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International University, Vietnam National University - HCMC 1

CHEMISTRY LABORATORY

REPORT
EXPERIMENT 1: CHEMICAL REACTIONS

Group: ______________ Class: ______________ Date: ____________

Group members:

Full name Student ID Declaration of Contribution Signature

Total score: _______/100


International University, Vietnam National University - HCMC 2
CHEMISTRY LABORATORY

Part 1. Introduction
(Introduce the general background and summarize the aims/objectives of the experiment)

Part 2. Materials and Methods


(Summarize the experimental design/structure of your experiment)

Part 3. Results and Discussion


1. REACTIONS OF Cu2+
Reaction Observation Chemical Equation
0.5M CuSO4
+ 2M NaOH
0.5M CuSO4
+ 2M NH4OH
Discussion:
(Discuss: i) Explanation for the above observation; ii) Possible reasons for any misconducted results)

2. REACTIONS OF SILVER HALIDES


Reaction Observation Chemical Equation
0.5M KCl
+ 0.1M AgNO3
0.5M KCl
+ 0.1M AgNO3
+ 2M NH4OH

0.5M KBr
+ 0.1M AgNO3
0.5M KBr
+ 0.1M AgNO3
+ 2M NH4OH
Discussion:
International University, Vietnam National University - HCMC 3
CHEMISTRY LABORATORY

3. REACTIONS OF H2O2
Reaction Observation Chemical Equation
0.1M KMnO4
+ 2M H2SO4
+ H2O2
0.1M KI
+ 2M H2SO4
+ H2O2
H2O2
+ MnO2

Discussion:

4. REACTIONS OF KMnO4
Reaction Observation Chemical Equation
0.5M Na2SO3
+ 2M H2SO4
+ 0.1M KMnO4
0.5M Na2SO3
+ 6N NaOH
+ 0.1M KMnO4
0.5M Na2SO3
+ H2O
+ 0.1M KMnO4
Discussion:
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5. A. REACTIONS OF Fe3+
Reaction Observation Chemical Equation
0.5M FeCl3
+ 2M KOH

0.5M FeCl3
+ 2M NH4OH

Discussion:

5. B. REACTIONS OF Fe2+
Reaction Observation Chemical Equation
0.5M FeSO4
+ 2M KOH

0.5M FeSO4
+ 2M NH4OH

Discussion:

6. REACTIONS OF Al3+
Reaction Observation Chemical Equation
0.5M Al2(SO4)3
+ 2N NaOH
+ 2M HCl
0.5M Al2(SO4)3
+ 2M NaOH
+ 2M NaOH
Discussion:
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7. FLAME TEST
Solution Dominant flame Wavelength Frequency Photon energy (J)
color (nm) (s1)
LiCl
NaCl
KCl
CaCl2
BaCl2
Discussion:

Part 4. Conclusions

END.
International University, Vietnam National University - HCMC 6
CHEMISTRY LABORATORY

REPORT
EXPERIMENT 2: pH AND BUFFERS

Group: ______________ Class: ______________ Date: ____________

Group members:

Full name Student ID Declaration of Contribution Signature

Total score: _______/100


International University, Vietnam National University - HCMC 7
CHEMISTRY LABORATORY

Part 1. Introduction
(Introduce the general background and summarize the aims/objectives of the experiment)

Part 2. Materials and Methods


(Summarize the experimental design/structure of your experiment)

Part 3. Results and Discussion


1. pH OF DEIONIZED WATER
Observed pH
Time
1st 2nd Discussion
(second)
(Group___) (Group___)
0
20
40
60

2. pH OF STRONG ACID
Measured pH
Theoretical
Solution 1st 2nd Discussion
pH
(Group___) (Group____)

10 mL of 0.1M HCl

Add 90 mL of distilled
water

Add 10 mL of
0.1M NaOH

Add 90 mL of
0.01M NaOH
Calculation:
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3. pH OF WEAK ACID
Measured pH
Solution 1st 2nd Ka Discussion
(Group___) (Group____)

0.1M acetic acid

0.01M acetic acid

0.001M acetic acid

Calculation:

4. pH OF SALTS
Measured pH
Predicted
Solution 1st 2nd Discussion
pH
(Group____) (Group____)
0.1M NaCl

0.1M CH3COONa

0.1M NH4Cl

Calculation:

5. pH OF BUFFERS
Buffer Volume Volume (mL) Acid Base Calculated Measured pH
(mL) 0.1M 0.1M pH 1st 2nd
CH3COOH CH3COONa
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(Group__) (Group__)

A 10.0 40.0

B 40.0 10.0
Calculation pH:

Discussion:

 Part I: Addition of 10 drops 0.1 M HCl


pH from pH after Total volume HCl (drops)
Buffer the start, adding 10 to change pH by one unit Discussion
pHo drops HCl (pHo-1)
A

 Part II: Addition of 10 drops 0.1 M NaOH


pH from pH after Total volume NaOH
Buffer the start, adding 10 (drops) to change pH by Discussion
pHo drops NaOH one unit (pHo+1)

Part 4. Conclusions

END.
International University, Vietnam National University - HCMC 10
CHEMISTRY LABORATORY

REPORT
EXPERIMENT 3: REDOX TITRATION

Group: ______________ Class: ______________ Date: ____________

Group members:

Full name Student ID Declaration of Contribution Signature

Total score: _______/100


International University, Vietnam National University - HCMC 11
CHEMISTRY LABORATORY

Part 1. Introduction
(Introduce the general background and summarize the aims/objectives of the experiment)

Part 2. Materials and Methods


(Summarize the experimental design/structure of your experiment)

