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20 - CompositesB59 (2014) 33 42 - Graded Auxkirigami SS
20 - CompositesB59 (2014) 33 42 - Graded Auxkirigami SS
Composites: Part B
journal homepage: www.elsevier.com/locate/compositesb
a r t i c l e i n f o a b s t r a c t
Article history: The work describes the manufacturing and testing of graded conventional/auxetic honeycomb cores. The
Received 19 July 2013 graded honeycombs are manufactured using Kevlar woven fabric/914 epoxy prepreg using Kirigami tech-
Received in revised form 20 September 2013 niques, which consist in a combination of Origami and ply-cut processes. The cores are used to manufac-
Accepted 29 October 2013
ture sandwich panels for flatwise compression and edgewise loading. The compressive modulus and
Available online 8 November 2013
compressive strength of stabilized (sandwich) honeycombs are found to be higher than those of bare
honeycombs, and with density-averaged properties enhanced compared to other sandwich panels
Keywords:
offered in the market place. The modulus and strength of graded sandwich panel under quasi-static edge-
A. Honeycomb
B. Mechanical properties
wise loading vary with different failure mode mechanisms, and offer also improvements towards avail-
B. Impact behavior able panels from open literature. Edgewise impact loading shows a strong directionality of the
E. Assembly mechanical response. When the indenter impacts the auxetic portion of the graded core, the strong local-
ization of the damage due to the negative Poisson’s ratio effect contains significantly the maximum
dynamic displacement of the sandwich panel.
Ó 2013 Elsevier Ltd. All rights reserved.
1359-8368/$ - see front matter Ó 2013 Elsevier Ltd. All rights reserved.
http://dx.doi.org/10.1016/j.compositesb.2013.10.084
34 Y. Hou et al. / Composites: Part B 59 (2014) 33–42
numerically demonstrated that the cellular wingbox was a major strong dependence over the direction of dynamic loading, with
contributor in the torsion stiffness and static divergence of the interesting potential implications for energy absorption during im-
wing structure. In terms of graded honeycomb core and pact (see Fig. 1).
corresponding sandwich structures, efforts have been produced
to design and develop gradient-type cellular and porous structures
2. Kirigami sandwich panels manufacturing process
[29–32]. Lim [33] theoretically designed a functionally graded
cellular structure exhibiting Poisson’s curving by combining the
Both hexagonal and auxetic honeycombs are manufactured
re-entrant and hexagonal honeycomb together, which is called
using one layer woven Kevlar/914 epoxy prepreg from Hexcel
positional semi-auxetics. Also the same author has shown that
Composites Ltd., Duxford, UK (Es = 29 GPa, q = 1380 kg/m3, thick-
the combination of conventional laminas (possessing positive
ness 0.250 mm).
Poisson’s ratio) and auxetic laminas (possessing negative Poisson’s
The Kirigami manufacturing process consists in the following
ratio) can give rise to effective in-plane composite laminates with a
five steps: cutting, molding, curing, folding and bonding. Periodic
stiffness that surpasses the one predicted by rule-of-mixture [34].
distributions of slits are introduced within the plain weave woven
Gradient honeycomb configurations have been produced and
using an Auto Prepreg Cutting machine following the patterns
tested showing high specific shear stiffness capabilities, together
shown in Fig. 2a. The ply-cut pattern is programmed based on
with control of the anisotropy of the cellular panel [35]. Gradient
the topology of the unit cell of honeycombs with parameters l, h
core configurations have been also proposed to design aeroengine
and h, and the gauge thickness of the honeycomb walls (b) [5].
fan blades with low dynamic displacement characteristics [36].
The automatic machining is illustrated in Fig. 3a. The solid lines
Gradient cellular structures with auxetic behavior for sandwich
in the cutting pattern (Fig. 2b) indicate cutting through the thick-
panels have also shown strong localization charcateristics in terms
ness of the prepreg (0.125 mm). The long cutting-through lines will
of damage and failure under 3-point bending loading [37]. Gradi-
form the open cores after folding, whereas the dot cutting lines are
ent cellular structures can be considered a form piezomorphing
applied to ease the subsequent folding. The pre-cut prepreg is then
porous material, in which the structure responds with shape
laid over an aluminum bar (Fig. 3b) designed according to the
changes due to an external mechanical loading [38]. Ruzzene
topology of the unit cell (Fig. 2c). The molded sample is subse-
et al. [39] have investigated the wave propagation characteristics
quently sealed in a vacuum bag and placed for curing in an auto-
of sandwich plates with periodic honeycomb core. Negative Pois-
clave. The curing temperature for the thermoset woven prepreg
son’s ratio (auxetic) core materials of different geometry placed
used is 175°. The other parameters of the autoclave curing
periodically in the plate have demonstrated to introduce the
(Fig. 3c) are the pressure (100 psi) and duration (125 min).
