K NLABORATORY Doc No KL-OF-7.8.1 K.N. Biosciences (India) Pvt Ltd, Survey. No. 487, Bachupally, ee Hyderabad-72 PageNo. tot ‘Cause effective diagram showing uncertainty components weighing uncertainty Mass concentration Z Temperature 7 flow uncertainty 1 Initial weight of filter papper 2. Uncertainty in conditioning 3. Final weight of filter papper 4 Calbration of Rotometer 5. Calibration of timer 6 Uncertainty in temperature 1 Initial Weight of Filter papper Weights were taken in calibrated balance ID no.kNL/CHEM/BAL, a Calibration: The variation in 2.8 gram weighing is 0.01 Filter paper Weight 2.5968grms Ucalib = 0.01/V3, 0.005773503, b ULinearity 0.0002 Ulinearity = 0.0002/v3 = 0.00011547 c Urepeatabilty (standard Deviation) 0.002 0.002 A Total uncertainty due to initial weight: va"+b*<* 0.006 2 Uncertainty In conditioning a Prebaked time variation 24 Uncertainity(HR} os 0.288675135 Total uncertainty calibration 0.2887 3 Final Weight of Filter papper Weights were taken In calibrated balance ID no.KNL/CHEM/BAL, a Calibration: The variation in 3 gram weighing is 0.01 Filter papper Weight 3ems Ucallb = 0.01/V3 0.00877 b ULinearity 0.0002 Ulinearity = 0.0002/V3 = 0.000115 c Urepeatabilty (standard Deviation) 0.002 0.002 B_ Total uncertainty due to Final weight: Va*4b*4c? 0.006 3 ‘calbration of Rotometer © The Uncertinity is given as (Type A) 0.001 0.001 4 Uncertinity in Calibration of timer D__ The Uncertinity is given as ( Type A) 02 Calculated value of PM10 = 173yg/m* . Taking time of monitoring as 480mints and Manometering= 1.26L/ 5. Uncertainity in Temperature Calibration set temperaturef*C) 25 Uncertainity["C] 03 Total uncertainty calibration =0.8+V3 0.173,UNCERTINITY BUDGET Standard Relative standard Uncertai uncertainty DESCRIPTION VALUEX U(X) uxyK 1 uncertainty due to initial weight of filter papper Uwtini 2.8grms 0.006 0.0021 2 uncertainty due to final ‘weight of flter papper Uwt-fin 2.9047¢em 0.006 0.00206 3° Uncertainty in conditioning _Ucond 24 hrs 0.288675 0.012028131 3. Uncertinity in calbration of Rotometer Ucal.roto 1.264/m 0.001 0.0008 4 Uncertinity in Calibration oftimer Ucal.tim 4gomints 0.2 0.000417 5 Uncertainity in temperature Utemp 25 0.173 0.00692 ‘The uncertinity associated with each component are combined as = ‘VUwt.ini*+Uwt fin*+Urot.cal2+Utim.cal?= 0.01421 Combined standard uncertinity in analysing PM10 in amient air = (Analysed value x 0.00307) = 173%0,0142 = 2.457 Expanded uncertinity = combined uncertinity x 2 (95% CL) =2 (4.36) Hence the values are expressed as PM10 IN AMBIENT AIR = 1734.92