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Effect of Post Welding Heat Treatment On The Mechanical and Microstructural Properties of Extra High Strength Steel Weld Metals For Application On
Effect of Post Welding Heat Treatment On The Mechanical and Microstructural Properties of Extra High Strength Steel Weld Metals For Application On
Jorge Carlos Ferreira Jorge, Sergio Maciel Faragasso, Luís Felipe Guimarães
de Souza & Ivaní de Souza Bott
To cite this article: Jorge Carlos Ferreira Jorge, Sergio Maciel Faragasso, Luís Felipe Guimarães
de Souza & Ivaní de Souza Bott (2015) Effect of post-welding heat treatment on the mechanical
and microstructural properties of extra high-strength steel weld metals, for application on mooring
equipment, Welding International, 29:7, 521-529, DOI: 10.1080/09507116.2014.932984
Effect of post-welding heat treatment on the mechanical and microstructural properties of extra
high-strength steel weld metals, for application on mooring equipment
Jorge Carlos Ferreira Jorgea,b,*, Sergio Maciel Faragassoa1, Luı́s Felipe Guimarães de Souzaa2 and Ivanı́ de Souza Bottc3
a
CEFET/RJ, DIPPG, Rio de Janeiro, RJ, Brazil; bFluke Engenharia Ltda., Rio de Janeiro, RJ, Brazil; cPUC-Rio, DEMA,
Rio de Janeiro, RJ, Brazil
Evaluation was performed of a weld metal with tensile strength higher than 860 MPa for welding R4 grade steel of standard
W22 of the International Association of Classification Societies, Ltd. Multipass joints were welded with preheating at 200
and 2508C, using the coated electrode process with a 4.0-mm-diameter consumable, the basic composition of which was:
C – 0.06%, Mn – 1.89% and Ni – 2.95%. After welding, mechanical and metallographic tests were performed on samples
entirely removed from the metal deposited in conditions as-welded and after post-weld heat treatment performed at 6008C
for 2 h. The results show that the weld metals obtained have mechanical properties suitable for all conditions of analysis,
providing properties superior to the minimum required for welding R4 grade steel used on petroleum platform mooring
equipment. The metallographic analysis enabled identification of the microstructure and explanation of the behaviour of the
mechanical properties after post-weld heat treatment.
Keywords: weld metal; mechanical properties; post-weld heat treatment
Table 1. Mechanical properties of steels according to IACS flame. Control of both the preheat and the interpass
standard W22 [3]. temperatures was performed with a properly calibrated
contact pyrometer.
LE LR Al RA Ecv to
Grade (MPa) (MPa) (%) (%) 2 208C (J) Table 4 shows the set of mean parameters used for
welding, while Figure 2 shows the sequence of deposition
R3 410 690 17 50 40 of weld passes.
R3S 490 770 15 50 45
R4 580 860 12 50 50
R4S 700 960 12 50 56
R5 760 1.000 12 50 58 2.3 Post-weld heat treatment (TTPS)
Notes: LE, yield strength; LR, endurance limit; Al-stretching; RA, Heat treatments consisting of heating at 6008C for 2 h were
reduction of area; Ecv, Charpy-V energy. performed, this condition being compared to the condition
of the as-welded joint.
The TTPSs were performed using equipment designed
investigate the influence of this treatment on the
specifically for this purpose, with electric resistance
mechanical properties of the weld metal, and thus the
heating, heat blanket insulation and temperature control
feasibility of using the same consumable for safe welding
via properly calibrated thermocouples. Controlled heating
of anchoring components made of R4 steels.
and cooling rates of 2008C per hour were used.
Table 2. Results of mechanical properties obtained for weld metals in the research programme [17 – 20].
Notes: CS, as-welded; TTPS, post-welding heat treatment; Ecv, Charpy-V energy; LR, tensile strength limit.
Element (% weight) C Si P S Mn Mo Ni Cr Cu V
Percentage of weight 0.06 0.24 0.007 0.008 1.89 0.58 2.95 0.46 0.02 0.02
Welding International 523
19
the minimum requirement for R4 grade steel;
(b) both the yield strength and the endurance limit
showed a decrease of approximately 10% due to the
25.4 9.5 increase of preheating;
(c) the TTPS did not cause changes in the mechanical
Figure 1. Details of the welding joint geometry used. properties.
Dimensions in mm.
Element C Si P S Mn Mo Ni Cr Cu V Ceqa
Percentage of weight 0.065 0.282 0.0105 , 0.008 1.978 0.412 2.661 0.435 0.010 0.025 0.748
a
Ceq ¼ C þ Mn/6 þ (Cr þ Mo þ V)/5 þ (Cu þ Ni)/15 [22].
