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Scale Up Solids Handling
Scale Up Solids Handling
Scale Up Solids Handling
Cover Story
Copyright © 2008 American Institute of Chemical Engineers (AIChE).
Successfully Scale Up
Solids Handling
A sound theoretical model of the process to
be scaled is the best approach;
John W. Carson
Thomas G. Troxel if one is not available, bench-scale testing,
K. Eric Bengtson physical scale modeling or full-scale modeling
Jenike & Johanson, Inc.
is required. Here are guidelines
as to which method is appropriate
for various solids-handling operations.
M
ost industrial plants handle powders or other bulk 24 to 60 months to reach complete steady-state operation at
solids (e.g., coal, plastic pellets, sand, alumina), the original design rates (1).
whether as incoming raw materials, intermediates At the root of such start-up and operating problems are
within the process, or finished products. Scale-up of new the lack of fundamental knowledge of bulk solids process-
solids handling processes can be very troublesome, particu- ing technology and the difficulty in extrapolating results
larly if they involve equipment or process steps that differ from one facility to another when the designs are not iden-
significantly from those of any existing facility. For tical. If scale-up is not handled correctly, commercial oper-
example, perhaps the solids themselves are different ation suffers in terms of the time and expense it takes to
because they come from new sources (a typical situation correct problems, the time needed to get a new product to
when the plant receives material from a mining operation), market, customer complaints, and perhaps derating of the
or the particle size distribution is to be changed. Maybe equipment or process.
process conditions (such as operating Whether the new equipment or
temperature, the amount of time the bulk 8
processes being designed involve gases,
“Raw”
solids will be stored without movement, Solid liquids or bulk solids, the best approach
Feedstock
throughput rate, type and flowrate of to scale-up is to use a sound theory that
Average Plant Start-Up Time, mo
process gas, batch vs. continuous operat- has been (or can be) developed to accu-
ing mode, etc.) will be different. 6 rately model the process and equipment
Previously
A study of more than 500 recently Processed, independent of scale. Key variables can
Reasonably
completed projects found a clear rela- Homogenous be readily identified, bench-scale tests
tionship between increased particle-pro- Feedstock can be run, and the results used as input
4
cessing difficulty and the time required data for the mathematical model.
Typical
for the plant to start up (Figure 1) (1). Liquid Lacking a sound theory, the next-best
or Gas
Furthermore, plant operability (defined Process approach is to test small physical models
as percent of design after start-up) 2 and scale up the results using well-under-
decreased as the number of process steps stood and proven scale-up rules. If neither
increased, most dramatically for solids- a sound theory nor proven scale-up rules
processing plants using bulk solid feed. 0 are available, the only safe approach is to
For example, a highly innovative solids- model some or all of the system’s critical
Figure 1. Particle processing, and its
processing facility with many new complexity, affect the time needed for
elements at or close to full-scale.
process elements commonly requires plant start-up. Source: (1). The key is determining which processes
σ = ρb gc r s (θ) (1)
Φ′ ψ = ψ (θ) (2)
0.010
70 60
and Phi (Φ), deg.
50 Delta (δ) 40
Phi (Φ)
Storage Time at Rest
20
30
0.0 200 400 600 800 1,000 0.0 h, 72°F 24.0 h, 72°F
Consolidating Pressure, σ1, kPa 0
0 40 80 120 160 200 240
600
Flow Functions Normal Stress, σ, kPa
Strength, f, kPa
60
Wall Friction Angle,
24.0 h, 72°F
400
Storage Time at Rest
40
Φ′, deg.
0 0
0.0 200 400 600 800 1,000 0 40 80 120 160 200 240
Consolidating Pressure, σ1, kPa Normal Stress, σ, kPa
Figure 9. Shear tests determine internal friction (top) and flow Figure 10. Wall friction tests are used to calculate mass flow
function (cohesive strength) hopper angles.
double-cone mixers. An alternative means of achieving Putting the principles into practice
kinematic similarity is to maintain a constant number of Blending plastic pellets. A new plant was being designed
revolutions of the blender; this has been found to be appro- to produce a wide range of acrylonitrile-butadiene-styrene
priate for tumble blenders, mostly for materials with low (ABS) pellets compounded to customer specifications.
cohesive strength (18). Production runs would be relatively short and formula
changes frequent. Based on experience at smaller plants,
When full-scale tests are required engineers selected a V-type rotating blender. Batch ingredi-
For some applications, neither a well-developed theory ents would be fed into a weigh hopper and discharged into
nor scaling rules have been developed that would allow con- the blender. The blended batch would then be discharged
fident design at full scale. Examples of such situations into a surge bin feeding the extruder. While this process
include: had worked successfully at other compounding plants, this
• transmission of vibrations. The ability of an external facility would blend ingredients with a wider size range.