impedance mismatch necessary to obstruct the propagation of
The cured prepreg is extracted and folded along a zigzag pattern
waves over specified frequency bands (stop bands) and along par-
along the cutting line to form the honeycombs (Fig. 3d). After fold-
ticular directions [39].
ing, the horizontal walls of the honeycomb ribbons are bonded to-
The work described in this paper is concerned about the phys-
gether using epoxy adhesive (Hexcel ReduxÒ 810) and cured for
ical realization of the concept proposed in Ref. [39], the graded core
10 min at 120° (Fig. 3e. The dimensions of the honeycomb config-
sandwich panel. The complex geometry of the core is produced
urations used in this work are l = h = 5.5 mm, h = 30° for the hexag-
using the Kirigami technique using woven Kevlar prepreg and
onal case, and h = 10.5 mm, l = 5.5 mm, h = 30° for the auxetic
modulus molds for autoclave curing. A portion of the graded hon-
cellular structure. The total gauge thickness of the two honeycomb
eycomb is made with hexagonal conventional cells, while the other
structures is b = 25 mm. According to the Cellular Material Theory
section is represented by a re-entrant (negative Poisson’s ratio)
(CMT), the in-plane Poisson’s ratio t12 for the hexagonal honey-
butterfly-type core. The graded honeycombs are then embedded
comb is 1.0, while the auxetic configuration would have a Poisson’s
into CFRP sandwich panels, and subjected to ASTM standards tests
ratio value of 1.06 [5].
related to flatwise compression and edgewise loading. A drop-
Conventional-auxetic graded honeycomb have been produced
tower impact edgewise test is also carried out, with the samples
by gluing together the hexagonal and auxetic core using the same
facing up the indenter alternatively along the conventional and
Hexcel ReduxÒ 810 epoxy adhesive. The final graded cellular
auxetic face. The experimental results are compared against avail-
structure is shown in Fig. 4. The graded cores have been used to
able cores and sandwich panels from open literature and the mar-
manufacture flat sandwich panels, with face skins made from
ket place. It will be shown that the graded core concept provides
two quasi-isotropic carbon fiber composites (stacking sequence
some significant enhancements in terms of specific flatwise and
of [0°/45°/–45°/90°]2s). The carbon prepreg chosen is T800/2020
edgewise compressive strength against commercial sandwich pan-
carbon/epoxy unidirectional prepreg (CYCOMÒ Corporation) with
els and core materials. The graded cellular concept shows also a
a sheet thickness of 0.125 mm. The skins are bonded to the
graded honeycomb core using a LH149 epoxy adhesive (LETOXITÒ
Corporation) cured at 120° for 1 hour and a half.
3. Testing
with the top plate being fixed and the bottom plate moving there is no relevant testing standard for edgewise impact loading,
upwards at a constant velocity of 0.5 mm/min. The deflection of the configuration and the specimen dimensions are designed to
the sandwich panel is calculated from the displacements of the meet the setup of the Instron drop weight tower (Fig. 7a and b).
bottom plate, which were tracked using a 2D digital image correla- The dimension of the specimen is 110 mm 80 mm 28 mm,
tion system (Davis 7). A total of three sandwich panels have been with the diameter of the impact roller equal to 50 mm. The bottom
tested, and the buckling morphology of one of them is shown in end of the graded sandwich panel is fixed by clamping between
Fig. 5d. two plates to prevent a fall during the impact. Two specimens have
been impacted edgewise, one with the roller hitting the hexagonal
3.2. Edgewise compression tests of graded sandwich panels core side, the other the re-entrant one. The tests have been carried
out using impact energy of 15 J.
