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Ellamera Formulation Guide - Dec 2022 Updated
Ellamera Formulation Guide - Dec 2022 Updated
FORMULATION GUIDE
VERSATILE FORMULAS
Skincare Color
Suncare
• Sunscreen
• Sunblock
• Lotion/spray/stick
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Green Cleansing Oil
Example Formulation*
Description
A cleansing oil with medium viscosity is described. The formula provides a pleasant texture
with cleaning capabilities and features Ellamera PER-SUST™ 504 by Kraton.
Physical Properties
Appearance Fluid
Color Green
Odor N/A
Solubility Soluble
*The formulation above is intended for information purposes only based on the best of our knowledge. It is the responsibility of
the customer to undertake the appropriate testing to determine the suitability of the product for their intended use.
COMPOSITION
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EQUIPMENT
- Top stirring laboratory mixer
- Heating plate
PREPARATION
Phase A Phase C
Ellamera PER-SUST 504 2,00 Unicert Yellow 0,004
Saboderm CSO 92,50 Unicert Geen 0,002
Tinogard TT 0,10 Saboderm CSO 0,394
Phase B
Radiasurf 7125 5,00
Add Phase A ingredients in a beaker and heat for 30 minutes at 120°C and Mix at 400RPM for
~ 20 Minutes Until a Clear Solution Appears.
Cool Phase A down to 60°C and pour Phase B into Phase A beaker while stirring. Wait until a
white solution appears. Add Phase C ingredients while stirring to colour the solution.
PREPARATION NOTES
To make working with small amounts of colour easier, add 0.1 grams Unicert Green, 0.2
grams Unicert Yellow and 19.7 grams Saboderm to a beaker, mix with a spatula and add 0.4
grams of the mixture to the final product.
PACKAGING
No specific packaging requirements
SAFETY NOTES
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Sun Care Oil
Example Formulation*
Description
The formula has been prepared with natural sunflower oil and includes UVA and UVB absorbing
compounds to protect the skin from harmful sunlight. It provides a pleasant feeling and moisture
retention of the skin with the texturizing and film-forming properties of Ellamera BI-THIN™ 602 by
Kraton.
Physical Properties
Appearance Fluid
Color Orange/brown
Odor Oily
SPF 15 (est.)
*The formulation above is intended for information purposes only based on the best of our knowledge. It is the responsibility of
the customer to undertake the appropriate testing to determine the suitability of the product for their intended use.
COMPOSITION
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Squalane
2.00 Phytosqualane Emollient
* DUB PO is a trademark of Stearinerie Dubois; SunSolv is a trademark of Innospec Performance Chemicals; Eusolex is a trademark
of Merck; Escalol is a trademark of Ashland Specialty Chemical; Parsol is a trademark of DSM; 1789 TINOGARD is a trademark of
BASF.
EQUIPMENT
Top stirring laboratory mixer | Heating plate
PREPARATION
Phase A PHASE C
Ellamera BI-THINTM 602 3.50 Escalol 587 5.00
DUB PO 27.00 Eusolex HMS 5.00
Phytosqualane 2.00 Parsol 1789 3.00
Tinogard TT 0.10 Vitamin E Acetate 1.00
Sunsolv BOS 10.00
PHASE D
PHASE B Beta-carotene 0.03
Sunflower Oil 38.37 DUB PO 5.00
Add Phase A ingredients to a beaker and heat for 20 minutes at 120°C, and mix with a
laboratory mixer at 400 RPM for about 30 minutes until a clear solution appears. Cool down
Phase A to around 100°C and add Phase B into Phase A beaker while stirring.
After Phase B is mixed in, cool down to 60°C and add phase C ingredients. After Phase C
ingredients dissolve, add phase D slowly to the mixture until the desired color has been
reached.
PACKAGING
Test the compatibility with packaging material when using fragrance.
