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Applied Thermal Engineering 211 (2022) 118515

Contents lists available at ScienceDirect

Applied Thermal Engineering


journal homepage: www.elsevier.com/locate/apthermeng

Research Paper

Online in-situ monitoring of melt pool characteristic based on a single


high-speed camera in laser powder bed fusion process
Heng Ma a, 1, Zhuangzhuang Mao a, 1, Wei Feng a, 1, Yang Yang b, Ce Hao c, Jiangfan Zhou d,
Sheng Liu e, Huimin Xie f, Guangping Guo b, Zhanwei Liu a, *
a
School of Aerospace Engineering, Beijing Institute of Technology, Beijing 100081, China
b
AECC Beijing Institute of Aeronautical Materials, Beijing 100095, China
c
AECC Commercial Aircraft Engine Co. Ltd., Shanghai 200241, China
d
Beijing Institute of Structure and Environment Engineering, Beijing 100076, China
e
School of Power and Mechanical Engineering, Wuhan University, Wuhan 430072, China
f
AML, Department of Engineering Mechanics, Tsinghua University, Beijing 100084, China

A R T I C L E I N F O A B S T R A C T

Keywords: In metal additive manufacturing (AM), the in-situ measurement of the melt pool characteristic plays a significant
Additive manufacturing role in monitoring the quality of the printed components. In this work, based on dual-wavelength thermometry, a
Laser powder bed fusion coaxial melt pool temperature measurement system with a single high-speed camera in the laser powder bed
Online in-situ monitoring
fusion (LPBF) process is developed, including the design of the relay and optical path amplification system, and
Melt pool characteristic
the beam splitting and chromatic aberration correction system. Moreover, a dual-waveband image-matching
Temperature measurement
method with sub-pixel accuracy, and an overall parameter calibration and optimization method are proposed to
improve the accuracy of the coaxial temperature measurement system. Besides, the validation experiment
measured by a high-temperature blackbody furnace and a standard photoelectric pyrometer indicates that the
temperature measuring error of the developed system is less than 1%. The melt pool characteristics including the
temperature distribution, profile, temperature gradient, and cooling rate were measured by the developed co­
axial temperature measurement system, and the distribution of average temperature and peak temperature under
different linear energy densities during single-line printing was also compared and analyzed. The single-line
printing results of different parameters show that the higher the linear energy density, the higher the average
temperature and peak temperature of the melt pool, and the optimized parameters minimize the fluctuation of
melt pool temperature and are more favorable to the formation of high-quality parts. In multi-layer printing
mode, the heat accumulation is strong, resulting in the slow cooling rate of the melt pool.

1. Introduction Nevertheless, the LPBF is an evolution process involving a variety of


physical fields and complex dynamics, including the melting, gasifica­
Laser Powder Bed Fusion (LPBF) is a common additive tion, and solidification of metal powder particles. In the process, macro
manufacturing (AM) process. In the LPBF, powder particles spread onto defects such as cracks, spheroidization, and warpage, as well as internal
a substrate, and are melted via interaction with a laser beam to manu­ metallurgical defects such as pores and inclusions may occur. Therefore,
facture a 3D part layer-by-layer using the data of a three-dimensional lack of quality assurance and performance control is the key techno­
(3D) model [1,2]. Owing to its ability to design new geometric shapes, logical barrier hindering the LPBF technology from being widely
manufacture complex parts, decrease pollutant emission, custom parts, employed. The implementation of in-situ monitoring and adaptive
and reduce cost, the LPBF is widely used in different industries such as feedback control appears to be a powerful strategy for understanding
medical, military, aerospace, construction, medical, and automotive defect formation [8–15].
[3–7]. The temperature measurement of melt pool characteristics is a

* Corresponding author.
E-mail address: liuzw@bit.edu.cn (Z. Liu).
1
Co-first authors.

https://doi.org/10.1016/j.applthermaleng.2022.118515
Received 18 November 2021; Received in revised form 9 March 2022; Accepted 10 April 2022
Available online 13 April 2022
1359-4311/© 2022 Elsevier Ltd. All rights reserved.
H. Ma et al. Applied Thermal Engineering 211 (2022) 118515

common approach to process monitoring, which helps to identify pro­ on the colorimetric thermometry principle.
cess instabilities, and provides insight into the qualities of parts. The The structure of the first type of measurement method is generally
research shows that the melt pool temperature is related to the defect not complicated. Krauss et al. [26] mounted the medium resolution
formation, microstructure of products, mechanical properties of prod­ infrared camera outside the building chamber enclosing an angle of 45◦
ucts, and printing parameters [8,16–22]. Khanzadeh et al. [8] proposed with the building platform to measure the spatial distribution charac­
a novel porosity prediction method based on the temperature distribu­ teristics and time-domain changes of the solidified layer temperature
tion of the melt pool in the directed energy deposition (DED) process, during the printing process. Zheng et al. [27] arranged an infrared
and results showed that the proposed method can predict the location of camera coaxially with the laser to monitor the temperature of the melt
porosity almost 96% of the time. Kriczky et al. [16] used a two- pool during the LPBF process. According to the gradient distribution
wavelength pyrometer to obtain the coaxial thermal image of the melt characteristics, the melt pool boundary was identified and extracted to
pool, and evaluated variations in build quality by extracting predict the width of the printing track. Lane et al. [28] adopted a high-
temperature-related features such as length-to-width ratio, temperature speed in-situ infrared camera with a maximum frame rate of 120 FPS
gradient, melt pool area, and peak temperature. Rezaeifar et al. [17] and a resolution of 1280 pixels × 1024 pixels to observe multiple phe­
controlled the temperature of the melt pool by controlling the laser nomena such as plasma plume and hot particle ejection in the melt re­
power, collected the temperature of the melt pool with a two- gion. Hua et al. [29] used a two-color infrared thermometer to measure
wavelength pyrometer, and studied the printed samples from both the temperature of the melt pool during the printing process and
microstructure and microhardness. The results showed that the tem­ investigated the influence of different parameters, such as powder feed
perature had a great impact on the uniformity of the microstructure and rate, scanning velocity of a laser beam, laser power, spot diameter,
mechanical properties of the final part. The researches of sun et al. [18] shielding gas flow rate and powder feeding position. However, in the AM
and song et al. [19] showed that the grain shape and size formed in the process, the powder particles are transformed from solid to liquid, and
printing process were determined by the temperature gradient G, the then cooled and solidified into a solid. In the whole process, the emis­
solidification rate R, and cooling rate. The temperature gradient de­ sivity of the melt pool will change [30], which makes it impossible to
termines the grain growth direction, the cooling rate determines the obtain an accurate melt pool temperature only by an infrared camera
grain size, and the ratio of a temperature gradient to solidification rate with a fixed emissivity.
G/R determines the grain morphology. With the decrease of the ratio G/ The principle of colorimetric thermometry is to establish a linear
R, the microstructure changes from plane crystals to cellular crystals, relationship between the radiation intensity ratio of two similar wave­
columnar crystals, and equiaxed crystals. With the increase of cooling lengths and the temperature of the object to be measured, so the
rate, the grains will become finer. However, the too fast cooling rate will colorimetric thermometry is not affected by the change of the surface
lead to greater brittleness or cracks. As the cooling rate increases, the emissivity of the object. Even in the area disturbed by soot, steam, and
crystal grains become finer, but a too fast cooling rate will cause larger particles, the ratio remains unchanged because the attenuation degree of
brittleness or cracks. Hojjatzadeh et al. [20] found that the movement the radiation energy of the two wavelengths is approximatively the
behavior of the pores in the melt pool is controlled by the competition same, therefore, high-temperature measurement accuracy can still be
between the melt flow resistance and the thermal capillary force caused obtained. In addition, the fast response speed and wide range make the
by the temperature gradient. A pore elimination method was proposed colorimetric thermometry have great development potential in the field
for the first time, that was, by adjusting the printing process parameters of melt pool temperature measurement. Furumoto et al. [31] built a
to obtain a higher temperature gradient in the melt pool, the resulting dual-wavelength colorimetric thermometry system based on the single-
thermal capillary force directionally drove and discharged the pores, to point measurement and integrated it into the LPBF equipment to mea­
obtain metal samples without pore defects. Lee et al. [21] used the near- sure the temperature of the melt pool during the printing process. The
infrared camera to observe the temperature change of each deposition temporal resolution can meet the measurement requirements, but the
layer during printing and identified the crack based on this criterion. It is spatial distribution of the melt pool temperature can’t be obtained.
summarized that crack defects appear and disappear periodically with Hooper et al. [32] proposed a coaxial imaging method through two high-
the scanning direction and position, and the crack is related to the speed cameras to obtain the melt pool surface temperature field at a high
scanning strategy and the geometry of the sample. Hermann et al. [22] frame rate (100000FPS) and high spatial resolution (20 µm). The
adopted the thermography technique to collect temperature images of colorimetric thermometry was used to measure the temperature field
the melt pool along the axis and established a neural network model distribution and cooling rate of the melt pool at different positions in the
with a detection accuracy of 96.80% for defects such as delamination process. However, the cost of two high-speed cameras is high, and their
and splashing. LI et al. [23] found that the average temperature of the synchronization is difficult to ensure.
powder bed gradually increased during the LPBF process, caused by the The focus of this paper is to highlight the proposed coaxial temper­
heat accumulation effect, and the microstructure of LPBF-produced ature measurement system based on a single high-speed camera and
parts was investigated. Liu et al. [24] discovered through the DED method. The coaxial temperature measurement system includes the
experimental results that the temperature of the melt pool was related to relay and optical path amplification system, the beam splitting and
its heat accumulation, and the profile of the melt pool was mainly chromatic aberration correction system, while the dual-waveband
affected by the overall heat accumulation. Wu et al. [25] analyzed that image-matching method with sub-pixel accuracy, and the overall
due to the influences of thermal accumulation, the layer’s surface parameter (K, λ1 and λ2 ) calibration and optimization method enhance
oxidation, microstructural evolution, grain size, and crystalline phase the accuracy of the system. Besides, the validation experiment proves
varied along the building direction of the as-fabricated wall, which the high accuracy of the system. The melt pool characteristics were
created variations in mechanical properties and fracture features. measured by the coaxial temperature measurement system, and the
Therefore, the melt pool temperature can be used as a significant temperature distribution, temperature gradient, cooling rate, and profile
parameter for defect detection and identification. of the melt pool under the different printing modes are obtained and
The non-contact temperature measurement method based on the discussed.
radiation temperature measurement principle is mostly used to detect
the melt pool temperature, which mainly includes two types. The first is
to measure the melt pool temperature based on the commercial high-
speed infrared camera or high-speed pyrometer, and then correct the
material emissivity; The second is to design the temperature measure­
ment optical path and build the temperature measurement system based

