Download as pdf or txt
Download as pdf or txt
You are on page 1of 31

Ellamera™

Multifunctional Rheology Modifiers

FORMULATION GUIDE
VERSATILE FORMULAS

Ellamera copolymer products can alter the rheology


of base ingredients, allowing formulators to achieve
results that enhance the beauty level while still
delivering a tactile experience. When dissolved in a
wide variety of synthetic, polar, ester or natural oils,
the products facilitate the transformation of these oils
into clear, thicker, shear thinning, thixotropic and
film-forming gels that meet a multitude of formulator
and consumer needs.

Ellamera grades may be used as a gelling agent or to


complement other ingredients. Increasing the oil
phase’s viscosity and enabling film-forming abilities
with high clarity allows formulators to reduce the
number of materials required for optimal effect.
Ellamera copolymer products deliver excellent oil
retention and water resistance – a perfect combination
for high-performing, long-lasting cosmetics.
POTENTIAL APPLICATIONS FEATURES & BENEFITS

Color Cosmetics Texture and Touch

• Lip gloss • Customizable texture


• Lipstick • Shear-thinning rheology
• Lip liner • Spreadable
• Mascara | Eye shadow • Film forming
• Blush | Foundation • Water resistant
• Concealer

Skincare Color

• Customizable color effects


• Mask
• High transparency to enhance
• Lotion & serum
truer,
• Face & body oil
• deeper, bolder colors
• High gloss
• Excellent suspension

Haircare Pro-natural & Sustainable

• Low residuals & hypoallergenic


• Oil treatment
• Compatible with natural oils
• Relaxer

Suncare

• Sunscreen
• Sunblock
• Lotion/spray/stick

3
Green Cleansing Oil
Example Formulation*
Description

A cleansing oil with medium viscosity is described. The formula provides a pleasant texture
with cleaning capabilities and features Ellamera PER-SUST™ 504 by Kraton.

Physical Properties

Appearance Fluid

Color Green

Odor N/A

Solubility Soluble

*The formulation above is intended for information purposes only based on the best of our knowledge. It is the responsibility of
the customer to undertake the appropriate testing to determine the suitability of the product for their intended use.

COMPOSITION

INCI Qty. % TRADE NAME FUNCTION

Cetearyl Ethylhexanoate 92.894 Saboderm CSO Emollient

Sorbitan Monolaurate 5.00 Radiasurf 7125 Cleansing agent

Hydrogenated Styrene Butadiene 2.00 Ellamera PER SUST Texturizer


Copolymer 504
Pentaerythrytyl Tetra di Butyl 0.10 Tinogard TT DD Antioxidant
Hydroxyhydrocinnamate
Unicert Yellow 0.004 Unicert Yellow Colorant

Unicert Green 0.002 Unicert Green Colorant


Saboderm is a trademark of SABO S.p.A; Radiasurf 7125 is a trademark from OLEON; TINOGARD is a trademark of BASF. Unicert
is a tradmark of Sensient Cosmetic Technologies.

4
EQUIPMENT
- Top stirring laboratory mixer
- Heating plate

PREPARATION
Phase A Phase C
Ellamera PER-SUST 504 2,00 Unicert Yellow 0,004
Saboderm CSO 92,50 Unicert Geen 0,002
Tinogard TT 0,10 Saboderm CSO 0,394

Phase B
Radiasurf 7125 5,00

Add Phase A ingredients in a beaker and heat for 30 minutes at 120°C and Mix at 400RPM for
~ 20 Minutes Until a Clear Solution Appears.

Cool Phase A down to 60°C and pour Phase B into Phase A beaker while stirring. Wait until a
white solution appears. Add Phase C ingredients while stirring to colour the solution.

PREPARATION NOTES
To make working with small amounts of colour easier, add 0.1 grams Unicert Green, 0.2
grams Unicert Yellow and 19.7 grams Saboderm to a beaker, mix with a spatula and add 0.4
grams of the mixture to the final product.

PACKAGING
No specific packaging requirements

SAFETY NOTES

- Always be attentive when using mechanical equipment


- Manage all the ingredients with correct PPE in accordance with safety guidelines
- Read the safety document from all the ingredients prior to formulating

Watch video for formulation guide to prepare Green Cleansing Oil

5
Sun Care Oil
Example Formulation*

Description

A sun care oil formulation exhibiting low viscosity is described.

The formula has been prepared with natural sunflower oil and includes UVA and UVB absorbing
compounds to protect the skin from harmful sunlight. It provides a pleasant feeling and moisture
retention of the skin with the texturizing and film-forming properties of Ellamera BI-THIN™ 602 by
Kraton.

Physical Properties

Appearance Fluid

Color Orange/brown

Odor Oily

Solubility Not soluble in water

SPF 15 (est.)

*The formulation above is intended for information purposes only based on the best of our knowledge. It is the responsibility of
the customer to undertake the appropriate testing to determine the suitability of the product for their intended use.