SAFETY NOTES
- Always be attentive when using mechanical equipment
- Manage all the ingredients with correct PPE in accordance with safety guidelines
Read the safety document from all the ingredients prior to formulating
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Concealer Cream
Example Formulation*
Description
Physical Properties
Appearance Fluid
Color Tan
Odor Fragrance
Solubility Insoluble
*The formulation above is intended for information purposes only based on the best of our knowledge. It is the responsibility of
the customer to undertake the appropriate testing to determine the suitability of the product for their intended use.
COMPOSITION:
EQUIPMENT
- Top stirring laboratory mixer
- Heating plate
- Ultra Turrax homogenizer
- Powder mixer
PREPARATION
PHASE A PHASE B
Ellamera TER-SET 403 4.50 DOWSIL ES 5600 3.00
DUB PO 6.00 Span 120 1.00
Hemisqualane 27.00 Velsan SC 0.50
Performalene 400 3.00 Miglyol Gel T 3.00
Tinogard TT 0.10
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PHASE D
PHASE C Water 30.00
FDP-C-PA White 12.70 Xylitol 2.50
FDP-C-DA-Yellow 0.8 Glycerin 2.00
FDP-C-DA-Black 0.15 Hydrolite 6 0.50
FDP-C-DA-Red 0.15
Zinc Oxide 3.00 PHASE E
Fragrance 0.10
- Add Phase A ingredients in a beaker and heat for 30 minutes at 90°C and mix with a
laboratory mixer at 400RPM for about 20 minutes until a clear solution appears.
- Add Phase B ingredients to a beaker and gently homogenize, then pour mixture into Phase
A beaker while stirring.
- Mix Phase C ingredients together using a powder mixer, and slowly add it to beaker
containing phases A+B slowly while stirring for a homogenous mixture.
- Cool down the A+B+C mixture to 60°C and check the Hemisqualane content via weigh scale
and correct if necessary. Homogenise using an Ultra Turrax.
PHASE D
Add Phase D solution to the A+B+C beaker while under high stirring.
- Finally, homogenise using the Ultra Turrax for a second time and cool down to about 40 °C
with slow mixing.
- In the final step, cool down to room temperature and add the fragrance.
PREPARATION NOTES
Keep the mixing speed relatively low (± 400 RPM) in Phase A & B to prevent air bubbles from
forming. Control the evaporation of the Hemisqualane before adding the water phase.
PACKAGING
The example formulation for a concealer cream is formulated with Hemisqualane and needs
packaging that protects the evaporation of the volatile solvent during storage and
transportation. Test the compatibility with packaging material when using fragrance.
SAFETY NOTES
Always be attentive when using mechanical equipment
Manage all the ingredients with correct PPE in accordance with safety guidelines.
Hemisqualane can evaporate and always better to cover the vessel and use the good
ventilation. Read the safety document from all the ingredients prior to formulating.
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LONG WEAR LIP GLOSS
Example Formulation*
Description
An example of a long-wear lip gloss formulation for a glossy finish is described. This lip gloss
formula provides long-lasting smoothness, color, and soft feel. Additionally, the formula
provides moisture retention with the film-forming properties of Ellamera™ from Kraton and
the skin-conditioning properties of phytosteryl isostearate.
Physical Properties
COMPOSITION
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Polyethylene Wax 5,00 PERFORMALENE 400 Wax
* DUB PO is a trademark of Stearinerie Dubois; MIGLYO is a trademark of IOI Oleo GmbH; PERFORMALENE is a trademark of Baker
Hughes; SUNCROMA is a trademark of Sun Chemical; HOMBITAN is a trademark of Hunstman; TINOGARD is a trademark of BASF.
