Si NPT75

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TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020

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Sample: SiNPT75 | Sample:
Operator: NHA | Operator:
Submitter: | Submitter:
File: C:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNPT75. | File:
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Started: 1/24/2019 3:1 Analysis AdsorN2 | Started:
Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C | Completed:
Report Time: 1/24/2019 7:1 Thermal Correc No | Report Time:
Sample Mass:0.2904 g Warm Free Sp11.2525 cm³ Measured | Sample Mass:
Cold Free Spa32.4840 cm³ Equilibration In5 s | Cold Free Spa
Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure
Automatic DegNo | Automatic Deg
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Summary Report | Isotherm Tabular Report
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| Relative Press
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Surface Area | 0.010384971
| 0.111036562
Single point s 33.2851 m²/g | 0.207685912
| 0.299798464
BET Surface A33.8075 m²/g | 0.402366759
| 0.500531648
t-Plot Micropo 2.0373 m²/g | 0.597911594
| 0.70300558
t-Plot External 31.7702 m²/g | 0.808254282
| 0.909620426
BJH Adsorption | 0.990964066
between 1.70041.083 m²/g | 0.89921883
| 0.801115016
BJH Desorption | 0.705633304
between 1.70048.7394 m²/g | 0.609744825
| 0.502150807
D-H Adsorption | 0.389453968
between 1.70031.880 m²/g | 0.303155257
| 0.210172854
D-H Desorption | 0.11002594
between 1.70038.4604 m²/g | 0.008728492
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Pore Volume |
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Single point ad |
less than 213. 0.143690 cm³/g |
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t-Plot micropo 0.001108 cm³/g |
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BJH Adsorption |
between 1.7000.143256 cm³/g |
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BJH Desorption |
between 1.7000.143981 cm³/g |
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Pore Size |
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Adsorption ave17.00095 nm |
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BJH Adsorption
13.9479 nm |
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BJH Desorption
11.8164 nm |
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D-H Adsorption17.3619 nm |
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D-H Desorption14.7870 nm |
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Freundlich |
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Qm·C: 3.5126 ± 0.0740 cm³/g STP |
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m: 4.9009 ± 0.2620 |
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Temkin |
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q·alpha/Qm: 0.371572 ± 0.051938 kJ/mol·(cm³/g STP) |
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A: 2.3734 ± 1.5946 mmHg |
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DFT Pore Size |
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Volume in Por < 1.483 nm : 0.00136 cm³/ |
Total Volume i<= 136.677 nm : 0.14068 cm³/ |
Area in Pores > 136.677 nm : 0.000 m²/g |
Total Area in >= 1.483 nm : 20.738 m²/g |
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DFT Surface Energy |
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Total Area : 33.934 m²/g |
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Nanoparticle Size: |
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Average Partic177.4755 nm |
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Horvath-Kawazoe |
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Maximum pore0.143690 cm³/g |
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Median pore wi25.5974 nm |
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MP-Method |
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Cumulative sur |
1.36450 nm and
30.6610 m²/g |
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Cumulative po |
1.36450 nm and
0.042075 cm³/g |
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Average pore h1.37225 nm |
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TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020
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SiNPT75 | Sample: SiNPT75
NHA | Operator: NHA
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNPT75. | File: C:\TriStar II 3020\data\SAMPEL\2019\J
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1/24/2019 3:1 Analysis AdsorN2 | Started: 1/24/2019 3:1
1/24/2019 7:1 Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1
1/24/2019 7:1 Thermal Correc No | Report Time: 1/24/2019 7:1
0.2904 g Warm Free Sp11.2525 cm³ Measured | Sample Mass:0.2904 g
32.4840 cm³ Equilibration In5 s | Cold Free Spa32.4840 cm³
None Sample Densit1.000 g/cm³ | Low Pressure None
No | Automatic DegNo
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otherm Tabular Report | Isotherm Linear Plot
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Absolute Pres Quantity AdsoElapsed Time S( aturation Pr |
760 | SiNPT75 - Adsorption
7.892577648 5.403267672 00:37 | Relative PressQuantity Adso
84.38778687 8.443159702 00:40 | 0.010384971 5.403267672
157.8412933 9.79161895 00:42 | 0.111036562 8.443159702
227.8468323 10.91989316 00:45 | 0.207685912 9.79161895
305.7987366 12.20610288 00:47 | 0.299798464 10.91989316
380.4040527 13.62650876 00:49 | 0.402366759 12.20610288
454.4128113 15.45711041 00:51 | 0.500531648 13.62650876
534.2842407 18.54141403 00:55 | 0.597911594 15.45711041
614.2732544 26.05197977 01:02 | 0.70300558 18.54141403
691.3115234 73.8386881 01:23 | 0.808254282 26.05197977
753.1326904 92.89490591 01:29 | 0.909620426 73.8386881
683.406311 85.55451492 01:34 | 0.990964066 92.89490591
608.8474121 30.74111089 02:04 |
536.281311 19.05851521 02:11 |
463.4060669 15.78018001 02:13 |
381.634613 13.63157616 02:15 |
295.9850159 11.97480343 02:18 |
230.397995 10.87722459 02:20 |
159.731369 9.724178732 02:22 |
83.61987305 8.293790711 02:25 |
6.633653641 5.025826995 02:42 |
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Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108 Page 1
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| Sample: SiNPT75
| Operator: NHA
| Submitter:
:\TriStar II 3020\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\Jan
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Analysis AdsorN2 | Started: 1/24/2019 3:1 Analysis AdsorN2
Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C
Thermal Correc No | Report Time: 1/24/2019 7:1 Thermal CorrecNo
Warm Free Sp11.2525 cm³ M| Sample Mass:0.2904 g Warm Free Sp11.2525 cm³ M
Equilibration In5 s | Cold Free Spa32.4840 cm³ Equilibration In5 s
Sample Densit1.000 g/cm³ | Low Pressure None Sample Densit1.000 g/cm³
| Automatic DegNo
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| Isotherm Log Plot
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SiNPT75 - Desorption | SiNPT75 - Adsorption SiNPT75 - Desorption
Relative PressQuantity Adso| Relative PressQuantity AdsoRelative PressQuantity Adso
0.990964066 92.89490591 | 0.010384971 5.403267672 0.990964066 92.89490591
0.89921883 85.55451492 | 0.111036562 8.443159702 0.89921883 85.55451492
0.801115016 30.74111089 | 0.207685912 9.79161895 0.801115016 30.74111089
0.705633304 19.05851521 | 0.299798464 10.91989316 0.705633304 19.05851521
0.609744825 15.78018001 | 0.402366759 12.20610288 0.609744825 15.78018001
0.502150807 13.63157616 | 0.500531648 13.62650876 0.502150807 13.63157616
0.389453968 11.97480343 | 0.597911594 15.45711041 0.389453968 11.97480343
0.303155257 10.87722459 | 0.70300558 18.54141403 0.303155257 10.87722459
0.210172854 9.724178732 | 0.808254282 26.05197977 0.210172854 9.724178732
0.11002594 8.293790711 | 0.909620426 73.8386881 0.11002594 8.293790711
0.008728492 5.025826995 | 0.990964066 92.89490591 0.008728492 5.025826995
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| TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020
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| Sample: SiNPT75 | Sample:
| Operator: NHA | Operator:
| Submitter: | Submitter:
| File: C:\TriStar II 3020\data\SAMPEL\2019\Jan | File:
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| Started: 1/24/2019 3:1 Analysis AdsorN2 | Started:
| Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C | Completed:
| Report Time: 1/24/2019 7:1 Thermal Correc No | Report Time:
| Sample Mass:0.2904 g Warm Free Sp11.2525 cm³ M| Sample Mass:
| Cold Free Spa32.4840 cm³ Equilibration In5 s | Cold Free Spa
| Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure
| Automatic DegNo | Automatic Deg
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| Isotherm Linear Absolute Plot | Isotherm Log Absolute Plot
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| SiNPT75 - Adsorption SiNPT75 - Desorption | SiNPT75 - Adsorption
| Absolute Pres Quantity AdsoAbsolute Pres Quantity Adso| Absolute Pres
| 7.892577648 5.403267672 753.1326904 92.89490591 | 7.892577648
| 84.38778687 8.443159702 683.406311 85.55451492 | 84.38778687
| 157.8412933 9.79161895 608.8474121 30.74111089 | 157.8412933
| 227.8468323 10.91989316 536.281311 19.05851521 | 227.8468323
| 305.7987366 12.20610288 463.4060669 15.78018001 | 305.7987366
| 380.4040527 13.62650876 381.634613 13.63157616 | 380.4040527
| 454.4128113 15.45711041 295.9850159 11.97480343 | 454.4128113
| 534.2842407 18.54141403 230.397995 10.87722459 | 534.2842407
