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3.

17 Topological Evaluation of Surfaces in Relation to Surface Finish


P Demircioglu, Adnan Menderes University, Aydın, Turkey
r 2017 Elsevier Inc. All rights reserved.

3.17.1 Topological Evaluation Methods 243


3.17.1.1 Contact Surface Measurement Techniques 243
3.17.1.1.1 Portable handheld surface finish instrument 243
3.17.1.1.2 SP 243
3.17.1.1.3 Atomic force microscopy (contact mode) 244
3.17.1.2 Noncontact Surface Measurement Techniques 244
3.17.1.2.1 Confocal microscopy 244
3.17.1.2.2 Focus variation microscopy 245
3.17.1.2.3 CSI 246
3.17.1.2.4 SPM 247
3.17.1.2.4.1 AFM (Noncontact mode) 247
3.17.1.2.4.2 STM 247
3.17.1.2.5 Electron microscopy 247
3.17.1.2.5.1 TEM 248
3.17.1.2.5.2 SEM 248
3.17.1.2.6 Comparison 248
3.17.2 Characterization of Parameters 248
3.17.2.1 Primary Profile 250
3.17.2.2 Waviness Profile 250
3.17.2.3 Roughness Profile 250
3.17.3 Surface Finishing 254
3.17.4 Conclusion 260
References 260

3.17.1 Topological Evaluation Methods opportunity to measure the surface parameters for finer and
smoother surfaces quantitatively.
Topological characterization methods are divided into two
categories. These are contact and noncontact measurement and
3.17.1.1.1 Portable handheld surface finish instrument
evaluation methods. These methods have pros and cons in
Portable handheld surface finish instruments measure multi-
different aspects. The technological developments are bringing
ple roughness parameters using diamond tip drawn across
new approaches and solutions. Therefore, evaluation methods
a sample part with motorized traverse mechanism. These
for surface characterization should be revised and adapted to
instruments produce a set of traceable measurement results
new approaching or emerging technologies.
including detailed profile graph with one-button operation.
Most common types of instruments use standard cutoff values
3.17.1.1 Contact Surface Measurement Techniques (0.8 mm), accuracy (ranges from 0.1 to 40 mm in Ra), dia-
mond tip with a radius of 5 mm, and traverse length of 5 mm.5
In the twentieth century, the attempts for development of the
There are two common types of surface finish measuring
surface instrumentation were initiated by industry and aca-
systems as skidded and nonskidded (can be called as skid-
demia. Surface topographical characterization was assessed by
less). These testers with skidded can measure roughness only
the judgment of the inspector either by eye or fingernail. The
(Figure 1(a)), whereas skidless testers can evaluate the surface
simplest way to characterize surface structure is visual inspec-
components as form, waviness, and roughness (Figure 1(b)).
tion. The mere eye can tell quite much about larger scale fea-
Workpiece belonging to surface being measured is used as
tures. The resolution of the human eye is limited to slightly
a reference surface by skidded instruments, while skidless
under 100 mm.1 Because of this reason, it is necessary to have
instruments can use an internal precision surface as a refer-
higher spatial resolution measurement systems, which can be
ence. Skid can be used as a mechanical filtering in the mea-
used for the surface topographical assessment.
surements. Skid radius is a key factor that determines the
The first contact type stylus profilometer (SP) was developed
obtained results from a tester.
for the surface topographical characterization by Schmaltz
in 1929.2 After G. Schmaltz, Abbott in 19363 and Hobson
in 19394 advanced the surface inspection and measurement 3.17.1.1.2 SP
know-how. Early stage evaluation methods were insufficient in SPs are supported with the most of the surface finish standards
order to put a numerical value to the surface texture. Contact for the prerequisites of the engineering communities and
type SPs advanced the evaluation methodologies and gave an academia (Figure 2).6 A stylus with diamond tip with different

Comprehensive Materials Finishing, Volume 3 doi:10.1016/B978-0-12-803581-8.09179-7 243


244 Topological Evaluation of Surfaces in Relation to Surface Finish

Figure 1 Portable handheld surface finish instrument. (a) with skid and (b) skidless.