EQUIPMENT
- Top stirring laboratory mixer
- Heating plate
- Three-roll mill for pigment grinding
PREPARATION
Phase A Phase B
Isododecane 45,35 Miglyol gel T 10,00
DUB PO 20,0 Phytosteryl isostearate 5,00
Ellamera RAD THICK 501 11,0 Homibitan anatase 0,80
Ellamera BI-THIN 402 1,50 Suncroma DC RED30 1,20
Tinogard TT 0,10
PERFORMALENE 400 PE 5,00 Phase C
Flavour 0,05
Add phase A in a beaker and heat for 30 minutes on 100°C, mixing it with a laboratory mixer
(400 RPM) for roughly 30 minutes until the polymers are melted. After mixing, cool down the
Phase A mixture to 70°C and check the isododecane content via weigh scale and correct it if
necessary.
While phase A is cooling down, prepare the colour phase B. Start by homogenizing the
Miglyol gel T and Phytosteryl isostearate, then slowly add and disperse the Hombitan anatase
and Suncroma DC RED30 and mix / homogenize with a spatula.
Add phase B to the three-roll mill on the smallest setting and mill the colour mixture 3 times,
obtaining a coloured paste.
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Add phase B coloured paste to phase A while stirring. Add the flavour component to the
product at 50°C and cool down to room temperature.
PREPARATION NOTES
Premix the Hombitan Anatase and Suncroma DC RED30 before to add at the liquid part
PACKAGING
Long Wear Lip Gloss is formulated with Isododecane and need packaging that protects the
evaporation of volatile solvent.
SAFETY NOTES
- Always be attentive when using mechanical equipment
- Manage all the ingredients with gloves and correct PPE
- Isododecane can evaporate and always better to cover the vessel and use good
ventilation
- Read the safety document from all the ingredients prior to formulating.
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MOISTURIZING BATH OIL
Example Formulation*
Description
An example of a moisturizing bath oil formulation providing moisture retention due to the
film-forming properties of Ellamera™ product from Kraton and Vitamin E. The moisturizing
bath oil with a micellar diffusion system disperses moisturizer components, which enable
long-lasting moisturizing effect on the skin.
Physical Properties
COMPOSITION
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Pentaerythrytyl tetra di butyl 0,10 Tinogard TT DD Antioxidant and
hydroxyhydrocinnamate discolorizing stabilizer
EQUIPMENT
- Top stirring laboratory mixer
- Heating plate
PREPARATION
Phase A
Add Ellamera PER-SUST 504, Tinogard TT DD and the DUB PO to a beaker, and mix with a
laboratory mixer at 100°C until dissolved.
Phase B
Add the Zetemol HE, Lameform TGI to a beaker and stir for another 30 minutes. Add Phase B
mixture to Phase A beaker after the Phase A mixture is cooled down to about 80°C.
Phase C
Add colorant Campo Siddha Indra Neelam Yenai, fragrance and the tocopheryl acetate to a
beaker and mix.
Finally, add the Phase C mixture to the Phase A+B mixture after it is cooled down to room
temperature.
PACKAGING
No restrictions, but always test the compatibility with packaging material when using
fragrances.
SAFETY NOTES
- Always be attentive when using mechanical equipment
- Manage all the ingredients with gloves and correct PPE
- Read the safety document from all the ingredients prior to formulating.
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SUNCARE CREAM
Example Formulation*
Description
An example of a long-lasting suncare cream formulation based on a water-in-oil emulsion with
medium viscosity is described. The formula provides a pleasant texture and moisture retention
with the film-forming properties of Ellamera™ by Kraton. This example formulation does not
contain chemical sunscreen; it is based on physical sun blocking agents such as
hydroxyapatite, titanium dioxide and zinc oxide.
Physical Properties
Appearance Fluid
Color White
Odor Fragrance
SPF 20 (est.)
COMPOSITION
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Cetyl Diglyceryl Tris(Trimethylsiloxy)
3,00 DOWSIL ES 5600 Emulsifier
Silyl ethyl Dimethicone
* DUB PO is a trademark of Stearinerie Dubois; MIGLYO is a trademark of IOI Oleo GmbH; DOWSIL is a trademark of Dow
Corning; XIVIA is a trademark of DuPont; PERFORMALENE is a trademark of Baker Hughes; TINOGARD is a trademark of BASF;
SPAN is a trademark of Croda; HYDROLITE is a trademark of Symrise; VELSAN is a trademark of Clariant.