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H. Ma et al. Applied Thermal Engineering 211 (2022) 118515

2. Development, accuracy improvement and validation of 2.2. Development of coaxial temperature measurement system with a
coaxial temperature measurement system single camera

2.1. Principles of dual-wavelength thermometry 2.2.1. Overall design scheme of coaxial temperature measurement system
with a single camera
The dual-wavelength thermometry is a non-contact radiation The schematic of the coaxial temperature measurement system with
temperature measurement method that has been widely used in the field a single camera for high-speed temperature measurement of the melt
of infrared temperature measurement because of its special advantages pool in the LPBF process is shown in Fig. 1, including a 1000 nm long-
such as high-temperature measurement accuracy, strong anti- pass dichroic mirror, a relay and optical path amplification system, a
interference ability, fast response, and large temperature measurement beam splitting and chromatic aberration correction system, and a high-
range. In the LPBF process, facing the measurement problems such as speed camera.
high melt pool temperature (up to 4000 K in the printing process of In Fig. 1, the 1000 nm long-pass dichroic mirror is located between
titanium alloy), interference by smoke and powder particle splash, wide the laser and the dynamic focus module. When the LPBF device starts
melt pool temperature range, and extremely short melt pool formation printing, the laser first passes through the 1000 nm long-pass dichroic
and solidification time, the dual-wavelength thermometry can still mirror placed at 45◦ to the laser beam. The dichroic mirror has a high
measure the melt pool with high accuracy. For a melt pool, the damage threshold to the continuous laser. The 1000 nm long-pass
temperature can be calculated by the following formula [24]: dichroic mirror divides the initial waveband into a transmission band
( ) and a reflection band. The side of the dichroic mirror coated with the
dichroic film faces the dynamic focus module, and this side reflects the
hc 1
− λ12
(1)
k λ1
T=
lnK + ln GG21 + 5ln λλ21 waveband shorter than 1000 nm. The side of the dichroic mirror coated
with the antireflection coating faces the laser, and this side transmits the
where c represents the speed of light, h represents Planck constant, k waveband longer than 1000 nm. The laser with a wavelength of 1070
represents the Boltzmann constant, K represents proportional coefficient nm passes through the 1000 nm long-pass dichroic mirror and then is
obtained by system calibration experiment, λ1 and λ2 represent two expanded by the dynamic focus module. The expanded laser is reflected
different wavelengths respectively, and G1 and G2 represent the gray by the galvanometer into the focusing lens and finally focused on the
value of the captured image at the two different wavelengths respec­ printing plane. Immediately afterward, the powder bed on the printing
tively. When calculating the temperature field distribution of the melt plane is heated and melted to produce the melt pool. The infrared light
pool, the gray values of different pixels are not the same. If m × n rep­ radiated by the melt pool passes through the focusing lens, the galva­
resents the pixel size of the melt pool, the temperature field distribution nometer, and the dynamic focus module in a coaxial reflection manner.
formula can be expressed as The radiant light from the melt pool is shrunk by the dynamic focus
( ) module into a near-parallel light and then enters the 1000 nm long-pass
c2 λ11 − λ12 dichroic mirror through the side coated with the dichroic film. The
T(x, y) = (x,y)
(2) waveband of the radiant light shorter than 1000 nm is reflected upwards
G
lnK + ln 2(x,y) + 5ln λλ21 into the relay and optical path amplification system. After the radiant
G1
light is extended and amplified by the relay and optical path amplifi­
where x = 1, 2, ⋯, n; y = 1, 2, ⋯, n, c2 is the second radiation constant, cation system, it is reflected into the beam splitting and chromatic ab­
andc2 = hc/k. erration correction system. The beam splitting and chromatic aberration
correction system divides the radiant light into the transmission wave­
band and the reflection waveband on the target surface of the high-speed
camera, to obtain the image containing the left and right sub-images of
the melt pool under two different wavebands, which will provide the
basis for obtaining the temperature field of the melt pool.

Fig. 1. Schematic of coaxial temperature measurement system with a single camera for high-speed temperature measurement of melt pool in LPBF process.

