Vallourec Tubes France (A01) INSPECTION CERTIFICATE (A02)

TUBERIE MONTBARD 3.1 EN 10204:2004

ROUTE DE SEMUR
21502 MONTBARD
FRANCE Hamilton Metals, //&
No. : 822Va19 (A03)
QC: JG
Page: 1 / 7
6SHF: 4140-80
RR: 16702-2 Date: 12.09.2019
Date: Sep 12, 2019
Please scan this QR Code with your device to access the Vallourec Inspection certificate check site or send an email to valguard@vallourec.com

(A01) (A08.1)

Vallourec Tubes France Vallourec-Order-No. 249283

(A08.2)

Suborder
(A06.1)

Customer
HAMILTON METALS
29315 KATY BROOKSHIRE RD
KATY 77494
(A06.2) (A07.2)

Orderer Orderer Order-No. 21008002-110455 28.06.2018

VALLOUREC USA CORPORATION / HOUSTON TX 77042
(A07.3)

Client's Client Order-No MO16702

(B01, B02, B04) Hot finished seamless
Description of the product Hot finished seamless steel pipes
For OCTG accessories
ASTM A519, 2006 reapproved 2012
NACE MR0175 / ISO 15156-2 : 2009 / EN ISO 15156-2 : 2009, annex A.2.1.2 / NACE MR0103 : 2010 paragraph
2.1
4140-80, according Vallourec Industry Division - OCTG Mechanicals data sheet 4140 (OGA-01), Rev. 7,
November 07-2016
Ends plain, square to tube axis
Outside with dry varnish
Without inside rust protection
NO MERCURY, MERCURY COMPOUNDS OR MERCURY CONTAINING INSTRUMENTS AND/OR EQUIPMENT HAVE BEEN USED IN ANY
MANNER WHICH MIGHT CAUSE A CONTAMINATION IN MANUFACTURE, ASSEMBLY, OR TEST OF MATERIAL.
NO WELD REPAIR WAS PERFORMED.
NO RADIATION CONTAMINATION

(A13) (A09) (B14) (B09) (B10)

Vallourec Orderer Item text Dimensions Single length

Item Item
2 OD 3.500 x WT 0.875 Inches Random length from 24 to 31 ft
OD Tol ± 1 %
WT Tol : ± 12.5 %
Deviation from straightness max. 0.2 %
of the tube length
Vallourec Tubes France (A01) INSPECTION CERTIFICATE (A02)

TUBERIE MONTBARD 3.1 EN 10204:2004

ROUTE DE SEMUR
21502 MONTBARD
FRANCE
No. : 822Va19 (A03)

Page: 2 / 7
Date: 12.09.2019

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(A13) (A09) (B07.1) (B07.2) (B08) (B11) (B13)

Vallourec Orderer Heat HT lot Quantity Total length Weight

Item Item ft lb
2 991621 15LT0220 24 727.740 17 824

(C71)

HEAT CHEMICAL ANALYSIS

Steel vacuum degassed

(B07.1) (B15)

Heat Process C Si Mn P S Cr Mo Ni Sn Cu
% % % % % % % % % %
min - 0.38 0.15 0.75 - - 0.90 0.15 - - -
max - 0.43 0.35 1.00 0.025 0.015 1.10 0.25 0.25 0.030 0.25

991621 Electric (EAF) 0.39 0.23 0.90 0.009 0.002 0.95 0.21 0.13 0.006 0.11

(B07.1)

Heat Al Ti Nb(Cb) V N B
% % % % % %
min - - - - - -
max 0.035 0.030 0.050 0.030 0.020 0.0008

991621 0.015 0.002 0.0000 0.003 0.007 0.0008

Heats fully killed

(C72)

PRODUCT CHEMICAL ANALYSIS

(B07.1) (C00.1)

Heat Test Piece C Si Mn P S Cr Mo Ni Sn Cu

% % % % % % % % % %
min 0.38 0.15 0.75 - - 0.90 0.15 - - -
max 0.43 0.35 1.00 0.025 0.015 1.10 0.25 0.25 0.030 0.25