EQUIPMENT
- Top stirring laboratory mixer
- Heating plate
- Ultra Turrax homogenizer
- Powder mixer
PREPARATION
Phase A
Ellamera RAD THICK 501 4,00
DUB PO 1,00 Phase C
Isododecane 35,50 Titanium Dioxide ST-410WB 5,00
Zinc Oxide 2,00
Performalene 400 1,80 Apalight MS 5,00
Tinogard TT 0,10
Phase D
Phase B Water 33,00
DOWSIL ES 5600 3,00 Xylitol 2,50
SPAN 120 1,00 Glycerin 2,00
Velsan SC 0,50 Hydrolite 6 0,50
Miglyol gel T 3,00
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Phase E
Fragrance 0,10
Add Phase A ingredients in a beaker and heat for 20 minutes on 90°C and mix with a laboratory
mixer at 400RPM for about 20 minutes until a clear solution appears.
Add Phase B ingredients to a beaker and gently homogenize, then pour mixture into Phase A
beaker while stirring.
Mix Phase C ingredients together using a powder mixer and add Phase C mixture to beaker
containing phases A+B while stirring for a homogenous mixture.
Cool down the A+B+C mixture to 60 deg. C and check the isododecane content via weigh scale and
correct if necessary.
Finally, homogenise using the Ultra Turrax for a second time and cool down to about 40 °C with
slow mixing.
In the final step, add fragrance and mix until cooled down to room temperature.
PREPARATION NOTES
- Keep the mixing on a relatively slow speed (± 400 RPM) to prevent air bubbles from forming
- Control the evaporation of the Isododecane before to add the water phase
PACKAGING
The example formulation for a suncare cream is formulated with isododecane and needs packaging
that protects the evaporation of the volatile solvent during storage and transportation.
SAFETY NOTES
- Always be attentive when using mechanical equipment
- Manage all the ingredients with gloves and correct PPE
- Isododecane can evaporate and always better to cover the vessel and use the good
ventilation
- Read the safety document from all the ingredients prior to formulating.
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Bio Shine Hair Serum
Example Formulation*
DESCRIPTION
An example of a natural-based hair serum with a 90% bio-renewable carbon index is described.
The formula provides a rich, viscous fluid due to the thickening properties of Ellamera PER-SUST
504 by Kraton. This example formulation glides onto the hair smoothly to give an instant shine.
PHYSICAL PROPERTIES
Color Colorless
Odor Fragrance
Solubility Insoluble
*The formulation above is intended for information purposes only based on the best of our knowledge. It is the responsibility of the
customer to undertake the appropriate testing to determine the suitability of the product for their intended use.
COMPOSITION
Olea Europaea (Olive) Fruit Oil 0.5 Olive Oil, Pomace Emollient, solvent
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Tocopheryl Acetate 0.2 d-α-Tocopheryl Acetate Vitamin E,
antioxidant
* SUSTOLEO and LEXFEEL are trademarks of Inolex; Olive Oil was supplied by Univar Solutions/Arista; Fragrance was supplied by
Lebermuth; Tocopheryl Acetate was supplied by Univar Solutions/DSM.
EQUIPMENT
Laboratory mixer, top stirring | Heating plate
PREPARATION
PHASE A PHASE B
- Add Phase A fluids in a beaker and begin heating to 90°C with mixing using a laboratory mixer at
200 rpm.
- Add Ellamera polymer to Phase A fluids with mixing during heating. Heat at 90⁰C for 30-60
minutes, or until a homogeneous solution is achieved.
- Cool down the Phase A mixture.
- Add Phase B ingredients once Phase A ≤ 50⁰C.
PREPARATION NOTES
A dispersion blade (or cowles blade) improved dispersion and increased rate of dissolution of the
Ellamera polymer in Phase A.