| 614.2732544 26.05197977 159.731369 9.724178732 | 614.2732544
| 691.3115234 73.8386881 83.61987305 8.293790711 | 691.3115234
| 753.1326904 92.89490591 6.633653641 5.025826995 | 753.1326904
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TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108
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NHA | Operator: NHA
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\Jan
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1/24/2019 3:1 Analysis AdsorN2 | Started: 1/24/2019 3:1 Analysis Adsor
1/24/2019 7:1 Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1 Analysis Bath
1/24/2019 7:1 Thermal Correc No | Report Time: 1/24/2019 7:1 Thermal Correc
0.2904 g Warm Free Sp11.2525 cm³ M| Sample Mass:0.2904 g Warm Free Sp
32.4840 cm³ Equilibration In5 s | Cold Free Spa32.4840 cm³ Equilibration In
None Sample Densit1.000 g/cm³ | Low Pressure None Sample Densit
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otherm Log Absolute Plot | Isotherm Pressure Composition
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NPT75 - Adsorption SiNPT75 - Desorption | SiNPT75 - Adsorption SiNPT75 - Desorption
Quantity AdsoAbsolute Pres Quantity Adso| Weight % N2 Absolute Pres Weight % N2
5.403267672 753.1326904 92.89490591 | 0.048213113 7.892577648 0.828897042
8.443159702 683.406311 85.55451492 | 0.075337932 84.38778687 0.763399065
9.79161895 608.8474121 30.74111089 | 0.087370173 157.8412933 0.274301541
10.91989316 536.281311 19.05851521 | 0.097437712 227.8468323 0.170057983
12.20610288 463.4060669 15.78018001 | 0.108914504 305.7987366 0.140805832
13.62650876 381.634613 13.63157616 | 0.121588721 380.4040527 0.121633937
15.45711041 295.9850159 11.97480343 | 0.137923097 454.4128113 0.106850629
18.54141403 230.397995 10.87722459 | 0.165444198 534.2842407 0.097056983
26.05197977 159.731369 9.724178732 | 0.232460637 614.2732544 0.086768407
73.8386881 83.61987305 8.293790711 | 0.658859272 691.3115234 0.074005119
92.89490591 6.633653641 5.025826995 | 0.828897042 753.1326904 0.044845227
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Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 |
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| Sample: SiNPT75 |
| Operator: NHA |
| Submitter: |
0\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\Jan |
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N2 | Started: 1/24/2019 3:1 Analysis AdsorN2 |
-195.850 °C | Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C |
No | Report Time: 1/24/2019 7:1 Thermal Correc No |
11.2525 cm³ M| Sample Mass:0.2904 g Warm Free Sp11.2525 cm³ M|
5s | Cold Free Spa32.4840 cm³ Equilibration In5 s |
1.000 g/cm³ | Low Pressure None Sample Densit1.000 g/cm³ |
| Automatic DegNo |
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| BET Surface Area Report |
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| BET Surface A33.8075 ± 0.4063 m²/g |
NPT75 - Desorption | Slope: 0.128250 ± 0.001520 g/cm³ STP |
Absolute Pres | Y-Intercept: 0.000515 ± 0.000290 g/cm³ STP |
753.1326904 | C: 250.216527 |
683.406311 | Qm: 7.7661 cm³/g STP |
608.8474121 | Correlation Coe
0.9998595 |
536.281311 | Molecular Cros0.1620 nm² |
463.4060669 | |
381.634613 | |
295.9850159 | |
230.397995 | |
159.731369 | Relative PressQuantity Adso1/[Q(Po/P - 1)] |
83.61987305 | 0.010384971 5.403267672 0.001942149 |
6.633653641 | 0.111036562 8.443159702 0.01479371 |
| 0.207685912 9.79161895 0.026770418 |
| 0.299798464 10.91989316 0.039209198 |
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TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020
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Sample: SiNPT75 | Sample: SiNPT75
Operator: NHA | Operator: NHA
File: C:\TriStar II 3020\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\J
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Started: 1/24/2019 3:1 Analysis AdsorN2 | Started: 1/24/2019 3:1
Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1
Report Time: 1/24/2019 7:1 Thermal Correc No | Report Time: 1/24/2019 7:1
Sample Mass:0.2904 g Warm Free Sp11.2525 cm³ M| Sample Mass:0.2904 g
Cold Free Spa32.4840 cm³ Equilibration In5 s | Cold Free Spa32.4840 cm³
Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure None
Automatic DegNo | Automatic DegNo
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BET Surface Area Plot | BET Isotherm Plot
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SiNPT75 Not Fitted | SiNPT75
Relative Press1/[Q(Po/P - 1)]Relative Press1/[Q(Po/P - 1)]| Relative PressQuantity Adso
0.010384971 0.001942149 | 0.010384971 5.403267672
0.111036562 0.01479371 | 0.111036562 8.443159702
0.207685912 0.026770418 | 0.207685912 9.79161895
0.299798464 0.039209198 | 0.299798464 10.91989316
| 0.402366759 12.20610288
| 0.500531648 13.62650876
| 0.597911594 15.45711041
| 0.70300558 18.54141403
| 0.808254282 26.05197977
| 0.909620426 73.8386881
| 0.990964066 92.89490591
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| Sample: SiNPT75
| Operator: NHA
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| Automatic DegNo
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| Langmuir Reports
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| Primary Data
SiNPT75 - BET Equation |
Relative PressQuantity Adso|
0.010384971 5.683213718 |
0.111036562 8.465297061 |
0.207685912 9.654624051 |
0.299798464 10.98869844 |
0.402366759 12.91811648 |
0.500531648 15.48701757 |
0.597911594 19.26269745 |
0.70300558 26.10498077 |
0.808254282 40.46383754 |
0.909620426 85.89375619 |
0.990964066 859.4397764 |
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| Freundlich Tabular Report | Freundlich Plot
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| Qm·C: 3.5126 ± 0.0740 cm³/g STP |
| m: 4.9009 ± 0.2620 | SiNPT75
| Correlation Coe
0.997154 | log(P)
| | 0.897218863
| | 1.926279597
| | 2.198220631
| | 2.357642995
| Absolute Pres Quantity Adsolog(P) log(Q) |
| 7.892577648 5.403267672 0.897218863 0.732656483 |
| 84.38778687 8.443159702 1.926279597 0.926505004 |
| 157.8412933 9.79161895 2.198220631 0.990854504 |
| 227.8468323 10.91989316 2.357642995 1.038218389 |
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NHA | Operator: NHA
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reundlich Plot | Temkin Tabular Report
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| q·alpha/Qm: 0.371572 ± 0.051938 kJ/mol·(cm³/g STP)
| A: 2.3734 ± 1.5946 1/mmHg
log(Q) | Correlation Coe
0.971921
0.732656483 |
0.926505004 |
0.990854504 |
1.038218389 |
| Absolute Pres Quantity Adsoln(P)
| 7.892577648 5.403267672 2.06592278
| 84.38778687 8.443159702 4.435422686
| 157.8412933 9.79161895 5.061590056
| 227.8468323 10.91989316 5.428673615
| 305.7987366 12.20610288 5.722927162
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| Sample: SiNPT75 |
| Operator: NHA |
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| Automatic DegNo |
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| Temkin Plot |
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1938 kJ/mol·(cm³/g STP) | |
| SiNPT75 |
| ln(P) Quantity Adsorbed (cm³/g STP) |
| 2.06592278 5.403267672 |
| 4.435422686 8.443159702 |
| 5.061590056 9.79161895 |
| 5.428673615 10.91989316 |
| 5.722927162 12.20610288 |
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t-Plot Report | t-Plot
| Harkins and Jura
Micropore Vol 0.001108 cm³/g |
Micropore Area2.0373 m²/g | SiNPT75
External Surfa31.7702 m²/g | Thickness (nmQuantity Adso
Slope: 20.539293 ± 0.000000 cm³/g·nm STP | 0.376195029 8.443159702
Y-Intercept: 0.716380 ± 0.000000 cm³/g STP | 0.441847689 9.79161895
Correlation Coe 1.000000 |
Surface Area C1.000 |
Density Conver0.0015468 |
Total Surface 33.8075 m²/g |
Thickness Ran0.35000 nm to 0.50000 nm |
Thickness Equa Harkins and Jura |
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Thickness Curve |
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t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 |
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t-Plot Report - Data |
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Relative PressStatistical Thi Quantity AdsoFitted |
0.010384971 0.263324877 5.403267672 |
0.111036562 0.376195029 8.443159702 * |
0.207685912 0.441847689 9.79161895 * |
0.299798464 0.501088877 10.91989316 |
0.402366759 0.570806632 12.20610288 |
0.500531648 0.64664565 13.62650876 |
0.597911594 0.737285649 15.45711041 |
0.70300558 0.864848795 18.54141403 |
0.808254282 1.051831155 26.05197977 |
0.909620426 1.364500977 73.8386881 |
0.990964066 1.920207729 92.89490591 |
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| Sample: SiNPT75
| Operator: NHA
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| Automatic DegNo
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| Alpha-S Method
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| 4029- At least two fitted data points are needed for Alpha
Not Fitted |
Thickness (nmQuantity Adso|
0.263324877 5.403267672 |
0.501088877 10.91989316 |
0.570806632 12.20610288 |
0.64664565 13.62650876 |
0.737285649 15.45711041 |
0.864848795 18.54141403 |
1.051831155 26.05197977 |
1.364500977 73.8386881 |
1.920207729 92.89490591 |
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| f-Ratio Method | BJH Adsorption Pore Distribution Repor
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| Primary Data |
| A reference file has not been chosen. |
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| Diameter Rang