Part 3. Results and Discussion


1. STANDARDIZATION OF PREPARED KMnO4 SOLUTION
Calculation:
Normality of the standard H2C2O4 solution, N(H2C2O4) = ___________________

Volume of the standard H2C2O4 solution used, V(H2C2O4) = ___________________

Trial # Burette reading (mL) Volume of KMnO4 (mL) Normality of KMnO4 (N)

1 -

2 -

Average Normality of KMnO4 = ____________


Discussion:

2. DETERMINATION OF UNKNOWN CONCENTRATION H2C2O4 SOLUTION


Calculation:
Normality of the standard KMnO4 solution, N(KMnO4) = ___________________

Volume of the unknown H2C2O4 solution used, V(H2C2O4) = ___________________


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Trial # Burette reading (mL) Volume of KMnO4 (mL) Normality of H2C2O4 (N)

1 -

2 -

Average Normality of H2C2O4 = ____________


Discussion:

3. DETERMINATION OF UNKNOWN CONCENTRATION FeSO4 SOLUTION


Calculation:
Normality of the standard KMnO4 solution, N(KMnO4) = ___________________
Volume of the unknown FeSO4 solution used, V(FeSO4) = ___________________

Trial # Burette reading (mL) Volume of KMnO4 (mL) Normality of FeSO4 (N)

1 -

2 -

Average Normality of FeSO4 = ____________


Discussion:

Part 4. Conclusions

END.
International University, Vietnam National University - HCMC 13
CHEMISTRY LABORATORY

REPORT
EXPERIMENT 4: CHEMICAL EQUILIBRIUM

Group: ______________ Class: ______________ Date: ____________

Group members:

Full name Student ID Declaration of Contribution Signature

Total score: _______/100


International University, Vietnam National University - HCMC 14
CHEMISTRY LABORATORY

Part 1. Introduction
(Introduce the general background and summarize the aims/objectives of the experiment)

Part 2. Materials and Methods


(Summarize the experimental design/structure of your experiment)

Part 3. Results and Discussion


1. ACID/BASE EQUILIBRIA

Equilibrium System: 2CrO42 + 2H+ (aq) ⇌ Cr2O72 + H2O(l)

Description of Predicted
Observation Discussion
conditions outcome

Initial solution

+ Conc. HCl

+ 6 N NaOH

Note:

2. EQUILIBRIA OF ACID/BASE INDICATORS

Equilibrium System: H(MV)(aq) + H2O(l) ⇌ H3O+(aq) + MV(aq)

Addition Predicted
Observation Discussion
outcome
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CHEMISTRY LABORATORY

None (control)

6 M HCl

6 M NaOH

6 M HCl

Note:

3. EQUILIBRIA OF PRECIPITATION REACTIONS

Equilibrium System: Ca2+(aq) + C2O42(aq) ⇌ CaC2O4(s)

Predicted
Addition Observation Discussion
outcome

Test tube 1:

0.1 M Na2C2O4

Test tube 2:

+ 0.1 M
H2C2O4

Test tube 2:

+ 6 M HCl

Test tube 2:

+ 6 M NH4OH

Note:
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4. TEMPERATURE EFFECTS ON EQUILIBRIA

Equilibrium System: Co(H2O)62+(aq) + 4Cl(aq) ⇌ CoCl42(aq) + 6H2O(l)

Description of Predicted
Observation Discussion
conditions outcome

Nothing changed

(control)

Hot water bath

Ice-water bath

Note:

Part 4. Conclusions

END.
International University, Vietnam National University - HCMC 17
CHEMISTRY LABORATORY

REPORT
EXPERIMENT 5: FACTORS AFFECTING
REACTION RATE

Group: ______________ Class: ______________ Date: ____________

Group members:

Full name Student ID Declaration of Contribution Signature

Total score: _______/100


International University, Vietnam National University - HCMC 18
CHEMISTRY LABORATORY

Part 1. Introduction
(Introduce the general background and summarize the aims/objectives of the experiment)

Part 2. Materials and Methods


(Summarize the experimental design/structure of your experiment)

Part 3. Results and Discussion


1. EFFECT OF CONCENTRATION ON REACTION TIME
Reaction 1: __________________________________________________
Reaction 2: __________________________________________________
Calculate the initial concentrations of I- and S2O82- ions:
Mixture # 5:
[I-] =

[S2O82-] =

Mixture Iodide ion Peroxydisulfate Time in seconds


1 0.08 0.04
2 0.068 0.04
3 0.056 0.04
4 0.044 0.04
5 0.032 0.04
6 0.02 0.04
Mixture Iodide ion Peroxydisulfate Time in seconds
7 0.08 0.034
8 0.08 0.028
9 0.08 0.022
10 0.08 0.016
11 0.08 0.01

Plotting the concentration of iodide ion versus time: [Note: X – axis: time; Y – axis: concentrations].
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* Mixtures # 1-6:
- Graph

- The order of reaction with respect to iodide ion?

- Discussion:

* Mixtures # 1, 7, 8, 9, 10, and 11:


- Graph

- The order of reaction with respect to iodide ion?

- Discussion:

2. EFFECT OF TEMPERATURE ON THE REACTION RATE


Reaction System:

Description of Predicted Reaction


Observation Discussion
conditions outcome time

Room
temperature

500C

900C

Note:
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3. EFFECT OF A CATALYST ON THE REACTION RATE


Reaction System:

Description of Predicted Observation


Trial Discussion
conditions outcome (Reaction rate)

1 + MnCl2

2 + MnO2

3 + NaCl

4 + CaCl2

5 + Zn

6 + KNO3

7 + Fe(NO3)3

The order of catalyst activity:


Note:

Part 4. Conclusions

END.

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