文件编码（ DOC NO.

）： PRF-COA-BP202001

产品分析证书
Certificate of Analysis

中文名称： 4'-甲基醚金连木黄酮
Structure
English Name：Ochnaflavone 4'-methyl ether
别名 (Alias):

产品编码 (Cat. No.):BP2020

CAS Number: 49619-87-6
分子式 (M. F.): C31H20O10
分子量 (M. W.): 552.491

批号 (Batch No.): PRF21083044

报告日期 (Report date): 2021-08-31

检验结果（ Analytical result） :

检验项目（ Test Item） 检验指标（ Specifications） 检验结果（ Results）

外观Appearance Yellow green powder Yellow green powder

干燥失重Loss on drying ＜3.0% 2.2%

纯度Purity (HPLC-DAD,330nm)* ≥98.0% 99.4%

质谱Mass 552.4±1 Conforms

核磁NMR Comply with the structure Conforms

* 色谱图见附件（ Please find HPLC chromatogram attached.）
检测方法（ Test Method）： Column: Thermo BDS Hypersil C18 ，4.6*100mm，2.4μm; Column temperature: 30℃; Detection Mode: UV330nm；Flow

Rate: 0.8ml/min; Sample dissolution: DMF; Mobile Phase: A, Acetonitrile B, 0.1% phosphoric acid in water； Gradient elution: A, 45%-55%,15min.

贮存条件（ Storage） :2~8℃, protected from light, keep package airproofed when not in use.
复测期（ Retest date） :Three years (2024-08-30) under conditions list above.

QC: QA:
Date: 2021-08-31 Date: 2021-08-31

备 注 (Remarks):The sample solutions should be prepared and used on the same day, it is the best preparing the solutions immediately before use. If the solutons have to be

made up in advance, it should be made as aliquots in tightly sealed vials at less than -20℃. Generally, these might be useable for up to two weeks. The quality of the

product is only guaranteed to comply with the attached COA.

In case of quality issue, please contact us within 30 days after receipt of the product.

Tel：+86-28-82633397 Fax：+86-28-82633165
http://www.phytopurify.com Email： sales@biopurify.com biopurify@gmail.com
 Chengdu Biopurify
SAMPLE INF O R MAT IO N
Sample Name: Ochnaflavone 4methylether Acquired By: PRF01
Sample Type: Unknown Sample Set Name
Vial: 58 Acq. Method Set: Ochnaflavone 4methylether
Injection #: 1 Processing Method sample
Injection Volume: 5.00 ul Channel Name: PDA Ch1 330nm@4.8nm
Run Time: 25.0 Minutes Proc. Chnl. Descr.: PDA Ch1 330nm@4.8nm

Date Acquired: 8/31/2021 11:52:08 AM CST

Date Processed: 8/31/2021 1:26:39 PM CST

Auto-Scaled Chromatogram

om
8.887

0.80

.c
0.60

ify
ur
0.40
op
yt

0.20
11.117

19.711
h
5.542

7.650
5.755
5.077

6.311
7.186

.P

0.00
w

0.00 2.00 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00
w

Peak Results
w

Height
Name RT Area % Area USP Plate Count USP Resolution
(µV)
1 5.077 5868 0.06 613 13662.72
2 5.542 13397 0.13 1170 7517.14
3 5.755 11719 0.11 897
4 6.311 5296 0.05 530 3225.33
5 7.186 3830 0.04 356 4041.21 4.01
6 7.650 13075 0.13 1262 8842.52 1.66
7 8.887 10188170 99.39 949309 16672.77 3.96
8 11.117 2742 0.03 306 25117.70 6.71
9 19.711 6354 0.06 323 13413.17 16.75

Reported by User: PRF01 Project Name: 2021\2021.7-9YUE

Report Method: Chengdu Date Printed:
Report Method ID4058 8/31/2021
Page: 1 of 1 1:27:54 PM PRC