| Adsorbate Prop
| Density Conver
| Fraction of Po
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| Pore Diameter
| 213.5 - 22.6
| 22.6 - 10.8
| 10.8 - 6.9
| 6.9 - 4.9
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TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020
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SiNPT75 | Sample:
NHA | Operator:
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNPT75.SMP | File:
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1/24/2019 3:1 Analysis AdsorN2 | Started:
1/24/2019 7:1 Analysis Bath -195.850 °C | Completed:
1/24/2019 7:1 Thermal Correc No | Report Time:
0.2904 g Warm Free Sp11.2525 cm³ Measured | Sample Mass:
32.4840 cm³ Equilibration In5 s | Cold Free Spa
None Sample Densit1.000 g/cm³ | Low Pressure
No | Automatic Deg
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JH Adsorption Pore Distribution Report | BJH Desorption Pore Distribution Repo
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Faas Correction |
Harkins and Jura |
t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 |
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1.7000 nm to 300.0000 nm | Diameter Rang
0.95300 nm | Adsorbate Prop
0.0015468 | Density Conver
0.00 | Fraction of Po
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Average Diame Incremental PoCumulative PoIncremental PoCumulative Por| Pore Diameter
24.36257367 0.036447018 0.036447018 5.984099792 5.984099792 | 213.4 - 20.1
12.77241912 0.098345755 0.134792773 30.79941354 36.78351333 | 20.1 - 10.2
7.926769199 0.008330647 0.143123419 4.203804436 40.98731777 | 10.2 - 6.8
5.53826243 0.000133 0.14325642 0.096059236 41.083377 |
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SiNPT75 | Sample:
NHA | Operator:
| Submitter:
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No | Automatic Deg
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JH Desorption Pore Distribution Report | Dollimore-Heal Adsorption Pore Distribu
|
Faas Correction |
Harkins and Jura |
t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 |
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| Diameter Rang
1.7000 nm to 300.0000 nm | Adsorbate Prop
0.95300 nm | Density Conver
0.0015468 |
0.00 |
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|
| Pore Diameter
| 213.8 - 22.8
Average Diame Incremental PoCumulative PoIncremental PoCumulative Por| 22.8 - 11.1
21.59279705 0.014079123 0.014079123 2.608114743 2.608114743 | 11.1 - 7.1
12.11425441 0.112328702 0.126407825 37.08976143 39.69787617 | 7.1 - 5.2
7.774270798 0.017572843 0.143980667 9.041538853 48.73941502 | 5.2 - 4.0
| 4.0 - 3.2
| 3.2 - 2.6
| 2.6 - 2.1
| 2.1 - 1.6
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SiNPT75 | Sample:
NHA | Operator:
| Submitter:
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No | Automatic Deg
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|
ollimore-Heal Adsorption Pore Distribution Report | Dollimore-Heal Desorption Pore Distribu
|
Harkins and Jura |
t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 |
|
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|
1.7000 nm to 300.0000 nm | Diameter Rang
0.95300 nm | Adsorbate Prop
0.0015468 | Density Conver
|
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|
Average Diame Incremental PoCumulative PoIncremental PoCumulative Por| Pore Diameter
118.3356792 0.030589421 0.030589421 1.033988094 1.033988094 | 213.8 - 20.6
16.95345884 0.092013908 0.122603329 21.70976655 22.74375464 | 20.6 - 10.7
9.097797198 0.011349433 0.133952763 4.989969817 27.73372446 | 10.7 - 7.2
6.159480521 0.002635101 0.136587863 1.711248793 29.44497325 | 7.2 - 5.4
4.613890393 0.000783098 0.137370962 0.678904875 30.12387813 | 5.4 - 4.1
3.641254524 0.000242739 0.137613701 0.266654352 30.39053248 | 4.1 - 3.1
2.909802717 9.81344E-05 0.137711835 0.134902014 30.5254345 | 3.1 - 2.6
2.340379983 0.000166679 0.137878514 0.284875267 30.81030976 | 2.6 - 2.1
1.857978127 0.000497005 0.13837552 1.069991497 31.88030126 | 2.1 - 1.6
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SiNPT75 | Sample:
NHA | Operator:
| Submitter:
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No | Automatic Deg
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|
ollimore-Heal Desorption Pore Distribution Report | Horvath-Kawazoe Report
|
Harkins and Jura |
t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 |
|
|
|
| Maximum Pore
1.7000 nm to 300.0000 nm | at Relative Pr
0.95300 nm | Median Pore W
0.0015468 | Relative Press
|
| Diameter of Ad
| Diameter of Ad
| Diameter of S
Average Diame Incremental PoCumulative PoIncremental PoCumulative Por| Diameter of Sa
117.203271 0.011760682 0.011760682 0.40137726 0.40137726 | Interaction Pa
15.62626975 0.107955008 0.11971569 27.63423634 28.0356136 |
8.935725452 0.020512637 0.140228327 9.182303992 37.21791759 | Density Conver
6.27809504 0.001950106 0.142178433 1.242482782 38.46040037 |
4.707611517 0 0.142178433 0 38.46040037 |
3.603672554 0 0.142178433 0 38.46040037 |
2.8739742 0 0.142178433 0 38.46040037 |
2.356178738 0 0.142178433 0 38.46040037 | Absolute Pres
1.86165859 0 0.142178433 0 38.46040037 | 7.892577648
| 84.38778687
| 157.8412933
| 227.8468323
| 305.7987366
| 380.4040527
| 454.4128113
| 534.2842407
| 614.2732544
| 691.3115234
| 753.1326904
|
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SiNPT75 | Sample:
NHA | Operator:
| Submitter:
|
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No | Automatic Deg
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|
orvath-Kawazoe Report |
|
Slit Pore Geometry (Original H-K) |
|
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|
|
0.143690 cm³/g |
0.990964066 |
25.5974 nm |
1.038e-002 to 9.910e-001 | Volume in Por
| Total Volume i
0.3000 nm | Area in Pores
0.2574 nm | Total Area in
0.3040 nm |
0.2609 nm |
3.49e-043 erg·cm^4 | Pore Size Table
|
0.0015468 | Pore Width (n
| 1.483289338
| 1.590515054
| 1.715611708
| 1.8585793
Relative PressQuantity AdsoPore Width (n Cumulative PoDifferential P | 2.001546978
0.010384971 5.403267672 1.029632 0.008357774 0.008117244 | 2.16238568
0.111036562 8.443159702 1.853816576 0.013059879 0.00570516 | 2.341095234
0.207685912 9.79161895 2.479583383 0.015145676 0.003333185 | 2.519804789
0.299798464 10.91989316 3.147643395 0.016890891 0.002612362 | 2.734256221
0.402366759 12.20610288 4.065780538 0.0188804 0.002166898 | 2.948707652
0.500531648 13.62650876 5.249991064 0.021077484 0.001855315 | 3.181030107
0.597911594 15.45711041 6.971728294 0.023909058 0.001644603 | 3.431223586
0.70300558 18.54141403 10.02753418 0.028679859 0.001561225 | 3.699287918
0.808254282 26.05197977 16.43308537 0.040297202 0.001813637 | 4.003093956
0.909620426 73.8386881 36.51758781 0.114213683 0.003680274 | 4.324771359
0.990964066 92.89490591 342.1367666 0.14368984 9.64473E-05 | 4.664319445
| 5.039609578
| 5.432770394
| 5.879544281
| 6.344189191
| 6.844575808
| 7.398575836
| 7.98831723
| 8.631671354
| 9.310767526
| 10.06134779
| 10.86554079
| 11.72334651
| 12.65263702
| 13.67128093
| 14.76140894
| 15.94089173
| 17.20973066
| 18.58579369
| 20.06908354
| 21.65959748
| 23.39307962
| 25.25166062
| 27.27107913
| 29.45133516
| 31.79242869
| 34.33010654
| 37.06436055
| 40.03094025
| 43.22984018
| 46.67893786
| 50.39609442
| 54.4170594
| 58.75969939
| 63.44189191
| 68.49937012
| 73.96788359
| 79.86529889
| 86.24523218
| 93.12554458
| 100.5598686
| 108.5660545
| 117.2334679
| 126.5799754
| 136.6770652
|
|
|
TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020
|
|
NHA | Operator: NHA
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNPT75. | File: C:\TriStar II 3020\data\SAMPEL\2019\J
|
|
1/24/2019 3:1 Analysis AdsorN2 | Started: 1/24/2019 3:1
1/24/2019 7:1 Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1
1/24/2019 7:1 Thermal Correc No | Report Time: 1/24/2019 7:1
0.2904 g Warm Free Sp11.2525 cm³ Measured | Sample Mass:0.2904 g
32.4840 cm³ Equilibration In5 s | Cold Free Spa32.4840 cm³
None Sample Densit1.000 g/cm³ | Low Pressure None
|
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|
Porosity Distribution by Original Density Functional Theor | Porosity Distribution by Original Density
Model: N2 @ 77K on Carbon, Slit Pores | Model: N2 @ 77K on Carbon, Slit Pores
Method: Non-negative Regularization: 0.00000 | Method: Non-negative Regularization:
Standard Deviation of Fit: 0.54492 cm³/g STP |
|
|
|
| Standard Deviation of Fit: 0.54492 cm³/
< 1.483 nm : 0.00136 cm³/ |
<= 136.677 nm : 0.14068 cm³/ |
> 136.677 nm : 0.000 m²/g | Isotherm Table
>= 1.483 nm : 20.738 m²/g | Relative Pressure
| (P/Po) Experimental
| 0.01178367 5.45684408
ore Size Table | 0.01451552 5.561272744
| 0.017706521 5.68280574
Cumulative VoIncremental VoCumulative AreIncremental Ar| 0.02139844 5.822656607
0.001363858 0 0 0| 0.02563123 5.981750036
0.00156081 0.000196952 0.247657552 0.247657552 | 0.03044224 6.160600367
0.00156081 0 0.247657552 0| 0.035865448 6.359166895
0.00156081 0 0.247657552 0| 0.041930798 6.576687103
0.00156081 0 0.247657552 0| 0.048663601 6.811487599
0.00156081 0 0.247657552 0| 0.056084011 7.060774909
0.00156081 0 0.247657552 0| 0.064206667 7.320414837
0.00156081 0 0.247657552 0| 0.073040441 7.584705146
0.00156081 0 0.247657552 0| 0.082588248 7.846150941
0.00156081 0 0.247657552 0| 0.092847057 8.09525804
0.00156081 0 0.247657552 0| 0.103808001 8.320354546
0.00156081 0 0.247657552 0| 0.115456402 8.511353206
0.00156081 0 0.247657552 0| 0.127772301 8.698306133