COMPOSITION

INCI Qty. % TRADE NAME FUNCTION

Sunflower oil 38.37 Sunflower Oil Emollient

Ethyl Hexyl Palmitate 32.00 DUB PO Emollient

Butyloctyl Salicylate 10.00 Sunsolv BOS Solubilizer and


photostabilizer
Homosalate 5.00 Eusolex HMS UV-B absorber

Octisalate 5.00 Escalol 587 UV-B absorber

Hydrogenated Styrene Isoprene 3.50 Ellamera BI-THIN 602 Film former


Copolymer

Avabenzone 3.00 Parsol 1789 UV-A absorber

6
Squalane
2.00 Phytosqualane Emollient

Tocopheryl acetate 1.00 Vitamin E Acetate Antioxidant

Pentaerythrytyl tetra di butyl 0.10 Tinogard TT DD Antioxidant


hydroxyhydrocinnamate

Beta-carotene 0.03 Beta-carotene UV-blocking colorant

* DUB PO is a trademark of Stearinerie Dubois; SunSolv is a trademark of Innospec Performance Chemicals; Eusolex is a trademark
of Merck; Escalol is a trademark of Ashland Specialty Chemical; Parsol is a trademark of DSM; 1789 TINOGARD is a trademark of
BASF.

EQUIPMENT
Top stirring laboratory mixer | Heating plate

PREPARATION
Phase A PHASE C
Ellamera BI-THINTM 602 3.50 Escalol 587 5.00
DUB PO 27.00 Eusolex HMS 5.00
Phytosqualane 2.00 Parsol 1789 3.00
Tinogard TT 0.10 Vitamin E Acetate 1.00
Sunsolv BOS 10.00
PHASE D
PHASE B Beta-carotene 0.03
Sunflower Oil 38.37 DUB PO 5.00

Add Phase A ingredients to a beaker and heat for 20 minutes at 120°C, and mix with a
laboratory mixer at 400 RPM for about 30 minutes until a clear solution appears. Cool down

Phase A to around 100°C and add Phase B into Phase A beaker while stirring.

After Phase B is mixed in, cool down to 60°C and add phase C ingredients. After Phase C
ingredients dissolve, add phase D slowly to the mixture until the desired color has been
reached.

PACKAGING
Test the compatibility with packaging material when using fragrance.

SAFETY NOTES
- Always be attentive when using mechanical equipment
- Manage all the ingredients with correct PPE in accordance with safety guidelines
Read the safety document from all the ingredients prior to formulating

Watch video for formulation guide to prepare Sun Care Oil

7
Concealer Cream
Example Formulation*

Description

An example of a concealer cream based on a water-in-oil emulsion with medium viscosity is


described. The formula provides a pleasant texture due to the film-forming properties of
Ellamera TER-SET™ 403 by Kraton. This example formulation is creamy to the skin and dries
quickly for easy and long-lasting use.

Physical Properties

Appearance Fluid

Color Tan

Odor Fragrance

Solubility Insoluble

*The formulation above is intended for information purposes only based on the best of our knowledge. It is the responsibility of
the customer to undertake the appropriate testing to determine the suitability of the product for their intended use.

COMPOSITION:

INCI Qty. % TRADE NAME FUNCTION

Water 30.00 Water Solvent

Squalane 27.00 Neossance Solvent


Hemisqualane
Talc/iron oxide/hydrogen 12.70 FDP-C-PA White Colorant
dimethicone
Ethyl Hexyl Palmitate 6.00 DUB PO Emollient

Hydrogenated Styrene Butadiene 4.50 Ellamera TER-SET 403 Film former


Copolymer

Caprylic/Capric Thickening and


Triglyceride/Stearalkonium 3.00 Miglyol Gel T
Emollient
Bentonite/Propylene Carbonate
8
Cetyl Diglyceryl Tris (Trimethylsiloxy)
3.00 DOWSIL ES 5600 Emulsifier
Silyl ethyl Dimethicone

Zinc Oxide 3.00 Zinc Oxide PHARMA Colorant

Polyethylene Wax 3.00 Performalene 400 Wax

Xylitol 2.50 Xivia Xylitol Humectant

Glycerin 2.00 Glycerin Humectant

Sorbitan Isostearate 1.00 Span 120 Emulsifier

Talc/iron oxide/hydrogen 0.80 FDP-C-DA Yellow Colorant


dimethicone
Hexandiol 0.50 Hydrolite 6 Preservative

Sorbitan Caprylate 0.50 Velsan SC Preservative

Talc/Iron oxide/hydrogen 0.15 FDP-C-DA-Black Colorant


dimethicone
Talc/Iron oxide/hydrogen 0.15 FDP-C-DA-Red Colorant
dimethicone
Pentaerythrytyl tetra di butyl 0.10 Tinogard TT Antioxidant
hydroxyhydrocinnamate
Frangrance 0.10 Fragrance Fragrance
* FDP-C-** is a trademark of Nikkol; DUB PO is a trademark of Stearinerie Dubois; MIGLYOL is a trademark of IOI Oleo GmbH;
DOWSIL is a trademark of Dow Corning; XIVIA is a trademark of DuPont; PERFORMALENE is a trademark of Baker Hughes; SPAN
is a trademark of Croda; HYDROLITE is a trademark of Symrise; VELSAN is a trademark of Clariant TINOGARD is a trademark of
BASF.