PACKAGING
The example formulation for a hair serum is formulated with emollient oils and needs packaging
that protects against leakage during storage and transportation. Test the compatibility with
packaging material when using fragrance.
SAFETY NOTE
- Always be attentive when using mechanical equipment
- Manage all the ingredients with correct PPE in accordance with safety guidelines
- It is always better to cover the vessel during mixing.
- Review the safety data sheets for all the ingredients prior to formulating.
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Creamy Satin Lipstick
Example Formulation*
DESCRIPTION
An example of a creamy, plum-colored, satin lipstick is described. The formula balances structure
and pay-off through a combination of various waxes and Ellamera BI-THIN 602 by Kraton to delivery
a creamy satin texture to the lips.
PHYSICAL PROPERTIES
Appearance Stick
Color Plum
Odor Unscented
Solubility Insoluble
*The formulation above is intended for information purposes only based on the best of our knowledge. It is the responsibility of the
customer to undertake the appropriate testing to determine the suitability of the product for their intended use.
COMPOSITION
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Hydrogenated Styrene/ 8.00 Ellamera BI-THIN 602 Rheology modifier,
Isoprene Copolymer oil thickener
* ISOFOL is a trademark of Sasol; SUSTOLEO, LEXOL, and LEXFEEL are trademarks of Inolex; PERFORMA V, PERFORMACOL, and
PERFORMALENE are trademarks of NuCera; Natural Wax Dispersion pigments were supplied by Univar Solutions/Sun Chemical;
Tocopheryl Acetate and Ascorbyl Palmitate were supplied by Univar Solutions/DSM.
EQUIPMENT
- Laboratory mixer, top stirring
- Heating plate
- Lipstick mold
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PREPARATION
PHASE A PHASE C
PHASE D
PHASE B
dl-α-Tocopheryl Acetate 0.50
Performalene 400 3.00 Ascorbyl Palmitate 0.05
Polyethylene
Performacol 425 Alcohol 6.00
Performa V 825 Polymer 9.00
LexFeel Vibrant MB 5.00
- At 40⁰C (once SustOleo TL has dissolved), add Ellamera polymer with mixing; continue heating to
95-100⁰C to dissolve the polymer.
- Once polymer has dissolved, add Phase B solids to Phase A with mixing. Return mixture to 95⁰C to
retain good melt mixture.
- Add pigment dispersions (Phase C) to A+B with mixing. Return mixture to 95⁰C to retain good melt
mixture.
- Pour into lipstick molds. Chill for thirty minutes and package cold into lipstick tubes.
PREPARATION NOTES
- A dispersion blade (or cowles blade) improved dispersion and increased rate of dissolution of
the Ellamera polymer in Phase A.
- Deaeration may not be necessary if a moderate mixing speed (≤ 400 rpm) can be achieved
with sufficiently large batch size where air is not entrained during mixing. Deaeration was
achieved on lab-scale batches by resting 10 min in an 110⁰C oven before moulding.
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PACKAGING
The example formulation for a lipstick requires lipstick tubes sized to the lipstick mold.
SAFETY NOTES
- Always be attentive when using mechanical equipment
- Manage all the ingredients with correct PPE in accordance with safety guidelines
- It is always better to cover the vessel during mixing.
- Review the safety data sheets for all the ingredients prior to formulating.
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Facial Primer SPF 30
Example Formulation*
DESCRIPTION
An example of a matte facial primer delivering sun protection (SPF 30*) is described. The formula
combines silicone elastomers with the film-forming properties of Ellamera BI-THIN 402 by Kraton
to provide a velvety texture and durable facial primer, which blurs imperfections, protects the
skin, and helps makeup apply and look better, longer.
PHYSICAL PROPERTIES
*The formulation above is intended for information purposes only based on the best of our knowledge. It is the responsibility of the
customer to undertake the appropriate testing to determine the suitability of the product for their intended use.
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COMPOSITION
* DOWSIL is a trademark of Dow Chemical; SUSTOLEO and LEXFEEL are trademarks of Inolex; PARSOL is a trademark of DSM;
Fragrance was supplied by Clarity Fragrances.