or internal vibrator to activate material within a storage The most extreme case involved blending two materials that
vessel is not well-understood. As a result, sizing and place- consisted of cylindrical pellets with a nominal size of about
ment of vibrators is done essentially by trial-and-error, and 3 mm and nearly spherical particles (beads) with a size
if possible, is based to some extent on past experience of range from about 1 mm down to 150 µm.
what works and what does not. Engineers evaluated V-type rotating blenders by analyz-
Sometimes vessels vibrate on their own due to move- ing samples from a scale-model blender (18). They found
ment of the material within. The resulting vibrations can that significant segregation could occur, and maintaining a
either be high-frequency, low-amplitude (a humming blend in the discharged material would be difficult. In a typ-
sound), or low-frequency, high-amplitude (known as “silo ical blending test (Figure15), only about 9% of the batch
quaking”). Vibrations can occur by various mechanisms fell within the acceptable range of 15% ±2% beads blended
(19, 20). Scale models may be effective in identifying with pellets. Numerous modifications were made to the
changes that will affect the severity of the vibrations, or model blender to try to improve discharge uniformity, with
may give a false impression of changes that will be effec- only moderate success.
30
Beads in Total Sample, %
25 V-Blender
20 Target Range
15
10 Conical Blender
with Insert
5
0
0 20 40 60 80 100 120
Material Discharged, lb
Figure 15. A conical mass-flow blending vessel with an insert Figure 16. A conical mass-flow blend vessel with an insert is
provides a more uniform product than a V-blender. successfully scaled up to a 6,000-lb blender.
Literature Cited amounts of air are injected into the material via a porous
membrane. The air fluidizes a small boundary layer of
1. Merrow, E., “Problems and Progress in Particle Processing,”
Chemical Innovation, 30 (1), pp. 35–41 (Jan. 2000).
material, thus reducing the boundary friction and enabling
2. Jenike, A. W., “Gravity Flow of Bulk Solids,” Bulletin No. the material to be discharged at higher rates than would
108, Univ. of Utah Engineering Experiment Station, Salt be possible without air injection. The discharger is com-
Lake City, UT (Oct. 1961).
3. Jenike, A. W., “Storage and Flow of Solids,” Bulletin No. prised of several different gas plenums, each designed to
123, Univ. of Utah Engineering Experiment Station, Salt allow, nominally, different amounts of gas to be injected
Lake City, UT (Nov. 1964). into the material. Control of the air-assisted discharger
4. Johanson, J. R., “Stress and Velocity Fields in the Gravity
Flow of Bulk Solids,” J. Appl. Mech. Series E, 31, pp. is critical from the standpoint of obtaining mass flow in
499–506 (1964). the silo above.
5. Sokolovski, V. V., “Statics of Soil Media,” Butterworths
Scientific Publications, London (1960).
Bench-scale fluidization tests are carried out to deter-
6. Ergun, S., “Fluid Flow through Packed Columns,” Chem. mine fluidization characteristics of the powder. Scale-model
Eng. Progress, 48 (2), pp. 89–94 (Feb. 1952). air-assisted discharger tests are also run. If both sets of tests
7. Leva, M., “Fluidization,” McGraw-Hill New York, NY (1959).
8. ASTM International, “Standard Test Method for Shear show that the powder is a good candidate for this type of
Testing of Bulk Solids Using The Jenike Shear Cell,” ASTM feed system, scale-up can proceed.
D6182-06, ASTM, West Conshohocken, PA (2006). This is an example of scale-up using a combination of
9. ASTM International, “Standard Shear Testing Method for
Bulk Solids Using Schulze Ring Shear Tester,” ASTM theoretical models with inputs from bench-scale tests, in
D6773-02, ASTM, West Conshohocken, PA (2002). conjunction with proper scaling approaches. CEP
10. ASTM International, “Standard Test Method for Measuring
Bulk Density Values of Powders and Other Bulk Solids,”
ASTM D6683-01, ASTM, West Conshohocken, PA (2001).
