Dote

Apermcnt
Poge No.
Kao/A I8/12
ExPERIMENT NO. 1

AIrl: 1o dSéle srire he stsernqlh of commetial hydeochkic

acid (HC), J0ml sf which have been dissolueb pes bte t the
qiven selution.

APPARAos INVOLVE D: Pipette

Busette
Stand an8 White papes
Ceni cal {lask
Measuaip Cylinder
No, Co, t Methyt Csange
ChemicalS invslve8: Sediom Cazbenate (Na,Co,)
Hydsschlo9ic Acid (HCL)
Dstiiled Wates
Metht Osange
IhegAy
Toatiom process involved belween HC anS Na,cO,_ Acid-Bose tratien,
. Methe Ozanqe is use9 a an indicaton intke give Htati en
A t pH valves less Thay 3-1, m t etanye s_pink an at pH vale
q7eaTes than . 4 ,itwlbe yelloo,
ond
In the ange between 3.1 and 44,'o mistose pink
the miJle othisxaOge,
yello colousy ase ebtaine8. Jn
in coleun,
&llion appe ars to be onange
4. En peint îs achieved when Soltion Toong em yellow
yellaw ts
to
pink.
DELTA
 Tadcatas MMethyl Oxanqe 2K.0/A1a
Resenalting Stuctuse ef Methyt Otange

-N=N- sN
CH)N
BenzenefI ST5uctuse, qellow în coleui

OH

eP =N- N , Na

celeu
dineneid Stuctose, Pink n

tnS peint: Yellow to Pink (ood go lotio)

in the buaete
 Expcrment Dotc

Poge No.

Proceduse:
(ornmeveial H
Hs the qiven 8eltion oHc havinq l0m of
(neasly_lON) in l00 mL. Hernce, The gtandaad 861ution ta
be
Poeared Sheuls neasly hae 8ome 0gAmality.

, Prepxation el 0-1N SelJtion 0 80drun Codbenate

q 4 q Caqa qrade Na,CO was dsieb n a ukighing
sttle at I50 -160c o heuR, and then Cocleend tel in
desiccars6
35 q dsied No,Co, wag acorately weighed out by methsd
tsanhesses t arbs ate 50ml vølbmTsic
o deseni and
lask, and 40-50ml distlle8 uwates was a8Ie and getly
stisres T dsselue te'selts.
make up the velume
3. Yhen msne distillewates wa adde0 to
upts50 nl and wa8 mixe8 wel.
his standas Na,C0 38ltien (0.IN) wh+ch as_poepaged.

.Ttotficn
selution.
Bubette uwas insed and iled uith qiven acid
Hobubbleg weve Becneve onswas Set en zes8 mash.
ot into
loml o 1he 31andasd N, CO galutien wal pipetel
100tfsatien lask.
1 doep o nhytanqe was adde) t this falion lask
|5. Na,co, 301hien in titaadibn ask was Htsatelh HC t8 a
Shaap
colgusn change thatg, tpiok coleun wa oUa inel
"Shis Pooceg8uwa epeated wh evesy loml aNa, Co, &slgfien
DELTAnthl Thsee Cerc@1darl ealinq a wese gbtaine.
 Chemical Roaction invalve
k0A/

Chemical Reacuens

HCL+Na,cO NaHCo, t NaCl

NaHCO, +HCl Nacl+ H,0 +Co
enic Reack cns:

co +Ht HCO
CO
HCO +H HO+ CO
Obsexvafiens
. Psepasoion of OlN geltion df 3edu casbenate:
wei ght s The weiqhinq bstle, w 80 gm
werqht of the eiqhing bettle + Nao, 81:395 g
weiqht the weighing bettle
affex fsassesaing the Salt, w=S0 n
weighTNa,co, fransfessed fo volometsic ask, w=(-e 1:395 qn
Velume esslutien made 250 m.

a. lToctien
Velune oNo, (0, Solution faken. te each htaton IO m
=

Busette eadngs: T tratien o Na, Co, vs HCL

S.No Ttial Readjog Final Realog Vol. of HCL_use{my
my 8.6
O 86
3-6
5:8 8.6
. 25-3 345
 NIoAI3/
Calclations
. Psepazat on e0N Solution sodium casbona te

N= hram eq, Selufe - Weight x l000

Velume Seln. Ta ltbe Egivalest Wetght Vml

Fouivaleat weiqht Melas fass

=
= l06-53 qm
n

Nemal'ty N a , Co el3en = u,-u) x looo

.325x 1000
53 250 53x25o
O-I N

Taon
.TS caldte Nohmalty s d. HCL 3oluten, apply nemalty equatien:

AVc= Nco. .to

) NH Na,co,
Vo,co,H
=NACE Oelxi =0.1163 N
86
Strength e d. HcL 3elston= NnC36.5 9/e (3senat- Nsimy xEh, ui
0 1163 36-5q/
42450 g/l

Sine, Cerneneaial H was dtes too tfimes (loml in 1000 mL) , tRe slsepalh
eCemmescial Hcl Con be eltaines by muJHplying tne slsength sf diei

et. HCL by 100.

Hen ce
sfrenqth o Commeris) HCl= Nnc *36 5 x 100 g/
OI163 x36-5 x1o0 q/

434.50 g/
 Experiment Date
Kao/A IS/R Page No.

Result: Ssength e Commesciol HCI S44-50 g/2

Precatns
||.Osoally an ais bubble 1S psesent in nO33le ef The
bugetfe if mosT be rerneved beto1e taking The initial
eoding.
Alas
.Hluayg Dead lowe s meniscI in_Cafe e Coleueless
6lutionan oppex meniscuR in caae celeused
8slotieng
Ds net blew thyeugh the_pipette to escape The last|
gelotifenreomt Simply Touch 7he ioney Sustace
the Tsati enflask with noz3le ef the_pipette
poeceSS

Shakinq othetisation lask SheulS be cestinvsus

during adJinq the 6the bvsetfe.
Selston sem

. The funnel 'muST be semove8 betee stasting Ith

the titoalTon

DELTA