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    This document contains the results of a surface area and porosity analysis of a sample using the TriStar II 3020 instrument. It reports the sample details, experimental conditions, dates and times. It then summarizes the surface area, pore volume, pore size distribution and reports values from various analysis models including BET, BJH, DFT and others.

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    This document contains the results of a surface area and porosity analysis of a sample using the TriStar II 3020 instrument. It reports the sample details, experimental conditions, dates and times. It then summarizes the surface area, pore volume, pore size distribution and reports values from various analysis models including BET, BJH, DFT and others.

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    14 views10 pages

    F04

    Uploaded by

    novi liana
    This document contains the results of a surface area and porosity analysis of a sample using the TriStar II 3020 instrument. It reports the sample details, experimental conditions, dates and times. It then summarizes the surface area, pore volume, pore size distribution and reports values from various analysis models including BET, BJH, DFT and others.

    Copyright:

    © All Rights Reserved
    Download as XLS, PDF, TXT or read online from Scribd
    Flag for inappropriate content
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    of 10

    |

    TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020


    |
    |
    Sample: F04 | Sample:
    Operator: FA | Operator:
    Submitter: | Submitter:
    File: C:\TriStar II 3020\data\SAMPEL\2019\Januari\F04.SMP | File:
    |
    |
    Started: 1/16/2019 4:5 Analysis AdsorN2 | Started:
    Completed: 1/17/2019 4:2 Analysis Bath -195.850 °C | Completed:
    Report Time: 7/15/2019 10: Thermal Correc No | Report Time:
    Sample Mass:0.2961 g Warm Free Sp10.6808 cm³ Measured | Sample Mass:
    Cold Free Spa31.2572 cm³ Equilibration In5 s | Cold Free Spa
    Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure
    Automatic DegNo | Automatic Deg
    |
    |
    |
    |
    |
    |
    |
    Summary Report | Isotherm Tabular Report
    |
    | Relative Press
    |
    Surface Area | 0.009571418
    | 0.109262848
    Single point s 513.2563 m²/g | 0.210853557
    | 0.296211865
    BET Surface A520.9387 m²/g | 0.404333737
    | 0.501775681
    t-Plot Micropo 30.6492 m²/g | 0.603527551
    | 0.70134711
    t-Plot External 490.2895 m²/g | 0.800478243
    | 0.897653118
    BJH Adsorption | 0.988750418
    between 1.700440.964 m²/g | 0.90608649
    | 0.806536383
    BJH Desorption | 0.706230645
    between 1.700499.6202 m²/g | 0.60900899
    | 0.505077643
    D-H Adsorption | 0.40438373
    between 1.700442.889 m²/g | 0.29755253
    | 0.212347372
    D-H Desorption | 0.112043321
    between 1.700480.9999 m²/g | 0.010270121
    |
    |
    |
    Pore Volume |
    |
    Single point ad |
    less than 172. 1.597000 cm³/g |
    |
    t-Plot micropo 0.014777 cm³/g |
    |
    BJH Adsorption |
    between 1.7001.526422 cm³/g |
    |
    BJH Desorption |
    between 1.7001.549999 cm³/g |
    |
    |
    |
    Pore Size |
    |
    Adsorption ave12.26248 nm |
    |
    BJH Adsorption
    13.8462 nm |
    |
    BJH Desorption
    12.4094 nm |
    |
    D-H Adsorption13.7085 nm |
    |
    D-H Desorption12.6472 nm |
    |
    |
    |
    Freundlich |
    |
    Qm·C: 53.5792 ± 1.2519 cm³/g STP |
    |
    m: 4.8801 ± 0.2891 |
    |
    |
    |
    Temkin |
    |
    q·alpha/Qm: 0.024031 ± 0.003693 kJ/mol·(cm³/g STP) |
    |
    A: 2.3210 ± 1.7100 mmHg |
    |
    |
    |
    DFT Pore Size |
    |
    Volume in Por < 1.483 nm : 0.01845 cm³/ |