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H. Ma et al. Applied Thermal Engineering 211 (2022) 118515

2.2.2. Design scheme of relay and optical path amplification system cameras and the beam splitter [24,32]. Although this design is rela­
The relay and optical path amplification system is located in the red tively simple and practical, it also has three obvious disadvantages.
box in Fig. 1, including relay lens 1, relay lens 2, adjusting lens barrel 1, Firstly, in this high-speed temperature measurement optical path, two
adjusting lens barrel 2, planar mirror 1. The relay lens 1 is the achro­ high-speed cameras are necessary, which significantly increases the cost
matic double glued lens pair, and one focal length of the two lenses is of the experiment. Secondly, the beam splitter equally divides the
100 mm and the other is 30 mm. Similarly, the relay lens 2 also consists radiant light into two identical beams, which must reduce the intensity
of a pair of lenses a pair of lens, and the focal length of them is 100 mm. of the melt pool radiant light, and may reduce the acquisition frame rate
On the LPBF equipment, the 1000 nm long-pass dichroic mirror can be of the high-speed camera. Thirdly, the two cameras need to be fully
placed on the experimental platform of the beam splitting and chromatic synchronized when acquiring images at high speed. Otherwise, the ac­
aberration correction system and the high-speed camera. The experi­ quired images are difficult to be accurately matched in time, which will
mental platform often has a long distance in the vertical direction, so to affect the accuracy of temperature measurement. To solve the above
ensure the flexibility of the placement and adjustment of the beam problems, a dual-channel beam splitting and chromatic aberration
splitting and chromatic aberration correction system and the high-speed correction system based on a single high-speed camera are designed, as
camera, it is necessary to extend the radiant light from the melt pool by shown in Fig. 3, where the relay and optical path amplification system is
adjusting the length of the relay lens 1. Since the diameter of the melt simplified to a convex lens. The optical components in the beam splitting
pool in the LPBF process is only 300–500 µm, the resolution of the high- and chromatic aberration correction system include 805 nm long-pass
speed camera is only 1024 pixels × 1024 pixels, and the size of a single dichroic mirror, 805 nm short-pass dichroic mirror, narrow-band filter
pixel on the target surface is 20 µm × 20 µm, a certain enlargement of 1 and narrow-band filter 2, chromatic aberration correction lens 1,
the melt pool is required. It is possible to obtain a melt pool image with chromatic aberration correction lens 2, right-angle optical adjustment
more pixels during high-speed acquisition, which requires the relay and frame 1, right-angle optical adjustment frame 2, planar mirror 2, planar
optical path amplification system to have an amplification function. The mirror 3, and non-rotating movable lens tube. Both the narrow-band
principle schematic of the relay and optical path amplification system is filter 1 and narrow-band filter 2 are 1 in. in diameter and 10 in. in full
shown in Fig. 2. The light emitted from points at different positions is width at half maximum. Both the 805 nm long-pass dichroic mirror and
magnified by 3.3 times through the relay lens, because the focal length the 805 nm short-pass dichroic mirror are 1 in. in diameter. The planar
of the relay lens 1–1 is 30 mm and the focal length of the relay lens 1–2 is mirror 1, planar mirror 2 and planar mirror 3 are all 1 in. in diameter.
100 mm. The magnification is equal to the ratio of the image distance to Both the chromatic aberration correction lens 1 and the chromatic ab­
the object distance, so by adjusting the distance between the light erration correction lens 2 are coated with the antireflection coating of
starting point and the lens, the magnification of the relay lens will also 650–1050 nm with a diameter of 1 in., and their focal length is 400 mm.
change. In the experiment, under the joint action of relay lens 1 and In the beam splitting and chromatic aberration correction system,
relay lens 2, the diameter of the melt pool image on the target surface of the center wavelength of narrow-band filter 1 is (780 ± 2) nm, the
the high-speed camera is about 800 µm. Assuming the true diameter of center wavelength of narrow-band filter 2 is (905 ± 2) nm. The 805 nm
the melt pool is 400 µm, the melt pool image can be magnified twice, and long-pass dichroic mirror can almost completely reflect the light con­
the distance between the high-speed camera and the relay lens 2 is about taining the waveband of narrow-band filter 1 in the beam splitting and
500 mm. Both relay lens 1 and relay lens 2 are coated with 650–1050 nm chromatic aberration correction system, while almost completely
antireflection coating to minimize the attenuation effect of the relay and transmitting the light containing the waveband of narrow-band filter 2.
optical path amplification system on the radiation intensity of the melt The side of the 805 nm long-pass dichroic mirror coated with a dichroic
pool. In addition, relay lens 1 and relay lens 2 have achromatic ability. film divides the light received from the relay and optical path amplifi­
Because there are many lenses between the melt pool and the high-speed cation system into a reflected beam with a waveband less than 805 nm
camera, the distance between the two is relatively long, which may and a transmitted beam with a waveband greater than 805 nm. The
cause strong chromatic aberration. In order to improve the accuracy of reflected beam passes through the narrow-band filter 1 and the planar
the captured melt pool images, it is necessary to use achromatic lenses. It mirror 2 and enters the camera target surface after transmitting by the
is worth noting that the achromatic lens has the effect of reducing 805 nm short-pass dichroic mirror. The transmitted beam passes
chromatic aberration, but it cannot completely eliminate chromatic through the narrow-band filter 2 and the planar mirror 3 and enters the
aberration. camera target surface after reflecting by the 805 nm short-pass dichroic
mirror. The surface of the 805 nm short-pass dichromatic mirror is
2.2.3. Design scheme of beam splitting and chromatic aberration correction coated with dichromatic film towards the high-speed camera.
system In the coaxial temperature measurement system developed based on
In general, two cameras are required to acquire two waveband im­ the principle dual-wavelength thermometry, the radiant light of the melt
ages of a tested object simultaneously. The optical path is typically pool pass through multiple lenses with different refractive indexes from
designed to split the radiant light into two beams using a beam splitter. the melt pool to the high-speed camera, so it is inevitable that a certain
The two beams are captured by two high-speed cameras through amount of chromatic aberration is generated, and the image of the dual-
different narrow-band filters, to obtain the images of the two wave­ waveband radiant light cannot be focused on the target surface of the
bands, and the chromatic aberration caused by different wavebands can high-speed camera at the same time. Therefore, it is necessary to correct
be eliminated by adjusting the distance between the two high-speed the dual-waveband chromatic aberration. The chromatic aberration

Fig. 2. Principle schematic of relay and optical path amplification system.

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H. Ma et al. Applied Thermal Engineering 211 (2022) 118515

Fig. 3. Schematic of beam splitting and chromatic aberration correction system with a single camera.

correction lens 1 and chromatic aberration correction lens 2 in the beam beam splitting and chromatic aberration correction system is
splitting and chromatic aberration correction system correct the dual- 90◦ 。
waveband chromatic aberration. After ignoring the reflection and (2). The dual-wavelength light is reflected by the dichroic mirror and
transmission, the simplified dual-waveband optical path chromatic ab­ the planar mirror, so the left and right sub-images of the object
erration correction schematic is shown in Fig. 4. Both the chromatic are in a translational relationship.
aberration correction lens 1 and the chromatic aberration correction (3). When measuring temperature on the LPBF equipment, there is no
lens 2 are achromatic double cemented convex lenses with a focal length need to add a light barrier between the two beams of light emitted
of 400 mm. The position of the chromatic aberration correction lens 2 from the beam splitting and chromatic aberration correction
remains unchanged, while the position of the chromatic aberration system, because the right-angle optical adjustment frame 1 and
correction lens 1 installed in the non-rotating movable lens tube can be the right-angle optical adjustment frame 2 can adjust the imaging
moved. The maximum movement range of the non-rotating movable position of the melt pool on the target surface of the high-speed
lens tube is 5 mm, and the range of movement per rotation is 0.25 mm, camera, as long as the left and right sub-images do not overlap,
so the left and right sub-images are all focused on the target surface of there is no interference between the two beams.
the high-speed camera by fine-tuning the chromatic aberration correc­
tion lens 1. The results before and after the chromatic aberration 2.2.4. Assembly of coaxial temperature measurement system
correction are shown in Fig. 5. The key to assembling the coaxial temperature measurement system
The supplementary explanation of the beam splitting and chromatic is to assemble the beam splitting and chromatic aberration correction
aberration correction system shown in Fig. 3 is as follows: system first. To assemble all the components in the beam splitting and
chromatic aberration correction system, the 3D model of the device is
(1). The positions of the 805 nm long-pass dichroic mirror and the designed in Creo software. After printing the 3D model with PLA wire,
805 nm short-pass dichroic mirror can be interchanged, and then the developed beam splitting and chromatic aberration correction sys­
the side coated with the dichroic film is adjusted. In addition, two tem with a size of 150 mm × 116 mm × 66 mm is shown in Fig. 6. The
identical 805 nm long-pass dichroic mirrors or 805 nm short-pass narrow-band filter 1 and the narrow-band filter 2 are installed in a one-
dichroic mirror can also be used for beam splitting, and the angle inch diameter lens barrel, and the lens barrel is fixed on a right-angle
between the light entering and exiting the beam splitting and the optical adjustment frame through a threaded connection. The chro­
matic aberration correction lens 1 and the chromatic aberration

Fig. 4. Schematic of dual-waveband optical path chromatic aberration correction.

