001 42.8 41.5 84.3 36.9 12.7 32.5 -4.1

1
v,s 2001 37.5 18.6 56.1 16.2 33.7 65.5 -51.6

2 64.6
v,s 3001 20.2 10.7 30.9 21.0 14.4 52.2
3 23.6
v.s 4001 24.3 17.9 42.2 12.6 -37.1 -49.9

1_ 0101 43.6 42.4 86.0 14.9 6.5 -26.1 18.6


v.ls 1101 43.0 36.8 79.8 5.5 50.4 -13.9 34.5
1
v_ls
.

2101 31.9 22.7 55.5 8.1 14.2 -48.9 -1 .0

v
2,Is 3101 36.1 21.3 57.4 64.3 3.2 44.8 -73.1

vfls 4101 31 .1 22.1 53.2 13.0 13.5 42.9 -49.3

4
as 0011 42.0 41.5 83.5 22.9 10.3 -4.1 -53.8

1011 39.3 39.1 78.4 5.5 4.8 -19.3 -13.3


v, as
1 61 2.3 11
v_as 2011 35.3 26.1 .4 -11.8 -17.1 .0

2 24.6 50.4 2.6


v.as 3011 25.8 -37.5 -30.2 -35.0

4011 24.8 25.6 50.4 1 .9 -51.3 10.3 -1.9


v, as
,4

las 0111 40.6 45.3 85.9 -6.4 -16.9 -5.7 -15.2

1111 39.9 36.4 76.3 2.7 -25.7 -19.1

v, las
.3

1 , 26.2 63.2 34.4


vlas 2111 37.0 -76.0 -8.3 -16.0

2. 25.8 58.1 17.4 34.1


v-las 3111 32.3 -12.9 -78.7

3. 55.0 74.1 56.7


v, las 4111 30.1 24.9 -17.5 -4.6

TOTAL: 68,635. 47
74

APPENDIX E (CONTINUED)

Sum of Calc F Sig


Divisor Squares Ratio at 5 Percent

30 60907.68
X
160 3971.05 185.9136 Total Sum of Squares
X
224 284.85 21.3597 of Replicates =
X
160 134.69 6.3058 68,635.47
1120 22.15 1 .0369

80 73.35 3.4338 Sum of Sum of Squares


160 56.05 2.6241 = 67,781.08
224 4.69 .2194

160 25.20 1 .1799 68,635.47 -


67,781 .08

1120 12.29 .5752


= 854.387
80 176.42 8.2591 X

160 86.58 4.0538 854.387/40 = 21 .36

224 17.83 .8348 (Error Term for 40


160 24.96 1.1687 Degrees of Freedom)
1120 6.86 .3215

80 6.84 .3204 Critical F = 4.0848


160 17.755 .8313

224 .0944 .0044

160 7.525 .3523

1120 7.475 .3500

X
80 1791 .72 83.8836
160 .105 .0049

224 11.89 .5565

160 26.08 1 .2211

1120 2.179 .1020

80 4.33 .2025

160 7.44 .3483

224 .0044 .0002

160 33.40 1.5636


1120 2.17 .1016

30 36.18 1.6939
160 1 .122 .0525

224 .540 .0253

160 7.656 .3584

1120 .0032 .0002

80 2.888 .1352

160 2.28 .1067

224 1.14 .0535

160 7.35 .3442

1120 2.87

TOTAL: 67,781 .08


75

APPENDIX F -
SUMMARY TABLES OF EXPERIMENT
(MEAN DENSITIES OF SOLID, 25 PERCENT,
50 PERCENT SQUARE DOT, 75 PERCENT,
FILL-IN, AND SLUR TARGETS; PERCENT
DOT OF 25, 50 AND 75 PERCENT TARGETS;
AND MICRONS AND PERCENT GAIN OF
FILL-IN SLUR TARGETS AND TOTAL DOT GAIN)
76

APPENDIX F -
SUMMARY TABLES OF EXPERIMENT

SUMMARY TABLE FOR EXPERIMENT

Run Ink Ink Scr 25% 50% Sq 75%


No. No. Paper Level Rul. Sol. Den Dot Den Dot Den Dot

i 1A Coat Opt (Lo) 100 1.31 .28 39.5 .58 71.5 .87 87.8
.07 .03 4.2 .06 3.1 .09 3.2
150 1 .47 .40 53.5 .84 84.5 1 .18 94.3
.06 .09 9.8 .10 7.0 .18 4.5
Uncoat Same ( Lo ) 100 1 .02 .31 41 .8 .55 72.3 .76 88.5
.06 .03 4.7 .04 2.3 .04 1 .6