    Total Volume i<= 117.233 nm : 0.99805 cm³/ |
    Area in Pores > 117.233 nm : 191.182 m²/g |
    Total Area in >= 1.483 nm : 319.136 m²/g |
    |
    |
    DFT Surface Energy |
    |
    Total Area : 481.393 m²/g |
    |
    |
    Nanoparticle Size: |
    |
    Average Partic11.5177 nm |
    |
    |
    |
    Horvath-Kawazoe |
    |
    Maximum pore1.597000 cm³/g |
    |
    Median pore wi31.6805 nm |
    |
    |
    |
    MP-Method |
    |
    Cumulative sur |
    1.89609 nm and
    0.0000 m²/g |
    |
    Cumulative po |
    1.89609 nm and
    0.000000 cm³/g |
    |
    Average pore h0.00000 nm |
    |
    |
    |
    |
    TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020
    |
    |
    F04 | Sample: F04
    FA | Operator: FA
    | Submitter:
    C:\TriStar II 3020\data\SAMPEL\2019\Januari\F04.SMP | File: C:\TriStar II 3020\data\SAMPEL\2019\J
    |
    |
    1/16/2019 4:5 Analysis AdsorN2 | Started: 1/16/2019 4:5
    1/17/2019 4:2 Analysis Bath -195.850 °C | Completed: 1/17/2019 4:2
    7/15/2019 10: Thermal Correc No | Report Time: 7/15/2019 10:
    0.2961 g Warm Free Sp10.6808 cm³ Measured | Sample Mass:0.2961 g
    31.2572 cm³ Equilibration In5 s | Cold Free Spa31.2572 cm³
    None Sample Densit1.000 g/cm³ | Low Pressure None
    No | Automatic DegNo
    |
    |
    |
    |
    |
    |
    |
    otherm Tabular Report | Isotherm Linear Plot
    |
    Absolute Pres Quantity AdsoElapsed Time S( aturation Pr |
    760 | F04 - Adsorption
    7.274277687 81.28752762 01:08 | Relative PressQuantity Adso
    83.0397644 128.2831883 01:21 | 0.009571418 81.28752762
    160.248703 150.4622628 01:35 | 0.109262848 128.2831883
    225.1210175 167.5266158 01:45 | 0.210853557 150.4622628
    307.2936401 190.1414537 01:57 | 0.296211865 167.5266158
    381.3495178 211.4694042 02:09 | 0.404333737 190.1414537
    458.6809387 237.3646325 02:24 | 0.501775681 211.4694042
    533.0238037 270.7025802 02:40 | 0.603527551 237.3646325
    608.3634644 330.3727489 03:00 | 0.70134711 270.7025802
    682.2163696 517.8356471 03:40 | 0.800478243 330.3727489
    751.4503174 1032.454104 05:11 | 0.897653118 517.8356471
    688.6257324 910.5891526 06:09 | 0.988750418 1032.454104
    612.9676514 377.2120903 08:34 |
    536.7352905 282.1431967 09:17 |
    462.8468323 243.539714 09:38 |
    383.8590088 215.3463724 09:57 |
    307.3316345 192.2666731 10:14 |
    226.1399231 169.5649683 10:29 |
    161.3840027 152.3945724 10:40 |
    85.15292358 130.5282134 10:54 |
    7.80529213 83.82197141 11:38 |
    |
    |
    |
    Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108 Page 1
    |
    |
    | Sample: F04
    | Operator: FA
    | Submitter:
    :\TriStar II 3020\data\SAMPEL\2019\Janu| File: C:\TriStar II 3020\data\SAMPEL\2019\Janu
    |
    |
    Analysis AdsorN2 | Started: 1/16/2019 4:5 Analysis AdsorN2
    Analysis Bath -195.850 °C | Completed: 1/17/2019 4:2 Analysis Bath -195.850 °C
    Thermal Correc No | Report Time: 7/15/2019 10: Thermal CorrecNo
    Warm Free Sp10.6808 cm³ M| Sample Mass:0.2961 g Warm Free Sp10.6808 cm³ M
    Equilibration In5 s | Cold Free Spa31.2572 cm³ Equilibration In5 s
    Sample Densit1.000 g/cm³ | Low Pressure None Sample Densit1.000 g/cm³
    | Automatic DegNo
    |
    |
    |
    |
    |
    |
    |
    | Isotherm Log Plot
    |
    |
    F04 - Desorption | F04 - Adsorption F04 - Desorption
    Relative PressQuantity Adso| Relative PressQuantity AdsoRelative PressQuantity Adso
    0.988750418 1032.454104 | 0.009571418 81.28752762 0.988750418 1032.454104
    0.90608649 910.5891526 | 0.109262848 128.2831883 0.90608649 910.5891526
    0.806536383 377.2120903 | 0.210853557 150.4622628 0.806536383 377.2120903
    0.706230645 282.1431967 | 0.296211865 167.5266158 0.706230645 282.1431967