EQUIPMENT
- Top stirring laboratory mixer
- Heating plate
- Ultra Turrax homogenizer
- Powder mixer

PREPARATION
PHASE A PHASE B
Ellamera TER-SET 403 4.50 DOWSIL ES 5600 3.00
DUB PO 6.00 Span 120 1.00
Hemisqualane 27.00 Velsan SC 0.50
Performalene 400 3.00 Miglyol Gel T 3.00
Tinogard TT 0.10

9
PHASE D
PHASE C Water 30.00
FDP-C-PA White 12.70 Xylitol 2.50
FDP-C-DA-Yellow 0.8 Glycerin 2.00
FDP-C-DA-Black 0.15 Hydrolite 6 0.50
FDP-C-DA-Red 0.15
Zinc Oxide 3.00 PHASE E
Fragrance 0.10

- Add Phase A ingredients in a beaker and heat for 30 minutes at 90°C and mix with a
laboratory mixer at 400RPM for about 20 minutes until a clear solution appears.
- Add Phase B ingredients to a beaker and gently homogenize, then pour mixture into Phase
A beaker while stirring.
- Mix Phase C ingredients together using a powder mixer, and slowly add it to beaker
containing phases A+B slowly while stirring for a homogenous mixture.
- Cool down the A+B+C mixture to 60°C and check the Hemisqualane content via weigh scale
and correct if necessary. Homogenise using an Ultra Turrax.
PHASE D

Combine ingredients together until you get a clear solution:

Water 30.00 Xylitol 2.50


Glycerin 2.00 Hydrolite 6 0.50%

Add Phase D solution to the A+B+C beaker while under high stirring.

- Finally, homogenise using the Ultra Turrax for a second time and cool down to about 40 °C
with slow mixing.

- In the final step, cool down to room temperature and add the fragrance.

PREPARATION NOTES
Keep the mixing speed relatively low (± 400 RPM) in Phase A & B to prevent air bubbles from
forming. Control the evaporation of the Hemisqualane before adding the water phase.

PACKAGING
The example formulation for a concealer cream is formulated with Hemisqualane and needs
packaging that protects the evaporation of the volatile solvent during storage and
transportation. Test the compatibility with packaging material when using fragrance.

SAFETY NOTES
Always be attentive when using mechanical equipment
Manage all the ingredients with correct PPE in accordance with safety guidelines.
Hemisqualane can evaporate and always better to cover the vessel and use the good
ventilation. Read the safety document from all the ingredients prior to formulating.

Watch video for Kraton Ellamera™ Concealer Formulation Guide

10
LONG WEAR LIP GLOSS
Example Formulation*
Description

An example of a long-wear lip gloss formulation for a glossy finish is described. This lip gloss
formula provides long-lasting smoothness, color, and soft feel. Additionally, the formula
provides moisture retention with the film-forming properties of Ellamera™ from Kraton and
the skin-conditioning properties of phytosteryl isostearate.

Physical Properties

Appearance: Viscous Paste

Color: Pigment specific

Odor: Fragrant specific

Solubility Not soluble in water

COMPOSITION

INCI Qty. % TRADE NAME FUNCTION

Isododecane 45,35 Isododecane Solvent

Ethyl Hexyl Palmitate 20,00 DUB PO Emollient

Hydrogenated Styrene/Isoprene 11,00 Ellamera RAD THICK Film former


Copolymer 501
Caprylic/Capric 10,00 MIGLYOL GEL T Thickening agent
Triglyceride/Stearalkonium and Emollient
Bentonite/Propylene Carbonate
Phytosteryl Isostearate 5,00 NIKKOL Phytosteryl Active and
Isostearate Emollient

11
Polyethylene Wax 5,00 PERFORMALENE 400 Wax

Hydrogenated Styrene/Isoprene 1,50 Ellamera BI-THIN 402 Thickening agent


Copolymer and film former

D&C RED 30 1,20 SUNCROMA RED30 Color Lake

Titanium Dioxide 0,80 HOMBITAN ANATASE Color Pigment


PHARMA

Pentaerythrytyl tetra di butyl 0,10 Tinogard TT DD Antioxidant


hydroxyhydrocinnamate

Flavour 0,05 Flavour Flavour

* DUB PO is a trademark of Stearinerie Dubois; MIGLYO is a trademark of IOI Oleo GmbH; PERFORMALENE is a trademark of Baker
Hughes; SUNCROMA is a trademark of Sun Chemical; HOMBITAN is a trademark of Hunstman; TINOGARD is a trademark of BASF.

EQUIPMENT
- Top stirring laboratory mixer
- Heating plate
- Three-roll mill for pigment grinding

PREPARATION
Phase A Phase B
Isododecane 45,35 Miglyol gel T 10,00
DUB PO 20,0 Phytosteryl isostearate 5,00
Ellamera RAD THICK 501 11,0 Homibitan anatase 0,80
Ellamera BI-THIN 402 1,50 Suncroma DC RED30 1,20
Tinogard TT 0,10
PERFORMALENE 400 PE 5,00 Phase C
Flavour 0,05

Add phase A in a beaker and heat for 30 minutes on 100°C, mixing it with a laboratory mixer
(400 RPM) for roughly 30 minutes until the polymers are melted. After mixing, cool down the
Phase A mixture to 70°C and check the isododecane content via weigh scale and correct it if
necessary.
While phase A is cooling down, prepare the colour phase B. Start by homogenizing the
Miglyol gel T and Phytosteryl isostearate, then slowly add and disperse the Hombitan anatase
and Suncroma DC RED30 and mix / homogenize with a spatula.
Add phase B to the three-roll mill on the smallest setting and mill the colour mixture 3 times,
obtaining a coloured paste.
12
Add phase B coloured paste to phase A while stirring. Add the flavour component to the
product at 50°C and cool down to room temperature.