cantilever is focused on a position sensitive photodetector.10


Such an optical beam deflection system is sensitive to sub-
nanometer deflections of the cantilever.11 The AFM performs
raster scanning and produces a topographic map of the sample
surface (Figure 3(a)). The imaging with contact mode AFM can
damage or distort some biological samples (Figure 3(b)).
AFM has abilities to measure the parameters in nanoscale
level (Figure 4). These parameters can be:
Figure 2 Working principle of stylus profilometer.
1. Nanomechanical properties such as elastic modulus,
hardness, stiffness, viscoelastic, frictional, etc.
sizes (ranges from 20 nm to 50 mm) is moved in vertical stylus
2. Nanochemical properties such as chemical composition of
displacement on the surface being measured, while the tip is
surface features, etc.
moved laterally across the sample for a predetermined contact
3. Nanoelectrical properties such as work function, con-
force (range from less than 1–50 mg). Measuring range for a
ductivity, etc.
typical SP is between 10 nm and 1 mm. An analog signal is
4. Nanomagnetic properties, for example, magnetostatic field,
produced, as diamond moves mechanically up and down in
field gradient above ferromagnets, etc.
vertical direction. Generated analog signals by transducer are
5. Texture parameters such as average roughness, maximum
converted into digital signals, and then this digital information
peak to valley height, root mean square roughness, 10-
is stored, analyzed, and displayed.
point mean height roughness, surface skewness, surface
The SPs have pros and cons in different aspects. Software
kurtosis, etc.
used by these profilometers is compatible with the world’s
6. Particle characterization such as parameters, volume, size,
surface finish standards. Stylus instruments are the only
shape, and particle surface morphology, etc.
instrument types that are fully covered by ISO specification
standards and there is good practice guidance available.7
Obtained measurement results from the SPs are reliable. SPs 3.17.1.2 Noncontact Surface Measurement Techniques
are more preferable since they have an ability to measure the
surface properties of a material with dirty layer, while non- The invention of noncontact optical techniques is in a sense
contact measurement systems can measure material surface due to the drawbacks of the contact type stylus measurement
properties plus surface contaminants. Vertical resolution of techniques. These noncontact measurement methods have
these profilometers is usually sub-nanometer level. ability to measure in-process and the different types of mate-
The contact type stylus measurement technique has con- rials. The optical systems and the SPs are two complementary
siderable drawbacks that the loaded stylus can damage or methods.12 This noncontact environment can also result in
scratch the surface being measured, particularly the situation much faster measurement times for the optical scanning
for soft surfaces. The transducer and stylus tips are often fra- instruments in the characterization of technical and non-
gile, the measurements with these instrument should be technical surfaces, while the SPs take more operation time
applied in a fairly vibration free environment. Consequently, in an aerial scanning mode. 3D noncontact optical surface
this direct contact measurement method may not be appro- inspection and measurement methods work with sensor-based
priate to be used on a test object undergoing a machining approach by being placed at a certain distance from the object.
process simultaneously.8 Since optical measurement systems contains many drawbacks
such as objective properties, spot size, numerical aperture
(NA), field of view (FOV), surface slopes and discontinuities,
3.17.1.1.3 Atomic force microscopy (contact mode) and multiple scattering, surface finish evaluation results seems
Atomic Force Microscopy (AFM) is one of the scanning probe to have higher values in other words overestimation of the
microscopy (SPM) techniques. The AFM9 was developed for values of surface texture parameters occurs.
imaging the insulating surfaces at atomic resolution levels. For In this section, confocal microscopy, focus variation
the working principle of AFM, the samples are scanned in microscopy, coherence scanning interferometry (CSI), SPM,
2-axes under the force-sensing probe with tip attached to a and electron microscopy as the noncontact methods for
cantilever. The interaction between the tip and sample occurs, measuring surface topography is mentioned.
when the tip is approached to the sample surface with proxi-
mity. Therefore, forces between the tip and the sample results 3.17.1.2.1 Confocal microscopy
in a deflection for the cantilever. The light from a laser is sent The fundamental working principle of confocal microscopy is
to the cantilever, and then reflected light from back of the that only focused-light is sent to detector by means of a spatial
Topological Evaluation of Surfaces in Relation to Surface Finish 245

Figure 3 (a) Contact mode AFM imaging and (b) Atomic force microscope (AFM).

Figure 4 Measurement parameters with AFM.

pinhole placed at the confocal plane of the lens to remove out disks. Scanning disk turns and captures light that represents a
of focus light. In the late 1800s, Ernst Abbe (The Abbe Cri- slice of image from sample surface. In PACM, programmable
terion) first enlightened that these traditional type fluorescence array takes the roles of beam scanning system in CLSM and
microscopes have the limits to spatial resolution. The principle motorized disk in DSCM. Programmable array works in a way
of confocal imaging was patented (US patent 3013467) in that only desired lights are taken into account. This each pixel of
1957 by Minsky13 with the purpose of surpassing the limita- micro display acts as an illumination and detection element at
tions of widefield fluorescence microscopes, since the resolu- the same time. Light from out of focus regions falls into
tion in confocal microscopy is augmented by eliminating out neighboring pixels and the signals on the correlated pixels are
of focus light. In recent technologies, the confocal microscopy used to reconstruct confocal image. The array of apertures can
has three main different types of working principles. These be opened or closed.
principles are named as confocal laser scanning microscopy
(CLSM or LSCM) (Figure 5(a)), disk scanning confocal 3.17.1.2.2 Focus variation microscopy
microscopy (DSCM) (Figure 5(b)) and programmable array The principle of focus variation was first published by von
scanning confocal microscopy (PACM) (Figure 5(c)). Helmholtz in 1924.14 The working principle of these instru-
The main differences among confocal microscopes are ments is based on focus variation. The visible light sends
beam scanning system, motorized scanning disk system, and through a lens and to a beam splitter, then light goes through
programmable array scanning system for CLSM, DSCM, and objective lens, finally to a sample. The driving unit connected
PACM, respectively. In CLSM, beam scanner provides the raster to sample compartment moves vertically to provide in focus,
scan of illumination to generate the confocal image. This is lateral movement of the sample compartment enables the
obtained by using two mirrors that move in perpendicular scanning of the sample. Reflected light from the sample goes
directions in order to bend the beam of the light. In DSCM, through objective lens, and passes through semitransparent
three different motorized disks are available in the market, these mirror and tube lenses to the Charge–Coupled Device (CCD)
are called as Nipkow disks, parallel slits, and point rotating slit array. In an array, the status of focusing such as out of focus,
246 Topological Evaluation of Surfaces in Relation to Surface Finish

Figure 5 Schematic representation of three working principles of confocal microscopes.11 (a) Confocal laser scanning microscopy (CLSM or
LSCM), (b) disk scanning confocal microscopy (DSCM), and (c) programmable array scanning confocal microscopy (PACM).

1. array detector
2. lenses
3. white light source
4. beam splitter
5. objective
6. specimen
7. vertical scan
8. focus curve
9. light beam
10. analyzer
11. polarizer
12. ring light

Figure 6 Schematic diagram of a typical measurement device based


on focus variation.15

almost in focus, and in focus is evaluated, calculating the focus


information (standard deviation) by 5  5 neighboring pixel
values with the pixel values for the point of interest. Working
principle of focus variation microscopy is depicted in Figure 6.