150 1.06 .40 54.3 .68 81.5 .89 91.5


.09 .06 6.3 .09 4.7 .15 3.6
Uncoat Opt (Hi) 100 1.11 .39 51.2 .68 79.8 .93 93.7
.06 .05 5.1 .09 5.2 .10 2.2
150 1.11 .46 60.3 .79 82.0 .96 94.8
.10 .10 9.6 .15 12.6 .14 4.C

Coat Same (Hi) 100 1.47 .39 51.5 .77 79.7 1.11 92.5
.16 .16 17.5 .14 4.7 .14 7.1

150 1.62 .53 65.5 1.07 91 .7 1 .43 98.2

.08 .12 8.4 .15 3.1 .12 .8

1B Coat Opt (Lo) 100 1.30 .28 40.8 .57 72.2 .87 89.0
.07 .02 3.1 .05 2.7 .07 1.7
150 1.45 .40 54.7 .84 84.8 1.18 95.0
8.6 6.7 .18
4.1
.07 .09 .09

Uncoat Same ( Lo ) 100 1.03 .32 43.2 .56 73.0 .77 88.8
.05 .02 2.2 .04 1 .8 .05 1 .2

150 1.06 .39 52.8 .66 80.7 .88 93.0


.09 .06 6.8 .10 4.0 .12 3.3
Uncoat Opt (Hi) 100 1 .10 .38 51.5 .67 80.3 .93 94.3
.08 .05 5.4 .08 4.6 .09 2.7
150 1 .08 .44 60.6 .77 86.5 .98 96.7
.10 .08 7.9 .15 6.5 .14 2.7
Coat Same (Hi) 100 1.47 .37 48.5 .74 78.5 1 .08 92. C
.06 .13 14. 3 .18 10.7 .14 5.6
150 1.63 .52 64.5 1.05 91 .2 1 .44 98.2
.08 .11 7.7 .14 2.6 .11

2 Coat Opt (Lo) 100 1 .24 .29 40.0 .57 71 .2 .85 89. C
.10 .03 3.8 .04 1 .6 .05 .
r

150 1.26 .37 51 .3 .72 81 .2 1 .02 94.2


.13 .04 4.4 3.9 .14
2.1
.09

Uncoat Same ( Lo ) 100 .94 .32 44.7 .55 74.5 .75 90.-:
.05 .01 1 .5 .01 1 .8 .02 1 .-

150 .95 .38 53.3 .62 80.7 .80 93 . :


.05 .03 3.4 .06 3.6 .05 1 . 1

Uncoat Opt (Hi) 100 1 .03 .34 46.7 .60 76.3 .85 92.2
.13 .04 4.8 -09 4.5 .14 3.3
150 1 .07 .46 60.8 .78 87.2 .98 97. C

Coat Same (Hi) 100 1 .40 .35 48.5 .75 80.0 1.17 93.3
.06 .10 10.9 .04 5.1 .05 2 . t
;
150 1 .48 .51 62.3 1.09 89.2 1 .34 96.

.09
.12 10.7 .05 3.9 .07
77

APPENDIX F (CONTINUED)

PRESS RUN 1, INKS 1 AND 2 (CONTINUED;

Fill- m Slur =) Total

% % %
Den Micr Gain Den Micr Gain Micr Gain

.52 27.1 10.7 .53 1.6 .6 28.6 11.3 Mean


.04 5.3 2.1 .05 3.6 1 .4 8.3 3.3 St Dev
.77 41 .0 24.2 .79 1.9 1 .1 42.8 25.3 Mean
.13 10.5 6.2 .13 .9 .5 10.4 6.1 St Dev
.52 43.1 17. C .53 2.3 .9 45.4 17.9 Mean
.04 4.2 1.7 .04 1 .3 .5 4.3 1.7 St Dev
.64 42.5 25.1 .64 .8 .5 43.3 25.5 Mean
.11
9.7 5.7 .11
1.7 1.0 8.8 5.2 St Dev
.59 53.3 21 .8 .64 8.7 3.4 62.0 24.4 Mean

.07 .7 4.6 .08 11.7 4.6 16.2 6.4 St Dev


.76 55.1 32.5 .74 -3.1 -1.8 55.1 32.5 Mean
.14 9.5 5.6 .12 13.3 7.8 9.6 5.7 St Dev

