Professional Documents
Culture Documents
Manual DSC204F1 e
Manual DSC204F1 e
DSC Apparatus
EN 61326:1997+A1:1998+A2:2001
EN 61326 :1997 table 3
EN 61000-3-2:2000
EN 61000-3-3:1995
EN 61000-4-2:1995
EN 61000-4-3:1996
EN 61000-4-4:1995
EN 61000-4-5:1995
EN 61000-4-6:1996
EN 61000-4-8:1993
EN 61000-4-11:1994
EN 61010-1:2002+Corrigendum 1:2002+2:2004
We hereby certify that the product is in accordance with the EU Electromagnetic Compatibility
Directive 2004/108/EC and the EU Low Voltage Directive 2006/95/EC.
NETZSCH
Gerätebau GmbH
(Dr. T. Denner)
Managing Director
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Contents
Chapter II Installation
Chapter V Appendix
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General Informationen
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Information
NETZSCH-Gerätebau GmbH
Wittelsbacherstraße 42
D - 95100 SELB
Telephone: 09287/881- 0
Telefax: 09287/881- 144
E-Mail: at@netzsch.com
Internet: http://www.netzsch-thermal-analysis.com
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In this manual, the symbols described below are used to simplify orientation.
NOTE
ATTENTION!
The tools listed after this symbol are required for the
installation or modification of your instrument.
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Unauthorized Access The operator must make sure that only trained personnel work
on the instrument.
Improper Operation Any type of operation which reduces the safety of the user
and the operability of the instrument should be avoided.
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Maintenance The operator of the system must ensure that the instrument is
Obligation operated in perfect condition at all times.
Proper Set-up of the The operator must guarantee the openness and cleanliness of
Work Stations the work stations at the instrument through appropriate
instruction and inspections.
Shut-down For all maintenance work, the instrument must be switched off
and unplugged.
Electrical Energy The unit may only be opened by qualified personnel, and only
Danger when it is turned off and disconnected from the power supply!
Any work on the electrical supply, electrical lines and electrical
components may only be carried out by qualified personnel
(electrical professionals).
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MATERIAL HAZARDS
Certain steels, such as carbon steel, and some other materials are
unsuitable for use at sub-zero temperatures because they lose
impact strength and become extremely brittle. Carbon steel
cannot be used safely at temperatures below -30°C (-20°F) and is
obviously unsuitable for use with liquid nitrogen. Materials
normally suitable for use at low temperatures are the austenitic
stainless steels, aluminum and copper and its alloys. In an area
where liquid nitrogen spillage can occur, care should be taken to
ensure that the liquid does not come into contact with vulnerable
steel structures and vehicle tires.
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HEALTH HAZARDS
Asphyxia
Nitrogen, although non-toxic, can constitute an asphyxation
hazard through the displacement of the oxygen in the
atmosphere. The potential for this type of hazard is significant
because of the widespread use of nitrogen as a purging or
blanketing gas in chemical, metallurgical, and other industrial
operations and because neither nitrogen gas nor oxygen depletion
are detectable by the normal human senses. Unless adequate
precautions are taken, persons can be exposed to oxygen-deficient
atmospheres if they enter equipment or areas which have
contained or have been purged with nitrogen.
Cold burns
Liquid nitrogen and cold nitrogen vapors or gases can produce
effects on the skin similar to a burn. Unprotected parts of the
body coming into contact with uninsulated parts of the equipment
may also stick fast (because all available moisture is frozen) and
the flesh may be torn on separation.
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Frostbite
Severe or prolonged exposure to cold nitrogen vapor and gas can
cause frostbite. Local pain usually gives warning of freezing, but
sometimes no pain is experienced. Frozen tissues are pain-free
and appear waxy with a pallid yellowish color. Thawing of the
frozen tissues can cause intense pain. Shock may also occur if the
frostbite is at all extensive.
Hypothermia
Low environmental temperatures can cause hypothermia and all
persons at risk should wear warm clothing. Hypothermia is
possible in any environmental temperature below 10°C (50°F), but
susceptibility depends on time, temperature and the individual.
Older persons are more likely to be affected. Individuals suffering
from hypothermia may find their physical and mental reactions are
adversely affected.