3.17.1.2.3 CSI
CSI (Figure 7) is often referred to as vertical scanning white- Figure 7 Working principle of coherence scanning interferometry
light interferometry. The light goes through beam splitter to an design (upper) with schema of how to build up an interferogram on a
objective lens and internal reference mirror driven by a piezo- surface using CSI. The vertical lines are intensity profiles at the image
sensor (lower).17
system, finally through the object to be measured. From here,
the light is reflected back to the objective, goes through beam
splitter, and finally reaches to the digital image sensor. The the sample and the reference must be almost identical, for
upper beam splitter directs light from the light source toward interference to be observed.16 This characterizes how well
the objective lens. The lower beam splitter in the objective lens a wave can interfere with itself at a different time. The detector
splits the light into two separate beams. One beam is directed measures the intensity of the light as the interferometric objec-
toward the sample and one beam is directed toward an tive is actuated in the vertical direction (z-axis) and finds the
internal reference mirror. The two beams recombine and the maximum interference. Each pixel of the sensor measures
recombined light is sent to the detector. Due to the low the intensity of the light and the fringe envelope obtained can
coherence of the white light source, the optical path length to be used to calculate the position of the surface.
Topological Evaluation of Surfaces in Relation to Surface Finish 247

Figure 8 (a) Atomic force microscope and (b) Noncontact mode AFM imaging mode.

3.17.1.2.4 SPM
The Scanning Probe Microscopes (SPMs) represent the fun-
damental instrumentations for Nanotechnology. Basic princi-
ple of SPM has two distinct functions. These are scanning and
probing. Scanning is performed by piezo raster 2D (X–Y)
scanning, while probing is achieved by a sharp tip mounted to
a z-scanner. The most common types of SPMs are noncontact
AFM and scanning tunneling microscopy (STM).

3.17.1.2.4.1 AFM (Noncontact mode)


The first Noncontact AFM (NC-AFM) was designed by Martin
et al. in 1987.18 Tapping mode or NC-AFM (Figure 8(b)) can be
classified in this section, since tip of the instrument does
not have contact with sample surface. These types of instru-
ments measure surface topography by utilizing attractive forces
(interatomic force) between the tip and the sample surface.
NC-AFM uses piezoelectric modulator to obtain the informa-
tion regarding the surface topography. Piezoelectric modulator
enables to keep minimum distance to the sample surface by
van der Waals forces between the tip and the sample surface.
Therefore, all the time the distance between the tip and the
sample surface remains in the same level by z-servo feedback
Figure 9 Working principle of scanning tunneling microscopy.20
loop control system. The light sends to the cantilever, and then
reflected back to photodetector. In photodetector, surface to-
pography information is monitored (Figure 8(a)). quantum object is sent on a material with a thick barrier, this
quantum object bounces off. If the barrier is thinner, it has the
ability to pass through the object. Metals are made of atoms
3.17.1.2.4.2 STM
and electrons. Electrons come off the metal surface, when
The STM is based on the quantum mechanical tunneling effect
electric current passes through the tip. This produces a tunnel
(Figure 9). Binnig and Rohrer developed this system in 1981
effect. Low current is amplified by a current amplifier. Distance
(at IBM Zürich) and earned the Nobel Prize in Physics in
control and scanning unit enable to control the voltage goes to
1986.19 For an STM, average lateral and depth resolutions are
the piezoelectric tube. Thus, the tip is moved, and then finally
considered to be 0.1 and 0.01 nm, respectively. With this
data is recorded and displayed.
resolution, individual atoms within materials are routinely
imaged and manipulated. STM performs well for all con-
ductive materials. However, it is possible to measure even 3.17.1.2.5 Electron microscopy
biological materials such as DNA. Working principle of these The working principle of electron microscopes is that the
instruments is that extremely fine conducting material creates system uses a beam of electrons instead of the light to produce
tunneling effect with conductive samples. In theory, when a an image of the sample specimen. There are two types of
248 Topological Evaluation of Surfaces in Relation to Surface Finish

Figure 10 Schematic representation of transmission electron


microscopy.

electron microscopes. These are Transmission Electron Micro-


scopy (TEM) and Scanning Electron Microscopy (SEM). Gen-
erally, TEM and SEM utilize electromagnetic and/or electrostatic
lenses to keep up the path of electrons. The resolution of these
Figure 11 Schematic representation of scanning electron microscopy.
systems depends upon the wavelength of the irradiation used
to create an image. Reducing the wavelength increases the
resolution. Thus, the resolution of the image obtained from beam electrons have more energy than secondary electrons,
the microscope can be increased if the accelerating voltage of secondary electrons from the atoms are kicked away by primary
the electron beam is increased. Hans Busch was a pioneer of electrons and scattered electrons carry information regarding the
electron optics and laid the theoretical basis for the electron surface properties of the specimen. Therefore, SEM is a vital
microscopy in 1920s. Knoll and Ruska21 succeeded in magni- measurement technique for the surface finish studies.
fying an electron image. The first prototype of electron micro-
scopy was actually built by Ruska in 1933 and was capable of 3.17.1.2.6 Comparison
resolving to 50 nm. In this section, the working principles of Table 1 gives the comparison of the measurement and
TEM and SEM are explicitly depicted. inspection techniques.
The sensitivity of instruments using cantilever beam with
3.17.1.2.5.1 TEM tip are affected by stiffness, size, and material type of the tip.
In these instruments (Figure 10), instead of using light, electrons TEM requires a special environmental conditioning such as
are produced and transmitted through an ultrathin specimen vacuum, while SEM and others does not require. When com-
(semitransparent for electrons) as an electron beam. Like in pared in terms of cost and complexity, TEM and SEM require
spectroscopy, electrons passing through a specimen interact special lenses and optics, and have the highest cost among others
with the atoms in sample. As a result of the specimen char- in investment. STM tip should be conducting, can be simply cut
acteristics, the properties of transmitted electron beam changes. freshly by normal wire cutter. STM works with the very top atom
The transmitted electron beam is projected on a fluorescent at the freshly cut tip, providing to atomic resolution. AFM tip
screen, and then the information is captured from fluorescent should be sharp enough to get good resolution (fat-tip effect),
surface to create the TEM image. In other words, TEM contains a and also AFM tip should be stiff enough to sense the atomic
high voltage electron beam emitted by a cathode and formed by interaction with sample surface. AFM tip is not necessary to be
magnetic lenses. The electron beam partly transmitted through conducting, but STM tip should be conductive.
the ultrathin specimen carries information about the structure From coarse to very fine surface finishes, it is important to
of the specimen. The spatial information is magnified by a test a specimen with proper instruments and to make decision
series of magnetic lenses, and finally the image formed on a with above mentioned measurement and inspection methods.
fluorescent screen. The image detected by a CCD camera played Therefore, surface finishing and quality measurements can be
and recorded in real time. done using above instruments. In surface finish measurement
studies or in industry, crucial task is that the selection of
3.17.1.2.5.2 SEM proper measurement methods according to surface finish.
In contrast to the TEM, SEM (Figure 11) produces the images
using secondary electrons which are emitted from a specimen
hit by the electrons of the primary beam. In SEM, the electron 3.17.2 Characterization of Parameters
beam is scanned across the surface being measured in a raster
scan with the detectors for building up an image by mapping Surface texture refers to the surface irregularities such as peaks
the detected signals with the beam position. Since primary and valleys, produced on a surface by any forming processes.
Topological Evaluation of Surfaces in Relation to Surface Finish 249