.57 30.1 11.9 .74 26.8 10.6 57.0 22.4 Mean

.14 10.6 7-7 .19 10.6 2.2 21 .8 8.6 St Dev


26.5 9.6 5.7 54.5 32.2 Mean
.35 44.9 .98

.10 7.2 4.2 .05 10.2 6.0 9.8 5.8 St Dev


.52 27.0 10.6 .52 1.9 .7 28.8 11.2 Mean

.03 3.5 1 .4 .05 3.4 1.3 7.0 2.8 St Dev


.76 40.6 24.0 .76 .6 1.5 41 .2 24.3 Mean

.12 9.7 5.8 .13 1.5 .9 11 .0 6.5 St Dev


.52 43.6 17.2 .53 3.0 1 .2 46.5 18.3 Mean

.04 5.4 2.1 .04 3.2 1.3 5.4 2.1 St Dev


42.0 24.8 .63 -.6 -.4 42.0 24.8 Mean
.63

.11 9.2 5.4 .1 1 1.2 .7 9.2 5.4 St Dev


54.8 21 .6 .62 6.7 2.6 61 .4 24.2 Mean
.59

.08 14.1 5.5 .07 10.0 3.9 14.4 5.7 St Dev


30.0 0.0 50.9 30.1 Mean
.71 50.9 .71 .1

9.8 5.8 .11 5.9 3.5 8.5 5.0 St Dev


.13

29.2 11.5 .68 19.8 7.8 49.0 19.3 Mean


.57

.12 19.8 7.3 .11 7.5 3.0 13.9 5.5 St Dev


26.5 7.9 4.6 52.7 31 Mean
44.9
.1
.96
.85

.11 7.6 4.5 .14 9.0 5.3 8.6 5.1 St Dev

.52
30.1 11.8 .53 2.2 .8 32.2 12.7 Mean
3.2 1.2 .03 1.8 .7 2.8 1 .1 St Dev
.03

.61 32.1 19.0 .63


2.1 1.3 34.2 20.2 Mean
4.1 4.8 2.9 3.5 2.1 St Dev
.10 6.9 .07

4.0 1.6 52.1 20.5 Mean


.51 48.1 18.9 .52

7.0 2.8 .02 3.2 1.3 4.7 1.9 St Dev


.02

25.2 43.6 25.8 Mean


.58 42.7 .59 .9 .5

1 1 2.6 1.5 St Dev


.03
2.6 .5 .03 .1 .7

2.6 1 54.6 21.5 Mean


.56 52.0 20.5 .57
.1

2.7 2.5 1 5.7 2.3 St Dev


.08 6.9 .08
.1

32.2 54.6 32.2 Mean


.75
54.6 .73 -1 .0 -.6

6.4 2.4 1 9.0 5.3 St Dev


.15
10.8 .12
.4

18.3 -.8 44.6 12.5 Mean


.64 46.5 .65 -1.9

6.2 2.4 .13 2.9 11.8 29.5 11.6 St Dev


.05

36.1 1.01 61 36.1 Mean


1 .01 61.2 -1 .1 -.7 .2

1 6.0 3.5 4.6 2.7 St Dev


.04 1.9 .1 .10
78

APPENDIX F (CONTINUED)

Run Ink Ink Scr 2 5% 50% Sq 75%


No. No. Paper Level Rul. Sol Den Dot Den Dot Den Dot

1 3 Coat Opt (Lo) 100 1.36 .37 52.0 .76 83.2 1.15 95.2
.13 .06 6.8 .13 5.1 .18 2.k
150 1.36 .48 64.2 1.00 91.8 1.25 97-5
.13 .08 6.4 .19 4.1 .15 3.3
Uncoat Same (Lo) 100 1 .01 .38 53.0 .64 80.7 .88 94.3
.05 .03 3.0 .05 2.1 .06 1 .2

150 1 .02 .45 62.7 .76 88.5 .93 97.0


.04 .04 3.1 .06 2.3 .05 .6.