The compressive properties of the graded sandwich topology
along the direction parallel to the plane of the sandwich face skin 4. Results and discussions
are evaluated through edgewise compression tests according
to the ASTM Standard ASTM C364/C364M-07 [43] carried out 4.1. Flatwise compression
on a Zwick testing machine (Fig. 6a). The specimen size
(51 mm 51 mm 28 mm) satisfies the requirements of the The stress and strain curves of the graded sandwich panels un-
ASTM standard, while being quite similar to the one used to der flatwise compression are shown in Fig. 8. Table 1 shows also
dimension the specimens for flatwise compression tests (Fig. 5a the compressive modulus and strength for different conventional,
and b). The specific machine configuration setup shown in Fig. 6a auxetic and graded configurations. Samples #1 and #2 are the re-
is the same used for the flatwise testing, with the top plate fixed ferred to the Kevlar woven epoxy (KWEP) fabric specimens, with
and the bottom plate moving upwards at a constant velocity of hexagonal and auxetic topology respectively [44]. Sample #3 is re-
0.5 mm/min. The 2D digital image correlation system (Davis 7) is ferred to KWEP graded sandwich core developed in this work. The
again used to track the displacement at the bottom plate, consid- table contains other comparative data available from open litera-
ered as the overall deflection of the sample. Three specimens are ture, like HRH78 core (Sample #4), the sandwich panel made with
tested in total, and different failure modes are observed during the same type core material (Sample #5), and core and sandwich
loading (Fig. 6b–d). Since the edgewise loading is quasi-static, panel made with HRH10 honeycomb (Samples #6 and #7 respec-
edgewise compression tests are only performed in only one direc- tively). HRH78 is made from aramid paper sheets (NOMEX paper),
tion, with the auxetic core over the hexagonal one. The use of qua- while aramid fiber sheets constitute the HRH10 core. Both honey-
si-static tests implies that the loading force has sufficient time to combs are impregnated with phenolic resin. The face skins of the
be transmitted throughout the whole graded sandwich structure benchmark sandwich panels with aramid core are made from glass
before the specimen fails. fiber [45]. Another core considered for comparison is the alumi-
num-based 5052 (pristine core and sandwich panel for Samples
3.3. Edgewise impact tests on graded sandwich panels #8 and #9 respectively). The data for the material properties are
available from Ref. [46].
The impact response of the graded sandwich panels under A sandwich panel with honeycomb core bonded to composite
edgewise loading from two different sides is investigated using skins has higher compressive strength than the pristine
an Instron Dynatup Model 9250HV Drop Weight System. Since honeycomb cores [40,41]. Flatwise compression tests on bare
36 Y. Hou et al. / Composites: Part B 59 (2014) 33–42
Fig. 3. Specific manufacturing process of hexagonal and re-entrant honeycombs using the Kirigami technique.
Fig. 4. Manufacturing of graded honeycomb core and corresponding sandwich panel. The sample on the left is the one used for edgewise loading, while the one on the right is
for flatwise compression.
Y. Hou et al. / Composites: Part B 59 (2014) 33–42 37
honeycomb core structure tend to provide an underestimation of When inserting the numerical values related to the conventional
the honeycomb performance in the sandwich panels, since the and auxetic bare honeycombs in Eq. (1), the hexagonal configura-
boundary conditions in the two cases are quite different [40]. tion provides an increase of the global buckling stress compared
The presence of face skins constrains the rotations in the plane to the conventional configuration by 34%. The experimental results
perpendicular to the loading and imposes a more uniform show however an opposite trend, suggesting that the Kirigami-
through-the-thickness deformation than the one guaranteed by based honeycombs do undergo a more complex compression failure
Fig. 6. Edgewise compression tests on graded sandwich panels and different failure modes observed.
38 Y. Hou et al. / Composites: Part B 59 (2014) 33–42
Fig. 7. Edgewise impact on graded sandwich panels from the re-entrant side and hexagonal side.
Table 1
Compression properties and density of different honeycomb cores and sandwich panels [45,46].
Specimens #1 #2 #3 #4 #5 #6 #7 #8 #9
Compressive modulus (MPa) 8.14 10.41 91.71 – 41.37 – 41.37 – 137.90
Compressive strength (MPa) 0.47 0.56 1.21 0.59 0.66 0.66 0.72 0.62 0.66
Density (kg/m3) 33.9 59.3 269.0 24 272.28 24 272.28 25.6 231.86
Y. Hou et al. / Composites: Part B 59 (2014) 33–42 39
and the same type of dynamic loading when the auxetic core faces
directly the impact. The maximum displacement occurred by the
graded specimen with the auxetic face against the indenter is
2.8 mm, against the 7 mm observed for the sample with the hexag-
onal honeycomb face-up. The peak loads are also quite different,
with the specimen with the auxetic side against the indenter
exhibiting peak force values of 8.7 kN, while the other sample sus-
tains peak force of 6 kN. It is interesting at this stage to observe the
damage occurred by the two samples around the impact area. The
area of the auxetic honeycomb facing up the indenter has a strong
localization of the damage, with the nearby cell walls (L direction
[1]) barely affected (Fig. 7c). The samples with the conventional
hexagonal side (W direction [1]) shows a larger portion of the ob-
lique cell walls affected by the impact (Fig. 7d). The contribution to
the damage mechanism given also by the relative scale between
cell sizes, their orientation and overall width of the sandwich spec-
imen is evident in this case. For the case where the full edge of the
wall of length h faces the indenter, the stress on the wall are likely
to be reduced due to the larger area of cell wall available to the in-
Fig. 11. Comparison of edgewise compressive strength of different sandwich
panels.