0.00156081 0 0.247657552 0| 0.140730694 8.889999212
0.00156081 0 0.247657552 0| 0.154301897 9.08504996
0.00156081 0 0.247657552 0| 0.168452203 9.281980468
0.001968401 0.000407591 0.409412661 0.161755109 | 0.183144197 9.479235962
0.002659964 0.000691563 0.664002224 0.254589563 | 0.198337302 9.675208265
0.003612367 0.000952403 0.987973894 0.323971669 | 0.213988706 9.868930168
0.004426832 0.000814464 1.24473307 0.256759177 | 0.230053101 10.06541718
0.00522348 0.000796649 1.477515569 0.232782499 | 0.246484801 10.26595972
0.006507632 0.001284151 1.824650234 0.347134665 | 0.263235897 10.47049035
0.008492746 0.001985114 2.32165464 0.497004406 | 0.280259013 10.6789992
0.011961887 0.003469141 3.125471412 0.803816772 | 0.297506303 10.89152092
0.016676578 0.004714691 4.138210861 1.012739449 | 0.314930797 11.10772099
0.025699901 0.009023323 5.931871803 1.793660943 | 0.332486212 11.32658894
0.039494255 0.013794354 8.470973099 2.539101296 | 0.35012731 11.54746993
0.054888331 0.015394076 11.09719862 2.626225518 | 0.367810607 11.76972606
0.069820363 0.014932032 13.45750209 2.360303472 | 0.385494202 11.99272959
0.083024888 0.013204525 15.38921938 1.931717287 | 0.40313831 12.21588979
0.093821545 0.010796657 16.85204143 1.462822053 | 0.420704991 12.44766045
0.10193734 0.008115795 17.87027743 1.018236001 | 0.4381589 12.69232544
0.107374398 0.005437058 18.50213606 0.631858625 | 0.455466807 12.94538034
0.110933207 0.003558808 18.88509611 0.382960052 | 0.472598106 13.20246974
0.114036275 0.003103068 19.19433475 0.30923864 | 0.489524394 13.4594489
0.116854162 0.002817887 19.45453228 0.260197531 | 0.506219923 13.71467588
0.119414599 0.002560438 19.67343784 0.218905559 | 0.522661209 13.99032289
0.121739901 0.002325302 19.85760803 0.184170191 | 0.5388273 14.28581384
0.12384906 0.002109159 20.01228906 0.154681036 | 0.5546996 14.59257696
0.125303476 0.001454416 20.11105645 0.09876739 | 0.570261598 14.90278579
0.126639834 0.001336358 20.19512416 0.084067706 | 0.585499227 15.2094114
0.12827875 0.001638916 20.29060394 0.095479783 | 0.60040009 15.50739457
0.129764951 0.001486202 20.37079967 0.080195729 | 0.614954293 15.84036301
0.131113717 0.001348766 20.43818583 0.067386158 | 0.629153311 16.2193967
0.132045269 0.000931552 20.48128346 0.043097636 | 0.642990828 16.62758203
0.132902616 0.000857347 20.51801724 0.036733774 | 0.656461716 17.05
0.133955117 0.001052502 20.55978641 0.041769177 | 0.669562697 17.4737588
0.134908751 0.000953634 20.5948355 0.035049084 | 0.682291925 17.88774551
0.135567168 0.000658417 20.61724599 0.022410496 | 0.694648683 18.28266255
0.136173333 0.000606165 20.63635528 0.019109291 | 0.706633508 18.65459429
0.136918387 0.000745054 20.65810888 0.021753595 | 0.71824801 19.05917644
0.137433215 0.000514828 20.67202918 0.013920302 | 0.729494929 19.52416064
0.137907397 0.000474183 20.68390374 0.01187456 | 0.740377605 20.05679288
0.138489938 0.000582541 20.69741269 0.013508944 | 0.750900388 20.66196214
0.139018386 0.000528448 20.70876184 0.011349149 | 0.761068285 21.34248066
0.139383657 0.000365271 20.71602657 0.007264738 | 0.770887017 22.09937127
0.139720218 0.000336561 20.72222669 0.006200118 | 0.780362606 22.93210286
0.140134158 0.00041394 20.72928851 0.007061814 | 0.789501607 23.83885368
0.140420299 0.00028614 20.73380961 0.0045211 | 0.798311174 24.81675478
0.140683878 0.000263579 20.73766657 0.003856967 | 0.806798697 25.86206911
| 0.814971626 27.3268763
| 0.822837889 29.72025776
| 0.830405474 32.7942176
| 0.837682605 36.32594671
| 0.844677329 40.13023798
| 0.851397991 44.05503194
| 0.857852995 47.97706474
| 0.864050388 51.79775566
| 0.869998574 55.4401887
| 0.875705481 58.84551887
| 0.881179392 61.97073119
| 0.886428118 64.78571091
| 0.891459525 67.27142033
| 0.896281302 69.41788297
| 0.9009009 71.22253295
| 0.90532577 72.68889207
| 0.909563184 73.82525186
| 0.913620114 74.77568746
| 0.917503417 75.68542118
| 0.921219707 76.55602927
| 0.924775481 77.38903375
| 0.928177178 78.18594267
| 0.931430817 78.94816634
| 0.934542298 79.67708715
| 0.937517405 80.37405955
| 0.940361619 81.04036818
| 0.943080306 81.67726975
| 0.945678592 82.28596512
| 0.948161721 82.86768308
| 0.950534225 83.42348485
| 0.95280093 83.95450146
| 0.954966187 84.46175226
| 0.957034409 84.94627054
| 0.959009588 85.40899185
| 0.960896015 85.85092156
| 0.962697208 86.27288351
| 0.964416981 86.67577137
| 0.96605891 87.06042295
| 0.967626274 87.42760622
| 0.969122529 87.77813109
| 0.970550597 88.11268175
| 0.971913695 88.43201224
| 0.973214507 88.7367509
| 0.974455774 89.02754006
| 0.975640416 89.30506393
| 0.976770699 89.56985312
| 0.977849126 89.8224941
| 0.978878021 90.06353143
| 0.979859591 90.29348178
| 0.980795979 90.51284781
| 0.981689274 90.72211827
| 0.982541502 90.92176789
| 0.98335427 91.1121737
| 0.984129488 91.29378253
| 0.984869003 91.46702724
| 0.985574186 91.632229
| 0.986246824 91.7898067
| 0.986888289 91.94
| 0.987500012 92.08338856
| 0.988083303 92.22
| 0.988639593 92.35035605
| 0.989170074 92.47463089
| 0.989675879 92.59312485
| 0.9901582 92.70611721
| 0.99061811 92.81385931
|
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Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108
|
|
| Sample: SiNPT75
| Operator: NHA
| Submitter:
:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNPT75. | File: C:\TriStar II 3020\data\SAMPEL\2019\Jan
|
|
Analysis AdsorN2 | Started: 1/24/2019 3:1 Analysis Adsor
Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1 Analysis Bath
Thermal Correc No | Report Time: 1/24/2019 7:1 Thermal Correc
Warm Free Sp11.2525 cm³ Measured | Sample Mass:0.2904 g Warm Free Sp
Equilibration In5 s | Cold Free Spa32.4840 cm³ Equilibration In
Sample Densit1.000 g/cm³ | Low Pressure None Sample Densit
| Automatic DegNo
|
|
|
|
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|
|
| Cumulative Surface Area vs. Pore Width
|
orosity Distribution by Original Density Functional Theor |
odel: N2 @ 77K on Carbon, Slit Pores | Cumulative Surface Area
ethod: Non-negative Regularization: 0.00000 | Pore Width (n Cumulative Surface Area (m²/g)
| 1.483289338 0
| 1.590515054 0.247657552
| 1.715611708 0.247657552
| 1.8585793 0.247657552
tandard Deviation of Fit: 0.54492 cm³/g STP | 2.001546978 0.247657552
| 2.16238568 0.247657552
| 2.341095234 0.247657552
| 2.519804789 0.247657552
| 2.734256221 0.247657552
Fitted Quantit Absolute ResidRelative Resid| 2.948707652 0.247657552
5.534967785 -0.07812371 -0.01431665 | 3.181030107 0.247657552
5.639772202 -0.07849946 -0.01411538 | 3.431223586 0.247657552
5.746809505 -0.06400376 -0.01126271 | 3.699287918 0.247657552
5.858415613 -0.03575901 -0.00614136 | 4.003093956 0.247657552
5.977404716 0.004345321 0.00072643 | 4.324771359 0.247657552
6.156120737 0.00447963 0.000727142 | 4.664319445 0.247657552
6.296730446 0.062436448 0.009818338 | 5.039609578 0.409412661
6.452401503 0.124285601 0.018897904 | 5.432770394 0.664002224
6.627402708 0.184084891 0.027025652 | 5.879544281 0.987973894
6.825961856 0.234813053 0.033255989 | 6.344189191 1.24473307
7.051329725 0.269085112 0.036758178 | 6.844575808 1.477515569
7.303771389 0.280933757 0.037039509 | 7.398575836 1.824650234
7.578119689 0.268031252 0.034160859 | 7.98831723 2.32165464
7.863404989 0.23185305 0.0286406 | 8.631671354 3.125471412
8.146647661 0.173706884 0.020877342 | 9.310767526 4.138210861
8.41804358 0.093309627 0.01096296 | 10.06134779 5.931871803
8.673058698 0.025247435 0.002902569 | 10.86554079 8.470973099
8.911277269 -0.02127806 -0.00239348 | 11.72334651 11.09719862
9.134479418 -0.04942946 -0.00544075 | 12.65263702 13.45750209
9.345289203 -0.06330874 -0.00682061 | 13.67128093 15.38921938
9.546492783 -0.06725682 -0.00709517 | 14.76140894 16.85204143
9.740768294 -0.06556003 -0.00677608 | 15.94089173 17.87027743
9.930629233 -0.06169907 -0.00625185 | 17.20973066 18.50213606
10.11843119 -0.05301401 -0.00526695 | 18.58579369 18.88509611
10.30643262 -0.0404729 -0.00394244 | 20.06908354 19.19433475
10.49683997 -0.02634963 -0.00251656 | 21.65959748 19.45453228
10.69185931 -0.01286011 -0.00120424 | 23.39307962 19.67343784
10.89369493 -0.002174 -0.0001996 | 25.25166062 19.85760803
11.10451559 0.003205404 0.000288574 | 27.27107913 20.01228906
11.32629164 0.00029729 2.62471E-05 | 29.45133516 20.11105645
11.56049467 -0.01302474 -0.00112793 | 31.79242869 20.19512416
11.80760893 -0.03788287 -0.00321867 | 34.33010654 20.29060394
12.06655445 -0.07382486 -0.0061558 | 37.06436055 20.37079967
12.33436762 -0.11847782 -0.00969866 | 40.03094025 20.43818583
12.60653982 -0.15887937 -0.01276379 | 43.22984018 20.48128346
12.87812386 -0.18579842 -0.01463864 | 46.67893786 20.51801724
13.14502367 -0.19964333 -0.01542197 | 50.39609442 20.55978641
13.40476139 -0.20229164 -0.01532226 | 54.4170594 20.5948355
13.6565159 -0.197067 -0.01464154 | 58.75969939 20.61724599
13.90072606 -0.18605017 -0.01356577 | 63.44189191 20.63635528
14.13863103 -0.14830814 -0.01060077 | 68.49937012 20.65810888
14.37191156 -0.08609772 -0.0060268 | 73.96788359 20.67202918
14.60246644 -0.00988948 -0.00067771 | 79.86529889 20.68390374
14.83231007 0.07047572 0.00472903 | 86.24523218 20.69741269
15.22223112 -0.01281971 -0.00084288 | 93.12554458 20.70876184
15.45546276 0.051931816 0.003348842 | 100.5598686 20.71602657
15.9705226 -0.13015959 -0.00821696 | 108.5660545 20.72222669
16.21387844 0.005518262 0.000340226 | 117.2334679 20.72928851
16.46559797 0.16198406 0.009741889 | 126.5799754 20.73380961
17.11402335 -0.06400826 -0.00375415 | 136.6770652 20.73766657
17.38003906 0.093686687 0.005361565 |