Uncoat Opt (Hi) 100 1.01 .40 54.2 .68 82.2 .87 93.3
.06 .05 6.3 .07 4.0 .08 2.3
150 1 .02 .49 64.8 .79 89.0 .94 97.5
.06 .08 7.5 .09 3.5 .10 1 .5

Coat Same (Hi) 100 1 .40 .34 48.8 .73 81 .2 1 .16 95.7
.10 .04 4.3 .10 3.5 .13 1.9
150 1.38 .43 59.3 .94 90.2 1 .28 98.2
.06 .06 4.4 .1 1 3.8 .09 .5

4 Coat Opt (Lo) 100 1.32 .40 51.2 .86 87.3 1 .17 96.5
.14 .07 6.6 .08 5.9 .12 2.3
150 1 .37 .57 71.5 1.14 96.2 1 .31 99.2
.03 .03 1.6 .03 .41 .04 .4

Uncoat Same (Lo) 100 .98 .39 53.8 .66 82.5 .86 94.8
.04 .03 2.9 .06 2.9 .06 1.3
150 1 .00 .51 68.3 .83 90.5 .96 98.5
.02 .05 4.9 .05 2.4 .04 .8

Uncoat Opt (Hi) 100 .99 .40 54.7 .68 83.3 .88 94.3
.05 .04 4.8 .07 3.8 .07 1 .c

150 1 .02 .52 69.3 .83 92.2 .98 98.7


.01 .03 2.7 .04 1.6 .02 .5

Coat Same (Hi) 100 1.35 .41 55.2 .86 86.3 1 .19 97. C
.05 .08 8.1 .12
7.1 .09 2.3
150 1.38 .60 73.2 1.18 96.8 1.35 99.6
.06 .04 2.3 .04 .41
.07
."4

5 Coat Opt (Lo) 100 1.19 .43 59.0 .84 88.7 1.08 96.7
.07 .06 5.5 .13 3.2 .07 2.0
150 1.19 .57 72.8 1 .00 94.8 1.13 98.8
.06 .10 6.1 .08 2.6 .08 1 .3

Uncoat Same (Lo) 100 .95 .42 59.3 .68 85.5 .63 95.5
.06 .05 4.8 .06 2.4 .08 1 .4

150 .94 .53 72.5 .80 92.8 .90 97. t


.08 .06 3.8 .09 1 .7 .09

Uncoat Opt (Hi) 100 1.01 .43 59.0 .73 86.7 .93 96. 8
.03 .03 3.6 .04 2.1 .04 .4

150 .98 .54 70.8 .82 92.0 .94 98.2


.07 .10 8.3 .11
3.7 .10 1 .7

Coat Same (Hi) 100 1.32 .43 58.3 .92 88.7 1 .23 97.8
.06 .06 5.2 .14 7.9 .14 2.4
99.=
150 1.36 .64 75.0 1.15 96.3 1.31
.07 .07 7.0 .10 2.7 .09
79

APPENDIX F (CONTINUED)

PRESS RUN 1, INKS 3 THROUGH 5 (CONTINUED)

Fill- In Slur ( -) Total

% % %
Den Micr Gain Den Micr Gain Micr Gain

.71 55.2 21 .7 .69 -2.6 -1.0 55.2 21 .7 Mean


.14 19.3 7.6 .09 7.4 2.9 14.1 5.6 St Dev
.99 63.6 37.5 .99 -.7 0.0 63.6 37.5 Mean
.14
4.9 2.9 .15 6.0 3.5 6.7 4.0 St Dev
.62 65.4 25.7 .62 0.0 0.0 65.4 25.7 Mean
.06 5.7 2.2 .05 2.2 .8 5.7 2.2 St Dev
.75 59.8 35.3 .73 -3.0 -1.8 59.8 35.3 Mean
.07 4.8 2.8 .07 1 .4 .8 4.9 2.9 St Dev
.63 67.9 26.7 .63 .4 .1 68.3 26.9 Mean
.09 12.1 4.8 .07 6.5 2.6 9.4 3.7 St Dev
.79 62.9 37.0 .77 -1.5 -.9 62.9 37.0 Mean
.09 5.8 3.4 .10 2.1 1 .2 6.4 3.8 St Dev
.67 49.7 19.6 .66 -.2 -1 .1 49.7 19.6 Mean
.10 11 .7 4.6 .08 3.5 1 .4 8.9 3.5 St Dev
.88 53.9 31 .8 .85 -2.3 -1 .4 53.9 31 .8 Mean
.12 8.3 4.9 .11 1 .6
.9 8.2 4.8 St Dev
.78 70.4 27.7 .76 -1 .6 -.6 68.8 27.1 Mean
.1 1 8.8 3.5 .09 2.3 .9 6.7 2.6 St Dev
1.10 70.9 41 .9 1 .13 1 .6 1.0 72.5 42.8 Mean
.03 1.9 1 .1 .02 1 .0 .6 1.5 .9 St Dev
.61 67.7 26.6 .63 2.7 1 .1 70.4 27.7 Mean
.06 6.7 2.7 .06 2.9 1 .1 7.2 2.8 St Dev
.79 65.4 38.6 .80 1 .1 .7 66.5 39.3 Mean
.06 5.0 2.9 .05 1.9 1 .1 4.0 2.4 St Dev
.63 71 .8 28.3 .65 2.0 .8 73.8 29.1 Mean
.09 12.8 5.0 .05 .8 0.0 12.7 5.0 St Dev
.82 67.6 39.9 .87 -.2 -.1 67.7 39.9 Mean
.04 3.5 2.0 .05 2.0 1 .2 4.3 2.6 St Dev
.80 72.9 28.7 .30 -.5 -.2 72.9 28.7 Mean