Table 1 Comparison of the measurement and inspection techniques

Criteria Contact stylus Noncontact optical AFM STM TEM SEM

Type of probe Tip Light beam Tip Tip Electron beam Electron beam
Type of contact Contact Noncontact Contact and Noncontact Noncontact Noncontact
Noncontact
Source Mechanical-electrical Photons Mechanical-electrical Atomic forces Electrons Electrons
energy energy/Photons
Detection Transducer Photodetector Photodetector Photodetector Fluorescent CCD
scene
Sample Little/Not required Little/Not Required Required Required Required
preparation required
Spatial 0.1 mm–1 mm 0.5 mm 20 nm 2.5 nm 2 nm–1 mm 10 nm
Resolution
Z-Resolution 0.3 nm 0.1 mm Sub-nanometer/ 0.2 nm 100 nm 2 nm
Angstrom
Z-Range 50 mm 20 mm 5 mm 100 nm 2 mm 2 mm
Output 2D/3D 2D/3D 3D 3D 2D 3D

Figure 12 Surface topography evaluation schema.

Form, waviness, and roughness are basic components of Surface parameters are obtained using two types of profil-
a surface texture, which is much more associated with the ing techniques. These techniques are based upon height
roughness, since in practice surface roughness is most com- measurements. These height measurements are made along a
monly used and measured. Forms typically appear due to the line (profile method) or over an area (raster area methods).
errors occurring from machining. This is commonly known Both types of techniques develop quantitative knowledge
as straightness errors. Waviness is a result of various vibra- of the surface peaks and valleys by point measurement using
tions during machining process related to both machine tool high resolution probe. Surface topography evaluation schema
and outside sources like work deflection, vibration, heat (Figure 12) indicates how primary profile, waviness, and
treatment, and other similar factors. Roughness occurs as a roughness are obtained using digital filters. Firstly, a profile
result of feed-rate tool geometry, tool condition, the process signal is extracted from a surface using any profilometer such
used, and hardness and other variations in material char- as with mechanical/optical probe. The extracted profile refers
acteristics. Since form, waviness, and roughness appears due to the sampled and digitized signal. Then, form removal
to different factors mentioned above, it is possible to remove process is applied to the extracted profile signal. This refers to
these errors with analyses. The removal of errors can be removal of errors caused by geometry of sample part/mea-
accomplished using selected filters or cutoff values. In this surand. After the removal of form type, low-pass filter is
section, primary profile, waviness, and roughness are detailed applied to the obtained signal. The result is the primary profile
explicitly. signal. The primary profile parameters such as Pa, Pz, Psk, etc.,
250 Topological Evaluation of Surfaces in Relation to Surface Finish

are obtained from primary profile signals. Low-pass filtering is and high-pass filtering with the cutoff wavelength lf. Waviness
applied to the primary profile signal and therefore, waviness profile is evaluated over the measured length In, which is
profile signal is obtained. Parameters obtained from these composed of several sampling lengths lw. The single measured
signals are Wa, Wz, Wsk, etc. High-pass filter is applied to the length Iw corresponds to the cutoff wavelength lf of the high-
primary profile signal. Then the roughness profile signal is pass filter. The original signal is illustrated in Figure 14(a). The
obtained. Roughness parameters are Ra, Rz, Rsk, etc. waviness profile signal obtained from a primary profile signal
using low-pass filter is shown in Figure 14(b).
3.17.2.1 Primary Profile
3.17.2.3 Roughness Profile
The primary profile is acronym as P, which is the profile after
low-pass filtering the measuring values using the cutoff The roughness profile is acronym as R, which results from high-
wavelength ls. The short-wave profile parts in the signal are pass filtering the primary profile with the cutoff wavelength
cutoff and evaluated within the sampling length (cutoff). lc. Roughness profile is evaluated over the measured length In,
This equals to the measured length or the length of the which is composed of five single measured lengths lr. The
measured surface profile.22 The primary profile signal single measured length Ir corresponds to the cutoff wavelength lc
obtained from a surface texture using low-pass filter is shown of the primary profile filter. The original signal is illustrated
in Figure 13(a). The profile is a superimposed image of in Figure 15(a). The roughness profile signal (Figure 15(b)) is
roughness, waviness, and profile. Figure 13(a) shows the obtained from a primary profile signal using high-pass filter.
surface texture profile signal for a surface while Figure 13(b) Table 2 shows the 2D surface profile parameters, their
illustrates the signals for original signal plus primary profile corresponding equations, and graphical representations. Here,
signal. for each 2D parameter, definitions are given with their equa-
tions in order to use in surface topological calculation and
evaluations. Furthermore, graphical representations for each
3.17.2.2 Waviness Profile
surface parameter are depicted so as to illustrate the phe-
The waviness profile is acronym as W, which results from low- nomena how 2D surface parameters are withdrawn for the best
pass filtering the primary profile with the cutoff wavelength lc comprehension.