17.99192143 -0.10417592 -0.00582387 |
18.26589541 0.016767143 0.000917106 |
18.54027495 0.114319337 0.006128214 |
19.14799887 -0.08882243 -0.00466035 |
19.41219327 0.111967371 0.005734811 |
20.22467031 -0.16787742 -0.0083701 |
20.47380899 0.188153152 0.009106258 |
21.59366045 -0.25117978 -0.01176901 |
21.82997121 0.269400064 0.012190395 |
23.62758802 -0.69548516 -0.03032802 |
23.85483195 -0.01597827 -0.00067026 |
24.08429512 0.732459652 0.029514723 |
26.47292544 -0.61085633 -0.02361978 |
26.70096573 0.625910566 0.022904578 |
31.13875817 -1.41850041 -0.0477284 |
31.3589684 1.435249199 0.043765313 |
38.12109634 -1.79514963 -0.04941783 |
38.31886402 1.811373963 0.045137384 |
45.9269022 -1.87187026 -0.04248936 |
46.09099469 1.886070047 0.03931191 |
53.54892385 -1.75116819 -0.0338078 |
53.67761356 1.762575139 0.031792373 |
60.35390914 -1.50839027 -0.02563305 |
60.45372829 1.517002902 0.024479345 |
65.98574023 -1.2000293 -0.01852306 |
66.06501667 1.20640366 0.017933376 |
70.28504576 -0.86716279 -0.01249192 |
70.35074921 0.871783742 0.01224028 |
73.22675119 -0.53785912 -0.00739947 |
73.28413396 0.541117901 0.007329713 |
75.20323676 -0.42754929 -0.00571776 |
75.25523636 0.430184819 0.005683853 |
76.94815432 -0.39212505 -0.00512207 |
76.99467275 0.394360994 0.005095825 |
78.54589565 -0.35995298 -0.00460381 |
78.58634843 0.36181791 0.004582981 |
80.0074199 -0.33033275 -0.00414589 |
80.04220254 0.331857008 0.004128907 |
81.34307517 -0.30270699 -0.00373526 |
81.37329569 0.303974063 0.003721648 |
82.56291814 -0.27695301 -0.00336574 |
82.58965857 0.278024513 0.003355041 |
83.42297217 0.000512674 6.14543E-06 |
84.19622654 -0.24172507 -0.00287924 |
84.21918571 0.242566551 0.00287191 |
85.1669046 -0.22063405 -0.00259734 |
85.18762889 0.221362958 0.002591799 |
86.05246929 -0.20154774 -0.00234765 |
86.0707234 0.202160112 0.002343264 |
86.859927 -0.18415563 -0.00212465 |
86.87576602 0.184656921 0.00212102 |
87.42738116 0.000225063 2.57427E-06 |
87.93869067 -0.16055958 -0.00182915 |
87.95175031 0.160931443 0.001826428 |
88.57835958 -0.14634734 -0.00165491 |
88.59 0.146669488 0.001652861 |
89.16085869 -0.13331863 -0.0014975 |
89.1714612 0.133602736 0.001496026 |
89.56973299 0.000120136 1.34125E-06 |
89.93846956 -0.11597547 -0.00129116 |
89.94733839 0.11619304 0.001290123 |
90.39919514 -0.10571336 -0.00117078 |
90.40695615 0.105891661 0.001169908 |
90.72204179 7.64767E-05 8.42978E-07 |
91.01367036 -0.09190247 -0.00101079 |
91.02013613 0.092037573 0.001010157 |
91.37745073 -0.0836682 -0.00091647 |
91.38324009 0.083787149 0.000916037 |
91.70838703 -0.07615804 -0.00083113 |
91.71354433 0.076262376 0.000830837 |
91.94 4.03173E-05 4.38517E-07 |
92.14955563 -0.06616707 -0.00071856 |
92.15379183 0.066243196 0.000718317 |
92.41059783 -0.06024178 -0.00065232 |
92.41432542 0.060305472 0.00065213 |
92.59309921 2.56412E-05 2.76923E-07 |
92.7582965 -0.05217929 -0.00056285 |
92.76137615 0.05248316 0.000565467 |
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| Sample: SiNPT75 |
| Operator: NHA |
| Submitter: |
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| Automatic DegNo |
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| Incremental Surface Area vs. Pore Width |
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| Incremental Surface Area |
ace Area (m²/g) | Pore Width (n Incremental Surface Area (m²/g) |
| 1.483289338 0 |
| 1.590515054 0.247657552 |
| 1.715611708 0 |
| 1.8585793 0 |
| 2.001546978 0 |
| 2.16238568 0 |
| 2.341095234 0 |
| 2.519804789 0 |
| 2.734256221 0 |
| 2.948707652 0 |
| 3.181030107 0 |
| 3.431223586 0 |
| 3.699287918 0 |
| 4.003093956 0 |
| 4.324771359 0 |
| 4.664319445 0 |
| 5.039609578 0.161755109 |
| 5.432770394 0.254589563 |
| 5.879544281 0.323971669 |
| 6.344189191 0.256759177 |
| 6.844575808 0.232782499 |
| 7.398575836 0.347134665 |
| 7.98831723 0.497004406 |
| 8.631671354 0.803816772 |
| 9.310767526 1.012739449 |
| 10.06134779 1.793660943 |
| 10.86554079 2.539101296 |
| 11.72334651 2.626225518 |
| 12.65263702 2.360303472 |
| 13.67128093 1.931717287 |
| 14.76140894 1.462822053 |
| 15.94089173 1.018236001 |
| 17.20973066 0.631858625 |
| 18.58579369 0.382960052 |
| 20.06908354 0.30923864 |
| 21.65959748 0.260197531 |
| 23.39307962 0.218905559 |
| 25.25166062 0.184170191 |
| 27.27107913 0.154681036 |
| 29.45133516 0.09876739 |
| 31.79242869 0.084067706 |
| 34.33010654 0.095479783 |
| 37.06436055 0.080195729 |
| 40.03094025 0.067386158 |
| 43.22984018 0.043097636 |
| 46.67893786 0.036733774 |
| 50.39609442 0.041769177 |
| 54.4170594 0.035049084 |
| 58.75969939 0.022410496 |
| 63.44189191 0.019109291 |
| 68.49937012 0.021753595 |
| 73.96788359 0.013920302 |
| 79.86529889 0.01187456 |
| 86.24523218 0.013508944 |
| 93.12554458 0.011349149 |
| 100.5598686 0.007264738 |
| 108.5660545 0.006200118 |
| 117.2334679 0.007061814 |
| 126.5799754 0.0045211 |
| 136.6770652 0.003856967 |
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Differential Surface Area vs. Pore Width | Cumulative Pore Volume vs. Pore Width
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Differential Surface Area | Cumulative Pore Volume
Pore Width (n Differential Surface Area (m²/g) | Pore Width (n Cumulative Pore Volume (cm³/g)
1.483289338 0 | 1.483289338 0.001363858
1.590515054 7.838116776 | 1.590515054 0.00156081
1.715611708 0 | 1.715611708 0.00156081
1.8585793 0 | 1.8585793 0.00156081
2.001546978 0 | 2.001546978 0.00156081
2.16238568 0 | 2.16238568 0.00156081
2.341095234 0 | 2.341095234 0.00156081
2.519804789 0 | 2.519804789 0.00156081
2.734256221 0 | 2.734256221 0.00156081
2.948707652 0 | 2.948707652 0.00156081
3.181030107 0 | 3.181030107 0.00156081
3.431223586 0 | 3.431223586 0.00156081
3.699287918 0 | 3.699287918 0.00156081
4.003093956 0 | 4.003093956 0.00156081
4.324771359 0 | 4.324771359 0.00156081
4.664319445 0 | 4.664319445 0.00156081
5.039609578 4.884421704 | 5.039609578 0.001968401
5.432770394 7.605730716 | 5.432770394 0.002659964
5.879544281 9.619857538 | 5.879544281 0.003612367
6.344189191 7.780242505 | 6.344189191 0.004426832
6.844575808 6.972458059 | 6.844575808 0.00522348
7.398575836 10.34543443 | 7.398575836 0.006507632
7.98831723 14.84774932 | 7.98831723 0.008492746
8.631671354 24.16397404 | 8.631671354 0.011961887
9.310767526 30.4302945 | 9.310767526 0.016676578
10.06134779 53.48953568 | 10.06134779 0.025699901
10.86554079 76.48420686 | 10.86554079 0.039494255
11.72334651 79.42650323 | 11.72334651 0.054888331
12.65263702 70.71264588 | 12.65263702 0.069820363
13.67128093 57.70905728 | 13.67128093 0.083024888
14.76140894 43.8604916 | 14.76140894 0.093821545
15.94089173 30.55643262 | 15.94089173 0.10193734
17.20973066 18.95523753 | 17.20973066 0.107374398
18.58579369 11.47386251 | 18.58579369 0.110933207
20.06908354 9.304710036 | 20.06908354 0.114036275
21.65959748 7.818452084 | 21.65959748 0.116854162
23.39307962 6.569837832 | 23.39307962 0.119414599
25.25166062 5.529397248 | 25.25166062 0.121739901
27.27107913 4.630125975 | 27.27107913 0.12384906
29.45133516 2.965035737 | 29.45133516 0.125303476
31.79242869 2.52568723 | 31.79242869 0.126639834
34.33010654 2.865849071 | 34.33010654 0.12827875
37.06436055 2.40392565 | 37.06436055 0.129764951
40.03094025 2.016730914 | 40.03094025 0.131113717
43.22984018 1.291795375 | 43.22984018 0.132045269
46.67893786 1.10289689 | 46.67893786 0.132902616
50.39609442 1.25406405 | 50.39609442 0.133955117
54.4170594 1.051219947 | 54.4170594 0.134908751
58.75969939 0.672573263 | 58.75969939 0.135567168
63.44189191 0.573792154 | 63.44189191 0.136173333
68.49937012 0.652603944 | 68.49937012 0.136918387
73.96788359 0.417578522 | 73.96788359 0.137433215
79.86529889 0.356102004 | 79.86529889 0.137907397
86.24523218 0.405000802 | 86.24523218 0.138489938
93.12554458 0.34035739 | 93.12554458 0.139018386
100.5598686 0.218077694 | 100.5598686 0.139383657
108.5660545 0.186114528 | 108.5660545 0.139720218
117.2334679 0.211840793 | 117.2334679 0.140134158
126.5799754 0.135679061 | 126.5799754 0.140420299
136.6770652 0.115718363 | 136.6770652 0.140683878
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| Sample: SiNPT75
| Operator: NHA
| Submitter:
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| Automatic DegNo
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e Volume vs. Pore Width | Incremental Pore Volume vs. Pore Width
|
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| Incremental Pore Volume
umulative Pore Volume (cm³/g) | Pore Width (n Incremental Pore Volume (cm³/g)
| 1.483289338 0
| 1.590515054 0.000196952
| 1.715611708 0
| 1.8585793 0
| 2.001546978 0
| 2.16238568 0
| 2.341095234 0
| 2.519804789 0
| 2.734256221 0
| 2.948707652 0
| 3.181030107 0
| 3.431223586 0
| 3.699287918 0
| 4.003093956 0
| 4.324771359 0
| 4.664319445 0
| 5.039609578 0.000407591
| 5.432770394 0.000691563
| 5.879544281 0.000952403
| 6.344189191 0.000814464
| 6.844575808 0.000796649
| 7.398575836 0.001284151
| 7.98831723 0.001985114
| 8.631671354 0.003469141
| 9.310767526 0.004714691
| 10.06134779 0.009023323
| 10.86554079 0.013794354
| 11.72334651 0.015394076
| 12.65263702 0.014932032
| 13.67128093 0.013204525
| 14.76140894 0.010796657
| 15.94089173 0.008115795
| 17.20973066 0.005437058
| 18.58579369 0.003558808
| 20.06908354 0.003103068
| 21.65959748 0.002817887
| 23.39307962 0.002560438
| 25.25166062 0.002325302
| 27.27107913 0.002109159
| 29.45133516 0.001454416
| 31.79242869 0.001336358
| 34.33010654 0.001638916
| 37.06436055 0.001486202
| 40.03094025 0.001348766
| 43.22984018 0.000931552