.07 7.3 2.9 .07


7.0 2.8 9.7 3.8 St Dev
1.14 72.7 42.9 1.14 .3 .2 72.9 43.2 Mean
.06
1 .3
.8 .05 1 .0 .6 .8 .5 St Dev
.73
70.4 27.7 .79 9.9 3.9 80.3 31 .6 Mean

.12 15.0 5.9 .13 1 .6 .7 14.7 5.8 St Dev


69.0 40.8 .98 1 .8 1 .1 70.8 41 .8 Mean
.96

.07 2.8 1 .7 .09 1.6 .9 3.8 2.3 St Dev

.63 74.7 29.4 .68 10.0 3.9 84.7 33.3 Mean

.06 6.3 2.5 .05


5.2 2.1 3.0 1 .1 St Dev

67.3 39.8 .80 3.8 2.3 71 .2 42.0 Mean


.77

.08 3.6 2.1 .06 3.8 2.2 2.0 1 .2 St Dev


7.7 3.0 83.7 32.9 Mean
.68 76.0 29.9 .72

5.0 2.2 .04 4.0 1.6 6.0 2.4 St Dev


.03

38.0 4.2 2.5 68.8 40.6 Mean


.79 64.3 .82

4.8 3.2 1.9 5.7 3.4 St Dev


.12 8.2 .10

79.8 31 .4 .87 3.8 1.5 83.6 32.9 Mean


.84

11 4.6 .1 1 2.0 .8 10.7 4.2 St Dev


.11 .7

41 1 4.0 2.4 73.9 43.6 Mean


1 .09 69.9 .3 .15

6.0 3.5 .11 2.4 1 .4 4.0 2.3 St Dev


.13
80

APPENDIX F (CONTINUED)

Run Ink Ink Scr 25% 50% Sq 75%


No. No. Paper Levels Rul Sol Den Dot Den Dot Den Dot

2 1 Coat Opt (Lo) 100 1 .46 .28 39.0 .61 72.8 .99 90.5
.07 .02 2.8 .05 2.9 .05 1 .1

150 1.52 .34 48.2 .75 80.0 1.19 94.3


.13 .07 8.0 .08 4.9 .17 3.1
Uncoat Same ( Lo ) 100 1 .05 .31 42.8 .56 72.5 .82 90.5
.09 .03 4.3 .07 4.0 .10 2.9
150 1.06 .38 52.3 .65 79.2 .93 95.2
.12 .07 6.9 .09 7.2 .08 3.3
Uncoat Opt (Hi) 100 1.09 .31 43.7 .57 73.2 .82 89.2
.06 .02 2.0 .05 3.5 .06 3.4
150 1.08 .38 53.2 .67 81.2 .92 94.3
.06 .05 5.4 .09 5.0 .09 2.3
Coat Same (Hi) 100 1.57 .30 44.7 .64 75.3 .99 90.8
.07 .08 8.5 .17 2.6 .04 2.8
150 1.51 .40 56.0 .86 86.0 1 .27 95.7
.07 .05 4.9 .08 4.6 .08 2.3
2 Coat Opt (Hi) 100 1.26 .26 41.5 .53 71 .3 .83 88.7
.11 .03 2.8 .04
1.9 .05 .82

150 1.37 .26 40.7 .55 71.7 .39 89.5


.03 .01 1 .2 .01 .56 .02 1 .1

Uncoat Same ( Lo ) 100 .95 .29 41.7 .53 73.2 .74 89.2
.04 .02 1.5 .03 1.7 .03 2.3
150 1 .01 .39 55.0 .66 82.2 .35 93.7
.02 .03 4.3 .05 3.0 .03 1 .2