11. Johanson, J. R., and T. A. Royal, “Abrasive Wear Tester,” JOHN W. CARSON, PhD, is president of Jenike & Johanson, Inc. (400 Business
U.S. Patent No. 4,446,717 (May 8, 1984). Park Dr., Tyngsboro, MA 01879; Phone: (978) 649-3300; E-mail:
12. Johanson, J. R., and T. A. Royal, “Measuring and Use of jwcarson@jenike.com), an engineering consulting firm specializing in the
Wear Properties for Predicting Life of Bulk Materials Handling storage, flow and processing of powder and bulk solids. He is the author of
Equipment,” Bulk Solids Handling, 2, pp. 517–523 (1982). more than 100 articles on various topics dealing with solids flow, including
13. Johanson, J. R., “The Use of Flow-Corrective Inserts in bin and feeder design, flow of fine powders, design of purge vessels, and
Bins,” J. Eng. Industry, Series B, 88, pp. 224–230 (1966). structural failures of silos, and he lectures extensively on such topics. He
14. Carson, J. W., “Addressing Critical Solids Handling Aspects received a BS in mechanical engineering from Northeastern Univ. in Boston
at the Pilot Scale,” presented at the AIChE Spring Meeting, and a PhD in mechanical engineering from the Massachusetts Institute of
New Orleans, LA (Mar. 1988). Technology. Carson is a member of AIChE and founding member of AIChE’s
15. Carson, J. W., and T. A. Royal, “In-Bin Blending Improves Powder Technology Forum, and he belongs to ASME, ASCE, and ASTM
Process Control,” Powder Handling & Processing, 4 (3), pp. International, where he is chair of committee D18.24, “Characterization and
301–307 (Sept. 1992). Handling of Powders and Bulk Solids.” He recently received the U.K.
16. Carson, J. W., et al., “Tumble Blending with Mass Flow Institution of Mechanical Engineers’ Solids Handling Award, and is a
Containers Improves Productivity and Quality,” Powder permanently invited guest to the European Federation of Chemical
Handling & Processing, 6 (4), pp. 413–416 (Oct/Dec 1994). Engineering’s Working Party Mechanics of Particulate Solids, one of few
17. Wang, R. H. and L. T. Fan, “Methods for Scaling up non-Europeans to be so honored.
Tumble Mixers,” “Solids Handling,” published by Chem. THOMAS G. TROXEL is vice president of Jenike & Johanson, Inc. (3485
Eng., McGraw-Hill, New York, NY, pp. 245–251 (1981). Empresa Dr., San Luis Obispo, CA 93401; Phone: (805) 541-0901; E-mail:
18. Troxel, T. G., “Modeling and Scale-Up of Tumble Blenders tgtroxel@slo.jenike.com), where he has been intimately involved in many
for Highly Segregating Materials,” presented at the 5th World aspects of the firm’s consulting and research activities on a wide range of
Congress on Particle Technology, Orlando, FL (Apr. 2006). projects, including flow properties testing, modeling, blending, pneumatic
19. Purutyan, H., et al., “Identifying and Controlling Silo conveying and fluidization. He has been a major force behind the firm’s
Vibration Mechanisms: Part I,” Powder and Bulk expansion of services in the areas of mechanical design engineering and
Engineering, 8 (11), pp. 58–65 (Nov. 1994). supply of custom-built equipment, such as mass-flow screw feeders,
20. Purutyan, H., et al., “Identifying and Controlling Silo portable anti-segregation bins for pharmaceuticals, tumble blenders and
Vibration Mechanisms: Part II,” Powder and Bulk storage bins for a wide variety of applications. Troxel has published
Engineering, 8 (12), pp. 19–28 (Dec. 1994).
numerous articles and papers in the field of bulk solids handling, and
21. Carson, J. W., et al., “Understanding and Eliminating
lectures frequently on the subject. He is a graduate of California
Particle Segregation Problems,” Bulk Solids Handling, 6, pp.
Polytechnic State Univ. (Cal Poly) in San Luis Obispo, CA, with a BS in
139–144 (Feb. 1986).
engineering science.
22. ASTM International, “Standard Practice for Measuring
K. ERIC BENGTSON is a senior project engineer and laboratory manager at
Sifting Segregation Tendencies of Bulk Solids,” ASTM
D6940-04, ASTM, West Conshohocken, PA (2004). Jenike & Johanson. Inc. (3485 Empresa Dr., San Luis Obispo, CA 93401;
23. ASTM International, “Standard Practice for Measuring Phone: (805) 541-0901; E-mail: ebengston@slo.jenike.com), where he has
Fluidization Segregation Tendencies of Powders,” ASTM been involved in a wide range of consulting and research projects, such as
D6941-05, ASTM, West Conshohocken, PA (2005). flow properties testing, physical scale modeling, feeder design, gas-
assisted discharge, blending, pneumatic conveying and fluidization. He has
published several technical papers in the field of bulk solids handling, and
has been awarded two U.S. patents in this field. He holds a BS in
Acknowledgment mechanical engineering from California Polytechnic State Univ. (Cal Poly) in
This article is based on a presentation given at the AIChE Annual Meeting, Salt San Luis Obispo.
Lake City, November 2007.