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PRECAUTIONS
Ideally, nitrogen should be vented into the open air well away
from areas frequented by personnel. Nitrogen should NEVER be
released or vented in enclosed areas or buildings where the
ventilation is inadequate.
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Personnel protection
It is recommended that persons handling gas containers wear
safety glasses, safety footwear and clean, sturdy gloves.
EMERGENCIES
In the event of accident or emergency, the instructions below
should be implemented without delay. After emergency action
has been taken, contact your nearest Air Products PLC Sales Office
(see list at the back) for further advice.
Asphyxiation
Persons showing symptoms of oxygen deprivation should be
moved immediately to a normal atmosphere. Persons who are
unconscious or not breathing must receive immediate first aid.
Medical assistance should be summoned without delay and first
aid measures include inspection of the victim's airway for
obstruction, artificial respiration and simultaneous administration
of oxygen. The victim should be kept warm and quiet.
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GAS CONTAINERS
The content of the container is primarily identified by a label
attached to the container shoulder and secondarily by the color of
the container. The Air Products identification colors for containers
containing nitrogen are:
Body: French gray; shoulder and guard: black (BS 349: 1973)
General
− Only trained persons should handle compressed gases.
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− Before connecting the container for use, ensure that back feed
from the system into the container is prevented.
− Ascertain that all electrical systems in the area are suitable for
service with each gas.
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Installation
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Contents
INSTALLATION .............................................................................................1
PACKING AND DELIVERY ............................................................................1
LOCATION REQUIREMENTS ..........................................................................2
INSTALLATION SCHEMATIC ..........................................................................3
CONNECTING THE SYSTEM COMPONENTS ........................................................6
CONNECTING THE COMPUTER SYSTEM .................................................................. 6
IMPORTANT NOTES FOR SOFTWARE INSTALLATION .............................................. 7
CONNECTING THE CC 200 F1 ............................................................................. 8
CONNECTING THE CC 300 F1 ............................................................................. 9
CONNECTING THE LN2 COOLER (MAGNETIC VALVE CONTROLLED) 6.351.24 OR 25 .. 10
CONNECTING THE LINEAR SMALL COMPRESSOR .................................................... 11
CONNECTING THE ON-OFF VALVE KIT FOR COMPRESSED AIR COOLING ...................... 12
CONNECTING THE COOLING DEVICE FOR PRESSURIZED AIR ...................................... 13
CONNECTING THE INTRACOOLER ....................................................................... 14
CONNECTING THE GAS SUPPLY .......................................................................... 15
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Installation
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Location requirements
LN2 cooling system The LN2 cooling system requires 0.5 m x 0.5 m space. The
cooling system should be placed beside the table.
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Installation schematic
520
360
250
300
electrical. connections:
230V, 5A
electrical. connections:
230V, 6A
measures in "mm"
580 150
depth 530 depth 350
230
250
de w ar pr es sur e
measuring part DSC 204 F1 Controller table
pre ssu re re lie f
CC 200 F1
powe r CC 200 F1
measures in "mm"
1030
825
Ø 520 Ø 390
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580
depth 530
250
measuring part DSC 204 F1 table
measures in "mm"
1050
900
Ø 520 Ø 390
580
depth 530
250
measures in "mm"
600
floor
500
depth 700
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580
depth 530 measures in "mm"
250
260
depth 180
200
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Requirements
The detailed requirements for installation are given in the enclosed installation schematic.
PC
USB
115V/T6,3A purge 1
230V/T4A
AC line
on/off purge 2
AC input
USB
50/60Hz
protective
optional
fuse LN 2 cooling
115V/T4A
230V/T2A CC 300
mechanical cooling
air cooling
LN 2 cooling
power supply
For connecting the computer system, see also the technical documentation
of the computer manufacturer.
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Your DSC 204 F1 instrument communicates with the PC using the USB interface of the PC.
This requires the installation of suitable drivers delivered together with the Proteus
Software.
→ Before initially connecting the DSC 204 F1 the Proteus Software must be installed first.
For details of installation, please read chapter 3 and chapter 4.2 in the document
“NETZSCH Proteus Software”.
Notes:
Do not use USB hubs (connect your DSC 204 F1 directly to the PC).