Uncoat Same (Hi) 100 .97 .29 41.5 .57 72.0 .74 89.0
.04 .03 4.2 .04 3.0 .04 1 .3

150 1 .02 .38 54.0 .66 82.2 .84 93.0


.04 .03 3.6 .05 2.7 .05 1 .6

Coat Same (Hi) 100 1 .37 .26 40.7 .55 71 .7 .89 89.5
.03 .01 1.2 .01 .52 .02 1 .1

150 1 .41 .37 54.5 .74 82.7 1 .08 94.5


.05 .01 1 .1 .04 1 .8 .09 1 .8

3 Coat Opt (Lo) 100 1.31 .26 38.2 .55 71 .2 .88 89.3
.06 .02 3.1 .02 1 .2 .03 .82

150 1.27 .33 48.5 .68


79.5 1 .00 93.5
.09 .05 6.2 .11 4.8 .04 1 .8

Uncoat Same ( Lo ) 100 .98 .31 43.7 .56 74.5 .78 91 .2

.02 .01 2.7 .02 1.8 .02 .75

150 .96 .37 53.0 .64 82.3 .84 94.8


.08 .06 7.5 .08 3.1 .1 1 2.6
Uncoat Same (Hi) 100 1 .01 .32 45.8 .57 75.2 .79 90.8
.05 .02 1.6 .03 .98 .04
.75

150 .99 .39 56.3 .66 82.7 .84 93.8


.06 .05 4.6 .07 3.7 .08
1.9
Coat Opt (Hi) 100 1 .32 .28 42.5 .58 73.0 .94
91.5
.06 .02 2.7 .03 2.0 .08 1.5
150 1.28 .36 51.5 .73 82.8 1.12 96.5
.07 .07 7.3 .10 5.8 .11 2.6
APPENDIX F (CONTINUED)

PRESS RUN 2, INKS 1 THROUGH 3 (CONTINUED;

Fill- in Slijr <:) Total

% % %
Den Micr Gain Den Micr Gain Micr Gain

.54 26.0 10.2 .55 1 .4


.5 27.3 10.8 Mean
.03 2.9 1 . 1 .01 4.1 1.6 3.0 1.2 St Dev
.67 30.8 18.2 .64 -3.9 -2.3 30.8 18.2 Mean
.09 8.0 4.7 .12 3.5 2.0 10.8 6.4 St Dev
.52 42.8 16.9 .57 1 .4 .6 44.3 17.4 Mean
.04 2.4 1.0 .04 14.1 5.5 13.0 5.1 St Dev
.64 42.8 25.3 .62 -1.3 -.8 42.8 25.3 Mean
.12 9.3 5.5 .11 2.1 1.3 8.1 4.8 St Dev
.52 39.8 15.7 .53 2.6 1.0 42.4 16.7 Mean
.04 4.1 1.6 .03 1.8 .7 2.8 1 .1 St Dev
.64 41 .9 24.7 .63 .4 .2 42.2 24.9 Mean
.08 7.5 4.4 .06 6.1 3.6 7.1 4.2 St Dev
.57 27.4 10.8 .57 .6 .2 28.0 11.0 Mean
.04 8.2 3.2 .05 3.7 1 .4 9.1 3.6 St Dev
.75 38.5 22.8 .74 -1 .2 -.7 38.5 22.8 Mean
.11 10.6 6.3 .11 2.9 1.7 11.3 6.7 St Dev
.49 23.3 9.2 .49 .2 .1 23.4 9.3 Mean
.03 3.5 1 .4 .04 3.7 1.5 6.2 2.4 St Dev
.51 14.7 8.7 .53 3.3 2.0 18.1 10.7 Mean
.02 2.4 1 .4 .03 1.6 .9 3.6 2.1 St Dev
.49 43.0 16.9 .49 -.1 0.0 43.0 16.9 Mean
.03 5.1 2.0 .04 5.8 2.3 9.9 3.5 St Dev
.59
40.1 23.7 .60 1.6 .9 41 .6 24.6 Mean
.02 3.5 2.1 .04 1.9 1 .1 4.5 2.7 St Dev
41 .4 16.3 .52 6.2 2.5 47.6 18.7 Mean
.49