Figure 13 Surface profile signals. (a) Original and (b) Original þ Primary profile.
Topological Evaluation of Surfaces in Relation to Surface Finish 251

Figure 14 Surface profile signals. (a) Original and (b) Waviness.

Figure 15 Surface profile signals. (a) Original and (b) Roughness.


252 Topological Evaluation of Surfaces in Relation to Surface Finish

Table 2 2D surface profile parameters23,24

2D surface profile Equation with description Graphical representation


parameters

Amplitude parameters (peak to valley)


Maximum profile Rp ¼ maxðZp ðx ÞÞ
peak height Rp,
Wp, and Pp Largest profile peak height Zp
within a sampling length.

Maximum profile Rv ¼ minðZpðx ÞÞ


valley depth Rv,
Wv, and Pv Largest profile valley depth Zv
within a sampling length.

Maximum height of Rz ¼ RpþRv


profile Rz, Wz,
and Pz Sum of height of the largest
profile peak height Rp and
the largest profile valley Rv
within a sampling length.

Mean height of P
m
Rc ¼ 1
Zti
profile elements m
i ¼1
Rc, Wc, and Pc
Mean value of the profile
element heights Zt within a
sampling length.

Total height of Rt ¼ maxðZpi Þ þ maxðZvi Þ


profile Rt, Wt,
and Pt Sum of height of the largest
profile peak height Rp and
the largest profile valley Rv
within an evaluation length.

(Continued )
Topological Evaluation of Surfaces in Relation to Surface Finish 253

Table 2 Continued

2D surface profile Equation with description Graphical representation


parameters

Amplitude parameters (average of ordinates)


Arithmetical mean Rl
Pa; Ra; Wa ¼ 1l 0 jZ ðx Þjdx
deviation of the
assessed profile Arithmetic mean of the
Ra, Wa, and Pa absolute ordinate values Z(x)
within a sampling length.

qffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi
R ffi
Root mean square 1 l 2
Pq; Rq; Wq ¼ l 0 Z ðx Þdx
deviation from
the assessed Root mean square value of the
profile Rq, Wq, ordinate values Z(x) within a
and Pq sampling length.

h R i
Skewness of the Rsk ¼ 1 1 lr
Z 3 ðx Þdx
Rq 3 lr 0
assessed profile
Rsk, Wsk, and Quotient of mean cube value
Psk of the ordinate values Z(x)
and cube Pq, Rq, Wq,
respectively, within a
sampling length.

Kurtosis of the 1 1 lr
R
Rku ¼ Rq 4 lr 0
Z 4 ðx Þdx
assessed profile
Rku, Wku, and Quotient of mean quartic of
Pku the ordinate values Z(x) and
4th power of Pq, Rq, Wq,
respectively, within a
sampling length.

Spacing Parameters
Mean width of P
m
Rsm ¼ 1
Xsi
profile elements m
i ¼1
Rsm, Wsm, and
Psm Mean value of the profile
element width Xs within a
sampling length.

(Continued )
254 Topological Evaluation of Surfaces in Relation to Surface Finish

Table 2 Continued

2D surface profile Equation with description Graphical representation


parameters

Hybrid Parameters
qffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi
R  2 ffi
Root mean square 1 l d
RDq ¼ l 0 dx Z ðx Þ dx
slope of the
assessed profile Root mean square value of the
RDq, WDq, and ordinate slopes dZ/dx within
PDq a sampling length.

Curves Related Parameters


Material ratio of the P
m
Rmr ðc Þ ¼ 1
Ml ðc Þi
profile Rmr(c), ln
i ¼1
Wmr(c) and
Pmr(c) Ratio of the material length of
the profile elements Ml(c) at
a given level c to the
evaluation length.

Profile section Rδc ¼ c ðRmr 1Þ  c ðRmr 2Þ


height difference : Rmr 1oRmr 2
Rδc, Wδc, and
Vertical distance between two
Pδc
section levels of given
material ratio.

Relative material Rmr ¼ Rmr ðc1 Þ


ratio Rmr, Wmr C1 ¼ C0  Rδc
and Pmr C0 ¼ C ðRmr 0Þ
Material ratio determined at a
profile section level Rδc,
related to a reference C0.

3D surface profile parameters are listed with their corre- 3.17.3 Surface Finishing
sponding equations in Table 3. Here, for each 3D parameter,
definitions are given with their equations in order to use in All machining processes leave characteristic topographic features
surface topological calculation and evaluations. This areal on the surfaces of components. Surface finishing is a very wide
information is needed to have better results for surface eva- range of industrial processes. These processes change and modify
luation since 3D parameters contain more information than the surface of produced sample to reach the desired properties.
information obtained from profiling. From deburring processes to a variety of technological processes,
Topological Evaluation of Surfaces in Relation to Surface Finish 255

Table 3 3D surface profile parameters25

3D surface profile parameters Equation with description

Amplitude characterization Sa ¼ ∬a jZ ðx ; y Þj dx dy

Sa: The average deviation of the surface


qffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi
Sq ¼ ∬a ðZ ðx ; y ÞÞ2 dx dy