PREPARATION NOTES

Premix the Hombitan Anatase and Suncroma DC RED30 before to add at the liquid part

PACKAGING

Long Wear Lip Gloss is formulated with Isododecane and need packaging that protects the
evaporation of volatile solvent.

SAFETY NOTES
- Always be attentive when using mechanical equipment
- Manage all the ingredients with gloves and correct PPE
- Isododecane can evaporate and always better to cover the vessel and use good
ventilation
- Read the safety document from all the ingredients prior to formulating.

Watch video for Long Wear Lip Gloss Formulation Guide

13
MOISTURIZING BATH OIL
Example Formulation*
Description
An example of a moisturizing bath oil formulation providing moisture retention due to the
film-forming properties of Ellamera™ product from Kraton and Vitamin E. The moisturizing
bath oil with a micellar diffusion system disperses moisturizer components, which enable
long-lasting moisturizing effect on the skin.

Physical Properties

Appearance: Liquid Fluid

Color: Pigment specific

Odor: Fragrant specific

Solubility Not soluble in water

COMPOSITION

INCI Qty. % TRADE NAME FUNCTION

Ethyl Hexyl Palmitate 74,90 DUB PO Protective emollient and


solubilizer for polymer.

PEG 7 Glyceryl Cocoate 19,00 ZETEMOL HE Non-ionic surfactant,


used as emollient for
skin care products

Hydrogenated Styrene/Butadiene 4,00 Ellamera PER-SUST Film-former


Copolymer 504

Polyglyceryl-3 Diisostearate 0,40 LAMEFORM TGI Emulsifier

Fragrance 1,00 Fragrance Fragrance

Tocopheryl Acetate 0,10 Tocopheryl Acetate Antioxidant, active


molecule for the skin

14
Pentaerythrytyl tetra di butyl 0,10 Tinogard TT DD Antioxidant and
hydroxyhydrocinnamate discolorizing stabilizer

Siddha Sky Blue Oil 0,50 Campo Siddha Colorant


Indra Neelam Yenai
* DUB PO is a trademark of Stearinerie Dubois; ZETEMOL is a trademark of Zchimmer & Schwarz; LAMEFORM and
TINOGARD are trademarks of BASF; CAMPO is a trademark of CAMPO.

EQUIPMENT
- Top stirring laboratory mixer
- Heating plate

PREPARATION
Phase A

Add Ellamera PER-SUST 504, Tinogard TT DD and the DUB PO to a beaker, and mix with a
laboratory mixer at 100°C until dissolved.

Phase B

Add the Zetemol HE, Lameform TGI to a beaker and stir for another 30 minutes. Add Phase B
mixture to Phase A beaker after the Phase A mixture is cooled down to about 80°C.

Phase C

Add colorant Campo Siddha Indra Neelam Yenai, fragrance and the tocopheryl acetate to a
beaker and mix.

Finally, add the Phase C mixture to the Phase A+B mixture after it is cooled down to room
temperature.

PACKAGING

No restrictions, but always test the compatibility with packaging material when using
fragrances.

SAFETY NOTES
- Always be attentive when using mechanical equipment
- Manage all the ingredients with gloves and correct PPE
- Read the safety document from all the ingredients prior to formulating.

Watch video for Moisturizing Bath Oil Formulation Guide

15
SUNCARE CREAM
Example Formulation*
Description
An example of a long-lasting suncare cream formulation based on a water-in-oil emulsion with
medium viscosity is described. The formula provides a pleasant texture and moisture retention
with the film-forming properties of Ellamera™ by Kraton. This example formulation does not
contain chemical sunscreen; it is based on physical sun blocking agents such as
hydroxyapatite, titanium dioxide and zinc oxide.

Physical Properties

Appearance Fluid

Color White

Odor Fragrance

Solubility Not soluble in


water

SPF 20 (est.)

COMPOSITION

INCI Qty. % TRADE NAME FUNCTION

Water 33,00 Water Solvent

Isododecane 35,50 Isododecane Solvent

Hydroxyapatite 5,00 Apalight EMS Matte agent and


UV sunscreen
booster
Titanium Dioxide 5,00 Titanium Dioxide ST- UV sunscreen
410WB
Hydrogenated Styrene/Isoprene 4,00 Ellamera RAD THICK Film former
Copolymer 501