.02 2.5 1 .0 .03 4.7 1.8 4.6 1 .8 St Dev


.62 43.8 25.9 .61 -1.6 -.9 43.8 25.9 Mean
5.0 2.9 .06 1 .4 .8 5.7 3.3 St Dev
.05

.51 22.8 9.0 .53 5.0 2.0 27.2 10.9 Mean

.02 3.5 1 .4 .03 2.3 .9 4.8 1.9 St Dev


36.2 21.3 .69 -.7 -.4 36.2 21.3 Mean
.69

.04 3.3 1.9 .06 2.8 1.6 5.5 3.2 St Dev


.51 24.2 9.5 .53 5.2 2.0 29.3 11.5 Mean

.02
3.1 1 .2 .02 2.1 .8 3.5 1 .4 St Dev

.62 31.5 18.6 .61 -.3 -.1 31.5 18.6 Mean


.10 9.5 5.6 .07 3.6 2.1 7.2 4.3 St Dev
17.7 6.1 2.4 51.0 20.1 Mean
.51 44.9 .53

.01 1.0 .4 .02 3.6 1.4 4.2 1.7 St Dev


26.1 44.3 26.1 Mean
.60 44.3 .59
-.6 -.3

2.3 1.5 4.9 2.9 St Dev


.06 3.9 .07 .9

17.2 4.1 1.6 47.6 18.8 Mean


.52 43.7 .54

3.0 1 .2 .03 3.8 1.5 4.5 6.8 St Dev


.01

26.2 0.0 0.0 44.3 26.2 Mean


.61 44.3 .61

5.1 3.0 .07 1.7 1.0 5.4 3.2 St Dev


.06

10.6 7.3 2.9 34.1 13.4 Mean


.52 26.9 .56

2.2 .03 3.1 1.2 3.4 1 .4 St Dev


.02 .9

40.1 23.7 Mean


.70
40.1 23.7 .68 -2.7 -1.6

4.1 2.4 12.3 7.3 St Dev


.10
8.3 4.9 .13
82

APPENDIX F (CONTINUED;

Run Ink Ink Scr 25% 50% Sq 75%


No. No. Paper Level Rul. Sol. Den Dot Den Dot Den Dot

2 4 Coat Opt (Lo) 100 1 .40 .38 53.3 .78 83.2 1.15 94.7
.11 .06 7.6 .11 7.6 .07 4.8
150 1.33 .54 67.5 1.05 91 .8 1 .30 98.5
.10 .10 7.6 .14
5.7 .12 1.8
Uncoat Same (Lo) 100 .99 .38 53.7 .65 82.2 .85 94.3
.04 .03 4.6 .02 1.8 .04 1.2
150 .98 .49 66.3 .77 89.5 -91 96.8
.11 .11 10.0 .13 4.9 .14 2.4
Uncoat Opt (Hi) 100 1.05 .41 58.3 .70 84.2 .92 95.5
.03 .01 1.5 .03 1.7 .04 1 .4

150 1.01 .48 66.2 .75 87.7 .89 95.8


.08 .11 9.6 . 1 1 4.7 .13 4.1

Coat Same (Hi) 100 1.43 .40 56.8 .86 87.2 1.23 96.8
.10 .04 4.1 .07 3.9 .10 4.8
150 1.37 .50 62.8 .97 87.5 1 .18 96.0
.08 .13 8.5 .22 3.9 .19 4.3

5 Coat Opt (Lo) 100 1 .41 .52 66.7 1 .04 92.0 1 .32 98.5
.07 .10 7.7 .12 2.6 .07 1 .8

150 1.39 .67 75.2 1 .15 94.3 1.37 99.3


.07 .08 5.7 .13 2.8 .05 .82

Uncoat Same (Lo) 100 1 .00 .44 62.2 .76 88.7 .93 97.2
.06 .09 9.1 .1 1 4.9 .09 1 .7

150 .98 .54 71.3 .82 92.2 .93 97.5


.10 .14 11.9 .16 5.5 .10 2.4

Uncoat Opt (Hi) 100 .99 .45 62.5 .74 88.0 .89 96.0
.08 .07 6.2 .11 4.1 .10 2.6
150 .98 .56 73.8 .85 93.7 .95 98.7
.09 .13 9.4 .13 3.4 .12 1 .8

Coat Same (Hi) 100 1.47 .52 66.3 1 .07 92.2 1 .37 98.5
.07 .09 7.3 .14 3.5 .09 1 .1

150 1.45 .73 79.3 1.25 97.2 1 .40 99.5


.08 .09 7.7 .08 1.3 .07 .55
83

APPENDIX F (CONTINUED)