Sq: The root mean square deviation of the surface

Ssk ¼ 1
Sq 3
∬ a ðZ ðx ; y ÞÞ3 dx dy

Ssk: Skewness of surface height distribution

Sku ¼ 1
Sq 4
∬ a ðZ ðx ; y ÞÞ4 dx dy

Sku: Kurtosis of surface height distribution


P5 P
jPeak Heightsj þ 51 jValley Depthsj
Sz ¼ 1
5
Sz: Ten point height of the surface
Spatial characterization Number of Peaks
Sds ¼
Area
Sds: Density of summits

Length of fastest decayð0:2Þ of ACF in any direction


Str ¼
Length of slowest decayð0:2Þ of ACF in any direction
Str: Texture aspect ratio; ACF¼Auto correlation function
Sal ¼Length of fastest decay of ACF to 0.2 in any direction
Sal: Fastest decay auto correlation length
Std ¼Major direction of lay derived from APSDF
Std: Texture direction of surface; APSDF¼Angular power spectral density function
rffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi
Hybrid characterization R Lx R Ly  ;y Þ2 ∂Z ðx ;y Þ2
Sdq ¼ A1 0 0 ∂Z ðx ∂x þ ∂y dy dx

Sdq: Root-mean square surface slope


Z Z    2 
1 Lx Ly ∂2 Z ðx ; y Þ ∂ Z ðx ; y Þ
Ssc ¼ þ dy dx
A 0 0 ∂x 2 ∂y 2
Ssc: Mean summit curvature

ðTotal surface areaÞ  ðCross sectional areaÞ


Sdr ¼
Cross sectional area
Sdr: Developed surface area ratio
Functional characterization Sq 1
Sbi ¼ ¼
True heightð0:05Þ hð0:05Þ
Sbi: Surface bearing index
 
Vv ðh0:05 Þ  Vv ðh0:80 Þ
Sci ¼ C Sq
A

Sci: Core fluid retention index; smoother¼Smaller sci


 
Vv ðh0:80 Þ
Svi ¼ C Sq
A

Svi: Valley fluid retention Index; good fluid retention¼larger Svi


(Continued )
256 Topological Evaluation of Surfaces in Relation to Surface Finish

Table 3 Continued

3D surface profile parameters Equation with description


 
Vmðh0:10 Þ
Sm ¼
A
Sm: Surface material volume – Volume from top to 10% bearing area
 
Vv ðh0:10 Þ  Vv ðh0:80 Þ
Sc ¼
A
Sc: Core void volume – Volume enclosed 10–80% bearing area
 
Vv ðh0:80 Þ  Vv ðh1:00 Þ
Sv ¼
A

Sv : Surface void volume – Volume from 80 to 100% bearing area

Table 4 Adding and altering methods

Adding and altering Working principle Topological evaluation Applications


methods of surface finish

Blanching Whitening of a surface using acid or coating 0.4–0.8 mm Tin based productions, etc.
with tin.
Case hardening Hardening of surface such as flame and 0.3–0.5 mm Screws, firing pins and rifle bolt faces,
induction hardening, carburizing, nitriding, or engine camshafts, etc.
cyaniding, carbonitriding, ferritic
nitrocarburizing.
Ceramic glaze Coating of vitreous materials to fuse with 0.3–0.5 mm Coloring, water-proofing, and
ceramic using fire. decorating purposes, etc.
Cladding Bonding of two different metals by pressing/ 0.5–1 mm Heat exchangers, coins productions,
extruding two metals through a die/rolling etc.
two metal sheets with high pressure.
Corona treatment Modificating surface using electrically 0.5–1 mm Polyethylene, polypropylene, vinyl,
discharge plasma. PVC, PET, metalized surfaces, etc.
Diffusion processes Diffusing carbon or nitrogen to a metal 0.5–1 mm Gears, crankshafts, valve parts,
surface. extruder screws, die-casting tools,
-Carburizing Diffusing carbon to a metal surface. forging and extrusion dies, injectors,
-Nitriding Diffusing nitrogen to a metal surface. and plastic-mold tools, etc.
Electroplating Coating metal objects with a thin layer of a 0.5–1 mm Circuits of cell phones, computers, and
different metal. other electronic devices, etc.
Galvanizing Coating steel with zinc to provide long term 150 mm Building and construction, etc.
corrosion protection and abrasion
resistance with hot metal bath or Electro-
deposition.
Gilding Coating metals and nonmetals with gold leaf, NA Hand application and glueing,
gold flakes, brass, etc. electroplating, etc.
Glazing Glazing by spraying, dipping, pouring, and NA Ceramic glaze, insulated glazing, etc.
painting etc.
Knurling Producing indentations on a part of a NA Tool handles, mechanical pencils, and
workpiece. the control knobs on electronic
equipment, etc.
Painting Applying paint, pigment, color, or other NA Knives, sponges, and airbrushes, etc.
medium to a surface.
Passivation/Conversion Coating with a chemical or electro-chemical NA Microelectronics, photovoltaics, etc.
coating process.
-Anodizing Increasing thickness of the natural oxide layer Usually, the higher the Baseball bats, signs, furniture, surgical
on metal surface by forming the anode anodizing voltage, the trays, motorcycle, architectural
electrode of an electrical circuit. more roughening molding, etc.
occurs.
-Bluing Heating the steel until a blue oxide film NA Guns, firearms, razor blades, etc.
appears without chemicals.
-Chromate conver- Applying chromate conversion coating to NA Aircraft industry, everyday items such
sion coating substrate to passivate steel, aluminum hardware, tools, etc.
alloys.
(Continued )
Topological Evaluation of Surfaces in Relation to Surface Finish 257

