Certificate of Analysis

Shell Trading (US) Company Our Reference Number: US230-0127621

Taylor Lippincott Lab Reference Number: 2020-DRPK-003620
1000 Main Street Level 12
Houston, TX 77002 Customer Reference Number: COLEX2DPR040820
United States of America

Customer Product Description:Ultra Low Sulfur Diesel Sample ID:2020-DRPK-003620-010

Location:Shell, Deer Park, Texas, United States Date Sampled:08-Apr-2020
Sample Representing:S/T V-8 Top After Transfer Date Submitted:08-Apr-2020
Drawn By:Intertek Date Tested:08-Apr-2020

Method Property Result Units

f
ASTM D4052 API Gravity @ 60°F 39.2 °API
Customer Product Description:Ultra Low Sulfur Diesel Sample ID:2020-DRPK-003620-012
Location:Shell, Deer Park, Texas, United States Date Sampled:08-Apr-2020
Sample Representing:S/T V-8 Upper After Transfer Date Submitted:08-Apr-2020
Drawn By:Intertek Date Tested:08-Apr-2020

Method Property Result Units

f
ASTM D4052 API Gravity @ 60°F 39.2 °API
Customer Product Description:Ultra Low Sulfur Diesel Sample ID:2020-DRPK-003620-014
Location:Shell, Deer Park, Texas, United States Date Sampled:08-Apr-2020
Sample Representing:S/T V-8 Middle After Transfer Date Submitted:08-Apr-2020
Drawn By:Intertek Date Tested:08-Apr-2020

Method Property Result Units

f
ASTM D4052 API Gravity @ 60°F 39.2 °API
Customer Product Description:Ultra Low Sulfur Diesel Sample ID:2020-DRPK-003620-016
Location:Shell, Deer Park, Texas, United States Date Sampled:08-Apr-2020
Sample Representing:S/T V-8 Lower After Transfer Date Submitted:08-Apr-2020
Drawn By:Intertek Date Tested:08-Apr-2020

Method Property Result Units

f
ASTM D4052 API Gravity @ 60°F 39.2 °API
Customer Product Description:Ultra Low Sulfur Diesel Sample ID:2020-DRPK-003620-018
Location:Shell, Deer Park, Texas, United States Date Sampled:08-Apr-2020
Sample Representing:S/T V-8 Bottom After Transfer Date Submitted:08-Apr-2020
Drawn By:Intertek Date Tested:08-Apr-2020

Method Property Result Units

f
ASTM D4052 API Gravity @ 60°F 39.2 °API
Customer Product Description:Ultra Low Sulfur Diesel Sample ID:2020-DRPK-003620-020
Location:Shell, Deer Park, Texas, United States Date Sampled:08-Apr-2020
Sample Representing:S/T V-8 TUMLB Equal Composite After Transfer Date Submitted:08-Apr-2020
Drawn By:Intertek Date Tested:09-Apr-2020

Method Property Result Units

f
ASTM D4052 Specific Gravity at 20°C/4°C 0.8263
f
ASTM D86 Barometric Pressure 757.0 mm Hg

1114 Seaco Avenue, Deer Park, Texas 77536 USA ISO 9001:2015
Tel.: +1 713 844 3200 Fax.: +1 713 844 3330 ABS-QE Certificate # 30701

Report Generated: 09-Apr-2020 00:18

AT-2072.03
Page 1 of 3
 Certificate of Analysis
Our Reference Number: US230-0127621
Lab Reference Number: 2020-DRPK-003620
Customer Reference Number: COLEX2DPR040820

Customer Product Description:Ultra Low Sulfur Diesel Sample ID:2020-DRPK-003620-020

Location:Shell, Deer Park, Texas, United States Date Sampled:08-Apr-2020
Sample Representing:S/T V-8 TUMLB Equal Composite After Transfer Date Submitted:08-Apr-2020
Drawn By:Intertek Date Tested:09-Apr-2020

