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    The document discusses various 0D-HEA nanostructure synthesis methods and their applications. Table 1 lists different 0D nanoparticle synthesis techniques such as carbothermal shock synthesis, aerosol synthesis, microwave heating, wet chemical synthesis, and others. It provides examples of alloys synthesized using each technique and their applications, including in areas such as ammonia oxidation, oxygen catalysis, energy storage, hydrogen evolution reaction, and more. Aerosol synthesis addresses challenges of carbothermal shock synthesis by producing smaller metal salt droplets that act as nanoreactors during rapid heating and quenching.

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    The document discusses various 0D-HEA nanostructure synthesis methods and their applications. Table 1 lists different 0D nanoparticle synthesis techniques such as carbothermal shock synthesis, aerosol synthesis, microwave heating, wet chemical synthesis, and others. It provides examples of alloys synthesized using each technique and their applications, including in areas such as ammonia oxidation, oxygen catalysis, energy storage, hydrogen evolution reaction, and more. Aerosol synthesis addresses challenges of carbothermal shock synthesis by producing smaller metal salt droplets that act as nanoreactors during rapid heating and quenching.

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    Nanostr

    Uploaded by

    SJ
    The document discusses various 0D-HEA nanostructure synthesis methods and their applications. Table 1 lists different 0D nanoparticle synthesis techniques such as carbothermal shock synthesis, aerosol synthesis, microwave heating, wet chemical synthesis, and others. It provides examples of alloys synthesized using each technique and their applications, including in areas such as ammonia oxidation, oxygen catalysis, energy storage, hydrogen evolution reaction, and more. Aerosol synthesis addresses challenges of carbothermal shock synthesis by producing smaller metal salt droplets that act as nanoreactors during rapid heating and quenching.

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    26884011, 0, Downloaded from https://onlinelibrary.wiley.com/doi/10.1002/nano.202200081 by National Medical Library The Director, Wiley Online Library on [07/11/2022].

    See the Terms and Conditions (https://onlinelibrary.wiley.com/terms-and-conditions) on Wiley Online Library for rules of use; OA articles are governed by the applicable Creative Commons License
    6 PAVITHRA and DEY

    TA B L E 1 0D-HEA nanostructures
    0D/Nanoparticles Application Alloys Refs.
    Carbothermal shock synthesis ∙ Ammonia PtCoNiFeCu, PtPdCoNiFe, [24,27]

    oxidation/decomposition PtCoNiFeCuAu,
    ∙ Oxygen reduction reaction PtPdCoNiFeCuAu,
    (ORR) PtPdCoNiFeCuAuSn,
    ∙ Oxygen catalysis (Li–O2 CoMoFeNiCu, RuRhCoNiIr,
    battery) PtPdRhRuIr,
    ∙ Energy storage PtPdRhRuIrFeCoNi,
    RuIrCeNiWCuCrCo,
    FeNiCoMnMg,
    FeNiCoMnCu
    Aerosol synthesis ∙ In situ Fe0.28 Co0.21 Ni0.20 Cu0.08 Pt0.23 , [22a,28]

    oxidation/high-temperature NiCoFeCuPt, NiCoFePdPt,


    reduction behavior NiCoCuFePd
    [29]
    Microwave heating PtPdFeCoNi
    Wet chemical synthesis ∙ Ethanol oxidation reaction NiFeCrCuCo, RuRhPdIrPt [23,30]

    Ultrasonication-assisted wet ∙ Hydrogen evolution reaction PtAuPdRhRu [31]

    chemistry (HER)
    Sol–gel autocombustion ∙ Magnetic CoCrCuNiAl [32]

    [33]
    Solvothermal synthesis Pt0.20 Pd0.20 Ir0.20 Rh0.20 Ru0.20,
    PtIrPdRhRu
    Chemical co-reduction ∙ Hydrogen evolution catalysis NiCoFePtRh [34]

    One-pot polyol process ∙ HER IrPdPtRhRu [35]

    Arc-discharge process ∙ Corrosion resistance AlCoCrCuFeNi, CoCrCuFeNi [36]

    ∙ Magnetic
    [16b]
    Spark discharge process CoCrFeNiPt, CoFeNiCr0.5 Pd0.8
    Pyrolysis of metallocenes ∙ Magnetic CrMnFeCoNi [37]

    Bed pyrolysis ∙ HER FeCoPdIrPt, [38]

    ∙ Water splitting Mn, Co, Ni, Cu, Rh, Pd, Sn, Ir,
    Pt, and Au,
    CuPdSnPtAu, NiCuPdSnPtAu,
    NiCuPdSnIrPtAu,
    CoNiCuPdSnIrPtAu
    [39]
    Scanning-probe block AuAgCuCoNi
    copolymer lithography
    method
    Direct current sputtering ∙ Oxygen reduction reaction CrMnFeCoNi [40]

    (OER)
    Laser-synthesis ∙ OER CoCrFeNiMn [41]

    picosecond-pulsed laser
    ablation
    [42]
    Vapor-source technique NiCrFeAuAg, NiCrCoAuAg,
    NiCrCoMoAuAg,
    NiCrFeCuPd,
    NiCrCoMoCuPd

    immiscible/unmixable elements is not possible through droplets of <1 µm in size, which are then subjected to
    conventional techniques. The steps of this process are fast heating and rapid quenching. The individual droplets
    similar to those of CTS, however, this method addresses of smaller-length scales with very low thermal mass act
    the challenges faced by CTS and is complimentary to as a nanoreactor, thereby affording NPs while avoiding
    it. Thus, aerosol synthesis[22a,28] also involves aqueous the thermal and mass transfer gradients within the par-
    solutions of metal salts containing the required alloy- ticles. Like CTS, fast heating in the aerosol process also
    ing elements. These aqueous solutions are nebulized into results in decomposition of the precursor followed by rapid

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