If you accidentally change the USB interface on the PC the Plug&Play procedure will
start again to install the drivers for this interface. Please note that this procedure has
to be done for any “not yet” connected USB interface.
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Dewar Head
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DSC 204 F1
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dewar heater
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AC line
on/off
Connecting the CC 200 F1
purge 2
Dewargefäß
AC input
50/60Hz USB
cooling gas
AC line controller protective
230V/115V
3,15AT optional
6,3AT
fuse LN 2 cooling
115V/T4A
dewar head 230V/T2A CC 300
mechanical cooling
LN2 inlet
power
supply
LN2 outlet
LN2 inlet
Please pay attention to all safety regulations for handling liquid nitrogen
8
Dewar Head
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DSC 204 F1
power
supply
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AC line
on/off
purge 2
Connecting the CC 300 F1
AC input
Dewargefäß
50/60Hz USB
protective
optional
fuse LN 2 cooling
115V/T4A
230V/T2A CC 300
mechanical cooling
LN2 inlet
LN2 outlet
LN2 inlet
Please pay attention to all safety regulations for handling liquid nitrogen
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LN2 inlet
LN2 inlet
LN2 outlet
protective
purge 1
purge 2
optional
mechanical cooling
LN2 cooling
CC 300
air cooling
115V/T6,3A
115V/T4A
230V/T2A
230V/T4A
AC input
50/60Hz
AC line
on/off
fuse
Please pay attention to all safety regulations for handling liquid nitrogen
(see chapter I and chapter III)!
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115V/T6,3A purge 1
230V/T4A
DSC 204 F1
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AC line
on/off purge 2
AC input
USB
50/60Hz
protective
optional
fuse LN2 cooling
115V/T4A
CC 300
230V/T2A
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measuring part DSC 204 F1 (rear)
power supply
compressor
Connecting the linear small compressor
outlet
inlet
11
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(compressed air)
hose connection
inlet
outlet
protective
purge 1
purge 2
optional
mechanical cooling
LN 2 cooling
CC 300
power supply
LN 2 cooling
air cooling
115V/T6,3A
115V/T4A
230V/T2A
230V/T4A
AC input
50/60Hz
AC line
on/off
fuse
Figure 7: connecting the on-off valve kit for compressed air cooling
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For minimum temperature of 0°C or below (dependent on air pressure). Includes cold air
generator and software controlled magnetic valve.
pressurized
air inlet
cooling air
outlet
inlet
outlet
protective
purge 1
purge 2
optional
mechanical cooling
LN2 cooling
CC 300
!
power supply
LN2 cooling
air cooling
115V/T6,3A
115V/T4A
230V/T2A
230V/T4A
AC input
50/60Hz
AC line
on/off
fuse
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Intracooler (rear)
power supply
protective
purge 1
purge 2
optional
mechanical cooling
LN2 cooling
CC 300
LN 2 cooling
air cooling
115V/T6,3A
115V/T4A
230V/T2A
230V/T4A
AC input
50/60Hz
AC line
on/off
fuse
For connecting the cooling compressor (intracooler), see also the technical
documentation of the NETZSCH cooling compressor.
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The gas supply unit (e.g. gas bottle) should be equipped with a gas pressure reducer.
The recommended input pressure at the gas inlet of the instrument is 0.5 bar overpressure.
After setting the gas pressure reducer to the recommended value of 0.5 bar overpressure
connect the gas hoses for purge 1, purge 2, and protective at the rear of the instrument.
The gas flow for all gases can be adjusted by means of MFCs via the software.
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System Components
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Contents
CONTROL DISPLAY............................................................................................. 4
BACK PANEL............................................................................................... 9
BACK PANEL............................................................................................. 12
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Measuring unit
height
250
depth
530
width
580
height
300
depth
530
width
580
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Operating principle
gas outlet
cooling air
protective gas
reference
sample
heat flux sensor
furnace block
purge gas
circulating cooling
LN2-/GN2-cooling
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• Heat flux sensor with support plate for sample and reference
crucible.
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operating elements
measuring unit
control display
label function
purge 1 control LED: purge gas 1 (sample chamber) "on/off"
purge 2 control LED: purge gas 2 (sample chamber) "on/off"
protective control LED: protective gas purging "on/off"
power green LED on: instrument is switched on
orange LED on: measurement is running
The gases "protective", "purge 1" und "purge 2" can be activated
via the software (see Help system Software).