EQUIPMENT
- Laboratory mixer, top stirring, side sweep
- Heating plate
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PREPARATION
PHASE A PHASE C
Fragrance 0.03
- In side vessel, combine Phase A ingredients. Begin heating to 80-90⁰C with mixing to dissolve
Parsol 1789.
- Add Phase B to Phase A with mixing. Continue heating to 80-90⁰C with mixing to dissolve
polymer. Turn off heat once polymer is dissolved but keep mixing while mixture cools.
- In main vessel, add DOWSIL EL-7314 and begin mixing to soften and "liquify" the elastomer
blend.
- Add DOWSIL EL-8051 IN to the main vessel in increments with mixing to fully blend the two
elastomers (Phase C).
- Slowly add Phase D to Phase C with mixing, giving time for elastomer phase to incorporate the
addition of fluid.
- Add A+B to C+D with mixing.
- Add fragrance (Phase E) with mixing. Mix until homogeneous.
PREPARATION NOTES
A dispersion blade (or cowles blade) improved dispersion and increased rate of dissolution of the
Ellamera polymer in Phase A+B. Sweeping the sides of the vessel during mixing is
recommended to produce a homogenous product.
PACKAGING
The example formulation for a facial primer is formulated with silicone elastomers and emollient
oils and needs packaging that protects against leakage during storage and transportation. Test
the compatibility with packaging material when using fragrance
.SAFETY NOTES
- Always be attentive when using mechanical equipment
- Manage all the ingredients with correct PPE in accordance with safety guidelines
- It is always better to cover the vessel during mixing.
- Review the safety data sheets for all the ingredients prior to formulating.
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Smooth Glide Deo Stick
Example Formulation*
DESCRIPTION
An example of an anhydrous deodorant stick is described. The formula balances pay-off through a
combination of Ellamera BI-THIN 402 and Ellamera TER-SET 603 by Kraton to thicken the oils,
eliminate syneresis, and minimize wax structuring agents. The formula delivers odor-fighting
ingredients in a smooth glide format to delivery underarm protection.
PHYSICAL PROPERTIES
Appearance Stick
Color White
Odor Fragrance
*The formulation above is intended for information purposes only based on the best of our knowledge. It is the responsibility of the
customer to undertake the appropriate testing to determine the suitability of the product for their intended use.
COMPOSITION
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Trilaurin 10.0 SustOleo TL Dry feel
emollient
* ISOPAR is a trademark of ExxonMobil; ADOL is a trademark of Peter Cremer; SUSTOLEO and LEXGARD are trademarks of Inolex; CITROFOL
is a trademark of Jungbunzlauer; PERFORMACOL is a trademark of NuCera; Kaolin Clay was supplied by Univar Solutions; DOWSIL is a
trademark of Dow Chemical; SYLOID is a trademark of Grace; Fragrance was supplied by Lebermuth.
EQUIPMENT
- Laboratory mixer, top stirring | Heating plate | Homogenizer
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PREPARATION
PHASE A PHASE C
PREPARATION NOTES
A dispersion blade (or cowles blade) improved dispersion and increased rate of dissolution of the
Ellamera polymers in Phase A. Each wax’s melt endotherm (Phase B) will reduce the temperature of
the batch. Add waxes slowly enough to maintain temperature ≥ 70⁰C. To prevent shock—product
cracking from rapid loss in temperature—in very small sticks (15 to 30 mL), filled packages were
cooled in two steps: (1) 30 minutes at 49⁰C and then (2) overnight at ambient temperature (~21⁰C).
PACKAGING: The example formulation for a deodorant stick requires AP/DEO-style packaging.
SAFETY NOTES
Always be attentive when using mechanical equipment. Manage all the ingredients with correct
PPE in accordance with safety guidelines. It is always better to cover the vessel during mixing.
Review the safety data sheets for all the ingredients prior to formulating.
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