    0.60900899 243.539714 | 0.404333737 190.1414537 0.60900899 243.539714
    0.505077643 215.3463724 | 0.501775681 211.4694042 0.505077643 215.3463724
    0.40438373 192.2666731 | 0.603527551 237.3646325 0.40438373 192.2666731
    0.29755253 169.5649683 | 0.70134711 270.7025802 0.29755253 169.5649683
    0.212347372 152.3945724 | 0.800478243 330.3727489 0.212347372 152.3945724
    0.112043321 130.5282134 | 0.897653118 517.8356471 0.112043321 130.5282134
    0.010270121 83.82197141 | 0.988750418 1032.454104 0.010270121 83.82197141
    |
    | |
    | TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020
    | |
    | |
    | Sample: F04 | Sample:
    | Operator: FA | Operator:
    | Submitter: | Submitter:
    | File: C:\TriStar II 3020\data\SAMPEL\2019\Janu| File:
    | |
    | |
    | Started: 1/16/2019 4:5 Analysis AdsorN2 | Started:
    | Completed: 1/17/2019 4:2 Analysis Bath -195.850 °C | Completed:
    | Report Time: 7/15/2019 10: Thermal Correc No | Report Time:
    | Sample Mass:0.2961 g Warm Free Sp10.6808 cm³ M| Sample Mass:
    | Cold Free Spa31.2572 cm³ Equilibration In5 s | Cold Free Spa
    | Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure
    | Automatic DegNo | Automatic Deg
    | |
    | |
    | |
    | |
    | |
    | |
    | |
    | Isotherm Linear Absolute Plot | Isotherm Log Absolute Plot
    | |
    | |
    | F04 - Adsorption F04 - Desorption | F04 - Adsorption
    | Absolute Pres Quantity AdsoAbsolute Pres Quantity Adso| Absolute Pres
    | 7.274277687 81.28752762 751.4503174 1032.454104 | 7.274277687
    | 83.0397644 128.2831883 688.6257324 910.5891526 | 83.0397644
    | 160.248703 150.4622628 612.9676514 377.2120903 | 160.248703
    | 225.1210175 167.5266158 536.7352905 282.1431967 | 225.1210175
    | 307.2936401 190.1414537 462.8468323 243.539714 | 307.2936401
    | 381.3495178 211.4694042 383.8590088 215.3463724 | 381.3495178
    | 458.6809387 237.3646325 307.3316345 192.2666731 | 458.6809387
    | 533.0238037 270.7025802 226.1399231 169.5649683 | 533.0238037
    | 608.3634644 330.3727489 161.3840027 152.3945724 | 608.3634644
    | 682.2163696 517.8356471 85.15292358 130.5282134 | 682.2163696
    | 751.4503174 1032.454104 7.80529213 83.82197141 | 751.4503174
    | |
    |
    TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108
    |
    |
    F04 | Sample: F04
    FA | Operator: FA
    | Submitter:
    C:\TriStar II 3020\data\SAMPEL\2019\Janu| File: C:\TriStar II 3020\data\SAMPEL\2019\Janu
    |
    |
    1/16/2019 4:5 Analysis AdsorN2 | Started: 1/16/2019 4:5 Analysis Adsor
    1/17/2019 4:2 Analysis Bath -195.850 °C | Completed: 1/17/2019 4:2 Analysis Bath
    7/15/2019 10: Thermal Correc No | Report Time: 7/15/2019 10: Thermal Correc
    0.2961 g Warm Free Sp10.6808 cm³ M| Sample Mass:0.2961 g Warm Free Sp
    31.2572 cm³ Equilibration In5 s | Cold Free Spa31.2572 cm³ Equilibration In
    None Sample Densit1.000 g/cm³ | Low Pressure None Sample Densit
    No | Automatic DegNo
    |
    |
    |
    |
    |
    |
    |
    otherm Log Absolute Plot | Isotherm Pressure Composition
    |
    |
    04 - Adsorption F04 - Desorption | F04 - Adsorption F04 - Desorption
    Quantity AdsoAbsolute Pres Quantity Adso| Weight % N2 Absolute Pres Weight % N2
    81.28752762 751.4503174 1032.454104 | 0.72532493 7.274277687 9.212541249
    128.2831883 688.6257324 910.5891526 | 1.144665084 83.0397644 8.125145802
    150.4622628 612.9676514 377.2120903 | 1.342567962 160.248703 3.365846412
    167.5266158 536.7352905 282.1431967 | 1.494832412 225.1210175 2.517550976
    190.1414537 462.8468323 243.539714 | 1.696623587 307.2936401 2.173093848
    211.4694042 383.8590088 215.3463724 | 1.886931924 381.3495178 1.921525936
    237.3646325 307.3316345 192.2666731 | 2.117993874 458.6809387 1.715586824