| 46.67893786 0.000857347
| 50.39609442 0.001052502
| 54.4170594 0.000953634
| 58.75969939 0.000658417
| 63.44189191 0.000606165
| 68.49937012 0.000745054
| 73.96788359 0.000514828
| 79.86529889 0.000474183
| 86.24523218 0.000582541
| 93.12554458 0.000528448
| 100.5598686 0.000365271
| 108.5660545 0.000336561
| 117.2334679 0.00041394
| 126.5799754 0.00028614
| 136.6770652 0.000263579
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| Differential Pore Volume vs. Pore Width | Goodness of Fit
| | Standard Deviation of Fit: 0.54492 cm³/
| |
| Differential Pore Volume | Input Data
| Pore Width (n Differential Pore Volume (cm³/g) | Relative Press
| 1.483289338 0 | 0.010384971
| 1.590515054 0.006233321 | 0.111036562
| 1.715611708 0 | 0.207685912
| 1.8585793 0 | 0.299798464
| 2.001546978 0 | 0.402366759
| 2.16238568 0 | 0.500531648
| 2.341095234 0 | 0.597911594
| 2.519804789 0 | 0.70300558
| 2.734256221 0 | 0.808254282
| 2.948707652 0 | 0.909620426
| 3.181030107 0 | 0.990964066
| 3.431223586 0 |
| 3.699287918 0 |
| 4.003093956 0 |
| 4.324771359 0 |
| 4.664319445 0 |
| 5.039609578 0.012307789 |
| 5.432770394 0.020660094 |
| 5.879544281 0.028280189 |
| 6.344189191 0.024679665 |
| 6.844575808 0.023861759 |
| 7.398575836 0.038270741 |
| 7.98831723 0.059304266 |
| 8.631671354 0.104287741 |
| 9.310767526 0.141664699 |
| 10.06134779 0.269088411 |
| 10.86554079 0.415521135 |
| 11.72334651 0.46557221 |
| 12.65263702 0.44735072 |
| 13.67128093 0.394478367 |
| 14.76140894 0.323721326 |
| 15.94089173 0.243548392 |
| 17.20973066 0.163107266 |
| 18.58579369 0.106625421 |
| 20.06908354 0.093368501 |
| 21.65959748 0.084672263 |
| 23.39307962 0.07684437 |
| 25.25166062 0.069813231 |
| 27.27107913 0.063134266 |
| 29.45133516 0.043662131 |
| 31.79242869 0.040148866 |
| 34.33010654 0.049192452 |
| 37.06436055 0.044549984 |
| 40.03094025 0.040365817 |
| 43.22984018 0.027922054 |
| 46.67893786 0.025741028 |
| 50.39609442 0.031599965 |
| 54.4170594 0.028602149 |
| 58.75969939 0.019760101 |
| 63.44189191 0.01820123 |
| 68.49937012 0.02235148 |
| 73.96788359 0.0154437 |
| 79.86529889 0.014220097 |
| 86.24523218 0.017464694 |
| 93.12554458 0.015847984 |
| 100.5598686 0.010964932 |
| 108.5660545 0.01010286 |
| 117.2334679 0.012417415 |
| 126.5799754 0.008587126 |
| 136.6770652 0.007908023 |
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NHA | Operator: NHA
| Submitter:
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oodness of Fit | Goodness of Fit
tandard Deviation of Fit: 0.54492 cm³/g STP | Standard Deviation of Fit: 0.54492 cm³/g STP
|
Model Fit | Input Data Model Fit
Quantity AdsoRelative PressQuantity Adso| Relative PressQuantity AdsoRelative Press
5.403267672 0.01178367 5.534967785 | 0.010384971 5.403267672 0.01178367
8.443159702 0.01451552 5.639772202 | 0.111036562 8.443159702 0.01451552
9.79161895 0.017706521 5.746809505 | 0.207685912 9.79161895 0.017706521
10.91989316 0.02139844 5.858415613 | 0.299798464 10.91989316 0.02139844
12.20610288 0.02563123 5.977404716 | 0.402366759 12.20610288 0.02563123
13.62650876 0.03044224 6.156120737 | 0.500531648 13.62650876 0.03044224
15.45711041 0.035865448 6.296730446 | 0.597911594 15.45711041 0.035865448
18.54141403 0.041930798 6.452401503 | 0.70300558 18.54141403 0.041930798
26.05197977 0.048663601 6.627402708 | 0.808254282 26.05197977 0.048663601
73.8386881 0.056084011 6.825961856 | 0.909620426 73.8386881 0.056084011
92.89490591 0.064206667 7.051329725 | 0.990964066 92.89490591 0.064206667
0.073040441 7.303771389 | 0.073040441
0.082588248 7.578119689 | 0.082588248
0.092847057 7.863404989 | 0.092847057
0.103808001 8.146647661 | 0.103808001
0.115456402 8.41804358 | 0.115456402
0.127772301 8.673058698 | 0.127772301
0.140730694 8.911277269 | 0.140730694
0.154301897 9.134479418 | 0.154301897
0.168452203 9.345289203 | 0.168452203
0.183144197 9.546492783 | 0.183144197
0.198337302 9.740768294 | 0.198337302
0.213988706 9.930629233 | 0.213988706
0.230053101 10.11843119 | 0.230053101
0.246484801 10.30643262 | 0.246484801
0.263235897 10.49683997 | 0.263235897
0.280259013 10.69185931 | 0.280259013
0.297506303 10.89369493 | 0.297506303
0.314930797 11.10451559 | 0.314930797
0.332486212 11.32629164 | 0.332486212
0.35012731 11.56049467 | 0.35012731
0.367810607 11.80760893 | 0.367810607
0.385494202 12.06655445 | 0.385494202
0.40313831 12.33436762 | 0.40313831
0.420704991 12.60653982 | 0.420704991
0.4381589 12.87812386 | 0.4381589
0.455466807 13.14502367 | 0.455466807
0.472598106 13.40476139 | 0.472598106
0.489524394 13.6565159 | 0.489524394
0.506219923 13.90072606 | 0.506219923
0.522661209 14.13863103 | 0.522661209
0.5388273 14.37191156 | 0.5388273
0.5546996 14.60246644 | 0.5546996
0.570261598 14.83231007 | 0.570261598
0.585499227 15.22223112 | 0.585499227
0.60040009 15.45546276 | 0.60040009
0.614954293 15.9705226 | 0.614954293
0.629153311 16.21387844 | 0.629153311
0.642990828 16.46559797 | 0.642990828
0.656461716 17.11402335 | 0.656461716
0.669562697 17.38003906 | 0.669562697
0.682291925 17.99192143 | 0.682291925
0.694648683 18.26589541 | 0.694648683
0.706633508 18.54027495 | 0.706633508
0.71824801 19.14799887 | 0.71824801
0.729494929 19.41219327 | 0.729494929
0.740377605 20.22467031 | 0.740377605
0.750900388 20.47380899 | 0.750900388
0.761068285 21.59366045 | 0.761068285
0.770887017 21.82997121 | 0.770887017
0.780362606 23.62758802 | 0.780362606
0.789501607 23.85483195 | 0.789501607
0.798311174 24.08429512 | 0.798311174
0.806798697 26.47292544 | 0.806798697
0.814971626 26.70096573 | 0.814971626
0.822837889 31.13875817 | 0.822837889
0.830405474 31.3589684 | 0.830405474
0.837682605 38.12109634 | 0.837682605
0.844677329 38.31886402 | 0.844677329
0.851397991 45.9269022 | 0.851397991
0.857852995 46.09099469 | 0.857852995
0.864050388 53.54892385 | 0.864050388
0.869998574 53.67761356 | 0.869998574
0.875705481 60.35390914 | 0.875705481
0.881179392 60.45372829 | 0.881179392
0.886428118 65.98574023 | 0.886428118
0.891459525 66.06501667 | 0.891459525
0.896281302 70.28504576 | 0.896281302
0.9009009 70.35074921 | 0.9009009
0.90532577 73.22675119 | 0.90532577
0.909563184 73.28413396 | 0.909563184
0.913620114 75.20323676 | 0.913620114
0.917503417 75.25523636 | 0.917503417
0.921219707 76.94815432 | 0.921219707
0.924775481 76.99467275 | 0.924775481
0.928177178 78.54589565 | 0.928177178
0.931430817 78.58634843 | 0.931430817
0.934542298 80.0074199 | 0.934542298
0.937517405 80.04220254 | 0.937517405
0.940361619 81.34307517 | 0.940361619
0.943080306 81.37329569 | 0.943080306
0.945678592 82.56291814 | 0.945678592
0.948161721 82.58965857 | 0.948161721
0.950534225 83.42297217 | 0.950534225
0.95280093 84.19622654 | 0.95280093
0.954966187 84.21918571 | 0.954966187
0.957034409 85.1669046 | 0.957034409
0.959009588 85.18762889 | 0.959009588
0.960896015 86.05246929 | 0.960896015
0.962697208 86.0707234 | 0.962697208
0.964416981 86.859927 | 0.964416981
0.96605891 86.87576602 | 0.96605891
0.967626274 87.42738116 | 0.967626274
0.969122529 87.93869067 | 0.969122529
0.970550597 87.95175031 | 0.970550597
0.971913695 88.57835958 | 0.971913695
0.973214507 88.59 | 0.973214507
0.974455774 89.16085869 | 0.974455774
0.975640416 89.1714612 | 0.975640416
0.976770699 89.56973299 | 0.976770699
0.977849126 89.93846956 | 0.977849126
0.978878021 89.94733839 | 0.978878021
0.979859591 90.39919514 | 0.979859591
0.980795979 90.40695615 | 0.980795979
0.981689274 90.72204179 | 0.981689274
0.982541502 91.01367036 | 0.982541502
0.98335427 91.02013613 | 0.98335427
0.984129488 91.37745073 | 0.984129488
0.984869003 91.38324009 | 0.984869003
0.985574186 91.70838703 | 0.985574186
0.986246824 91.71354433 | 0.986246824
0.986888289 91.94 | 0.986888289
0.987500012 92.14955563 | 0.987500012
0.988083303 92.15379183 | 0.988083303
0.988639593 92.41059783 | 0.988639593
0.989170074 92.41432542 | 0.989170074
0.989675879 92.59309921 | 0.989675879
0.9901582 92.7582965 | 0.9901582
0.99061811 92.76137615 | 0.99061811
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| Sample: SiNPT75 |
| Operator: NHA |
| Submitter: |
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| Automatic DegNo |
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492 cm³/g STP | |
| Surface Energy Distribution by Modified De|
| Model: N2 @ 77K, Surface Energy Distribut|
Quantity Adso| Method: Non-negative Regularization: 0.0 |
5.534967785 | Standard Deviation of Fit: 0.01283 cm³/g S |
5.639772202 | |
5.746809505 | |
5.858415613 | |
5.977404716 | |
6.156120737 | Total Area : 33.934 m²/g |
6.296730446 | |
6.452401503 | |
6.627402708 | Surface Energy Table |
6.825961856 | |
7.051329725 | Energy (e/k) Cumulative AreIncremental Area (m²/g) |
7.303771389 | 20 0 0 |
7.578119689 | 22 0 0 |
7.863404989 | 24 0 0 |
8.146647661 | 26 0 0 |
8.41804358 | 28 0 0 |
8.673058698 | 30 0 0 |
8.911277269 | 32 5.266920597 5.266920597 |
9.134479418 | 34 6.131006193 0.864085596 |
9.345289203 | 36 6.131006193 0 |
9.546492783 | 38 6.131006193 0 |
9.740768294 | 40 6.131006193 0 |
9.930629233 | 42 6.984331387 0.853325194 |
10.11843119 | 44 17.45201228 10.46768089 |
10.30643262 | 46 17.45201228 0 |
10.49683997 | 48 17.45201228 0 |
10.69185931 | 50 17.45201228 0 |
10.89369493 | 52 17.45201228 0 |
11.10451559 | 54 17.45201228 0 |
11.32629164 | 56 17.45201228 0 |
11.56049467 | 58 20.75391801 3.301905731 |
11.80760893 | 60 20.75391801 0 |
12.06655445 | 62 20.75391801 0 |
12.33436762 | 64 22.99080173 2.236883719 |
12.60653982 | 66 22.99080173 0 |
12.87812386 | 68 25.08872035 2.097918626 |
13.14502367 | 70 25.08872035 0 |