991621 . 0.40 0.24 0.90 0.008 0.003 0.95 0.21 0.13 0.005 0.11
15LT0220
991621 1AAV 0.39 0.22 0.91 0.009 0.002 0.94 0.19 0.12 0.006 0.12
15LT0220
Vallourec Tubes France (A01) INSPECTION CERTIFICATE (A02)

TUBERIE MONTBARD 3.1 EN 10204:2004

ROUTE DE SEMUR
21502 MONTBARD
FRANCE
No. : 822Va19 (A03)

Page: 3 / 7
Date: 12.09.2019

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(C72)

PRODUCT CHEMICAL ANALYSIS

(B07.1) (C00.1)

Heat Test Piece Al Ti Nb(Cb) V N B

% % % % % %
min - - - - - -
max 0.035 0.030 0.050 0.030 0.020 0.0008

991621 . 0.017 0.002 0.0000 0.003 0.007 0.0008

15LT0220
991621 1AAV 0.016 0.002 0.0000 0.002 0.007 0.0007
15LT0220

(C00.1)

Test Piece Sample

HT lot / Inspection Lot

PROCESS GUARANTEE
Merchandise is free of mercury contamination and no weld repair was
performed. No radiation contamination

(B04)

HEAT TREATMENT
Induction heat treatment

Heat treatment type Temperature Soaking time Cooling

Tempering 1207 °F 7 min Air

Induction Quenching 1657 °F 3 min Polymer

TENSILE TEST RESULTS

Type (C10.1) Round
Test temperature (C03) Room temperature
Direction (C02) longitudinal
Vallourec Tubes France (A01) INSPECTION CERTIFICATE (A02)

TUBERIE MONTBARD 3.1 EN 10204:2004

ROUTE DE SEMUR
21502 MONTBARD
FRANCE
No. : 822Va19 (A03)

Page: 4 / 7
Date: 12.09.2019

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TENSILE TEST RESULTS

(B07.1) (C00.1) (C10.2) (C11) (C11) (C12) (C13.2) (C15)

Heat Test Piece Dimension YS YS TS Elong. Red.Area

Rp0,2 Rp0,5 Rm 2" Z
in / sq in psi psi psi % %
min - 80000 80000 95000 20.0 45
max - 95000 95000 120000 - -

991621 1AAV 0.50 87168 87458 105297 29.5 68

15LT0220 0.19

(C00.1)

Test Piece Sample

HT lot / Inspection Lot
(C10.2)

Dimension Test piece dimensions

Test piece area

IMPACT TEST RESULTS

Type (C40) Charpy V
Test temperature (C03) 32 °F
Direction (C02) longitudinal

(B07.1) (C00.1) (C41) (C42.1) (C42.1) (C42.1) (C43.1) (C42.2) (C42.2) (C42.2)

Heat Test Piece Dimension Impact1 Impact2 Impact3 Mean Shear fr1 Shear fr2 Shear fr3
in / sq in ft-lbf ft-lbf ft-lbf ft-lbf % % %
min - 22.1 22.1 22.1 30 - - -
max - - - - - - - -

991621 1AAV 0.39x0.39 101.0 104.7 105.2 104 80 80 80

15LT0220 0.12

(B07.1) (C00.1) (C41) (C42.3) (C42.3) (C42.3)

Heat Test Piece Dimension L.Exp1 L.Exp2 L.Exp3

in / sq in in in in
min - - - -
max - - - -

991621 1AAV 0.39x0.39 0.026 0.030 0.026

15LT0220 0.12

(C00.1)

Test Piece Sample

HT lot / Inspection Lot
Vallourec Tubes France (A01) INSPECTION CERTIFICATE (A02)

TUBERIE MONTBARD 3.1 EN 10204:2004

ROUTE DE SEMUR
21502 MONTBARD
FRANCE
No. : 822Va19 (A03)

Page: 5 / 7
Date: 12.09.2019

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IMPACT TEST RESULTS

(C41)

Dimension Test piece dimensions

Test piece area

IMPACT TEST RESULTS

Type (C40) Charpy V
Test temperature (C03) 14 °F
Direction (C02) longitudinal

(B07.1) (C00.1) (C41) (C42.1) (C42.1) (C42.1) (C43.1) (C42.2) (C42.2) (C42.2)

