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Pt5% SBA15
Pt5% SBA15
Pt5% SBA15
Page 1
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24
Surface Area
Single Point Surface Area at p/po=0.20000: 418.465 (m2/g)
BET Surface Area: 415.877 (m2/g)
Langmuir Surface Area: 425.420 (m2/g)
t-Plot Micropore Area: 11.017 (m2/g)
t-Plot External Surface Area: 404.860 (m2/g)
BJH Adsorption Cumulative Surface Area: 365.835 (m2/g)
BJH Desorption Cumulative Surface Area: 401.461 (m2/g)
Pore Volume
Total Pore Volume at p/p0 = 0.99000: 0.744 (cm3/g)
t-Plot Micropore Volume: 0.015 (cm3/g)
BJH Adsorption Cumulative Volume: 0.700 (cm3/g)
BJH Desorption Cumulative Volume: 0.715 (cm3/g)
DR Micropore Volume: 0.000 (cm3/g)
Pore Size
Average Pore Diameter (4V/A): 7.152 (nm)
BJH Adsorption Average Pore Diameter (4V/A): 7.651 (nm)
BJH Adsorption Most Frequent Pore Diameter (dV/dD): 8.865 (nm)
BJH Desorption Average Pore Diameter (4V/A): 7.123 (nm)
BJH Desorption Most Frequent Pore Diameter (dV/dD): 6.863 (nm)
HK/SF Micropore Analysis (< 2 nm)
Micropore Volume: 0.176 (cm3/g)
Most Frequent Pore Diameter: 1.251 (nm)
Median Pore Diameter: 0.697 (nm)
Isotherm Plot
Adsorption Desorption
530.07
477.06
424.05
Quantity Adsorbed(cm3/g STP)
371.05
318.04
265.03
212.03
159.02
106.01
53.01
0.00
0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0
p/p0
477.06
424.05
Quantity Adsorbed(cm3/g STP)
371.05
318.04
265.03
212.03
159.02
106.01
53.01
0.00
1e-2 1e-1
p/p0
0.00283
0.00252
0.00220
0.00189
1/[V(p0/p-1)]
0.00157
0.00126
0.00094
0.00063
0.00031
-0.00000
0.000 0.030 0.059 0.089 0.119 0.149 0.178 0.208 0.238 0.267 0.297
p/p0
0.00046
0.00041
0.00036
0.00031
p0/p/V
0.00025
0.00020
0.00015
0.00010
0.00005
0.00000
0.00 0.00 0.01 0.01 0.02 0.02 0.03 0.03 0.04 0.04 0.05
p/p0
t-Plot Report
t-Plot
194.5
175.0
155.6
Quantity Adsorbed(cm3/g STP)
136.1
116.7
97.2
77.8
58.3
38.9
19.4
0.0
0.000 0.069 0.139 0.208 0.278 0.347 0.417 0.486 0.556 0.625 0.695
t (nm)
Kelvin Equation
rk = -0.414/ln(P/Po)
Broekhoff-de Boer Equation
log(p/p0) = 0.1682 exp(-0.1137t) - 16.11/t^2
0.25331
0.22517
0.19702
0.16887
dV/dD
0.14073
0.11258
0.08444
0.05629
0.02815
0.00000
1e+0 1e+1 1e+2
D (nm)
5.16910
4.59476
4.02041
3.44607
dV/dlogD
2.87172
2.29738
1.72303
1.14869
0.57434
0.00000
1e+0 1e+1 1e+2
D (nm)
0.69278
0.61581
0.53883
sum_dV(cm3/g)
0.46186
0.38488
0.30790
0.23093
0.15395
0.07698
0.00000
1e+0 1e+1 1e+2
D (nm)
0.69901
0.62134
0.54367
0.46601
dV/dD
0.38834
0.31067
0.23300
0.15534
0.07767
0.00000
1e+0 1e+1 1e+2
D (nm)
0.70771
0.62907
0.55044
sum_dV(cm3/g)
0.47180
0.39317
0.31454
0.23590
0.15727
0.07863
0.00000
1e+0 1e+1 1e+2
D (nm)
DR Plot
2.951
2.656
2.361
Quantity Adsorbed(cm3/g STP)
2.066
1.771
1.476
1.180
0.885
0.590
0.295
0.000
0.000 0.451 0.903 1.354 1.806 2.257 2.709 3.160 3.612 4.063 4.515
log(p0/p)^2
DA Equation
dV/dr = 6 * Vo * (Ks/E)^2 * r^(-7) * exp^[-(Ks/E)^2 * r^(-6)]
r(nm) dV/dr
0.40000 nan
0.45000 nan
0.50000 nan
0.55000 nan
0.60000 nan
0.65000 nan
0.70000 nan
0.75000 nan
0.80000 nan
0.85000 nan
0.90000 nan
0.95000 nan
1.00000 nan
2.00000 nan
3.00000 nan
0.000
0.000
0.000
0.000
dV/dD
0.000
0.000
0.000
0.000
0.000
0.000
0.000 0.212 0.424 0.636 0.848 1.059 1.271 1.483 1.695 1.907 2.119
DD (nm)
0.204
0.181
0.159
sum_dV(cm3/g)
0.136
0.113
0.091
0.068
0.045
0.023
0.000
0.000 0.212 0.424 0.636 0.848 1.059 1.271 1.483 1.695 1.907 2.119
DD (nm)
0.097
0.086
0.075
0.065
dV/dD
0.054
0.043
0.032
0.022
0.011
0.000
0.000 0.306 0.611 0.917 1.222 1.528 1.833 2.139 2.444 2.750 3.055
DD (nm)
0.205
0.183
0.160
sum_dV(cm3/g)
0.137
0.114
0.091
0.068
0.046
0.023
-0.000
0.000 0.306 0.611 0.917 1.222 1.528 1.833 2.139 2.444 2.750 3.055
DD (nm)
0.76
11.27
0.02897
0.02575
0.02253
sum_dV(cm3/g)
0.01931
0.01609
0.01287
0.00966
0.00644
0.00322
0.00000
0.00 1.13 2.25 3.38 4.51 5.64 6.76 7.89 9.02 10.15 11.27
D (nm)