Experiment - 1 KMnO. Vs. Mobr's Salt Calculation for weight of Moht's salt Motarty « 222k moles of solute Olay = fume of solution (L) s of the solute 1 fthe solute ee Molar mass of solute Volume of solution (ml) m 1 = —» —* 1000 0.05 332" 700 0.05 *392 10 M= = 1.96 gferent 1 ‘a0, Mob Sl Ans To dette the many an stent Sotasunpesmangante wing “sation of eons ‘of the given solution of rponium sulphate (Mohn ssa) ‘Materials required: Surette, pipette, measuring cylinder, measuring lak, beaker, watch glass, spatula, digital balance, coma fask Chemical required: KMtnO, solution, Festus ammonium sulphate (Moby's salt), distilled water, ttete HSO,, Teeory: This isa edo tration ‘Chemial Equation Se" + MnO, + SHY SFeANIN + AIO Indicator ANNO. act as seh indicator, End point: Colouriess to permanent pink Solution in Burette: KMnO, solution Solution conical ask ferrous ammonium sulphate solution (Mohr’s salt solution, Procedure: (i) Preparation 2 Mob’ soiton \Weghe he ean a yah ss an recorded is wg in the nae Book Weighs accurately 1969 oF Ma's sls onthe woth es 3. Trastevere the meighad Nols fom ihe watchin den 0D renin Ga ig fone oda spac, 4 Washed the watch glass thoroughiy with dstiled water 5. Shook the measuring flask gentytodssolve the salt 8 Added enough distilled water tothe measuring Hask catelully upto just below the etched mark on ts neck with the help ofa wash bottle 2 Added the last few drops of dstiled water with a pipette until the lower level ofthe ‘meniscus just touches the mark on the measuring fash . S __Stoppered the measuring flask and shook its gently to make the solation homogenous (he. uniform throughout) and labelled it as Mohr’ salt solution @) Estimation of molarity of yen solution of KM. 1 Risad an file! te rete with the gen KANO, soliton and noted the til ean of the buete Ainsed the pipette withthe “Mobs sl slain Added one tes tube (20 lal of lt 50, tthe solatonin the tivation ask Then added x10, solution om the burette tia permanent ight pink cour was imparted to the slution nthe tivation ask on addition ct st single dap ol Kens solution Noted the final eating ofthe burette Repeated the above steps to geta st of two concordant reading. 8 ‘Result: The molarity ofthe given KMnO, solution is_ The strength of the given KMnO, solution is aftCi sla Mevense “Vemma, Myeonr’ sett sotution “Y mony’ ssalt sotution meme ® wor’ ssait eens we . s Mewes” “ ‘Concordant reading: x milPrecautions. Pree “ee De mot nme the titration Mask Read the uppe: mMenecus whe taking the burette reading with KMnO, solution ‘Check the state of the balance before weighing Wm case, om adkhbon of EMnO, a brown precipitate is obtained, this shows that esther H)SO. das ant been ating or has been added in insufficient smcunt In such @ case, throw away the solunon and bitrate agen De not hold papette from its bulb to avoud errors Last drop of solution in the pypette should not be biown out Surette should de filed till ts nozzie hip