Caprylic/Capric 3,00 MIGLYOL GEL T Thickening and


Triglyceride/stearalkonium Emollient
Bentonite/Propylene Carbonate

16
Cetyl Diglyceryl Tris(Trimethylsiloxy)
3,00 DOWSIL ES 5600 Emulsifier
Silyl ethyl Dimethicone

Xylitol 2,50 XIVIA XYLITOL Humectant

Zinc Oxide 2,00 ZINC OXIDE PHARMA UV sunscreen

Glycerin 2,00 GLYCERIN Humectant

Polyethylene Wax 1,80 PERFORMALENE 400 Wax

Ethyl Hexyl Palmitate 1,00 DUB PO Emollient

Sorbitan Isostearate 1,00 SPAN 120 Emulsifier

Hexandiol 0,50 HYDROLITE 6 Preservative

Sorbitan Caprylate 0,50 VELSAN SC Preservative

Pentaerythrytyl tetra di butyl 0,10 Tinogard TT DD Antioxidant


hydroxyhydrocinnamate

Frangrance 0,10 Fragrance Fragrance

* DUB PO is a trademark of Stearinerie Dubois; MIGLYO is a trademark of IOI Oleo GmbH; DOWSIL is a trademark of Dow
Corning; XIVIA is a trademark of DuPont; PERFORMALENE is a trademark of Baker Hughes; TINOGARD is a trademark of BASF;
SPAN is a trademark of Croda; HYDROLITE is a trademark of Symrise; VELSAN is a trademark of Clariant.

** Isododecane can be substituted with Hemisqualane or C15-19 Alkane.

EQUIPMENT
- Top stirring laboratory mixer
- Heating plate
- Ultra Turrax homogenizer
- Powder mixer

PREPARATION
Phase A
Ellamera RAD THICK 501 4,00
DUB PO 1,00 Phase C
Isododecane 35,50 Titanium Dioxide ST-410WB 5,00
Zinc Oxide 2,00
Performalene 400 1,80 Apalight MS 5,00
Tinogard TT 0,10
Phase D
Phase B Water 33,00
DOWSIL ES 5600 3,00 Xylitol 2,50
SPAN 120 1,00 Glycerin 2,00
Velsan SC 0,50 Hydrolite 6 0,50
Miglyol gel T 3,00
17
Phase E

Fragrance 0,10

Add Phase A ingredients in a beaker and heat for 20 minutes on 90°C and mix with a laboratory
mixer at 400RPM for about 20 minutes until a clear solution appears.

Add Phase B ingredients to a beaker and gently homogenize, then pour mixture into Phase A
beaker while stirring.

Mix Phase C ingredients together using a powder mixer and add Phase C mixture to beaker
containing phases A+B while stirring for a homogenous mixture.

Cool down the A+B+C mixture to 60 deg. C and check the isododecane content via weigh scale and
correct if necessary.

Mix Phase D ingredients together until you get a clear solution.

Add Phase D solution to the A+B+C beaker while stirring.

Finally, homogenise using the Ultra Turrax for a second time and cool down to about 40 °C with
slow mixing.

In the final step, add fragrance and mix until cooled down to room temperature.

PREPARATION NOTES
- Keep the mixing on a relatively slow speed (± 400 RPM) to prevent air bubbles from forming
- Control the evaporation of the Isododecane before to add the water phase

PACKAGING
The example formulation for a suncare cream is formulated with isododecane and needs packaging
that protects the evaporation of the volatile solvent during storage and transportation.

Test the compatibility with packaging material when using fragrance.

SAFETY NOTES
- Always be attentive when using mechanical equipment
- Manage all the ingredients with gloves and correct PPE
- Isododecane can evaporate and always better to cover the vessel and use the good
ventilation
- Read the safety document from all the ingredients prior to formulating.

Watch video for Sun Cream Formulation Guide

18
Bio Shine Hair Serum
Example Formulation*

DESCRIPTION
An example of a natural-based hair serum with a 90% bio-renewable carbon index is described.
The formula provides a rich, viscous fluid due to the thickening properties of Ellamera PER-SUST
504 by Kraton. This example formulation glides onto the hair smoothly to give an instant shine.

PHYSICAL PROPERTIES

Appearance Clear Fluid

Color Colorless

Odor Fragrance

Solubility Insoluble

Viscosity (LV- 950 cP


02, 20 rpm,
25⁰C)

*The formulation above is intended for information purposes only based on the best of our knowledge. It is the responsibility of the
customer to undertake the appropriate testing to determine the suitability of the product for their intended use.

COMPOSITION

INCI Wt % TRADE NAME FUNCTION

Diisooctyl Succinate 79.5 SustOleo DCS Emollient, solvent

Triheptanoin (and) C13-C15 Alkane 9.8 LexFeel WOW-A Emollient, solvent

Hydrogenated Styrene/ Butadiene 8.0 Ellamera PER-SUST 504 Rheology modifier


Copolymer

Propylene Glycol Dibenzoate 1.5 LexFeel Shine Shine


enhancement

Olea Europaea (Olive) Fruit Oil 0.5 Olive Oil, Pomace Emollient, solvent

Fragrance 0.5 Snowkissed Sugar (93-0130-15) Fragrance

19
Tocopheryl Acetate 0.2 d-α-Tocopheryl Acetate Vitamin E,
antioxidant

* SUSTOLEO and LEXFEEL are trademarks of Inolex; Olive Oil was supplied by Univar Solutions/Arista; Fragrance was supplied by
Lebermuth; Tocopheryl Acetate was supplied by Univar Solutions/DSM.