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115V/T6,3A
230V/T4A
purge 1 13
AC line
2 on/off purge 2
AC input
USB
50/60Hz
protective
optional
fuse LN2 cooling
115V/T4A
230V/T2A CC 300
mechanical cooling
12
air cooling
LN2 cooling
3 4 5 6 7 8 9 10 11
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Cooling systems
®
The DSC 204 F1 Phoenix can be used with different cooling possibilities:
liquid nitrogen
temperature range: 700°C to -180°C
quickest possible cooling time from 600°C to -170°C: >15 min
linear cooling: - with 100 K/min to 380°C
- with 40 K/min to -60°C
- with 20 K/min to -100°C
- with 10 K/min to -150°C
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Dewar head
front panel
working pressure:
0.5 bar
power green LED on: dewar head is connected to the control electronics
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back panel
1 2
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TR 60:
volume: 60 l
height: 1050 mm
outer diameter: 520 mm
TR 26:
volume: 26 l
height: 900 mm
outer diameter: 390 mm
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Dewar head
front panel
working pressure:
0.5 bar
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back panel
1
2
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front view
2
3
1
4
LN2 cooler; manually controlled supply system, 1 - gas supply (forced N2, 0.5 bar)
operated with compressed gas (N2), 2 - manometer
software-controlled magnetic valve for 3 - magnetic valve
switching the LN2 supply, 4 - gas inlet to measuring unit
with LN2 storage vessel, content 26 l 5 - dewar vessel
6 - shut-off valve (pressure generation)
7 - shut off valve (pressure release)
top view
6 7
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You must never touch objects which have been in contact with
liquid nitrogen with your bare hands.
Always wear special gloves and visors when handling liquid
nitrogen.
Safety Regulations for LN2 Dewar Vessels with NETZSCH Dewar Head
The low pressure vessels are limited to a maximum working pressure of 0.5 bar according
to the pressure equipment directive.
The low pressure vessels with dewar head are designed in such a way that a multilevel
safety circuit prevents possible hazards for the operator when using LN2.
These safety features are:
1. Dewar heating for a controlled pressurization of the vessel incl. pressure relief valve
(opening pressure 0.5 bar) to reduce overpressure inside the vessel.
2. Sufficient big outlet on the pressure relief valve to reduce an overpressure for the case
that the dewar heating control is out of operation and the heating is permanently on.
ATTENTION!
• In order to avoid damages to the dewar head it is forbidden to use hot air instruments
for deicing the components!
• Under no circumstances should the dewar vessel be opened until the pressure has
completely dissipated! Monitor the pressure reduction.
• Escaping liquid nitrogen can lead to serious injuries!
• When removing the supply system from the dewar vessel it can be extremely cold or
extremely hot after switching on by a mistake. Danger of burning! Really wait until the
supply system has cooled down to room temperature.
• If it is not possible to let the cooling head outside the dewar vessel completely dry,
water is collected by time inside the dewar vessel. This water must be regularly removed
by emptying the dewar completely, dumping the ice (water) and drying out the dewar.
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• Liquid nitrogen used in storage tanks (e.g. dewar vessel) evaporates into the air; 1 litre
of liquid nitrogen releases around 700 litres of nitrogen in the gaseous state. Nitrogen is
an inert, non-toxic gas, but displaces oxygen when released into the atmosphere. Once
the atmospheric oxygen content falls below 19% the human organism is at risk.
• All rooms and areas housing vessels containing liquid nitrogen should be well ventilated
at all times and equipped with at least one oxygen gauge. All personnel should be
informed of the risks associated with the use of nitrogen.
• The dewar vessel is designed for use with liquid nitrogen only.
• The dewar vessel must not be moved with its control head fitted. It must only be moved
when the neck is open.
• Never seal the neck of the dewar vessel hermetically. Use only the stopper provided or
the NETZSCH dewar heads.
• The dewar vessel must always be kept vertical.
• The dewar vessel must always be transported empty, in its original packaging and in
compliance with the current national and international regulations. Never stack vessels
on top of each other.