Table 4 Continued

Adding and altering Working principle Topological evaluation Applications


methods of surface finish

Phosphate conversion Spraying to the surface with dilute solution of NA Application of supplemental coatings:
coating phosphoric acid and phosphate salts to lubricants, sealers, oil, etc.
form phosphates layer.
♦♦ Parkerizing The process involves submerging the metal NA Automobiles, firearms, etc.
part into a phosphoric acid solution.
-Plasma electrolytic Producing oxide coatings on metals, using NA Aerospace and defense (gearboxes,
oxidation higher potentials, so that discharges occur, gear bearing carriers, etc.).
resulting plasma modifies structure of the
oxide layer.
Plasma spraying Producing coatings on structural materials NA Corrosion protection, medical implants,
into the plasma jet, emanating from a etc.
plasma torch.
Powder coating Producing thicker coatings without sagging, NA Automobile parts, bicycle frames and
and producing minimal appearance parts, etc.
differences between horizontally coated
surfaces and vertically coated surfaces.
Thin-film deposition Depositing a thin film of material onto a Sub-micrometer and Electronic semiconductor devices and
substrate or onto previously deposited nanometer optical coatings, etc.
layers.
-Chemical vapor Depositing thin films of materials on wafers
deposition (CVD) or other substrates.
-Electroplating/ Using electrical current to reduce metal Car parts, bath taps, kitchen gas
Electrodeposition cations in an electrolytic solution in order to burners, wheel rims, and coins such
coat a conductive object with a thin as pennies, etc.
adherent layer, modifying the surface
properties.
-Electrophoretic Suspending colloidal particles in a liquid Automobile bodies and parts, tractors
deposition (EPD) under the electric field, depositing onto an and heavy equipment, electrical
electrode. switch gear, industrial products, etc.
-Mechanical plating/ Descaling and removing soil from the Nails, screws, nuts, washers,
Peen plating/ workpiece in tumbler without electrical stampings, springs, clips, and
Mechanical charge passing through the plating sintered iron components, etc.
deposition/Cold medium.
welding
-Sputter deposition Removing atoms from a solid target's Photovoltaics, flat panel display, etc.
surface, projecting them into gas phase
from condensing on another surface.
-Physical vapor Depositing thin films by the condensation of a Aerospace, Dies, and molds,
deposition (PVD) vaporized form of the desired film material Automotive, Surgical/Medical, Cutting
onto workpiece surfaces. tools, Fire arms, etc.
-Vacuum plating Depositing layers of material atom-by-atom/ Metallic films, semiconductor films,
molecule-by-molecule on a solid surface at solar cells, automotive applications,
below atmospheric pressure (i.e., vacuum). etc.
Vitreous enamel/ Fusing a thin layer of glass at high NA Jewelry and decorative art, housing and
Porcelain enamel temperature on to the surface of a metal. interior walls of major kitchen
appliances, chemical reactors and
pharmaceutical process tanks, etc.

surface finishing covers a wide-ranging of industries and appli- process, their characteristics, tolerances, and roughness values.
cations. The main functions of the surface finishing are the Here, it is clear that each machining process produce different
improvement of the surface appearance, the enhancement of surface topography. Average roughness values for each
the corrosion resistance and the impartment of the required machining process prove that each machining process results
surface properties. Surface finishing processes can be categorized in different surface texture.
by how they affect the workpiece as adding or altering finishing Table 7 explicitly indicates the general characteristics of
(Table 4) and removing or reshaping finishing (Table 5). advanced machining processes.26 Information regarding the
Table 6 represents the general characteristics of machining process, their characteristics, tolerances and roughness values
processes.26 This table gives detail information regarding the are detailed.
258 Topological Evaluation of Surfaces in Relation to Surface Finish

Table 5 Removing and reshaping methods

Removing and Working principle Topological evaluation range Applications


reshaping methods

Abrasive blasting Propelling a stream of abrasive material NA The lettering and engraving on most
against a surface under high pressure modern cemetery monuments and
to smooth a rough surface. markers, etc.
-Sandblasting Producing 3D-signage. These signs often Refurbish buildings, cleaning boat
incorporate gold leaf overlay and hulls, brick, stone, concrete work,
crushed smalts. etc.
Burnishing Burnishing smears the texture of a rough 0.125–0.5 mm The inner ring of the ball bearing,
surface and makes it shinier. burnishing tools, etc.
Chemical-mechanical Using abrasive chemical slurry, to Sub-micrometer and nanometer Semiconductor devices,
planarization (CMP) remove material and making any photolithographic applications, etc.
irregular topography the wafer flat.
Electropolishing Removing surface imperfections from a Sub-micrometer and nanometer Drums of washing machines,
sample to polish, passivate, deburr surgical devices, etc.
metal parts using chemicals and
electrical current.
Flame polishing Exposing the material to a flame smooths Sub-micrometer Glass pipettes, electronic industry, IC
tension of the surface out. encapsulation, etc.
Gas cluster ion beam Bombarding to a surface by a beam of Sub-nanometer Semiconductor devices, optical thin
high energy nano cluster ions using films, fixed disk memory systems.
gas cluster ion beam.
Grinding Using a rotating abrasive wheel to 0.1–1.6 mm Sealing surfaces between cylinder
smooth the flat surface of materials to head and cylinder liner and
reach an ideal surface for a functional between cylinder liner and engine
purpose. frame, etc.
Industrial etching/ Using baths of temperature-regulated Sub-micrometer and nanometer Printed circuit board, semiconductor,
Chemical milling etching chemicals to remove material integrated circuits and
to attain the desired shape. microelectromechanical systems
etc.
Linishing Using grinding or belt sanding 0.1–3.2 mm Profiles with square and rectangular
techniques to improve the flatness of a section, etc.
surface and produces a matt finish.
Mass finishing Deburring, radiusing, smoothing, Sub-micrometer and nanometer Metal parts, etc.
processes/Vibratory polishing and degreasing the mass
finishing produced parts by mechanical/chemical
means.
Pickling Remove impurities from ferrous metals Pickled surfacing increases Jewelry, sheet steel, plate, coil, etc.
with a solution called pickle liquor roughness range (2–6 mm)
containing strong acids.
Polishing Rubbing the surface or using a chemical 0.05–0.5 mm Household cleaners, car polish,
action in order to create a smooth and stone polishing, jewelry, plastics,
shiny surface. brake linings, ball bearings,
aerospace, etc.
-Buffing Smoothing the surface using an abrasive Automotive, aviation, composite,
and a work wheel or a leather strop. marine, etc.
-Lapping Rubbing two surfaces together with an Aircraft and motor manufacturers,
abrasive by hand movement or using a electronics companies,
machine. clockmakers, toolmakers, etc.
Peening/Shot peening Bombarding to a metal part by tiny balls Shot peening treatment Crankshafts, gears, torsion bars,
of steel, stainless steel, cut-wire, glass, increases roughness range springs, valves, exhaust manifolds,
or ceramic shot. (1–6 mm) blades, disks, turbines, etc.
Superfinishing Using bonded abrasive stick moved with 0.025–0.2 mm Computer memory drums, sewing
a reciprocating motion and pressed machine parts, automotive
against the surface to be finished cylinders, bearing components,
(similar to honing). pistons rods, axles, shafts, clutch
plates, etc.
Magnetic field- Using a magnetic field to force abrasive Sub-micrometer and nanometer Medical components, fluid systems,
assisted finishing particles against the target surface. optics, dies and molds,
microelectromechanical systems,
etc.
Topological Evaluation of Surfaces in Relation to Surface Finish 259