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H. Ma et al. Applied Thermal Engineering 211 (2022) 118515

system is divided into upper and lower parts, and is compact and
convenient to adjust.
The developed coaxial temperature measurement system is shown in
Fig. 7, which mainly includes the beam splitting and chromatic aber­
ration correction system, the relay and optical path amplification sys­
tem, the high-speed camera, and a replaceable telephoto microscope
lens (or a lens barrel).

2.3. Dual-waveband image-matching method with sub-pixel accuracy

The image collected by the high-speed camera can be divided into


left and right sub-images. According to the temperature calculation
formula (1), the temperature of a region can be obtained only by
calculating the temperature of each pixel unit in the region. Only by
obtaining the gray value of the pixel point corresponding to a point in
the dual-waveband image can the temperature of the point be calcu­
lated. This means that before using the dual-wavelength thermometry
principle to calculate the temperature field, it is necessary to match the
two sub-images, and the accuracy of the dual-waveband image matching
directly affects the accuracy of the temperature calculation. Therefore, a
dual-waveband image-matching method with sub-pixel accuracy based
on speckle correlation is developed herein.
The speckle calibration plate is filled with easy-to-identify black and
white speckles, and the positional correspondence between the two sub-
images of the speckle calibration plate at the same position as the object
Fig. 5. Dual-waveband image before and after chromatic aberration correction. to be measured is calculated, and the positional correspondence be­
tween the two sub-images of the object can be obtained. This image
correction lens 2 are respectively installed in a non-rotating movable position calibration method is equivalent to using a speckle calibration
lens tube and a one-inch diameter lens barrel and are also fixed on a plate to indirectly provide a large number of position reference points
right-angle optical adjustment frame through a threaded connection. for the surface of the object, paving the way for the subsequent accurate
The model of the beam splitting and chromatic aberration correction matching of dual-waveband image. To ensure the validity of the cali­
bration, after the image position calibration is completed, the positions

Fig. 6. Developed beam splitting and chromatic aberration correction system.

Fig. 7. Developed coaxial temperature measurement system with a single high-speed camera.

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of the relay and optical path amplification system, spectroscopic and



M
chromatic aberration correction system, high-speed camera, and other Cf ,g (→
p )=
equipment will not change. x=− M
The specific process of the dual-waveband image-matching method ∑
M
f (x, y) − fm

g(x ,y ) − gm

with sub-pixel accuracy as shown in Fig. 8 is as follows: × [√̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅ − √̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅ ]2


y=− M ∑M ∑M ∑M ∑M
[f (x,y) − fm ]2 [g(x′ ,y′ ) − gm ]2
(1). After setting up the coaxial temperature measurement system on x=− M y=− M x=− M y=− M

the LPBF equipment, put the speckle calibration plate close to the (3)
surface of the object to be measured, focus on the high-speed
camera and adjust the appropriate exposure time, and use the where, f(x, y) is the gray level of the coordinates of point (x, y)
xenon lamp to fill the light to collect a dual-waveband image as in Fig. 8 (b), g(x , y ) is the gray level of the corresponding point (x , y )
′ ′ ′ ′

∑ M ∑ M 2
shown in Fig. 8 (a). in Fig. 8 (c),fm = 1
(2M+1)2 x=− M y=− M [f(x, y)] ,gm =
(2). Cover the left and right sides of the image with white and save 1
∑ M ∑ M 2
y=− M [g(x , y )] , fm and gm are the average gray levels of
′ ′
x=− M
them as Fig. 8 (b) and Fig. 8 (c). (2M+1)2

(3). Divide Fig. 8 (b) into n (n is a positive integer) sub-areas evenly, two image sub-area, respectively, and → p is the vector of the deformation
and then find the corresponding sub-area of each sub-area of parameters to be determined.
Fig. 8 (b) in Fig. 8 (c) according to the correlation function for­ In the image-matching process, multiple image interpolation algo­
mula (3). Calculate the correlation coefficients Cf ,g (→
p ) between rithms including Newton-Rapson algorithm, genetic algorithm, neural
the sub-areas of Fig. 8 (b) and Fig. 8 (c). The sub-area of Fig. 8 (c) network algorithm, sub-pixel grayscale interpolation method [33] are
with the smallest correlation coefficient corresponds to the sub- used in the digital image correlation (DIC), which can increase the
area of Fig. 8 (b). The correlation function formula is as follows: matching accuracy to 0.005 to 0.1 pixels, and the sub-pixel accuracy
matching of the dual-waveband image can also be realized.

Fig. 8. Specific process of dual-waveband image-matching method, (a) Dual-waveband image of speckle calibration plate, (b) Left sub-area, (c) Right sub-area, (d)
Relative displacement field in × direction, (e) Relative displacement field in y direction.

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The relative displacement field of Fig. 8 (b) and Fig. 8 (c) is shown in The specific process of the overall parameters calibration and opti­
Fig. 8 (d) and Fig. 8 (e), where Fig. 8 (d) is the relative displacement field mization method is as follows:
in the x direction, and Fig. 8 (e) is the relative displacement field in the y
direction. Although the left and right images are in a translational (1). Dual-waveband image matching: Fig. 9 shows the temperature
relationship in theory, the displacements of different pixels are not the measurement system in the calibration stage. The speckle cali­
same in practice. The errors caused by the rotation and chromatic ab­ bration plate and the black body furnace are set on the same
erration of the left and right sub-images can be eliminated by matching vertical plane, and the left and right sub-images are matched
the left and right images. through the speckle image.
(2). Heating black body furnace: Determine the temperature range
that needs to be calibrated, and select multiple temperatures in
2.4. Calibration and optimization method of overall parameters
this range as a reference. Every time the temperature of the
blackbody furnace reaches the reference value, the high-speed
The proportional coefficient K in formula (1) is mainly affected by
camera collects a dual-waveband image, while the temperature
the spectral response intensity of the high-speed camera, the trans­
of the standard photoelectric thermometer is recorded. Fig. 10 is
mittance and reflectivity of the optical components, the assembly of the
a dual-waveband image, in which the area-λ1 and area-λ2 are all
optical components, the spectral absorptivity of the atmosphere and the
divided into the furnace bottom area and the furnace wall area.
environment, so the value or distribution of the proportional coefficient
During the calibration process, only the furnace bottom area is
needs to be calibrated through experiments. Besides, in the principle of
calibrated, so the furnace wall area does not affect the calibration
dual-wavelength thermometry, the relationship between the gray ratio
accuracy.
of the two wavelengths and the temperature needs to be calibrated.
(3). Multi-parameter fitting calibration: The formula (1) is isomor­
However, it is difficult to find a filter that can only pass a single wave­
phically deformed into
length, and it will not only reduce the signal strength of high-speed ( )
cameras but also may bring greater noise effects, so the wavelength hc 1 1
λ1 − λ2
range of the filter should be selected reasonably. In addition, the center
k
exp G(x,y)
(4)
T(x,y) 2
=K
wavelength of the filter is often not a certain value, but a range value. (
λ2
)5
G(x,y)
Hence, when calculating the temperature, the specific values of λ1 and λ2
1
λ1

need to be reasonably selected within the center wavelength range of the


filter, otherwise it may cause larger measurement errors. Therefore, an Suppose
overall parameters calibration method is proposed, and combined with hc
(
1 1
)
the system parameter optimization method, the distribution of the three exp
k λ1 − λ2

parameters K, λ1 and λ2 can be obtained, which improves the tempera­ (5)


