SHIMADZU
Solutions for Science
since 1875
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TG-DTA Sim
Measuring Iq
OD)Simultaneous TG/DTA improves ease of operation,
sensitivity and analytical accuracy of conventional
standalone systems
If flexibility and high performance is needed in Atmosphere control is programmable. As in
various applications, the new DTG-60/60H. DSC, the TA-GOWS provides advanced
combines them all: Basic functions required by acquisition, analysis and report functions which
simultaneous thermogravimetry/differential ensure comfortable simultaneous measurement,
thermal analysis (TG/DTA) measurements are
improved.Des ee eae
Cie
‘The balance assembly is the heart of every thermogrametric
analyzer. The newly designed X-shaped fulcrum provides.
high sensitivity and excellent vibration-proof structure
because of the light weight and extremely reduced friction
and resistance. New A/D technology allows the DTG-60/60H
to operate in a very large dynamic mass range.
DTG-60/60H has the unique feature of lfferential weight
measurement.
eee
‘Thermal Analysis Data
Fumace
Photoelectric conversion
ment
DTG-60/60H provides a true DTA setup, The sample and the
reference position are located at the ends of the balance
beam. This differential balance system minimizes baseline
drits caused buoyancy or convection during the heating
process, ensuring a stable baseline even at high
‘temperatures.
Boeke eens
Clay shows distinctive characteristics depending on its
producing area and composition.
In particular, differential thermal analyses (DTA) for clay
minerals show distinctive patterns of (1) “Endothermic peak
between 50 and 200'C", (2) "Endothermic peak between 300
‘and 800°C", and (8) "Endothermic/Exothermic peak between
900 and 120°C" depending on the type of clay minerals.
Therefore, it can be used for qualitative analysis.
‘The exothermic peak around 1015°C is caused by a change
in the crystal structure, With thermogravimetry (T), weight
reduction is observed in two steps, corresponding to
dehydration of adsorbent water and OH,
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[SOLENOID
VALVE
During TG/DTA measurements, qualitative and quantitative
analysis, examination of reaction mechanisms and
evaluation of heat resistance are performed by studying
various reactions and interactions between a sample and
special atmospheres. The unique channel structure of the
DTG-60/60H offers the solution for these applications. While
an inert gas purges the balance, reactive gases are directly
‘connected to the reaction pan. In combination with the FC~
0A the measurement is fully software controlled.
Tr ee es
‘Tne DTA detector of DTG-60/60H is well balanced between
contradictory factors “sensitivity” and “resolution”. Since
symmetrical arrangement of two detectors in the furnace
provides excellent temperature distribution, even very smal
DTA signals such as noise and drift are well matched.
Using the convenient plug-in method, the DTA detector ean
be quickly replaced.\Specifications \iSpecifications
‘Model DTG-60 (P/N 346-68750-02/89)
TA COWS OTe s0/eoH DTG-60H (P/N 346-68700-82/83)
S906 ACIPOY,~B3 ar C2900
Balance type Parallel guide diferential top pan type
Temperature range | DTG-60: Room temperature to 1100°C
DTG-60H: Room temperature to 1500°C
Range 500mg.
£1000
Readability ‘on0ima
‘Sample quantity | 19 max in gross weight
‘Atmosphere Reaction gas, purge gas and cleaning gas can
'bo supplied. Gas can be exhausted for gas
replacement
Dimensions W867 D650 1453 (am)
ight 5g
{installation requirements
Power supply: DIG-60: AG100,120V 1300VA So/60Hz
DTG-60H:AC100.120V 1S00VA Save0Hiz
‘Ambient temperature: | 5 to 40°C (No condensation)
‘Atmosphere gas control: | A gas cylinder, pressure governor, piping components and Shimadzu atmosphere gas contrller FC-60A
are required,
System construction: _| Shirsadzu Thermal Analysis Data Processing System TA-GOWS, commercially-avallable personal
‘computer (Windows"85/98/Me/NT), perioheral equipment (e.g. printer) and software (OS and driver) are
required,
‘Autosampler: “The Autosampler can be mounted when ordering the DTG-60/60H or afterward
General environment: | Do not install this equipment ina dusty place or in a place where it may be directly exposed to sunlight,
wind from a coaling/heating appliance, vibration or large temperature fluctuations.
* We reserve the right to modify he appearance and specifications
of our products without a prior notice.
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