Table 6 General characteristics of machining processes

Process Characteristics Commercial tolerances Roughness average, Ra (mm)


(7mm)

Turning Turning and facing operations are performed on all types Fine: 0.05–0.13, 0.4–6.3
of materials; requires skilled labor; low production rate, Rough: 0.13,
but medium to high rates can be achieved with turret Skiving: 0.025–0.05
lathes and automatic machines, requiring less skilled
labor.
Boring Internal surfaces or profiles, with characteristics similar to 0.025 0.4–6.3
those produced by turning; stiffness of boring bar is
important to avoid chatter.
Drilling Round holes of various sizes and depths; requires boring 0.075 1.6–6.3
and reaming for improved accuracy; high production
rate; labor skill required depends on hole location and
accuracy specified.
Milling Variety of shapes involving contours, flat surfaces, and 0.13–0.25 0.8–6.3
slots; wide variety of tooling; versatile; low to medium
production rate; requires skilled labor.
Planing Flat surfaces and straight contour profiles on large 0.08–0.13 1.6–12.5
surfaces; suitable for low-quantity production; labor
skill required depends on part shape.
Shaping Flat surfaces and straight contour profiles on relatively 0.05–0.13 1.6–12.5
small workpieces; suitable for low-quantity production;
labor skill required depends on part shape.
Broaching External and internal flat surfaces, slots, and contours 0.025–0.15 0.8–3.2
with good surface finish; costly tooling; high production
rate; labor skill required depends on part shape.
Sawing Straight and contour cuts on flats or structural shapes; 0.8 1.6–25
not suitable for hard materials unless the saw has
carbide teeth or is coated with diamond; low production
rate; requires only low skilled labor.

Table 7 General characteristics of advanced machining processes

Process Characteristics Commercial tolerances (7mm) Roughness


average, Ra (μm)

Chemical machining Shallow removal (up to 12 mm) on large flat or curved 0.025–0.1 mm min  1 1.6–6.3
surfaces; blanking of thin sheets; low tooling and
equipment cost; suitable for low production runs.
Electrochemical Complex shapes with deep cavities; highest rate of material V: 5–25 DC; A: 0.2–3.2
machining removal; expensive tooling and equipment; high power 2.5–12 mm min  1, depending
consumption; medium to high production quantity. on current density
Electrochemical Cutting off and sharpening hard materials, such as A: 1–3 A mm  2; typically 0.1–1.6
grinding tungsten–carbide tools; also used as a honing process; 1500 mm3 m  1 in per 1000 A
higher material removal rate than grinding.
Electrical-discharge Shaping and cutting complex parts made of hard materials; V: 50–380; A: 0.1–500; typically 0.05–6.3
machining (EDM) some surface damage may result; also used for grinding 300 mm3 min  1
and cutting; versatile; expensive tooling and equipment.
Wire EDM Contour cutting of flat or curved surfaces; expensive Varies with workpiece material 0.8–1.6
equipment. and its thickness
Laser-beam Cutting and hole making on thin materials; heat-affected 0.50–7.5 m min  1 0.2–6.3
machining zone; does not require a vacuum; expensive equipment;
consumes much energy; extreme caution required in use.
Electron-beam Cutting and hole making on thin materials; very small holes 1–2 mm3 min  1 0.2–6.3
machining and slots; heat-affected zone; requires a vacuum;
expensive equipment.
Water-jet machining Cutting all types of nonmetallic materials to 25 mm and Varies considerably with 0.1–3.2
greater in thickness; suitable for contour cutting of flexible workpiece material
materials; no thermal damage; environmentally safe
process
(Continued )
260 Topological Evaluation of Surfaces in Relation to Surface Finish

Table 7 Continued

Process Characteristics Commercial tolerances (7mm) Roughness


average, Ra (μm)

Abrasive water-jet Single or multilayer cutting of metallic and nonmetallic Up to 7.5 m min  1 0.1–1.6
machining materials.
Abrasive-jet Cutting, slotting, deburring, flash removal, etching, and Varies considerably with 0.1–1.6
machining cleaning of metallic and nonmetallic materials; tends to workpiece material
round off sharp edges; some hazard because of airborne
particulates.

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