EQUIPMENT
Laboratory mixer, top stirring | Heating plate

PREPARATION
PHASE A PHASE B

LexFeel WOW-A 9.8 Olive Oil, Pomace 0.5


SustOleo DCS 79.5 d-α-Tocopheryl 0.2
Acetate
LexFeel Shine 1.5 Fragrance 0.5
Ellamera PER-SUST 504 8.0

- Add Phase A fluids in a beaker and begin heating to 90°C with mixing using a laboratory mixer at
200 rpm.
- Add Ellamera polymer to Phase A fluids with mixing during heating. Heat at 90⁰C for 30-60
minutes, or until a homogeneous solution is achieved.
- Cool down the Phase A mixture.
- Add Phase B ingredients once Phase A ≤ 50⁰C.

PREPARATION NOTES
A dispersion blade (or cowles blade) improved dispersion and increased rate of dissolution of the
Ellamera polymer in Phase A.

Alternatively, a homogenizer may be used to disperse/dissolve the Ellamera polymer in Phase A


while heating.

PACKAGING
The example formulation for a hair serum is formulated with emollient oils and needs packaging
that protects against leakage during storage and transportation. Test the compatibility with
packaging material when using fragrance.

SAFETY NOTE
- Always be attentive when using mechanical equipment
- Manage all the ingredients with correct PPE in accordance with safety guidelines
- It is always better to cover the vessel during mixing.
- Review the safety data sheets for all the ingredients prior to formulating.

Watch video for Bio Shine Hair Serum Formulation Guide

20
Creamy Satin Lipstick
Example Formulation*

DESCRIPTION

An example of a creamy, plum-colored, satin lipstick is described. The formula balances structure
and pay-off through a combination of various waxes and Ellamera BI-THIN 602 by Kraton to delivery
a creamy satin texture to the lips.

PHYSICAL PROPERTIES

Appearance Stick

Color Plum

Odor Unscented

Solubility Insoluble

*The formulation above is intended for information purposes only based on the best of our knowledge. It is the responsibility of the
customer to undertake the appropriate testing to determine the suitability of the product for their intended use.

COMPOSITION

INCI Wt % TRADE NAME FUNCTION

Octyldodecanol 20.45 Isofol 20 Alcohol Solvent, emollient

Triheptanoin 20.00 SustOleo MCT Solvent, emollient

Red 7 Lake (CI 15850) (and) 14.40 NWD-7722 Natural Pigment


Hydrogenated Rapeseed Oil Wax Dispersion D&C
(and) Heptyl Undecylenate Red 7 Ca Lake

Synthetic Wax 9.00 Performa V 825 Luster


Polymer

21
Hydrogenated Styrene/ 8.00 Ellamera BI-THIN 602 Rheology modifier,
Isoprene Copolymer oil thickener

Isopropyl Palmitate 7.00 Lexol IPP Solvent, emollient

C20-C40 Alcohols 6.00 Performacol 425 Structurant


Alcohol

Palm Acid/Adipic Acid/ 5.00 LexFeel Vibrant MB Payoff


Pentaerythritol
Crosspolymer

Blue 1 Lake (CI 42090) (and) 3.60 NWD-2125 Natural Pigment


Hydrogenated Rapeseed Oil Wax Dispersion
(and) Heptyl Undecylenate FD&C Blue 1 Al Lake

Trilaurin 3.00 SustOleo TL Solvent, emollient

Polyethylene 3.00 Performalene 400 Structurant


Polyethylene

Tocopheryl Acetate 0.50 dl-α-Tocopheryl Antioxidant


Acetate

Ascorbyl Palmitate 0.05 Ascorbyl Palmitate Antioxidant

* ISOFOL is a trademark of Sasol; SUSTOLEO, LEXOL, and LEXFEEL are trademarks of Inolex; PERFORMA V, PERFORMACOL, and
PERFORMALENE are trademarks of NuCera; Natural Wax Dispersion pigments were supplied by Univar Solutions/Sun Chemical;
Tocopheryl Acetate and Ascorbyl Palmitate were supplied by Univar Solutions/DSM.

EQUIPMENT
- Laboratory mixer, top stirring
- Heating plate
- Lipstick mold

22
PREPARATION

PHASE A PHASE C

SustOleo MCT 20.00 NWD-7722 Natural Wax 14.40


Dispersion D&C Red 7 Ca Lake
Lexol IPP 7.00
Isofol 20 Alcohol 20.45 NWD-2125 Natural Wax 3.60
Dispersion FD&C Blue 1 Al Lake
SustOleo TL 3.00

Ellamera BI-THIN 602 8.00

PHASE D
PHASE B
dl-α-Tocopheryl Acetate 0.50
Performalene 400 3.00 Ascorbyl Palmitate 0.05
Polyethylene
Performacol 425 Alcohol 6.00
Performa V 825 Polymer 9.00
LexFeel Vibrant MB 5.00

- Combine emollients of Phase A. Begin mixing while heating to 40⁰C.

- At 40⁰C (once SustOleo TL has dissolved), add Ellamera polymer with mixing; continue heating to
95-100⁰C to dissolve the polymer.

- Once polymer has dissolved, add Phase B solids to Phase A with mixing. Return mixture to 95⁰C to
retain good melt mixture.

