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分析化學實驗4
分析化學實驗4
NaOH滴定體積(ml)
pH NaOH滴定體積(ml)
pH/V(1/ml)NaOH滴定體積(ml)
1.52 0.00 2.60
1.90 0.38 2.64 0.19 0.11 NaOH 滴
2.55 1.03 2.76 0.71 0.18 0.45 0.15 14.00
2.95 1.43 2.84 1.23 0.20 0.97 0.03
12.00
3.45 1.93 2.95 1.68 0.22 1.46 0.04
3.95 2.43 3.09 2.18 0.28 1.93 0.12 10.00
4.45 2.93 3.28 2.68 0.38 2.43 0.20 8.00
4.95 3.43 3.52 3.18 0.48 2.93 0.20
pH 值
6.00
5.45 3.93 3.94 3.68 0.84 3.43 0.72
5.95 4.43 4.50 4.18 1.12 3.93 0.56 4.00
6.50 4.98 4.91 4.71 0.75 4.44 -0.71 (3.93, [Y 值
2.00
7.00 5.48 5.19 5.23 0.56 4.97 -0.35
7.50 5.98 5.39 5.73 0.40 5.48 -0.32 0.00
0.00 5.00
8.00 6.48 5.61 6.23 0.44 5.98 0.08
8.55 7.03 5.86 6.76 0.45 6.49 0.03
9.00 7.48 6.09 7.26 0.51 7.01 0.11
9.50 7.98 6.64 7.73 1.10 7.49 1.24
9.80 8.28 8.81 8.13 7.23 7.93 15.33 NaOH 滴定丙
9.95 8.43 9.44 8.36 4.20 8.24 -13.48 8.00
(8.13,
10.10 8.58 10.07 8.51 4.20 8.43 0.00 7.00
10.20 8.68 10.31 8.63 2.40 8.57 -14.40
6.00
10.50 8.98 10.62 8.83 1.03 8.73 -6.83
11.00 9.48 10.95 9.23 0.66 9.03 -0.93 5.00
0.00
20.10 18.58 11.94 18.28 0.05 18.01 0.02 0.00 5.00
20.50 18.98 11.95 18.78 0.02 18.53 -0.05 -5.00
-15.00
-20.00
N
0.00
Axis T
0.00 5.00
-5.00
-10.00
21.60 20.08 11.99 19.88 0.05 19.61 0.04 -15.00
22.00 20.48 12.00 20.28 0.02 20.08 -0.06
-20.00
22.50 20.98 12.01 20.73 0.02 20.51 -0.01
N
3.93 0.56
4.44 -0.71
7.93 15.33
8.24 -13.48
NaOH 滴定丙二酸 : 滴定曲線
14.00
12.00
10.00
(8.28, [Y 值 ])
8.00
6.00
4.00
(3.93, [Y 值 ])
2.00
0.00
0.00 5.00 10.00 15.00 20.00 25.00
(8.13, 7.23)
(4.18, [Y 值 ])
15.00
10.00
5.00
0.00
0.00 5.00 10.00 15.00 20.00 25.00
-5.00
-10.00
-15.00
-20.00
-10.00
-15.00
-20.00