524 J.C.J. Ferreira et al.
(a) In the columnar region (RC) of the last pass (‘Top the results were all above the level of 860 MPa. This is an
Bead’ (TB)), the predominance of martensitic extremely important fact, as, as discussed in the literature
microstructure is noted for both conditions and [10,11], obtaining high structural robustness values for the
(b) From the cut-out region of the Charpy-V specimens, consumables with greater resistance has been the greatest
it was found that the microstructure consists of focus of concern. Indeed, Surian and coworkers [11,23,24]
tempered martensite and bainite, with predominance emphasize that in some cases, it is important to control heat
of the latter constituent both in the RC as in the input in order to obtain the required strength, which was
reheated region (RR) in all conditions of analysis. also observed by Jorge et al. [17]. In the previous studies
conducted [17 –20], it was found that this parameter is a
critical point to overcome, as shown in Table 2. Note that in
this table, the yield strength was always below or very near
4. Discussion
the lower limit of 860 MPa, not providing conditions for
4.1 Mechanical properties safe behaviour of consumables used when considering
Table 6 shows the structural robustness results for the normal variations that may occur as a result of a different
different analysis conditions strength, which shows that race of the same consumable, changes of welder, welding
position or change of base metal [10].
Table 6. Results of tensile tests of the weld metal. According to Ramirez [10] and Surian et al. [11], one
way to get an estimate of the structural robustness of the
Weld LE LR Al RA
high-strength weld metal is by controlling the carbon
metal Condition (MPa) (MPa) (%) (%)
equivalent of the weld metal. However, this statement
M200 CS 875 967 21.4 62.9 should be regarded only from a qualitative point of view
TTPS 892 984 21.4 61.5 when working with high and extra high-strength weld
M250 CS 796 892 21.1 63.2
TTPS 772 900 22.3 63.2
metals, given the high degree of dispersion of results
Minimum 580 860 12.0 50.0 that the various weld metals can generate, depending on
R4 [3] the interactive effect of different alloy elements acting
on high-strength weld metals, which are still not fully
Notes: CS, as welded; TTPS, post-welding heat treatment. understood. Indeed, Figure 7 shows a compilation of
results from several authors [8,10,11,18– 20], where it
appears that the dispersion of results is enhanced for higher
Table 7. Results of impact tests at 2208C (J).
values of carbon equivalent, which prevents a reliable
First Second Third extrapolation of results based on other experimental
Weld metal Condition test test test Mean results.
M200 CS 97.0 95.0 86.0 92.7
This high degree of dispersion may be associated with
TTPS 84.0 85.0 98.0 89.0 significant microstructural changes. In fact, according to
M250 CS 90.5 89.5 107.5 95.8 Ramirez [25], for carbon equivalent values greater than
TTPS 99.0 93.5 101.0 97.8 0.47, low-temperature transformation products begin to
Minimum Base metal 50.0 predominate, including martensite. Moreover, Lord and
R4 [3]
Minimum Weld metal 36.0
Jennings [8] state that for the normal range of welding
R4 [3] cooling speeds, there is not sufficient temperability to form
only martensite, and the microstructure of the high-
Notes: CS, as-welded; TTPS, post-welding heat treatment. strength weld metal is a mixture of martensite and bainite.
140 CS 140 CS
TTPS TTPS
120 120
Absorbed energy (joules)
100 100
80 80
60 60
40 40
Minimum for R4 Weld Metal = 36 J Minimum for R4 Weld Metal = 36 J
20 20
0 0
–60 –40 –20 0 20 –60 –40 –20 0 20
Test Temperature (°C) Test Temperature (°C)
M200 M250
Figure 3. Variation of the energy absorbed from the weld metals with the test temperature.
Welding International 525
400 400
CS CS
380 TTPS 380 TTPS
360 360
340 340
320 320
300 300
280 280
260 260
0 2 4 6 8 10 12 14 16 0 2 4 6 8 10 12 14 16
Distance from the Surface (mm) Distance from the Surface (mm)
M200 M250
Yet Svensson [9] states that weld metals with yield ferrite, martensite and bainite, and depending on the
strength higher than 690 MPa have a microstructure percentage of each of these constituents, there will be a
consisting of acicular ferrite, martensite and bainite. change in the mechanical properties of the weld metal.
Concurring with these arguments, Karlsson et al. [12] Therefore, in this range of chemical composition, it is not
report that the microstructures of high-strength weld surprising that the cooling rate has a strong influence on
metals containing from 2% to 3% Ni consist of acicular mechanical properties.
As-welded TTPS
TB
B
RC
RR
Figure 5. Microstructural aspect of M200 weld metal observed by MEV. Attack: 2% nital.
526 J.C.J. Ferreira et al.
As-welded TTPS
TB
M
RC
RR
Figure 6. Microstructural aspect of M250 weld metal observed by MEV. Attack: 2% nital.
