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Peroxide value Accurately measure 10ml of this product, freeze-dry or add 20ml of absolute ethanol, and rotate

it under reduced pressure in a 60℃ water bath until all the water is removed. Starting from "adding 20ml of absolute

ethanol", repeat the operation three times in accordance with the same procedure to remove all water. Add 30ml of

glacial acetic acid-trichloromethane (3:2) mixture to dissolve the residue. Accurately add 0.5ml of saturated

potassium iodide solution, close tightly, shake and extract for 1 minute, add 30ml of freshly boiled cold water and

5ml of starch indicator solution, and immediately titrate with sodium thiosulfate titrant (0.01mol/L) to the upper

water phase The purple-blue color disappeared, and the titration result was corrected with a blank test. The

consumption of sodium thiosulfate titrant (0.01mol/L) shall not exceed 0.50ml.

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