(ERA A Waters Company Reference Material « Certificate of Analysis « Product: Total Petroleum Hydrocarbons (TPH) in Soil Catalog Number: 570 Lot No. Di00-632 Pret ues wr nse a pr of Certificate Issue Dat January 08, 2018 sepaatly fom ts Contests of Anas. Please Expiration Dé ‘September 12, 2020 ee oe ae ae Revision Number: Original CERTIFICATION Certified QC Performance PT Performance Parameter Value’ Uncertainty? Acceptance Limits* Acceptance Limits* moks * moka moa ‘non-Polar Extractable Material 988 ost4 287-1310 29.6- 1570 (TPH)(Grav) rnon-Polar Extractable Material 1220 0514 ‘580 - 1630 316- 1900 (TPH(IR) ANALYTICAL VERIFICATION Certified Parameter Value Proficiency Testing Study NIST Traceability Mean Recovery’ on - SRMNumber Recovery mong mas * * ‘non-Polar Extractable Material 988 847 8 (17 > > (TPH)(Grav) nnon-Polar Extractable Material 1220 1050 86.2 3 5 : (TPH)(IR) Page 1 of 2 Lot: 0100-632 16341 Table Mountain Pkwy « Golden, CO 80403 + T: 800.372.0122 - 303.431.8454 + www.eragc.comReference Material « Certificate of Analysis = {,,7e Certiied Values sre the actual "made-o" concentrations confimed by ERA analytical veriication, The certified values are monitored and purchasers ibe notified of any sigrieant changes rsuting in recertification or withcrawal of his certified reterence material curing the porod ot valty el are Content. 2, The Uncertainty isthe otal propagated uncertainty atthe 85% confidence interval, The uncertainty is based on the preparation and intemal ‘Nattcaton ofthe productby ERA mulpied by a coverage fectr. The uncertainty apps to the product as Supplid ond sce nat take nto secon equirec or optional ution andior preparations the laboratory may perform while sing this product 3, {R82 Performance Acceptance Limits (QC PALS ™)aro based on actual historical data colected in ERA‘s Proficiency Testing program, The QO Pals ‘elect any inherent bases in the mathods used to estabsh the limits and closely approximate @ 95% confidence imenel fe cavomeres eat experienced laberateres should achieve using accepted environmental methods. Use the GC PALS™ to realstealy evaluate yout pertomance agane your peers, Selig PT Performance Acceptance Limits (PT PALS™) are calculated using the regression equations and fixed acceptance ceria sped inthe NELAG proficiency testing requirements. Use the PT PALS™ when analyzing i's QC stancard alongside USEPA and NELAG comment e erssoe te Please note that many PT study acceptance mits are concentration dependent (some nomineary) and, therstore, the acceptance ae of ie Standard and ary PT standard may ifr relative to their ference in concentahons, §, The PT Data/Traceabilty data inciudo the mean value, percent recovery and number of datapoints reported by the laboratories in our Protce Testing study compared tc the Certfied Values. n addon, where NIST Slandard Reference Matera (Srl) are avatacn analytical raced 'o the NIST SRM Istod. This products traceable tothe lot numbers of ts staring materials. All gravmewG and veloronie ne sar ements ‘elated tos manutactue are traceable to NIST through an unbroken chain of comparsone, Traceability Recovery (%) = (% recovarycertied standara(% recovery NIST SEM)| 00 ‘The traceabity data shows were complied by analyzing the ERA standards or ther associated stock solutions against the applicable NIST SAMS. 5. For adtonalnformaten on tis preduct suchas intended use, instruction fr use, level of homogeneity, and safety information, please rotor to the Provided Instruction Sheet If you have any questions or need technical assistance, please call ERA technic: at 1-800-372-0122 or send an email to info@eraqc.com. assistance Certitying Officer Quality Officer Brian Miller Matthew Seebeck Bian Hild. fk At wi wan Page 2 of 2 Lot: 0100-632 16341 Table Mountain Pkwy + Golden, CO 80403 « T: 800.372.0122 - 303.431.8454 + www.eragc.comInstructions for Catalog #570 Total Petroleum Hydrocarbons (TPH) in Soil Revision 042715, Description: + This standard is packaged in a 2-ounce glass jar containing approximately 50 grams of soil, This standard is not preserved. + The standard can be stored at room temperature. *+ This product is intended to be used as a quality control check of the entire analytical process for the analytes/matrix included in the standard. + BRA suggests that when subsampling this product prior to analysis you use a minimum sample size of at least 20 grams. Using a smaller sample size may invalidate the assigned value and/or uncertainty shown on the certificate of analysis. * The standard contains Total Petroleum Hydrocarbons (TPH) in the range of 300 to 3,000 mg/kg. Helpful Hints: ‘* Although all ERA soil standards have been thoroughly blended prior to shipping, the standards should be homegenized prior to taking an aliquot for analysis due to setting which may occur during shipping, Instructions: 1. Open the TPH in Soil standard in a fume hood to avoid inhalation of dust 2. Mix the sample well prior to removing an aliquot for analysis. 3. Prepare and analyze the standard using your normal procedures. Safety: ERA products may be hazardous and are intended for use by professional laboratory personnel trained in the competent handling of such materials. Responsibility for the safe use of these products rests entirely with the buyer and/or user. Material Safety Data Sheets (MSDS) for all ERA products are available by calling 1-800-372- 0122,(ERA 04-Feb-2016 To the bes: of our knowledge, the product listed below does not require a Safety Data Sheet (SDS) in accordance with 29 CFR Subpart Z 1910.1200(d)(1) as the substance or mixture it contains does not meet any of the established hazard classes. ‘Always use our products for the intended use(s) in accordance with published user manuals or product instructions. Product Number Product Name 570 Total Petroleum Hydrocarbons (TPH) in Soil #1iev"2 ginG vote? a miipor ion Balai Iouborg on epbeiworut we ie teso ¢ 4 syhint wo sonstadue $f ae (tb) 0 Fat S neqdue AFD @S rite eonstaasas 6 ¥ 7 ; a berelidsiee eit! to yrs teem ton eeah ecisines avNO f | || +e slaw rem seeu berieildug dliw aa me (e}eets bobneini art wt etauberg = aeiclionsien Nb io8 ni (HIT) it | LPF | if : He eee 4 A. i Fen} aA | * i | | : 4