All of this evidence reinforces the need to seek a weld metal number 6, which also showed interesting
consumable that facilitates a weld metal with tensile behaviour from the point of view of endurance limit, did
properties superior to those found in Table 2, so that all not have the same behaviour of impact toughness after the
these variations are considered when qualifying a welding post-weld heat treatment.
procedure. Thus, the weld metal that meets these In this respect, it is important to mention that some
characteristics is precisely the one used in this study, as publications [8,12,14] using consumables with basic
chemical composition (C – 0.05, Mn – 2.0, Si – 0.30, Cr
1200 – 0.40, Mo – 0.60, Ni – 3.0) similar to this study have shown
that the properties are maintained within the same level,
1100 regardless of welding conditions. In fact, Table 8 shows a
Structural Robustness (MPa)
Table 8. Mechanical properties obtained with the welding consumable similar to that of this study, for various experimental conditions
[8,12,14].
Weld number 1 [12] 2 [12] 3 [12] 4 [12] 5 [12] 6 [12] 7 [12] 8 [12] 9 [8] 10 [14]
Temperature interpass (8C) 125 150 200 200 200 125 200 250 250 250
AT (kJ/mm) 1.4 1.3 1.1 1.3 1.3 1.8 1.7 1.7 1.0 1.4
LE (MPa) 978 885 922 885 844 939 858 734 872 756
LR (MPa) 994 942 953 929 938 972 931 924 922 945
Ecv (þ208C) 86 101 94 105 104 84 87 88 102 80
Ecv ( – 408C) 74 87 77 64 78 77 74 50 79 50
both preheatings (Figures 5 and 6) permit inference by the case, and in most cases, the value of occurrence was
uniformity of these same regions. The major difference approximately 1% variation.
observed in the microstructure is precisely in the RC in In the specific case of the weld metal in the study
the last pass (TB), which, however, does not contribute to (Table 6), the differences were similar to this, also in the
impact resistance, as it is not part of the Charpy-V order of 1% for both cases. It should also be pointed out
specimen. that, of equal importance, for studies involving the
This same evidence is also noted in the results of the variation of heat treatment time on structural robustness
Vickers hardness tests (Figure 4), where a drop in hardness [18], significant variations were not observed (Figure 8).
of the region near the surface for the rest of the welded In this figure, it is noted that the biggest difference in
joint is observed, with stabilization of this property for the structural robustness is due to the difference in preheating,
remainder of the thickness. confirming the discussion of the previous item.
Implementation of post-weld heat treatments tends to
produce microstructural changes that affect toughness, in
4.2 Effect of post-weld heat treatment some cases improving it and in other cases weakening it,
There are many studies on high-strength welding metal, as this effect being highly dependent on the chemical
previously mentioned, which are important reviews on the composition and microstructure of the weld metal in the
effect of chemical composition on microstructure and as-welded condition.
mechanical properties. Yet there are few publications The microstructural analysis conducted by electron
available on the effect of post-weld heat treatments on microscopy (Figures 5 and 6) highlighted the predominant
these weld metals. Publications that address this issue are occurrence of martensitic microstructure in the region of
normally studying the effect of a particular element [26 – the last pass, and bainite in the region at the tip of the
33], excluding compositions rich in various alloying Charpy-V notch, with similar morphology for both weld
elements, and hence the synergistic effect between these metals.
elements. Other studies [34 – 36] that address this type of This microstructural evidence is important because it
composition do not involve weld metals with structural shows that the occurrence of similar microstructure is the
robustness of the order of 860 MPa, as studied in this case. reason that the toughness of the weld metal is the same for
Thus, this paper aims to contribute in this regard to all experimental conditions used in this study.
conduct an analysis of the effect of TTPS on the As with the results of structural robustness (Figure 8),
mechanical properties of extra high-strength weld metal, a similar behaviour was observed for impact toughness in
mainly because the previous results have registered the
complex effect of this procedure on these properties. 1200
Most studies involving the effect of TTPS on
mechanical strength [6,17 – 20,26 – 40] report a drop of
Resistance Limit (MPa)
100
under study can be used in welding R4 grade steels [3],
M250 using preheating to 2008C and post-weld heat treatment at
80
M200 6008C for 2 h.
60
40
Minimum for R4 weld metal 5. Conclusions
20 Based on what was shown in the course of this study, it can
be concluded that:
0
0 1 2 3
Treatment time (h) (a) the weld metal studied was suitable for use in welding
R4 grade steel of the IACS standard W22;
Figure 9. Effect of TTPS time on the mechanical strength/ (b) all results of mechanical strength/structural robust-
structural robustness of the weld metal [18].
ness and impact toughness were higher than the
minimum required for the R4 grade steel of IACS
regard to variation in heat treatment time, as shown in standard W22;
Figure 9, showing not only an important uniformity of the (c) the impact toughness showed better results than those
results but also proximity of values for the experimental required, even for temperatures of 2 608C;
conditions used. (d) the post-weld heat treatment did not cause changes in
the impact toughness of the weld metal under study.
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