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it under reduced pressure in a 60℃ water bath until all the water is removed. Starting from "adding 20ml of absolute
ethanol", repeat the operation three times in accordance with the same procedure to remove all water. Add 30ml of
glacial acetic acid-trichloromethane (3:2) mixture to dissolve the residue. Accurately add 0.5ml of saturated
potassium iodide solution, close tightly, shake and extract for 1 minute, add 30ml of freshly boiled cold water and
5ml of starch indicator solution, and immediately titrate with sodium thiosulfate titrant (0.01mol/L) to the upper
water phase The purple-blue color disappeared, and the titration result was corrected with a blank test. The