13.40476139 | 72 25.31424634 0.225525989 |
13.6565159 | 74 25.31424634 0 |
13.90072606 | 76 25.31424634 0 |
14.13863103 | 78 25.31424634 0 |
14.37191156 | 80 27.14173167 1.827485331 |
14.60246644 | 82 27.14173167 0 |
14.83231007 | 84 27.14173167 0 |
15.22223112 | 86 31.11836999 3.976638319 |
15.45546276 | 88 31.11836999 0 |
15.9705226 | 90 31.11836999 0 |
16.21387844 | 92 31.11836999 0 |
16.46559797 | 94 31.62016542 0.50179543 |
17.11402335 | 96 31.62016542 0 |
17.38003906 | 98 31.62016542 0 |
17.99192143 | 100 33.9338413 2.313675876 |
18.26589541 | |
18.54027495 | |
19.14799887 | |
19.41219327 | |
20.22467031 | |
20.47380899 | |
21.59366045 | |
21.82997121 | |
23.62758802 | |
23.85483195 | |
24.08429512 | |
26.47292544 | |
26.70096573 | |
31.13875817 | |
31.3589684 | |
38.12109634 | |
38.31886402 | |
45.9269022 | |
46.09099469 | |
53.54892385 | |
53.67761356 | |
60.35390914 | |
60.45372829 | |
65.98574023 | |
66.06501667 | |
70.28504576 | |
70.35074921 | |
73.22675119 | |
73.28413396 | |
75.20323676 | |
75.25523636 |
76.94815432 |
76.99467275 |
78.54589565 |
78.58634843 |
80.0074199 |
80.04220254 |
81.34307517 |
81.37329569 |
82.56291814 |
82.58965857 |
83.42297217 |
84.19622654 |
84.21918571 |
85.1669046 |
85.18762889 |
86.05246929 |
86.0707234 |
86.859927 |
86.87576602 |
87.42738116 |
87.93869067 |
87.95175031 |
88.57835958 |
88.59 |
89.16085869 |
89.1714612 |
89.56973299 |
89.93846956 |
89.94733839 |
90.39919514 |
90.40695615 |
90.72204179 |
91.01367036 |
91.02013613 |
91.37745073 |
91.38324009 |
91.70838703 |
91.71354433 |
91.94 |
92.14955563 |
92.15379183 |
92.41059783 |
92.41432542 |
92.59309921 |
92.7582965 |
92.76137615 |
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TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020
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Sample: SiNPT75 | Sample:
Operator: NHA | Operator:
File: C:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNPT75. | File:
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Started: 1/24/2019 3:1 Analysis AdsorN2 | Started:
Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C | Completed:
Report Time: 1/24/2019 7:1 Thermal Correc No | Report Time:
Sample Mass:0.2904 g Warm Free Sp11.2525 cm³ Measured | Sample Mass:
Cold Free Spa32.4840 cm³ Equilibration In5 s | Cold Free Spa
Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure
Automatic DegNo | Automatic Deg
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| Cumulative Surface Area vs. Energy
|
Surface Energy Distribution by Modified Density Function |
Model: N2 @ 77K, Surface Energy Distribution | Cumulative Surface Area
Method: Non-negative Regularization: 0.00000 | Energy (e/k)
| 20
| 22
| 24
| 26
Standard Deviation of Fit: 0.01283 cm³/g STP | 28
| 30
| 32
Isotherm Table | 34
Relative Pressure | 36
(P/Po) Experimental Fitted Quantit Absolute ResidRelative Resid| 38
0.010592537 5.411222445 5.369489401 0.041733045 0.007712314 | 40
0.011220185 5.43526798 5.406492751 0.028775229 0.005294169 | 42
0.011885022 5.46072372 5.443212327 0.017511393 0.00320679 | 44
0.012589254 5.487670197 5.479771991 0.007898206 0.001439264 | 46
0.013335214 5.516192105 5.516296136 -0.00010403 -1.88591E-05 | 48
0.014125375 5.546378436 5.552915147 -0.00653671 -0.00117855 | 50
0.014962357 5.578322588 5.589764189 -0.0114416 -0.00205108 | 52
0.015848932 5.61212246 5.626984407 -0.01486195 -0.00264819 | 54
0.01678804 5.647880518 5.664732141 -0.01685162 -0.00298371 | 56
0.017782794 5.685703826 5.703176277 -0.01747245 -0.00307305 | 58
0.018836491 5.725704034 5.742504175 -0.01680014 -0.00293416 | 60
0.019952623 5.767997308 5.782931842 -0.01493453 -0.00258921 | 62
0.02113489 5.812704195 5.824706996 -0.0120028 -0.00206493 | 64
0.022387211 5.859949398 5.868120928 -0.00817153 -0.00139447 | 66
0.023713737 5.90986145 5.913524011 -0.00366256 -0.00061974 | 68
0.025118864 5.962572252 5.961348491 0.001223761 0.00020524 | 70
0.026607251 6.018216465 6.012134761 0.006081703 0.001010549 | 72
0.028183829 6.076930694 6.066579723 0.010350972 0.001703322 | 74
0.029853826 6.138852457 6.125588089 0.013264368 0.002160724 | 76
0.031622777 6.204118855 6.190289689 0.013829166 0.00222903 | 78
0.033496544 6.272864915 6.261783979 0.011080936 0.001766487 | 80
0.035481339 6.345221518 6.340151287 0.00507023 0.000799063 | 82
0.03758374 6.42131283 6.423312855 -0.00200002 -0.00031147 | 84
0.039810717 6.501253147 6.508495746 -0.0072426 -0.00111403 | 86
0.04216965 6.585143026 6.59473232 -0.00958929 -0.0014562 | 88
0.044668359 6.673064558 6.682615179 -0.00955062 -0.00143122 | 90
0.047315126 6.765075627 6.773023594 -0.00794797 -0.00117485 | 92
0.050118723 6.861202942 6.866412831 -0.00520989 -0.00075933 | 94
0.053088444 6.961433603 6.963015957 -0.00158235 -0.0002273 | 96
0.056234133 7.065704932 7.06337959 0.002325342 0.000329103 | 98
0.059566214 7.173892201 7.168484862 0.00540734 0.000753753 | 100
0.063095734 7.28579388 7.279544607 0.006249273 0.000857734 |
0.066834392 7.401113906 7.397260832 0.003853074 0.000520607 |
0.070794578 7.519440408 7.520226316 -0.00078591 -0.00010452 |
0.074989421 7.640220204 7.644579592 -0.00435939 -0.00057058 |
0.079432823 7.762728258 7.767032161 -0.0043039 -0.00055443 |
0.084139514 7.886031134 7.886926394 -0.00089526 -0.00011352 |
0.089125094 8.00894329 8.005047519 0.003895771 0.000486428 |
0.094406088 8.12997486 8.121734337 0.008240523 0.001013598 |
0.1 8.247269289 8.236300504 0.010968785 0.00132999 |
0.105925373 8.358528883 8.34815329 0.010375593 0.001241318 |
0.112201845 8.461194435 8.457688715 0.00350572 0.000414329 |
0.118850223 8.563324849 8.566009746 -0.0026849 -0.00031353 |
0.125892541 8.670058594 8.674517104 -0.00444921 -0.00051317 |
0.133352143 8.781489077 8.784684886 -0.00319581 -0.00036393 |
0.141253754 8.897626337 8.897968178 -0.00034184 -3.84192E-05 |
0.149623566 9.01848346 9.015789565 0.002693895 0.000298708 |
0.158489319 9.144022231 9.13933824 0.004683991 0.000512246 |
0.167880402 9.274153183 9.269031639 0.005121544 0.000552238 |
0.177827941 9.408724659 9.404463987 0.004260673 0.000452843 |
0.188364909 9.547509902 9.545268819 0.002241083 0.00023473 |
0.199526231 9.690191816 9.691352838 -0.00116102 -0.00011981 |
0.211348904 9.836568605 9.842401987 -0.00583338 -0.00059303 |
0.223872114 9.989891211 9.998351909 -0.0084607 -0.00084693 |
0.237137371 10.15190002 10.16028726 -0.00838723 -0.00082617 |
0.251188643 10.32336114 10.33011772 -0.00675658 -0.00065449 |
0.266072506 10.50517331 10.50930076 -0.00412745 -0.0003929 |
0.281838293 10.69839707 10.69811555 0.000281519 2.63141E-05 |
0.298538262 10.90429027 10.89693721 0.007353054 0.000674327 |
0.316227766 11.12385631 11.10817151 0.015684801 0.001410015 |
0.334965439 11.35757605 11.33605761 0.02151844 0.001894633 |
0.354813389 11.60628959 11.58400253 0.02228706 0.001920257 |
0.375837404 11.87086415 11.85348432 0.017379827 0.001464074 |
0.398107171 12.15218544 12.14786253 0.004322904 0.000355731 |
0.421696503 12.46121099 12.47293343 -0.01172244 -0.00094071 |
0.446683592 12.81589403 12.83265745 -0.01676342 -0.00130802 |
0.473151259 13.21084017 13.22977314 -0.01893296 -0.00143314 |
0.501187234 13.63646151 13.67059475 -0.03413325 -0.00250309 |
0.530884444 14.1380546 14.16384123 -0.02578663 -0.00182392 |
0.562341325 14.74413813 14.71449958 0.029638549 0.002010192 |
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NHA | Operator: NHA
| Submitter:
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umulative Surface Area vs. Energy | Incremental Surface Area vs. Energy
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umulative Surface Area | Incremental Surface Area
Cumulative Surface Area (m²/g) | Energy (e/k) Incremental Surface Area (m²/g)
0 | 20 0
0 | 22 0
0 | 24 0
0 | 26 0
0 | 28 0
0 | 30 0
5.266920597 | 32 5.266920597
6.131006193 | 34 0.864085596
6.131006193 | 36 0
6.131006193 | 38 0
6.131006193 | 40 0
6.984331387 | 42 0.853325194
17.45201228 | 44 10.46768089
17.45201228 | 46 0
17.45201228 | 48 0
17.45201228 | 50 0
17.45201228 | 52 0
17.45201228 | 54 0
17.45201228 | 56 0
20.75391801 | 58 3.301905731
20.75391801 | 60 0
20.75391801 | 62 0
22.99080173 | 64 2.236883719
22.99080173 | 66 0
25.08872035 | 68 2.097918626
25.08872035 | 70 0
25.31424634 | 72 0.225525989
25.31424634 | 74 0
25.31424634 | 76 0
25.31424634 | 78 0
27.14173167 | 80 1.827485331
27.14173167 | 82 0
27.14173167 | 84 0
31.11836999 | 86 3.976638319
31.11836999 | 88 0
31.11836999 | 90 0
31.11836999 | 92 0
31.62016542 | 94 0.50179543
31.62016542 | 96 0
31.62016542 | 98 0
33.9338413 | 100 2.313675876
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| Sample: SiNPT75 |
| Operator: NHA |
| Submitter: |
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| Automatic DegNo |
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| Differential Surface Area vs. Energy |
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| Differential Surface Area |
face Area (m²/g) | Energy (e/k) Differential Surface Area (m²/g-K) |
| 20 0 |
| 22 0 |
| 24 0 |
| 26 0 |
| 28 0 |
| 30 0 |
| 32 2.633460299 |
| 34 0.432042798 |
| 36 0 |
| 38 0 |
| 40 0 |
| 42 0.426662597 |
| 44 5.233840445 |
| 46 0 |
| 48 0 |
| 50 0 |
| 52 0 |
| 54 0 |
| 56 0 |
| 58 1.650952865 |
| 60 0 |
| 62 0 |
| 64 1.11844186 |
| 66 0 |
| 68 1.048959313 |
| 70 0 |
| 72 0.112762995 |
| 74 0 |
| 76 0 |
| 78 0 |
| 80 0.913742665 |
| 82 0 |
| 84 0 |
| 86 1.988319159 |
| 88 0 |
| 90 0 |
| 92 0 |
| 94 0.250897715 |
| 96 0 |
| 98 0 |
| 100 1.156837938 |
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Goodness of Fit | Goodness of Fit