denter, leading to reduced displacement of the core. On the other
hand, for the conventional side facing the indenter the vastly re-
duced area of the edge of the oblique cell wall (length l) contributes
compressive strengths between 1.2 MPa and 1.6 MPa under to a much higher stress with which to cause deformation of the
ASTM C-3694-94 standard [51]. Glass–phenolic/Nomex honey- wall, which itself is free at the facing edge (away from the skins)
combs subjected to edgewise loading have shown maximum and therefore easier to deform. These interactions between local
compressive strengths of 235.2 MPa in larger sandwich panel sam- deformations, size and geometry of the cells are an important com-
ples (25.4 mm 75 mm 115 mm) [52]. FRP/PMI/PVC sandwich ponent of the different edgewise-loading behavior observed in
panels with overall thickness around 40 mm have been observed these tests. The strong localization of the damage is however a
to provide edgewise compressive strengths varying between characteristic feature of auxetic materials, and it has been observed
4 MPa and 14 MPa, depending on the type of collapse mode [53]. experimentally in CFRP laminates with cross-ply [±30]6s stacking
Similar values of the compressive edgewise strength recorded for sequence showing a negative through-the-thickness Poisson’s ratio
the graded panels (26 MPa) at 2% of edgewise strain have been (t13 = 0.156 [55,56]). It is also worth noticing that the auxetic
observed recently in sandwich panels made with glass/epoxy face laminates have also shown a higher peak load during low kinetic
skins (1.5 mm of thickness) and composite Nomex/sintactic foam energy impact (5 J) compared to analogous CFRP plates with equiv-
cores, albeit with densities around 624 kg m3 [54]. A comparative alent in-plane stiffness [56]. However, contrary to auxetic plates
analysis of the specific edgewise compressive strength for com- impacted along the through-the-thickness direction, the maximum
mercially available sandwich panels is shown in Fig. 11. The graded displacement observed in these graded core structures (auxetic
core panel shows an improvement of the compressive strength per side face up) is significantly lower than the analogous one from
density by a factor varying between 6.3 and 13.1. the sandwich panel with conventional side bearing the load. It ap-
pears that the auxetic portion of the core absorbs a significant
amount of the deformation of the panel, leaving the rest of the
4.2.2. Edgewise impact tests
structure relatively unaffected by the dynamic loading. Stress
Load–displacement curves of the graded sandwich structures
waves in 1D gradient configurations have shown a clear depen-
subjected to edgewise impact are shown in Fig. 12. One can ob-
dence of the maximum displacement of the structure versus the
serve a significant difference between the impact sustained by
density variation, with the minimum deformation occurring in lay-
the sample with the hexagonal core side against the indenter,
ered configuration towards higher linear density distributions [57].
Another aspect to be considered for these graded cellular struc-
tures is the mismatch impedance existing at the interface between
the two sets of cellular cores. The use of cellular cores with differ-
ent topologies and discrete interface can induce a strong change in
pass-stop band distributions in one dimensional periodic struc-
tures, with deeper attenuation of the dynamic displacements
[39,58]. Graded distributions of foams in finite size samples have
shown a marked reduction of the transmitted waves through the
portion of the foam with diminishing density [59]. For low kinetic
energy impacts, the relative scale of the wavelength with the
dimension of the samples allows to use one a 2D wave propagation
theory between mismatched media. Because of the finite size scale
effects between number and dimensions of the cells and the inter-
face between the two cellular sections, the theoretical consider-
ations based on asymptotic homogenization have some
limitations in terms of validity, however they are able to capture
some underlying physics aspects occurring during the impact. It
can be demonstrated that for a wave with propagation direction
Fig. 12. Load displacement curves of graded sandwich panels impacted from of 0° (i.e., along the loading direction of the impact), the Christoffel
hexagonal and re-entrant side. equation to calculate the wave group velocities cph reduces to [60]:
Y. Hou et al. / Composites: Part B 59 (2014) 33–42 41
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