T(x,y)
(x, y) = ( )5
ture measurement accuracy.
λ2
λ1
A high-temperature blackbody furnace and a standard photoelectric
pyrometer are used in the calibration experiment of the overall pa­ G(x,y)
rameters. The emissivity of the high-temperature blackbody furnace is x(x, y) = 2
(x,y)
(6)
G1
greater than 0.99, and the temperature measurement error is about
0.1℃. The temperature measurement accuracy of the standard photo­ Then y = Kx. For a single pixel, set the initial values λ1 and λ2 to 780 nm
electric pyrometer can reach 0.1℃. Both the high-temperature black­ and 905 nm, respectively, calculate the yi and xi corresponding to all
body furnace and the standard photoelectric pyrometer have high temperature points (i is the number of reference temperature), and use
accuracy and meet the needs of calibration. Therefore, the developed the least square method [34] to fit yi and xi into the form of y = Kx. The
coaxial temperature measurement system for high-speed temperature linear correlation coefficient isr (0 < r⩽1), and then the Newton’s
measurement is calibrated with the value of the center point of the black method [35,36] is used to iteratively update the values of λ1 and λ2
body furnace bottom measured by the standard photoelectric pyrometer within the center wavelength range. The least square method has the
as the standard.

Fig. 9. Calibration scene of development coaxial temperature measurement system.

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Fig. 10. Dual-waveband image.

characteristic of excellent parameter estimation, and the Newton’s order to more intuitively display the statistical data of the actual cali­
method has the characteristic of fast convergence. Therefore, the New­ bration results of each pixel, the coefficient of determination of each
ton’s method based on the least square method has good convergence pixel after linear fitting is calculated, as shown in Fig. 12 (b). The value
performance, and its positioning accuracy is obviously better than the range of the coefficient of determination is between 0 and 1. The closer it
least square method. Given the criterion α and criterionβ (0 < β < 1), is to 1, the better the linear fitting. The range of the coefficient of
only when b⩽α andr⩽β , the iteration stops, and the corresponding K, λ1 determination is 0.9752–0.9975, which proves the accuracy of fitting
and λ2 are the optimal values of the fitting. The K, λ1 and λ2 of all the results and the accuracy of iterative results of parameters K, λ1 andλ2 .
remaining pixels are obtained by the same method. The result of the
overall parameter calibration is shown in Fig. 11, where K gradually
increases from left to right, and the average value of K is about 4.05. It is 2.5. Validation experiment
worth noting that the gray value at the bottom of the furnace in Fig. 10
should be the same under ideal conditions, but because the trans­ After calibrating and optimizing the distribution of the overall
mittance and reflectivity of the light with different wavelengths and parameter, a validation experiment is carried out at the National In­
different direction passing through the optical components are different, stitute of Metrology of China. Comparing the temperature measurement
the gray values of λ1 and λ2 in the furnace bottom area also present a results of the developed coaxial temperature measurement system with
regular distribution. The closer to the image center line, the more slowly the standard photoelectric pyrometer, the error is less than 1%. The
the gray values of area-λ1 and area-λ2 increase. Therefore, the calculated third-party certificate issued by the National Institute of Metrology of
K also present a regular distribution. In addition, the physical meaning China is shown in the appendix.
of λ1 and λ2 is the optimal wavelength value, which is determined by all The measurement results of the validation experiment are shown in
optical components, and does not represent the distribution of the center Fig. 13. The standard temperature is measured by the standard photo­
wavelength of the filter. electric pyrometer, and the measurement temperature is measured by
The fitted straight line y = K x +b of a pixel is shown in Fig. 12 (a), the developed coaxial temperature measurement system. Although only
where K = 4.05,b < 10− 6 , λ1 = 780.38 nm, λ2 = 904.89 nm, indicating some temperatures between 1000 ℃ and 1200 ℃ have been verified,
that the fitted straight line has a good linear correlation coefficient. In according to formula (4), the accuracy of dual-wavelength thermometry
is mainly related to the proportional coefficient K. According to the

Fig. 11. Calibration result of (a) Proportional coefficient K, (b) Parameterλ1 , (c) Parameterλ2 .

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Fig. 12. Fitting straight line of a pixel’ K value (a) and coefficient of determination of each pixel after linear fitting (b).

Fig. 13. Measurement results of validation experiment.

influencing factors of the proportional coefficient K, it can be seen that follows: the model is HK M125, the laser center wavelength is 1070 nm,
within the range of 1000 K to 5000 K, reasonably adjust the camera the maximum molded part size is 125 mm × 125 mm × 125 mm, the
exposure time so that the brightness of the melt pool is as high as distance between the molding plane and the focusing lens is 500 mm, the
possible but not more than 4095, and the measurement accuracy will not scanning galvanometer system is Hurry Scan, and the control system is
be reduced. Therefore, the accuracy of the developed coaxial tempera­ the independently developed HUST 3DP software. The material used in
ture measurement system using a single camera for high-speed tem­ the experiment is 316L stainless steel metal powder with a melting point
perature measurement meets the requirements of online measurement of 1371–1398 ℃. As shown in Fig. 14, the integrated melt pool tem­
of the melt pool temperature field. perature measurement equipment mainly includes an experimental
platform, the relay and optical path amplification system, the beam
3. Experimental results and analysis splitting and chromatic aberration correction system, the high-speed
camera, and a computer with a gigabit network port.
3.1. Integration of coaxial temperature measurement system and LPBF The relay and optical path amplification system and the beam
equipment splitting and chromatic aberration correction system have been intro­
duced in section 2.2. The model of the high-speed camera is FASTCAM
To realize the online in-situ measurement of the melt pool temper­ NOVA S12, which achieves a 12,800 FPS acquisition speed at full res­
ature, the coaxial temperature measurement system is integrated into olution, provides a 12-bit gray depth range, has a memory of 64 GB, has
the LPBF equipment consisting of a laser, a workbench, and a powder an image resolution of 1024 pixels × 1024 pixels, uses a square chip
feeding device. The main parameters of the LPBF equipment are as with a single-pixel size of 20 × 20 µm, and has a monochrome sensitivity

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3.2. Measurement and analysis of melt pool characteristics

As shown in Fig. 15, this experiment designed three different print­


ing modes: single-line printing, single-layer printing, and multi-layer
printing. The single-line printing refers to the process in which the
laser prints only once along with a line on the powder bed surface; the
single-layer printing refers to the process of spreading powder once and
continuously printing on this layer; the multi-layer printing refers to the
process of multiple single-layer printing by continuous spreading pow­
der. Analyzing the temperature distribution changes of the melt pool
under these three printing modes is beneficial to provide a basis for
optimizing process parameters and improving printing quality.