Heat Test Piece Dimension Impact1 Impact2 Impact3 Mean Shear fr1 Shear fr2 Shear fr3
in / sq in ft-lbf ft-lbf ft-lbf ft-lbf % % %
min - 22.1 22.1 22.1 30 - - -
max - - - - - - - -

991621 1AAV 0.39x0.39 104.5 109.0 110.0 108 80 80 80

15LT0220 0.12

(B07.1) (C00.1) (C41) (C42.3) (C42.3) (C42.3)

Heat Test Piece Dimension L.Exp1 L.Exp2 L.Exp3

in / sq in in in in
min - - - -
max - - - -

991621 1AAV 0.39x0.39 0.028 0.028 0.028

15LT0220 0.12

(C00.1)

Test Piece Sample

HT lot / Inspection Lot
(C41)

Dimension Test piece dimensions

Test piece area

HARDNESS TEST RESULTS

Method of test (C30) Rockwell C
Vallourec Tubes France (A01) INSPECTION CERTIFICATE (A02)

TUBERIE MONTBARD 3.1 EN 10204:2004

ROUTE DE SEMUR
21502 MONTBARD
FRANCE
No. : 822Va19 (A03)

Page: 6 / 7
Date: 12.09.2019

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HARDNESS TEST RESULTS

(B07.1) (C00.1) (C01.5) (C31.3) (C31.3) (C31.3)

Heat Test Piece Orientation Readings Readings Readings

HRC HRC HRC
min - - -
max 22.0 22.0 22.0

991621 1AAV O 17.5 17.9 17.5

15LT0220 M 17.9 17.9 17.1
I I 17.5 16.9 17.6

(C00.1)

Test Piece Sample

HT lot / Inspection Lot
Quadrant
(C01.5)

Orientation O : Outside
M : Middle
I : Inside
(C31.3)

Readings Hardness impressions

(D51)

MICROGRAPHY
Test Conditions Test rate Result
Grain size ASTM E112 : 6 OR FINER 100% Guarantee

MICROGRAPHY - OTHER TESTS

Test Conditions Test rate Result
Inclusion count ASTM E 45 Méthode A, série fine : 1 per heat Satisfactory
A2.5-B2.5-C2.5-D2.5, série épaisse :
A1-B1.5-C1.5-D1.5

(D55)

OTHER TESTS ON PIPE

Test Conditions Test rate Result
UT longitudinal UT test to API L4 (ID) / L2 (OD) Without Frequency Satisfactory
Appearance & Dimensions Aspect & Dimensions (spécifique) Without Frequency Satisfactory
Ultrasonic testing for transverse UT test to API L4 (ID) / L2 (OD) Without Frequency Satisfactory
defect
UT wall thickness API 5CT Without Frequency Satisfactory

(A04, B06)

MARKING, IDENTIFICATION
Vallourec Tubes France (A01) INSPECTION CERTIFICATE (A02)

TUBERIE MONTBARD 3.1 EN 10204:2004

ROUTE DE SEMUR
21502 MONTBARD
FRANCE
No. : 822Va19 (A03)

Page: 7 / 7
Date: 12.09.2019

Please scan this QR Code with your device to access the Vallourec Inspection certificate check site or send an email to valguard@vallourec.com

(A04, B06)

MARKING, IDENTIFICATION

2 Marking painted in continious %% LOGO VLR - VALLOUREC - VBT - ASTM A519 - 3.500 0.875 INCH -
4140-80 - %%HT N° COULEE - ZFI - 249283 - 2 -21008002-110455 -
MO167 02 - FRANCE

Enclosures
Test samples taken at mid-wall

(Z01)

The supplied products are in compliance with the requirements of the order

(A05, Z02, Z03)

Date 12.09.2019
Validated by Inspection Representative
Jonathan SPINELLI

+33 3 80 89 54 40

@ jonathan.spinelli@vallourec.com
Stamp

Indication in parentheses correspond to attributes according to EN 10168

This testimonial and certification respectively may neither be modified nor used for other products. Offences are regarded as falsification of documents and will be subject to criminal prosecution.