Method Property Result Units

f
ASTM D86 Initial Boiling Point 159.0 °C
f
5% Recovery 176.8 °C
f
10% Recovery 184.0 °C Max 275.0
f
20% Recovery 199.8 °C
f
30% Recovery 216.7 °C
f
40% Recovery 234.6 °C
f
50% Recovery 251.2 °C
f
60% Recovery 268.0 °C
f
70% Recovery 284.8 °C
f
80% Recovery 302.3 °C
f
90% Recovery 325.1 °C Max 345.0
f
95% Recovery 342.4 °C
f
Final Boiling Point 352.4 °C
f
Recovery 97.9 Vol %
f
Residue 1.4 Vol %
f
Total Recovery 99.3 Vol %
f
Loss 0.7 Vol %
f
Corrected Loss 0.7 Vol %
f
Corrected Recovery 97.9 Vol %
f
Corrected Total Recovery 99.3 Vol %
f
ASTM D93 Procedure Used A
f
Corrected Flash Point 55.0 °C Min 45.0
f
ASTM D97 Pour Point -21 °C Max 0
f
ASTM D2500 Cloud Point -9 °C
f
ASTM D976 Cetane Index 50.8 Min 45
f
ASTM D613 Cetane Number 48.4 Min 45
f
ASTM D5453 Sulfur Content 7.8 mg/kg Max 15
f
ASTM D130 Copper Corrosion @ 50ºC (122ºF)/3 hr 1a Max 1
f
ASTM D524 Ramsbottom Carbon Res. (10% Dist.) 0.02 Wt % Max 0.35
f
ASTM D2709 Sediment and Water < 0.01 Vol % Max 0.05
ASTM D445 f
Kinematic Viscosity at 104 ºF/40 ºC 2.167 mm²/s 1.9 – 4.1
f
ASTM D482 Ash < 0.010 Wt % Max 0.01
f
ASTM D1500 ASTM Color <0.5 Max 2.5
ASTM D5186 Total Aromatics by SFC: 22.9 Vol % Max 35
Note: Result in Vol %
obtained utilizing
(CARB) correlation
calculation.
f
ASTM D6079 Major Axis 470 µm
f
Minor Axis 390 µm
f
Wear Scar Diameter 430 µm Max 520

1114 Seaco Avenue, Deer Park, Texas 77536 USA ISO 9001:2015
Tel.: +1 713 844 3200 Fax.: +1 713 844 3330 ABS-QE Certificate # 30701

Report Generated: 09-Apr-2020 00:18

AT-2072.03
Page 2 of 3
 Certificate of Analysis
Our Reference Number: US230-0127621
Lab Reference Number: 2020-DRPK-003620
Customer Reference Number: COLEX2DPR040820

Customer Product Description:Ultra Low Sulfur Diesel Sample ID:2020-DRPK-003620-020

Location:Shell, Deer Park, Texas, United States Date Sampled:08-Apr-2020
Sample Representing:S/T V-8 TUMLB Equal Composite After Transfer Date Submitted:08-Apr-2020
Drawn By:Intertek Date Tested:09-Apr-2020

Method Property Result Units

f
ASTM D2624 Temperature 20.0 °C
f
Electrical Conductivity 357 pS/m Min 25
f - Denotes analysis results which are ISO/IEC 17025 accredited by ANSI-ASQ National Accreditation Board
Product Meets NOM_016 SPECS
Results are only representative of the sample tested. All tests have been performed using the latest version unless otherwise indicated. This report shall not be reproduced except
in full without written approval of Intertek. Report is subject to our standard Terms and Conditions which can be obtained at our website: http://www.intertek.com/terms

Signed By: Date: 04/09/2020

William Riley

1114 Seaco Avenue, Deer Park, Texas 77536 USA ISO 9001:2015
Tel.: +1 713 844 3200 Fax.: +1 713 844 3330 ABS-QE Certificate # 30701

Report Generated: 09-Apr-2020 00:18

AT-2072.03
Page 3 of 3