3.2.1. Single-line printing process results and analysis


The single-line printing is the basic unit in the continuous printing
process, and measuring the temperature distribution of the melt pool in
the single-line printing process is significant for understanding the entire
printing process.
In this experiment, a variety of different process parameters are
designed for single-line printing. Since the melting point of 316L
stainless steel is in the range of 1371–1398 ℃, the area with a tem­
perature higher than 1672 K in the temperature field is regarded as the
melt pool. Fig. 15(a) is the single-line printing result, each single-line
length is about 22 mm, and the scanning direction is from left to right.
Table 1 shows the parameters of different single-line printing.
Fig. 16 and Fig. 17 respectively show the evolution process of the
melt pool temperature field distribution and the melt pool profile dis­
tribution over time, and the evolution of the average temperature, peak
temperature, and profile area of the melt pool overtime when the laser
Fig. 14. Developed melt pool temperature measurement equipment. power is 320 W, the scanning speed is 650 mm/s, and the high-speed
camera’s acquisition frame rate is 3000FPS. It is worth noting that the
of ISO64000. profile of melt pool is calculated by temperature gradient. After the melt
It should be noted that the difference between the coaxial tempera­ pool temperature field is obtained, combined with the scanning speed,
ture measurement system in the experiment and the overall parameters the preset printing path and the acquisition frame rate of the camera, the
calibration process is that a telephoto microscope lens is added to the three-dimensional position coordinates of the melt pool can be obtained.
optical path during the overall parameters calibration process. In addi­ The parameters of NO.1 single-line printing is one of the best printing
tion, the radiant light of the melt pool in the experiment pass through parameters for printing stainless steel, and the best printing parameters
the lens (focusing lens, beam expander in the dynamic focus module) on are often related to the printing material and the printing shape. The
the LPBF equipment, and the radiant light of the black body furnace evolution process of the melt pool can be divided into three stages:
during the calibration process directly enter the 1000 nm long-pass formation stage (0 ms to 0.33 ms), stabilization stage (0.33 ms to 35 ms),
dichroic mirror. Since in the dual-wavelength thermometry, the tem­ and cooling stage (35 ms to 35.33 ms).
perature is only related to the gray ratio of the dual-waveband, the light
intensity of the dual-waveband is also synchronized after passing
through the lens. Therefore, the accuracy of temperature calibration is
still valid.
Table 1
In the LPBF process, the main factors that affect the quality of the
Parameters of different single-line printing.
printed part are the laser power, scanning speed, scanning strategy,
NO. Laser power Scanning speed Linear energy density
hatch spacing, powder layer thickness. In this experiment, the thickness
of the powder layer is 50 μm, the hatch spacing is 120 μm, the scanning 1 320 W 650 mm/s 492.3 J/m
strategy is raster scanning, and the scanning direction is unidirectional 2 320 W 300 mm/s 1066.7 J/m
3 240 W 300 mm/s 800.0 J/m
scanning.

Fig.15. Printing modes of (a) Single-line printing, (b) Single-layer printing, (c) Multi-layer printing.

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Fig. 16. Evolution of (a) temperature field and (b) profile of melt pool with time in the process of NO.1 single-line printing.

Fig. 17. Evolution of average temperature, peak temperature, and profile area of melt pool with time in the process of NO.1 single-line printing.

(1). Formation stage. The time of the first melt pool dual-waveband thickness of the spreading powder at the end of the single line is
image captured by the camera is considered as t = 0 ms. Due to slightly larger than that at the beginning, and the temperature is
the limitation of the acquisition frame rate, only one temperature easier to transfer downward. The average temperature of the melt
field in the process of melt pool formation can be obtained at the pool varies steadily between 2000 K and 2150 K, and its
formation stage. The tail profile of the melt pool has not been maximum temperature changing rate is 610 K/ms. The peak
formed at 0 ms, and the laser spot is located at x = 0.73 mm. temperature of the melt pool varies between 2800 and 3090 K,
According to the scanning distance of laser spot in 0.33 ms is and its maximum temperature changing rate is 1790 K/ms. The
214.5 µm, it can be inferred that the initial position of the laser peak temperature of the melt pool fluctuates more violently than
spot is between x = 0.51 mm and x = 0.73 mm. With the rapid the average temperature, which indicates that the peak temper­
increase of the temperature and area of the melt pool, the width ature of the molten pool is more easily affected by other factors.
of the melt pool reaches 400 µm, the average temperature (3). Cooling stage. The corresponding temperature field of the melt
changing rate reaches 5315 K/ms, and the peak temperature pool is not obtained at the cooling stage, which is mainly caused
changing rate reaches 7758 K/ms. by two reasons. On the one hand, the high-speed camera’s
(2). Stabilization stage. The peak temperature, average temperature, acquisition frame rate in this experiment is low, and only one
and area of the melt pool vary reposefully at the stabilization image is collected every 0.33 ms. On the other hand, after the
stage. The peak temperature and average temperature of the melt single-line printing, the laser spot will be instantly turned off and
pool generally show a slow rising trend, and the average rising quickly return to the origin, and the substrate lacks heat accu­
rate is 7.6 K/ms and 3.3 K/ms, respectively. The area of the melt mulation during single-line printing [23,24], which will lead to
pool generally shows a slow downward trend. At the end of an excessively fast cooling rate of the melt pool temperature.
printing, the area of the melt pool is slightly reduced, because the

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Fig. 18. Evolution of temperature field of melt pool with time in the process of NO.2 single-line printing.

Fig. 19. Evolution of average temperature, peak temperature, and profile area of melt pool with time in the process of NO.2 single-line printing.

Fig. 18 and Fig. 19 respectively show the evolution process of the The time of the first melt pool dual-waveband image captured by the
melt pool temperature field distribution over time and the evolution of camera is considered as t = 0 ms. The evolution process of the melt pool
the average temperature, peak temperature, and profile area of the melt can also be divided into three stages: formation stage (0 ms to 0.25 ms),
pool overtime when the laser power is 320 W, the scanning speed is 300 stabilization stage (0.25 ms to 67.25 ms), and cooling stage. With the
mm/s, and the high-speed camera’s acquisition frame rate is 4000FPS. rapid increase of the temperature and area of the melt pool at the

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formation stage, the width of the melt pool reaches 400 µm, the average 67.33 ms). With the rapid increase of the temperature and area of the
temperature reaches 2091 K, the peak temperature reaches 2679 K, the melt pool, the width of the melt pool at the formation stage reaches 400
average temperature changing rate reaches 7164 K/ms, and the peak µm, the average temperature changing rate reaches 5194 K/ms, and the
temperature changing rate reaches 9516 K/ms. The average tempera­ peak temperature changing rate reaches 7221 K/ms. The average tem­
ture of the melt pool at the stabilization stage varies between 2100 K and perature of the melt pool varies between 2000 K and 2200 K, and its
2400 K, and its maximum temperature changing rate is 1200 K/ms. The maximum temperature changing rate is 782 K/ms. The peak tempera­
peak temperature of the melt pool at the stabilization stage varies be­ ture of the melt pool at the stabilization stage varies between 2600 K and
tween 2500 K and 3300 K, and its maximum temperature changing rate 3200 K, and its maximum temperature changing rate is 2273 K/ms.
is 4400 K/ms. As shown in Fig. 18, it is not that the edge solidifies first During the cooling stage, the size of the melt pool decreases rapidly, and
and the area where the high-temperature center is located solidifies the profile is only half of that in the stabilization state.
later, which is slightly different from the cooling rule in Fig. 16. Through The linear energy density in Table 1 is a parameter that measures the
analysis and inference, this phenomenon is related to the violent heat comprehensive influence of the laser power and scanning speed on the
exchange inside the melt pool. As in the cooling stage of NO.1 single-line printed parts. Assuming that the linear energy density is represented
printing, no temperature field of the melt pool at the cooling stage is byL, L it can be expressed as.
captured.
P
Fig. 20, and Fig. 21 respectively show the evolution process of the L= (7)
v
melt pool temperature field distribution over time and the evolution of
the average temperature, peak temperature, and profile area of the melt where p is the laser power, and v is the scanning speed.
pool overtime when the laser power is 240 W, the scanning speed is 300 In the LPBF process, the main factors that affect the quality of the
mm/s, and the high-speed camera’s acquisition frame rate is 3000FPS. printed part are the laser power, scanning speed, scanning strategy,
The time of the first melt pool dual-waveband image captured by the hatch spacing, powder layer thickness. However, in the single-line
camera is considered as t = 0 ms. The evolution process of the melt pool printing process, the scanning strategy and the hatch spacing don’t
can still be divided into three stages: formation stage (0 ms to 0.33 ms), need to be considered, and the powder layer thickness is a fixed value.
stabilization stage (0.33 ms to 66.66 ms), and cooling stage (66.66 ms to Therefore, the linear energy density can be used to measure the heat

Fig. 20. Evolution of temperature field of melt pool with time in the process of NO.3 single-line printing.