    270.7025802 226.1399231 169.5649683 | 2.415466873 533.0238037 1.513020539
    330.3727489 161.3840027 152.3945724 | 2.947901088 608.3634644 1.359809873
    517.8356471 85.15292358 130.5282134 | 4.620624046 682.2163696 1.164697342
    1032.454104 7.80529213 83.82197141 | 9.212541249 751.4503174 0.747939658
    |
    | |
    Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 |
    | |
    | |
    | Sample: F04 |
    | Operator: FA |
    | Submitter: |
    0\data\SAMPEL\2019\Janu| File: C:\TriStar II 3020\data\SAMPEL\2019\Janu|
    | |
    | |
    N2 | Started: 1/16/2019 4:5 Analysis AdsorN2 |
    -195.850 °C | Completed: 1/17/2019 4:2 Analysis Bath -195.850 °C |
    No | Report Time: 7/15/2019 10: Thermal Correc No |
    10.6808 cm³ M| Sample Mass:0.2961 g Warm Free Sp10.6808 cm³ M|
    5s | Cold Free Spa31.2572 cm³ Equilibration In5 s |
    1.000 g/cm³ | Low Pressure None Sample Densit1.000 g/cm³ |
    | Automatic DegNo |
    | |
    | |
    | |
    | |
    | |
    | |
    | |
    | BET Surface Area Report |
    | |
    | BET Surface A520.9387 ± 4.4252 m²/g |
    04 - Desorption | Slope: 0.008317 ± 0.000070 g/cm³ STP |
    Absolute Pres | Y-Intercept: 0.000039 ± 0.000013 g/cm³ STP |
    751.4503174 | C: 212.104361 |
    688.6257324 | Qm: 119.6680 cm³/g STP |
    612.9676514 | Correlation Coe
    0.9999297 |
    536.7352905 | Molecular Cros0.1620 nm² |
    462.8468323 | |
    383.8590088 | |
    307.3316345 | |
    226.1399231 | |
    161.3840027 | Relative PressQuantity Adso1/[Q(Po/P - 1)] |
    85.15292358 | 0.009571418 81.28752762 0.000118886 |
    7.80529213 | 0.109262848 128.2831883 0.00095621 |
    | 0.210853557 150.4622628 0.001775807 |
    | 0.296211865 167.5266158 0.00251233 |
    | |
    | |
    |
    TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020
    |
    |
    Sample: F04 | Sample: F04
    Operator: FA | Operator: FA
    Submitter: | Submitter:
    File: C:\TriStar II 3020\data\SAMPEL\2019\Janu| File: C:\TriStar II 3020\data\SAMPEL\2019\J
    |
    |
    Started: 1/16/2019 4:5 Analysis AdsorN2 | Started: 1/16/2019 4:5
    Completed: 1/17/2019 4:2 Analysis Bath -195.850 °C | Completed: 1/17/2019 4:2
    Report Time: 7/15/2019 10: Thermal Correc No | Report Time: 7/15/2019 10:
    Sample Mass:0.2961 g Warm Free Sp10.6808 cm³ M| Sample Mass:0.2961 g
    Cold Free Spa31.2572 cm³ Equilibration In5 s | Cold Free Spa31.2572 cm³
    Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure None
    Automatic DegNo | Automatic DegNo
    |
    |
    |
    |
    |
    |
    |
    BET Surface Area Plot | BET Isotherm Plot
    |
    |
    F04 Not Fitted | F04
    Relative Press1/[Q(Po/P - 1)]Relative Press1/[Q(Po/P - 1)]| Relative PressQuantity Adso
    0.009571418 0.000118886 | 0.009571418 81.28752762
    0.109262848 0.00095621 | 0.109262848 128.2831883
    0.210853557 0.001775807 | 0.210853557 150.4622628
    0.296211865 0.00251233 | 0.296211865 167.5266158
    | 0.404333737 190.1414537
    | 0.501775681 211.4694042
    | 0.603527551 237.3646325
    | 0.70134711 270.7025802
    | 0.800478243 330.3727489
    | 0.897653118 517.8356471
    | 0.988750418 1032.454104
    |
    Serial #: 1108 Page 1

    :\TriStar II 3020\data\SAMPEL\2019\Januari\F04.SMP

    Analysis AdsorN2
    Analysis Bath -195.850 °C
    Thermal Correc No
    Warm Free Sp10.6808 cm³ Measured
    Equilibration In5 s
    Sample Densit1.000 g/cm³

    F04 - BET Equation


    Relative PressQuantity Adsorbed (cm³/g STP)
    0.009571418 81.20676506
    0.109262848 129.3746588
    0.210853557 149.0129876
    0.296211865 168.1505626
    0.404333737 199.5120291
    0.501775681 239.069892
    0.603527551 300.8999393
    0.70134711 399.8898415
    0.800478243 599.070318
    0.897653118 1168.61139
    0.988750418 10636.98205

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