- Add pigment dispersions (Phase C) to A+B with mixing. Return mixture to 95⁰C to retain good melt
mixture.

- Add antioxidants (phase D) to A+B+C with mixing at 92-95⁰C. Mix 2 minutes.

- Pour into lipstick molds. Chill for thirty minutes and package cold into lipstick tubes.

PREPARATION NOTES
- A dispersion blade (or cowles blade) improved dispersion and increased rate of dissolution of
the Ellamera polymer in Phase A.
- Deaeration may not be necessary if a moderate mixing speed (≤ 400 rpm) can be achieved
with sufficiently large batch size where air is not entrained during mixing. Deaeration was
achieved on lab-scale batches by resting 10 min in an 110⁰C oven before moulding.

23
PACKAGING
The example formulation for a lipstick requires lipstick tubes sized to the lipstick mold.

SAFETY NOTES
- Always be attentive when using mechanical equipment
- Manage all the ingredients with correct PPE in accordance with safety guidelines
- It is always better to cover the vessel during mixing.
- Review the safety data sheets for all the ingredients prior to formulating.

Watch video for Creamy Satin Lipstick Formulation Guide

24
Facial Primer SPF 30
Example Formulation*

DESCRIPTION

An example of a matte facial primer delivering sun protection (SPF 30*) is described. The formula
combines silicone elastomers with the film-forming properties of Ellamera BI-THIN 402 by Kraton
to provide a velvety texture and durable facial primer, which blurs imperfections, protects the
skin, and helps makeup apply and look better, longer.

PHYSICAL PROPERTIES

Appearance Translucent gel

Color Colorless to very


light yellow

Odor Light fragrance

Solubility (in water) Insoluble

Viscosity (T-F, 0.5 rpm, 25⁰C) 227,000 cP

Viscosity (T-F, 15 rpm, 25⁰C) 59,000 cP

*The formulation above is intended for information purposes only based on the best of our knowledge. It is the responsibility of the
customer to undertake the appropriate testing to determine the suitability of the product for their intended use.

25
COMPOSITION

INCI Wt % TRADE FUNCTION


NAME

Isodecyl Neopentanoate (and) 50.00 DOWSIL EL-8051 Elastomer,


Dimethicone/Bis Isobutyl PPG- IN Silicone sensorial
20 Crosspolymer Organic
Elastomer Blend

Neopentyl Glycol Diheptanoate 9.97 LexFeel D5 Emollient,


(and) Isododecane solvent

Octocrylene 8.50 Parsol 340 UVB filter

Isododecane (and) 8.00 DOWSIL EL-7314 Elastomer,


Hexyl/Succinyl Dimethicone Silicone sensorial
Crosspolymer Elastomer Blend

Ethylhexyl Methoxycinnamate 7.50 Parsol MCX UVB filter

Diisooctyl Succinate 5.00 SustOleo DCS Emollient,


solvent

Ethylhexyl Salicylate 5.00 Parsol EHS UVB filter

Butyl 3.00 Parsol 1789 UVA filter


Methoxydibenzoylmethane

Hydrogenated 3.00 Ellamera BI- Film former


Styrene/Isoprene Copolymer THIN 402

Fragrance 0.03 Wild Oats Fragrance


(CF0030777)

* DOWSIL is a trademark of Dow Chemical; SUSTOLEO and LEXFEEL are trademarks of Inolex; PARSOL is a trademark of DSM;
Fragrance was supplied by Clarity Fragrances.

EQUIPMENT
- Laboratory mixer, top stirring, side sweep
- Heating plate

26
PREPARATION
PHASE A PHASE C

SustOleo DCS 5.00 DOWSIL EL-7314 8.00


Parsol EHS 5.00 Silicone Elastomer
Blend
Parsol MCX 7.50 DOWSIL EL-8051 50.00
Parsol 340 8.50 IN Silicone
Organic Elastomer
Parsol 1789 3.00 PHASE
Blend D
PHASE B
LexFeel D5 9.97
Ellamera BI-THIN 402 3.00 PHASE E

Fragrance 0.03

- In side vessel, combine Phase A ingredients. Begin heating to 80-90⁰C with mixing to dissolve
Parsol 1789.
- Add Phase B to Phase A with mixing. Continue heating to 80-90⁰C with mixing to dissolve
polymer. Turn off heat once polymer is dissolved but keep mixing while mixture cools.
- In main vessel, add DOWSIL EL-7314 and begin mixing to soften and "liquify" the elastomer
blend.
- Add DOWSIL EL-8051 IN to the main vessel in increments with mixing to fully blend the two
elastomers (Phase C).
- Slowly add Phase D to Phase C with mixing, giving time for elastomer phase to incorporate the
addition of fluid.
- Add A+B to C+D with mixing.
- Add fragrance (Phase E) with mixing. Mix until homogeneous.

PREPARATION NOTES
A dispersion blade (or cowles blade) improved dispersion and increased rate of dissolution of the
Ellamera polymer in Phase A+B. Sweeping the sides of the vessel during mixing is
recommended to produce a homogenous product.