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Fig. 21. Evolution of average temperature, peak temperature, and profile area of melt pool with time in the process of NO.3 single-line printing.

Fig. 22. Evolution of the average temperature of the melt pool with time under different linear energy densities.

input rate of the laser energy in the single-line printing process. energy input per unit time of the melt pool, and the higher the average
In the single-line printing process, the evolution of the average temperature. The fluctuation is the smallest when the linear energy
temperature of the melt pool with time under different linear energy density is 492.3 J/m, and its printing parameters is one of the best
densities is shown in Fig. 22. In terms of the distribution range of tem­ printing parameters of stainless steel. Inappropriate printing parameters
perature, when the linear energy density is 492.3 J/m, the average will bring about the fluctuation of melt pool temperature field, which
temperature is mainly distributed between 2000 K and 2150 K; when the may cause the formation of undesirable microstructure and even the
linear energy density is 800 J/m, the average temperature is mainly emergence of defects [17–19,37–38].
distributed between 2000 K and 2200 K; when the linear energy density The evolution of the peak temperature of the melt pool with time
is 1066.7 J/m, the average temperature is mainly distributed between under different linear energy densities is shown in Fig. 23. In terms of
2100 K and 2400 K. The higher the linear energy density, the more the distribution range of temperature, when the linear energy density is

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H. Ma et al. Applied Thermal Engineering 211 (2022) 118515

Fig. 23. Evolution of peak temperature of the melt pool with time under different linear energy densities.

492.3 J/m, the peak temperature is mainly distributed between 2800 K When the laser is concentrated on the measuring point, the surface
and 3090 K; when the linear energy density is 800 J/m, the peak tem­ temperature of the melt pool exceeds the normal boiling point temper­
perature is mainly distributed between 2600 K and 3200 K; when the ature of the material, and the higher the linear energy density, the more
linear energy density is 1066.7 J/m, the peak temperature is mainly peak temperatures exceed the boiling point (3090 K) of stainless steel.
distributed between 2500 K and 3300 K. Similar to the evolution of Semak et al. [39,40] and Ki et al. [41,42] showed that the temperature of
average temperature, the higher the linear energy density, the higher the the melt surface would not be limited to the normal boiling point of the
peak temperature, and the fluctuation is the smallest when the linear material due to the backwash pressure of the melt surface. Semak et al.
energy density is 492.3 J/m. [40] predicted that the peak temperature of iron was 4000 K, far higher

Fig. 24. Evolution of temperature field of melt pool with time in the process of single-layer printing.

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H. Ma et al. Applied Thermal Engineering 211 (2022) 118515

than the normal boiling point (3134 K). Ki et al. [42] predicted that FPS. A total of 140 layers are printed in this process, and a single line in
when the recoil pressure was 200–600 kpa, the laser welding tempera­ the middle of the 120th layer is selected for calculation and analysis.
ture of the steel plate was 500–900 K higher than the normal boiling Fig. 25 shows the evolution of the melt pool temperature field from
point. In this study, when linear energy density was 1066.7 J/m, the the formation stage (0 ms to 0.4 ms) to the stabilization stage (0.4 ms to
temperature was about 400 K above the boiling point at 24 ms. In this 3 ms) in the multi-layer printing process. The time of the first melt pool
study, when linear energy density is 1066.7 J /m, the temperature is dual-waveband image captured by the camera is considered as t = 0 ms.
about 400 K above the boiling point at 24 ms, which is consistent with The profile of the melt pool at the formation stage is approximatively
the experimental research in the above literature. stable, and the temperature of the melt pool rises steadily. There is al­
ways an area higher than 3090 K in the high-temperature center of the
3.2.2. Single-layer printing process results and analysis melt pool during the stabilization stage, which is caused by the recoil
Fig. 15 (b) shows the single-layer printed part with a size of 20 mm × pressure. Laser selective melting is a process that includes complex
20 mm when the laser power is 320 W, the scanning speed is 650 mm/s, physical and chemical phenomena such as heat transfer, mass transfer,
and the high-speed camera’s acquisition frame rate is 5000 FPS. As convection, radiation, evaporation, melting, and solidification. The
shown in Fig. 15 (b), the raster scanning strategy is inclined upward, and printing process is accompanied by very light vibrations due to water
only the first two single lines are calculated and analyzed. cooling, and the printing power is not in an ideal stable state, so the
In the single-layer printing process, the evolution process of the high-temperature center is also in constant change. The melt pool in the
temperature field distribution of the first two single-line melt pools over stable stage has a long tail, and the overall temperature is higher than
time is shown in Fig. 24. The time of the first melt pool dual-waveband the temperature field distribution of the NO.1 single-line printing under
image captured by the camera is considered as t = 0 ms.The printing the same parameters. The reason for the above phenomenon is that the
time of the first single line is about 1.2 ms, and the volution process of strong heat accumulation in the last stage of multi-layer printing leads to
the melt pool can be divided into three stages: formation stage (0 ms to a higher temperature in the high-temperature center, a slower cooling
0.6 ms), stabilization stage (0.6 ms to 1 ms), and cooling stage (1 ms to rate of the melt pool, and an excellent formation of the solidification
1.2 ms). The peak temperature of the melt pool exceeded 3090 K during structure.
the stabilization stage. After the laser spot prints the first single line, it
returns to the initial position of the second single line and starts printing. 3.2.4. Temperature gradient and cooling rate results and analysis under
The printing time of the second single line is about 2 ms, and the evo­ different printing modes
lution process of the melt pool can be divided into three stages: forma­ During the printing process, the profile and temperature field of the
tion stage (2 ms to 2.6 ms), stabilization stage (2.6 ms to 3.8 ms), and melt pool is constantly changing with time, as do the temperature
cooling stage (3.8 ms to 4 ms). gradient and cooling rate. Fig. 26 shows the temperature and distance
curves of the melt pool at the stabilization stage under different printing
3.2.3. Multi-layer printing process results and analysis modes, where the abscissa represents the centerline distribution of the
Fig. 15 (c) shows the multi-layer printed part with a size of 7 mm × 7 melt pool with the laser center as the origin and the ordinate represents
mm × 7 mm when the laser power is 320 W, the scanning speed is 650 the corresponding temperature. It can be seen from Fig. 26 that the
mm/s, and the high-speed camera’s acquisition frame rate is 10,000 temperature gradient at the head of the melt pool is greater than the

Fig. 25. Evolution of temperature field of melt pool with time in the process of multi-layer printing.