If you suspect that the integrity of the equipment has been compromised (for example as a
result of damage sustained during transit or during use), it should be withdrawn from
service. Make sure that the withdrawn equipment cannot be accidentally used by others.
The defective equipment should be handed over to authorized technicians for inspection.
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Air cooling
Technical data
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* Impact pressure is adjusted on the pressure reducer of the compressed air supply without
consumption.
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Accessories
Sealing Press
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Contents
CALIBRATION ................................................................................................... 3
CALIBRATION KIT ............................................................................................. 3
PREPARING THE SAMPLE .............................................................................4
POWDERED SOLIDS ........................................................................................... 4
COMPACT SOLIDS ............................................................................................. 4
FILMS ............................................................................................................. 4
FIBERS ............................................................................................................ 5
LIQUIDS .......................................................................................................... 5
UNSTABLE SAMPLES .......................................................................................... 5
EVAPORATION REACTIONS ................................................................................. 5
MEASUREMENTS IN DEFINED ATMOSPHERES .......................................................... 5
SELECT THE SAMPLE CRUCIBLE ............................................................................. 6
WEIGH THE SAMPLE .......................................................................................... 6
SEAL THE CRUCIBLE ........................................................................................... 6
INSERT THE CRUCIBLES ...............................................................................7
SAMPLE CRUCIBLE ............................................................................................. 7
REFERENCE CRUCIBLE ........................................................................................ 9
PLACE THE COVERS ......................................................................................... 10
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• calibration
• sample preparation
• sample weight
• reference material
• sample chamber temperature
• temperature program
• atmosphere
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ATTENTION!
• A complete recalibration of the instrument should be carried
out at least once per year and additionally after the
exchange of sensors, thermocouples or electronic
components resp. before longer measurement runs.
• A control of the calibration should be made at least once per
month or on spec of contamination or explicit changes of
the test conditions.
®
Calibration Kit A calibration kit is supplied with the DSC 204 F1 Phoenix .
We calibrate your instrument prior to delivery.
A detailed description of the calibration procedure can be
found in the Help system of the Software.
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Powdered solids The sample is evenly distributed in the bottom of the sample
crucible.
PVC
PVC samples should only be heated in inert gas
atmospheres (N2) to a maximum of 220°C.
Otherwise, HCl can evolve and cause serious
damage to the sensor.
Films Discs are punched from films with a hollow drill or punch
pliers. The discs should completely cover the bottom of the
crucible.
In order to improve the contact between the sample and
crucible bottom, the lid should be placed on the crucible, with
the convex side down, and sealed.
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Fibers The fiber can be cut into small pieces, which are then spread
parallel on the bottom of the crucible.
The fiber is wound around a small rod. The coiled fiber is then
removed from the rod and placed in the crucible.
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Seal the crucible Certain types of crucibles (see chapter V: crucibles) can be cold-
sealed with a special sealing press.
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Sample crucible
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Reference crucible
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Recommended:
Use a dry, inert purge gas in the sample chamber
above 500°C.
Required:
The use of a dry, inert purge gas in the sample
chamber above 600°C is absolutely necessary.
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The mass flow controller are not designed for the use of
corrosive, flammable or reducing gases!
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ATTENTION!
Please pay attention to all safety regulations for
handling liquid nitrogen (see chapter I and chapter III)
and purge gases (see chapter IV).
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CC 300 F1 CC 200 F1
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A B
DSC 204 F1
E D
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Handling Be sure that the on-off valve kit for compressed air
cooling is connected to the measuring unit (see:
chapter II – "Installation").
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Xp Tn Tv
furnace 2 5 4
sample 6 3 4
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Maintenance
cover ring
furnace
wall
slot
sensor
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In dynamic mode the sample chamber is purged with gas during measurement.
Inert gases, air and some reaction gases (non toxic, non flammable) can be used.
Dry, inert gases are recommended for purging the sample chamber. Prior to the intro-
duction of gas, a leakage test should be carried out whilst pre-evacuating the system in
order to assure the purity of the sample atmosphere. We also recommend that the ex-
pelled purge gas be passed into a suitable exhaust hood. Depending on the measuring
conditions (sample material, atmosphere, temperature range), derivative products can also
be formed due to thermal reactions when using inert gases. These products (e.g. HCN, CO,
SO2, dioxine), even in small amounts, are very detrimental to health and must not be
allowed to pass into the work room.