Standard Deviation of Fit: 0.01283 cm³/g STP | Standard Deviation of Fit: 0.01283 cm³/g STP
|
Input Data Model Fit | Input Data
Relative PressQuantity AdsoRelative PressQuantity Adso| Relative PressQuantity Adso
0.010384971 5.403267672 0.010592537 5.369489401 | 0.010384971 5.403267672
0.111036562 8.443159702 0.011220185 5.406492751 | 0.111036562 8.443159702
0.207685912 9.79161895 0.011885022 5.443212327 | 0.207685912 9.79161895
0.299798464 10.91989316 0.012589254 5.479771991 | 0.299798464 10.91989316
0.402366759 12.20610288 0.013335214 5.516296136 | 0.402366759 12.20610288
0.500531648 13.62650876 0.014125375 5.552915147 | 0.500531648 13.62650876
0.597911594 15.45711041 0.014962357 5.589764189 | 0.597911594 15.45711041
0.70300558 18.54141403 0.015848932 5.626984407 | 0.70300558 18.54141403
0.808254282 26.05197977 0.01678804 5.664732141 | 0.808254282 26.05197977
0.909620426 73.8386881 0.017782794 5.703176277 | 0.909620426 73.8386881
0.990964066 92.89490591 0.018836491 5.742504175 | 0.990964066 92.89490591
0.019952623 5.782931842 |
0.02113489 5.824706996 |
0.022387211 5.868120928 |
0.023713737 5.913524011 |
0.025118864 5.961348491 |
0.026607251 6.012134761 |
0.028183829 6.066579723 |
0.029853826 6.125588089 |
0.031622777 6.190289689 |
0.033496544 6.261783979 |
0.035481339 6.340151287 |
0.03758374 6.423312855 |
0.039810717 6.508495746 |
0.04216965 6.59473232 |
0.044668359 6.682615179 |
0.047315126 6.773023594 |
0.050118723 6.866412831 |
0.053088444 6.963015957 |
0.056234133 7.06337959 |
0.059566214 7.168484862 |
0.063095734 7.279544607 |
0.066834392 7.397260832 |
0.070794578 7.520226316 |
0.074989421 7.644579592 |
0.079432823 7.767032161 |
0.084139514 7.886926394 |
0.089125094 8.005047519 |
0.094406088 8.121734337 |
0.1 8.236300504 |
0.105925373 8.34815329 |
0.112201845 8.457688715 |
0.118850223 8.566009746 |
0.125892541 8.674517104 |
0.133352143 8.784684886 |
0.141253754 8.897968178 |
0.149623566 9.015789565 |
0.158489319 9.13933824 |
0.167880402 9.269031639 |
0.177827941 9.404463987 |
0.188364909 9.545268819 |
0.199526231 9.691352838 |
0.211348904 9.842401987 |
0.223872114 9.998351909 |
0.237137371 10.16028726 |
0.251188643 10.33011772 |
0.266072506 10.50930076 |
0.281838293 10.69811555 |
0.298538262 10.89693721 |
0.316227766 11.10817151 |
0.334965439 11.33605761 |
0.354813389 11.58400253 |
0.375837404 11.85348432 |
0.398107171 12.14786253 |
0.421696503 12.47293343 |
0.446683592 12.83265745 |
0.473151259 13.22977314 |
0.501187234 13.67059475 |
0.530884444 14.16384123 |
0.562341325 14.71449958 |
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| Sample: SiNPT75
| Operator: NHA
| Submitter:
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| Automatic DegNo
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| Dubinin Reports
ion of Fit: 0.01283 cm³/g STP |
| 4035- Cannot calculate optimized Astakhov exponent:
Model Fit | 4031- Not enough points with a relative pressure in the r
Relative PressQuantity Adso| 4026- Cannot calculate Dubinin-Astakhov: bad least squa
0.010592537 5.369489401 | 1017- (INTERNAL) Cannot calculate Radushkevich: bad le
0.011220185 5.406492751 |
0.011885022 5.443212327 |
0.012589254 5.479771991 |
0.013335214 5.516296136 |
0.014125375 5.552915147 |
0.014962357 5.589764189 |
0.015848932 5.626984407 |
0.01678804 5.664732141 |
0.017782794 5.703176277 |
0.018836491 5.742504175 |
0.019952623 5.782931842 |
0.02113489 5.824706996 |
0.022387211 5.868120928 |
0.023713737 5.913524011 |
0.025118864 5.961348491 |
0.026607251 6.012134761 |
0.028183829 6.066579723 |
0.029853826 6.125588089 |
0.031622777 6.190289689 |
0.033496544 6.261783979 |
0.035481339 6.340151287 |
0.03758374 6.423312855 |
0.039810717 6.508495746 |
0.04216965 6.59473232 |
0.044668359 6.682615179 |
0.047315126 6.773023594 |
0.050118723 6.866412831 |
0.053088444 6.963015957 |
0.056234133 7.06337959 |
0.059566214 7.168484862 |
0.063095734 7.279544607 |
0.066834392 7.397260832 |
0.070794578 7.520226316 |
0.074989421 7.644579592 |
0.079432823 7.767032161 |
0.084139514 7.886926394 |
0.089125094 8.005047519 |
0.094406088 8.121734337 |
0.1 8.236300504 |
0.105925373 8.34815329 |
0.112201845 8.457688715 |
0.118850223 8.566009746 |
0.125892541 8.674517104 |
0.133352143 8.784684886 |
0.141253754 8.897968178 |
0.149623566 9.015789565 |
0.158489319 9.13933824 |
0.167880402 9.269031639 |
0.177827941 9.404463987 |
0.188364909 9.545268819 |
0.199526231 9.691352838 |
0.211348904 9.842401987 |
0.223872114 9.998351909 |
0.237137371 10.16028726 |
0.251188643 10.33011772 |
0.266072506 10.50930076 |
0.281838293 10.69811555 |
0.298538262 10.89693721 |
0.316227766 11.10817151 |
0.334965439 11.33605761 |
0.354813389 11.58400253 |
0.375837404 11.85348432 |
0.398107171 12.14786253 |
0.421696503 12.47293343 |
0.446683592 12.83265745 |
0.473151259 13.22977314 |
0.501187234 13.67059475 |
0.530884444 14.16384123 |
0.562341325 14.71449958 |
|
|
| TriStar II 3020TriStar II 3020Serial #: 1108 Page 1
|
|
| Sample: SiNPT75
| Operator: NHA
| Submitter:
| File: C:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNPT75.SMP
|
|
| Started: 1/24/2019 3:1 Analysis AdsorN2
| Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C
| Report Time: 1/24/2019 7:1 Thermal CorrecNo
| Sample Mass:0.2904 g Warm Free Sp11.2525 cm³ Measured
| Cold Free Spa32.4840 cm³ Equilibration In5 s
| Low Pressure None Sample Densit1.000 g/cm³
| Automatic DegNo
|
|
|
|
|
|
|
| MP Tabular Report
|
| t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5
|
|
|
|
| Total Pore Sur83.7036 m²/g
| Density Conver0.0015468
|
|
|
|
| Pore HydraulicAverage Pore Incremental PoCumulative PoDifferential P Incremental Po
| 0.000 - 1.365 0.682250489 0 0 0 0
| 1.365 - 1.380 1.372250489 0.042074545 0.042074545 2.714657972 30.66098017
| 1.380 - 1.400 1.39 8.29628E-16 0.042074545 4.14815E-14 5.96856E-13
| 1.400 - 1.420 1.41 0 0.042074545 0 0
| 1.420 - 1.440 1.43 0 0.042074545 0 0
| 1.440 - 1.460 1.45 0 0.042074545 0 0
| 1.460 - 1.480 1.47 0 0.042074545 0 0
| 1.480 - 1.500 1.49 0 0.042074545 0 0
| 1.500 - 1.520 1.51 0 0.042074545 0 0
| 1.520 - 1.540 1.53 -1.68505E-15 0.042074545 -8.42525E-14 -1.10134E-12
| 1.540 - 1.560 1.55 1.70708E-15 0.042074545 8.53538E-14 1.10134E-12
| 1.560 - 1.580 1.57 0 0.042074545 0 0
| 1.580 - 1.600 1.59 0 0.042074545 0 0
| 1.600 - 1.620 1.61 0 0.042074545 0 0
| 1.620 - 1.640 1.63 0 0.042074545 0 0
| 1.640 - 1.660 1.65 0 0.042074545 0 0
| 1.660 - 1.680 1.67 0 0.042074545 0 0
| 1.680 - 1.700 1.69 0 0.042074545 0 0
| 1.700 - 1.720 1.71 0 0.042074545 0 0
| 1.720 - 1.740 1.73 0 0.042074545 0 0
| 1.740 - 1.760 1.75 -1.92735E-15 0.042074545 -9.63674E-14 -1.10134E-12
| 1.760 - 1.780 1.77 1.94937E-15 0.042074545 9.74687E-14 1.10134E-12
| 1.780 - 1.800 1.79 0 0.042074545 0 0
| 1.800 - 1.820 1.81 0 0.042074545 0 0
| 1.820 - 1.840 1.83 0 0.042074545 0 0
| 1.840 - 1.860 1.85 0 0.042074545 0 0
| 1.860 - 1.880 1.87 0 0.042074545 0 0
| 1.880 - 1.900 1.89 0 0.042074545 0 0
| 1.900 - 1.920 1.91 0 0.042074545 0 0
|
|
| |
| |
| |
| |
| |
| |
| |
| |
| |
| |
| |
| |
| Options Report | Sample log
| |
| | Date
| | 1/24/2019
| Analysis Conditions | 1/24/2019
| | 1/24/2019
| | 1/24/2019
| | 1/24/2019
| Preparation | 1/24/2019
| |
| Fast evacuatioNo |
| Evacuation rat5.0 mmHg/s |
| Evacuation tim0.10 h |
| Leak test: No |
| Use TranSeal:No |
| |
| |
| Free Space |
| |
| Measured |
| Lower dewar foYes |
| Evacuation tim0.10 h |
| Outgas test: No |
| |
| |
| Po and Temperature |
| |
| Po and T type:Enter Po below. Enter the Analysis Bath T |
| Po: 760.000 mmHg |
| Temperature: -195.850 °C |
| |
| |
| Dosing |
| |
| Use first pressNo |
| Use maximumNo v |
| Target toleran 5.0% or 5.000 mmHg |
| |
| |
| Equilibration |
| |
| Equilibration 5 s |
| Minimum equili600 s |
| |
| |
| Sample Backfill |
| |
| Backfill at star Yes |
| Backfill at end Yes |
| Backfill gas: N2 |
| |
| |
| Adsorptive Properties |
| |
| Adsorptive: Nitrogen |
| Maximum manif 1,050.00 mmHg |
| Non-ideality fa0.0000620 |
| Density conver0.0015468 |
| Therm. tran. h 0.38600 nm |
| Molecular cros0.162 nm² |
| Adsorbate Mol2.00 |
| |
| |
| Inside diamete9.53 mm |
| |
| |
|
|
|
NHA | Operator: NHA
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNPT7
|
|
|
|
|
|
|
|
|
| Validation Report
|
Time Log Message |
3:11:07 PM Started analysis of file SiNP |
3:11:07 PM System volume: 18.1544 cm³| Isotherm Reports
3:22:31 PM Pressure transducer zeroed. |
3:30:18 PM Measured free space on port| Free Space: Low free space values may be
3:41:17 PM Pressure transducer zeroed. | observed when using liquid argon or ice baths.
7:14:39 PM Finished a sample analysis |
| Po Passed
|
|
| Pressure/Volu Passed
|
|
| Desorption Not within limits. Increase the sample mass, increase
| the equilibration interval, or check the free space.
|
|
|
|
| BET Reports
|
| C Value: Passed
|
|
| Correlation Coe
Passed
|
|
| Surface area: Passed
|
|
| Pressure RangThe selected BET relative pressure range is outside th
| recommended values of 0.05 to 0.30.
|
|
|
|
Page 1
0\data\SAMPEL\2019\Januari\SiNPT75.SMP
N2
-195.850 °C
No
11.2525 cm³ Measured
5s
1.000 g/cm³
values may be
using liquid argon or ice baths.
Increase the sample mass, increase

interval, or check the free space.
ET relative pressure range is outside the
alues of 0.05 to 0.30.

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TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020

Increase the sample mass, increase

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