PRESS RUN 2, INKS 4 AND 5 (CONTINUED;

Fill-:Ln Slur ( -) Total

% % %
Den Micr Gain Den Micr Gain Micr Gain

.78 57.4 22.6 .84 6.8 2.7 64.2 25.3 Mean

.07 20.9 8.2 .13 6.5 2.5 24.2 9.5 St Dev


1 .06 70.2 41.5 1.07 0.0 0.0 70.2 41.5 Mean
.12 4.8 2.8 .09 3.3 1.9 2.2 1.3 St Dev
.61 66.0 26.0 .65 7.9 3.1 73.8 29.1 Mean
5.4 2.1 5.6 2.2 St Dev
.03 4.9 1.9 .04

2.7 1.6 66.2 39.1 Mean


.77 63.5 37.5 .79

.16 10.4 6.2 .14 3.2 1.9 7.7 4.6 St Dev


68.6 27.0 .68
5.1 2.0 73.8 29.0 Mean
.67

8.4 3.3 .04 4.2 1 .6 5.0 2.0 St Dev


.05

36.4 61 36.1 Mean


.77 61.7 .77 -.6 .3 .1

.14 11.1 6.5 .14 2.7 1 .6 11 .9 7.0 St Dev


2.8 1 67.6 26.6 Mean
.77 64.8 25.5 .79
.1

3.1 1 8.8 3.5 St Dev


.09 8.9 3.5 .09
.2

3.3 2.0 62.4 36.8 Mean


.95
59.1 34.9 .99

.20 12.0 7.1 .17 3.3 1 .9 9.5 5.6 St Dev


37.2 1 4.0 1.6 98.4 38.7 Mean
1 .01 94.5 .04

.10 7.0 2.8 .09 1 .2 .9


6.0 2.4 St Dev
1.15 2.3 1 72.6 42.9 Mean
1.11 70.3 41.5 .4

1.9 1 3.9 2.3 St Dev


.10 3.2 1.9 .11
.1

2.6 1 90.2 35.5 Mean


.75 87.6 34.5 .75
.0

6.1 6.9 2.7 10.4 4.1 St Dev


.12 15.5 .10

2.7 1.6 70.3 41.5 Mean


.81 67.6 39-9 .83

5.4 3.2 3.8 2.3 St Dev


.12 6.5 3.9 .09

35.0 2.3 91 35.9 Mean


.73 89.0 .75 .9 .2

3.6 1 8.2 3.2 St Dev


.10 8.6 3.3 .09
.4

71 42.4 Mean
.85
71.6 42.3 .85 .2
.1 .7

3.8 6.6 3.9 St Dev


.13 6.5 .13 .9 .5

38.0 1 2.1 98.6 38.8 Mean


1 .06 96.6 .08
.8

3.4 3.4 1.3 5.8 2.3 St Dev


.1 1 8.5 .09

44.0 1 2.2 1 76.7 45.3 Mean


1 .22 74.5 .27
.3

1 1 2.9 1.7 St Dev


.07
2.1 .2 .10 .4 .9
84

APPENDIX G

TACK VALUES AND RELATION TO VISCOSITY

Ink Number 1 2 3 4 5
% Solvent 0 5 10 15 20

Time Tack at Med ium Speed

20 seconds 9.6 7.0 4.7 4.6 4.0

1 minute 10.2 7.5 5.0 4.9 4.1

2 minutes 11 .3 8.0 5.2 5.0 4.2

3 minutes 12.4 8.8 5.6 5.3 4.4

4 minutes 13.5 9.7 6.0 5.6 4.5

5 minutes 14.8 10.3 6.7 6.0 4.7


6 minutes 16.3 11 .5 7.3 6.4 4.9

7 mintues 17.8 12.2 8.0 6.8 5.2

8 minutes 19.2 13.5 8.7 7.3 5.5

9 minutes 20.7 14.4 9.4 7.8 5.7

10 minutes 22.2 15.5 10.2 8.4 6.0

VISCOSITY AND 10 MINUTE TACK FOR INKS

10 Minute Tack
Ink Number % Solvent Viscosity (Poise) (Medium Speed)

1 0 3600 22.2

2 5 2000 15.5

3 10 1120 10.2

4 15 840 8.4

5 20 600 6.0

Corr _
.99
85

APPENDIX H

TEST FORM FOR EXPERIMENT

II
I

: ii

iSS&E

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