The user must decide in advance whether toxic gases might be released during a measure-
ment. Should this be so, then safety precautions are absolutely essential.
When the measurement requires special reaction gases to be used in the sample chamber,
then a safety check of the potentially hazardous gas or gas mixture is imperative. In this
case the following aspects have to be taken into consideration:
Do explosive gas mixtures or explosive compounds evolve when the sample has contact
with oxygen (air)?
Is it certain that no toxic compounds can evolve from the gases or gas mixtures when using
the chosen application temperatures? In this connection, possible reactions between the
purge gas in the weighing chamber and the reaction gas in the sample chamber should
also be investigated.
Can it be ruled out that the gases neither corrode the leads nor the seals which are used in
either the system or the surrounding equipment (valves, manometer or flow meter)? If not,
then leakages are to be expected.
What side effects do the gases or gas mixtures have on the system's accessories? These ef-
fects do not result in leakages but would considerably increase wear and tear or could lead
to a total failure of the system.
Under no circumstances may explosive gas mixtures be used. The mass flow
controllers are not designed for the use of corrosive, flammable or reducing
gases!
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Information concerning the possibilities of using various gases can be found in the appro-
priate technical literature or can be requested from the manufacturer or retailer of gases.
The following is a selection of purge gases including their limiting properties. The list
makes no claim on being complete.
Air Oxidizing
No technical safety limitations, but sample reactions are possible.
Application is possible above room temperature (maximum
application temperature is determined by furnace material, sample
holder type, crucible material). The oxygen could liquefy if used in
the low temperature range (LN2).
Hydrogen (H2) The instrument is not destined and suitable for use under
hydrogen atmosphere.
It can happen that explosible mixtures are formed inside the
system during the respective experiments.
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Other reducing For safety reasons it is not possible to use these gases as contact
gases or gas with oxygen or air could result in an explosive compound.
mixtures However, certain gas compounds with inert gases are possible
where the mixture ratio excludes all technical safety doubts while
complying with the required analytical conditions. The
manufacturers of gases and gas mixtures can provide the required
information.
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Appendix
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Contents
QMS-COUPLING ................................................................................................. 3
FT-IR-COUPLING ................................................................................................. 4
SPARE PARTS ...................................................................................................... 5
CRUCIBLES .................................................................................................6
MOUNTING ........................................................................................................ 7
HANDLING THE DYNAMOMETRIC KEY .................................................................... 8
SPARE PARTS LIST (SEALING TOOL 6.239.2-92.4) .................................................... 9
LITERATURE ..............................................................................................10
BROCHURES ...................................................................................................... 11
STANDARDS FOR THERMAL ANALYSIS ................................................................... 11
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Technical data
Heating System
Temperature range: -180°C ... 700°C (depending on sensor)
τ sensor: -180 ... +700°C
µ sensor: -150 ... +375°C
(max. working temperature +400°C)
Heating rates: 0.001 to 100 (200*) K/min
(*depending on temperature range
and cooling system)
Cooling System
liquid nitrogen: 700°C to -180°C
cold gas: 700°C to -100°C
compressor (Intracooler): 600°C to -85°
linear small compressor: 700°C to 40°C
cooling time: from 600°C to -170°C : >15min (liquid nitrogen)
Measuring System
digital resolution: 24-Bit converter
signal noise: < 60 nV peak to peak
signal time constant: measurement with laserpulse (only verifiable by
manufacturer):
about 0.6 s (τ-Sensor)
experimental (aluminium-crucible):
about 3.6 s (τ-Sensor, Indium)
reproducibility onset-temperature: < 0.2 K (Indium-peak, aluminium-crucible)
Computer System
Operating system MS-WINDOWS XP Professional,
MS-WINDOWS Vista Business/Enterprise,
MS-WINDOWS 7 Professional/Enterprise/Ultimate
USB Interface,
Windows-compatible printer
Appropriateness
coupling of the DSC 204 F1 with FT-IR Tensor and/or QMS Aëolos.
General
Before starting FT-IR or MS measurements the measuring cell must be purged with
protective gas for approx. 10 minutes since the measuring cell can not be evacuated.