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Fig. 26. Temperature distribution along centerline of melt pool in scanning direction.

temperature gradient at the tail, so the peak temperature gradients are accumulation, printing time, and scanning direction. The greater the
all located at the head of the molten pool. The calculation shows that the amount of heat accumulation during the printing process, the longer its
peak temperature gradient in front of the head in the three printing cooling time and the longer the length of the melt pool. In addition, the
modes ranges from 10 K/µm to 20 K/µm. Because the tail of the melt laser does not print along the horizontal direction when printing, and
pool is located in the non-laser heating zone, the slope of the tempera­ the scanning direction of different printing modes is different. Fig. 26 is
ture and distance curve at the tail can be used to calculate the cooling the temperature distribution along the centerline of the melt pool in the
rate of the melt pool. By calculation, the range of the slope of the straight scanning direction, so the scanning direction will also affect the length
line is 1.5–3 K/µm, so according to the scanning speed, the average of the melt pool.
cooling rate of the melt pool is approximately 0.8–2 K/µs, and the There have been several studies on the cooling rate of the melt pool
cooling rate in the multi-layer printing process is about 1 K/µs. in the LPBF process. Hooper et al. [32] measured the temperature data of
The analysis shows that the length of the melt pool in the single-line the centerline of the melt pool with Ti6Al4V material at different
printing and the single-layer printing is less than that in multi-layer printing positions on the 142nd layer. The results show that the peak
printing, which is mainly caused by the difference in heat temperature gradient at different positions in the LPBF process ranges

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H. Ma et al. Applied Thermal Engineering 211 (2022) 118515

from 5 K/µm to 20 K/µm, the average cooling rate at the tail of the melt pool.
pool is about 1.5 K/µs, and the peak cooling rate during the melt pool Fig. 27 (b) shows the shape and size of the melt pool profile at the
cooling stage is about 4 K /µs. In addition, they observed a flat area with stabilization stage under different printing modes. It can be seen from
a length of about 0.4–0.6 mm in different printing positions, while the Fig. 27 (b) that the width of the melt pool under different printing modes
flat area with a length of about 0.5 mm can be observed in the multi- is about 400 µm, and the shape is similar to an ellipse. The length of the
layer printing in this paper, as shown in Fig. 27. Lee et al. [43] simu­ melt pool in single-line printing and single-layer printing is about 500
lated the evolution of the melt pool temperature field with time during µm, while the length of the melt pool in multi-layer printing is about
the single-layer printing of the IN718 alloy material in the LPBF process. 1000 µm, which is mainly caused by the slow cooling rate of the tail of
The analysis showed that the temperature gradient at the tail of the melt the melt pool in multi-layer printing. The position of the molten pool
pool was about 3 K/µm, and the temperature gradient at the edge of the profile is also different under different printing modes. The different
melt pool was about 7.88 ~ 18.4 K/µm. Compared with the above re­ position of the melt pool on the printing plane affects the angle at which
searches, the temperature gradient and cooling rate calculated in this the radiant light enters the temperature measurement system, which
paper have higher reliability. changes the position focused on the target surface of the high-speed
camera. The instability of the laser will also have a certain impact on
3.2.5. Temperature field and profile results and analysis under different the position of the melt pool profile.
printing modes
Fig. 27 (a) shows the temperature field of the melt pool at the sta­ 4. Conclusions
bilization stage under different printing modes. The similarity of the
temperature field of these melt pools is that there is a high-temperature In this study, the online in-situ monitoring of the melt pool tem­
center that coincides with the center of the laser at the center of the melt perature in LPBF processes was investigated by using a developed co­
pool head, the temperature gradually decreases outward along the high- axial temperature measurement system. A dual-waveband image-
temperature center, and the temperature gradient in front of the melt matching method with sub-pixel accuracy, and an overall parameter
pool head is greater than that at the tail of the melt pool. calibration and optimization method are proposed to improve the
The difference in the temperature field of these melt pools is that the temperature measurement accuracy. The experimental results of the
distribution of temperature field and peak temperature are different three printing modes of single-line, single-layer, and multi-layer printing
under different printing modes. In the single-line printing, the peak are compared and analyzed. The following conclusions can be drawn
temperature of the melt pool is mainly related to the linear energy from this study:
density. The greater the linear energy density of the melt pool, the
greater the peak temperature. Therefore, the peak temperature of the (1). The measurement error of the developed coaxial temperature
NO.2 single-line printing is the largest, and the NO.1 single-line printing measurement system is less than 1%, which is validated by a
is the smallest. The printing parameters of the single-layer printing and high-temperature blackbody furnace and a standard photoelec­
the single-line printing are the same, but the peak temperature in the tric pyrometer.
single-layer printing is significantly higher than that of the single-pass (2). The high acquisition frame rate of the high-speed camera can
printing. The main reason is that during the single-layer printing, the provide online in-situ temperature measurement of the melt pool.
hatch spacing is 120 µm, and the size of the molten pool is about 400 µm, (3). The melt pool characteristics including the temperature distri­
resulting in more heat exchange between two adjacent single lines. The bution, profile, temperature gradient, and cooling rate under the
biggest difference between the multi-layer printing, the single-line different printing are measured, and the experimental results are
printing and the single-layer printing is that the tail of the melt pool is proven to be reliable. The optimized parameters in the single-line
longer in multi-layer printing. The main reason is that more heat ex­ printing mode minimize the fluctuation of melt pool temperature
change and accumulation will occur between different layers and be­ and are more favourable to the formation of high-quality parts.
tween different single lines in the multi-layer printing process, resulting The higher the linear energy density in the single-line printing
in more cooling time and longer cooling distance at the tail of the melt mode, the higher the average temperature and peak temperature

Fig. 27. Temperature field (a) and profile shape and size of melt pool at stabilization stage under different printing modes.

19
H. Ma et al. Applied Thermal Engineering 211 (2022) 118515

of the melt pool. The heat accumulation in multi-layer printing Conceptualization, Data curation. Jiangfan Zhou: Conceptualization,
mode is strong, resulting in the slow cooling rate of the melt pool, Data curation. Sheng Liu: Funding acquisition, Methodology. Huimin
which indicates that there are more grain types conducive to the Xie: Funding acquisition, Conceptualization, Methodology. Guangping
enhancement of mechanical properties. Guo: Formal analysis, Methodology. Zhanwei Liu: Funding acquisition,
(4). This study mainly measures the melt pool temperature field Conceptualization, Methodology, Resources, Supervision, Validation,
characteristics and evolution process, but the relationship be­ Writing – review & editing.
tween the temperature field characteristics and the defect for­
mation mechanism of the printed part has not been established. Declaration of Competing Interest
Using the neural network to correlate the temperature field with
the defect formation mechanism of the printed part is the focus of The authors declare that they have no known competing financial
our future work. interests or personal relationships that could have appeared to influence
the work reported in this paper.

CRediT authorship contribution statement Acknowledgement

Heng Ma: Conceptualization, Writing – review & editing, Method­ This work was financially supported by the National Key R&D Pro­
ology, Validation, Data curation, Formal analysis. Zhuangzhuang Mao: gram of China (Grant No. 2017YFB1103900), National Natural Science
Methodology, Validation, Data curation, Formal analysis, Writing – re­ Foundation of China [Grant No. 11972084], National Science and
view & editing. Wei Feng: Data curation, Formal analysis, Methodol­ Technology Major Project (2017-VI-0003-0073), Beijing National Sci­
ogy, Validation. Yang Yang: Data curation, Formal analysis, ence Foundation (1192014), and Rapid Support Project of Equipment
Methodology. Ce Hao: Formal analysis, Methodology, Development Department of Military Commission (80904010502).

20
H. Ma et al. Applied Thermal Engineering 211 (2022) 118515

Appendix

Third-party certificate issued by National Institute of Metrology of China.

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