PACKAGING
The example formulation for a facial primer is formulated with silicone elastomers and emollient
oils and needs packaging that protects against leakage during storage and transportation. Test
the compatibility with packaging material when using fragrance

.SAFETY NOTES
- Always be attentive when using mechanical equipment
- Manage all the ingredients with correct PPE in accordance with safety guidelines
- It is always better to cover the vessel during mixing.
- Review the safety data sheets for all the ingredients prior to formulating.

Watch video for Facial Primer SPF30 Formulation Guide

27
Smooth Glide Deo Stick
Example Formulation*

DESCRIPTION

An example of an anhydrous deodorant stick is described. The formula balances pay-off through a
combination of Ellamera BI-THIN 402 and Ellamera TER-SET 603 by Kraton to thicken the oils,
eliminate syneresis, and minimize wax structuring agents. The formula delivers odor-fighting
ingredients in a smooth glide format to delivery underarm protection.

PHYSICAL PROPERTIES

Appearance Stick

Color White

Odor Fragrance

Solubility (in water) Insoluble

*The formulation above is intended for information purposes only based on the best of our knowledge. It is the responsibility of the
customer to undertake the appropriate testing to determine the suitability of the product for their intended use.

COMPOSITION

INCI Wt % TRADE NAME FUNCTION

C13-14 Isoalkane 22.0 Isopar M Fluid Solvent

Cetyl Alcohol 20.0 Adol 52 Cetyl Alcohol NF Structurant

Brassica Alcohol 12.5 SustOleo BA Structurant

Triethyl Citrate 12.0 CITROFOL AI Extra Odor control/


cosolvent

28
Trilaurin 10.0 SustOleo TL Dry feel
emollient

C20-40 Alcohols 9.0 Performacol 425 Structurant


Alcohol

Kaolin 4.0 Kaolin Clay TH-1 Texturizer/ dry


feel

Hydrogenated Styrene/ 3.0 Ellamera BI-THIN 402 Rheology


Isoprene Copolymer modifier

Stearoxytrimethylsilane (and) 2.0 DOWSIL 580 Wax Glidant, sensory


Stearyl Alcohol

Hydrated Silica 2.0 Syloid 9005 PC Sebum


absortion, odor
control, dry feel

Fragrance 2.0 Red Rose Apple (94- Fragrance


4003-23)

Hydrogenated Styrene/ 1.0 Ellamera TER-SET 603 Rheology


Butadiene Copolymer modifier

Methylheptylglycerin 0.5 Lexgard MHG Natural Bacteriastatic


MB agent

* ISOPAR is a trademark of ExxonMobil; ADOL is a trademark of Peter Cremer; SUSTOLEO and LEXGARD are trademarks of Inolex; CITROFOL
is a trademark of Jungbunzlauer; PERFORMACOL is a trademark of NuCera; Kaolin Clay was supplied by Univar Solutions; DOWSIL is a
trademark of Dow Chemical; SYLOID is a trademark of Grace; Fragrance was supplied by Lebermuth.

EQUIPMENT
- Laboratory mixer, top stirring | Heating plate | Homogenizer

29
PREPARATION
PHASE A PHASE C

Isopar M Fluid 22.0 Kaolin Clay TH-1 4.0


CITROFOL AI Extra 12.0 Syloid 9005 PC 2.0
SustOleo TL 10.0
Ellamera TER-SET 603 1.0 PHASE D
Ellamera BI-THIN 402 3.0 Lexgard MHG Natural 0.5
MB
Fragrance 2.0
PHASE B
Performacol 425 9.0
Alcohol
SustOleo BA 12.5
Adol 52 Cetyl 20.0
Alcohol NF
DOWSIL 580 2.0
Wax
- Combine Phase A emollients. Heat to 40⁰C with mixing.
- At 40⁰C (once SustOleo TL has dissolved), add Ellamera polymers with mixing; continue heating to
95-100⁰C to dissolve the polymers.
- Once polymers have dissolved, add Phase B waxes sequentially to Phase A with mixing. Maintain
melt mixture’s temperature ≥ 70⁰C. Return mixture to 75⁰C to retain good melt mixture.
- Disperse Phase C solids into A+B using an homogenizer (3000-5000 rpm).
- Cool mixture to 75-77⁰C and add Phase D ingredients sequentially with mixing.
- Pour into AP/DEO stick molds at ≥ 75⁰C. Cool to room temperature before use.

PREPARATION NOTES
A dispersion blade (or cowles blade) improved dispersion and increased rate of dissolution of the
Ellamera polymers in Phase A. Each wax’s melt endotherm (Phase B) will reduce the temperature of
the batch. Add waxes slowly enough to maintain temperature ≥ 70⁰C. To prevent shock—product
cracking from rapid loss in temperature—in very small sticks (15 to 30 mL), filled packages were
cooled in two steps: (1) 30 minutes at 49⁰C and then (2) overnight at ambient temperature (~21⁰C).

PACKAGING: The example formulation for a deodorant stick requires AP/DEO-style packaging.

SAFETY NOTES
Always be attentive when using mechanical equipment. Manage all the ingredients with correct
PPE in accordance with safety guidelines. It is always better to cover the vessel during mixing.
Review the safety data sheets for all the ingredients prior to formulating.

Watch video for Smooth Glide Deo Stick Formulation Guide

30
31

You might also like