QMS-coupling
1 5
open
close
2 3
The adapter head (1) is attached by the screwings (2) on the cover of the DSC 204 F1. The
gas tube (3) can be unscrewed for cleaning. The transfer line (4) is fixed upright to the gas
flow on the adapter head. The excess gas is dissipated via the gas outlet tube (6). The
length of the gas outlet tube (PTFE tube) is about 1 m. The protective outlet valve (5) must
be opened for measurements in QM-mode. The adapter can be heated up to 300°C.
During normal measurements without active adapter heating and active QMS, the
protective outlet valve (5) must be opened.
FT-IR-coupling
4 1 6 5
open
close
2
3
The adapter head (1) is attached by the screwings (2) on the cover of the DSC 204 F1. The
gas tube (3) can be unscrewed for cleaning. The transfer line (4) is screwed on the end of
the adapter head. The connection to the QMS is closed with a cover (6). The protective
outlet valve (5) must be closed for measurements in FT-IR-mode.
During normal measurements without active adapter heating and active FT-IR the
protective outlet valve (5) must be opened.
Attention!
The adapter may be heated only up to 230°C because of the FT-IR transfer
line.
Additionally to the FT-IR configuration the transfer line to the QMS is mounted.
At simultaneous mode the FT-IR transfer line is used as a bypass for the QMS.
The protective outlet valve (5) must be opened for simultaneous measurements in FT-IR
and QM-mode.
Attention!
The adapter may be heated only up to 230°C because of the FT-IR transfer
line.
Spare parts
3
2
4
open
5
close
6
7
8
Crucibles
Al 600 6.0 25/40 µl set pans / lids, cold-weldable, 500 pcs. 6.239.2-64.51.00
Al 600 6.0 40 µl set pans / lids, punched, cold-weldable, 100 pcs. 6.239.2-64.8.00
Al 600 6.0 40 µl set pans / lids, punched, cold-weldable, 500 pcs. 6.239.2-64.81.00
CrNi steel, gold-plated 500 27 µl re-usable, max. 100 bar, set: 1 crucible/5 sealings 6.239.2-92.3.00
CrNi steel, gold-plated 500 27 µl re-usable, max. 100 bar, set: 10 crucible/50 sealings 6.239.2-92.31.00
CrNi steel, gold-plated 500 100 µl re-usable, max. 100 bar, set: 1 crucible/5 sealings 6.239.2-92.8.00
CrNi steel 500 27 µl re-usable, max. 100 bar, set: 1 crucible/5 sealings 6.239.2-93.3.00
CrNi steel 500 27 µl re-usable, max. 100 bar, set: 10 crucible/50 sealings 6.239.2-93.31.00
CrNi steel 500 100 µl re-usable, max. 100 bar, set: 1 crucible/5 sealings 6.239.2-93.4.00
Titanium 500 27 µl re-usable, max. 100 bar, set: 1 crucible/5 sealings 6.239.2-92.6.00
Titanium 500 90 µl re-usable, max. 100 bar, set: 1 crucible/5 sealings 6.239.2-92.2.00
Titanium 500 100 µl re-usable, max. 100 bar, set: 1 crucible/5 sealings 6.239.2-92.9.00
special steel 200 120 µl max. 20 bar, set: 25 crucible/25 lids/25 sealings 6.240.1-68.1.00
Mounting
Literature
Brown
Introduction to Thermal Analysis
Chapman and Hall, London, New York, 1988
DIN 51005
Thermische Analyse [TA] Begriffe
Beuth-Verlag GmbH, Berlin, 1983
Hill [ICTA]
For Better Thermal Analysis and Calorimetry
ICTA, 1991
Mackenzie
Differential Thermal Analysis
[Vol. 1, Fundamental Aspects]
Academic Press, 1970
Mackenzie
Differential Thermal Analysis
[Vol. 2, Applications]
Academic Press, 1972
Turi
Thermal Analysis in Polymer Characterization
Heyden & Son, Philadelphia, London, Rheine, 1996
Wendlandt
Thermal Analysis
Vol.19, 3rd edition
John Wiley & Sons, New York/London/Sydney/Toronto, 1986
Brochures
Thermochimia Acta
Elsevier Science Publishers B.V.