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User Manual: Model 5100 HD Tunable Diode Laser Spectrometer
User Manual: Model 5100 HD Tunable Diode Laser Spectrometer
User Manual
Process Instruments
150 Freeport Road
90709VE REV R Pittsburgh, PA 15238
Offices
CANADA GERMANY
2876 Sunridge Way N.E. AMETEK GmbH
Calgary, AB T1Y 7H9 Rudolf-Diesel-Strasse 16
Ph. 403-235-8400 D-40670 Meerbusch
Fax 403-248-3550 Ph. 49 21 59 91 36 0
Fax 49 21 59 91 3680
© 2014 AMETEK
This manual is a guide for the use of the Model 5100 HD Version Analyzer. Data herein has been verified and validated and is believed adequate for
the intended use of this instrument. If the instrument or procedures are used for purposes over and above the capabilities specified herein, confirmation
of their validity and suitability should be obtained; otherwise, AMETEK does not guarantee results and assumes no obligation or liability. This publica-
tion is not a license to operate under, or a recommendation to infringe upon, any process patents.
| iii
CHAPTER 2 Specifications
CHAPTER 6 Maintenance
Cleaning............................................................................................................... 6-2
Replacing the MCU Battery................................................................................ 6-2
Containment System Leaks................................................................................. 6-4
Parameter ID & Modbus Registers...................................................................... 6-5
System Alarm/Warning bit map......................................................................... 6-15
Common Modbus Registers.............................................................................. 6-16
| v
Safety Notes
WARNINGS, CAUTIONS, and NOTES contained in this manual emphasize critical
instructions as follows:
Electrical Safety
Hazardous voltages are present in the analyzer housings when power is applied to the
system. Always shut down power source(s) before performing maintenance or trouble-
shooting. Only a qualified electrician should make electrical connections and ground
checks.
Any use of the equipment in a manner not specified by the manufacturer may impair the
safety protection originally provided by the equipment.
Grounding
Instrument grounding is mandatory. Performance specifications and safety protection are
void if instrument is operated from an improperly grounded power source.
Sample Gas
Potential hazards of the sample gas should be taken into consideration
before connecting the sample to the analyzer. Personal protective equipment
and proper ventilation should be used if sample gas is toxic, flammable, or
corrosive. Check the sample line and all connections for leaks before pow-
ering up. Consult plant safety personnel for appropriate exhaust venting
guidelines for specific sample gas type.
Waste Electrical and Electronic Equipment (WEEE) should never be disposed of in a municipal waste
system (residential trash). The Wheelie Bin marking on this product is a reminder to dispose of the prod-
uct properly after it has completed its useful life and been removed from service. Metals, plastics, and
other components are recyclable and you can do your part by doing one of the following steps:
| vii
Secondary Process Seals Requirement
A”This instrument is supplied with a primary process seal only (single seal
device) in accordance with ANSI/ISA 12.27.01-2003. Proper installation of
this instrument requires a secondary process seal if failure of the primary
process seal could allow process fluids to enter the conduit or field wiring
system. The maximum process gas pressure and temperature that will be ap-
plied are 10 psig (170KPa) and 140F (60C).
For more information refer to ANSI/ISA 12.27.01-2003, the 2006 NEC (clauses 501.15
(F) (3) (CI Div 1/2), and 505.16 (E) (3) (CI Zone 1/2)) or the 2006 CEC Part 1 Rules
18-092 (CI Zone 0), 18-108 (CI Zone 1), 18-158 (CI Zone 2), J18-108 (CI Div1), and
J18-158 (CI Div2).
Refer to Chapter 2 – Specifications for details about the suitability of this equipment in hazard-
ous areas.
All input and output wiring must be in accordance with Class I, Division 2 and Zone 2 wiring methods (NEC
Sec 501.4(b) or CEC 18-152) and in accordance with the authority having jurisdiction.
This equipment must be used in a manner not specified by AMETEK, or the protection provided
by the equipment may be impaired.
c) The 5100 HD analyzer is suitable for both indoor and outdoor use. Shield from
direct sunlight.
| ix
Electromagnetic Compatibility (EMC)
Read and follow the recommendations in this section to avoid performance
variations or damage to the internal circuits of this equipment when installed
in harsh electrical environments.
The various configurations of the Model 5100/5100 HD Analyzer should not produce, or fall victim to,
electromagnetic disturbances as specified in the European Union’s EMC Directive. Strict compliance to
the EMC Directive requires that certain installation techniques and wiring practices are used to prevent or
minimize erratic behavior of the Analyzer or its electronic neighbors. Below are examples of the tech-
niques and wiring practices to be followed.
In meeting the EMC requirements, the various Analyzer configurations described in this manual rely
heavily on the use of metallic shielded cables used to connect to the customer’s equipment and power.
Foil and braid shielded I/O and DC power cables are recommended for use in otherwise unprotected situ-
ations. In addition, hard conduit, flexible conduit, and armor around non-shielded wiring also provides
excellent control of radio frequency disturbances. However, use of these shielding techniques is effective
only when the shielding element is connected to the equipment chassis/earth ground at both ends of the
cable run. This may cause ground loop problems in some cases. These should be treated on a case-by-case
basis. Disconnecting one shield ground may not provide sufficient protection depending on the electronic
environment. Connecting one shield ground via a 0.1 microfarad ceramic capacitor is a technique allow-
ing high frequency shield bonding while avoiding the AC-ground metal connection. In the case of shield-
ed cables the drain wire or braid connection must be kept short. A two-inch connection distance between
the shield’s end and the nearest grounded chassis point, ground bar or terminal is highly recommended.
An even greater degree of shield performance can be achieved by using metallic glands for shielded cable
entry into metal enclosures. Expose enough of the braid/foil/drain where it passes through the gland so
that the shield materials can be wrapped backwards onto the cable jacket and captured inside the gland,
and tightened up against the metal interior.
Inductive loads connected to the low voltage “Alarm Contacts” are not recommended. However, if this
becomes a necessity, adhere to proper techniques and wiring practices. Install an appropriate transient
voltage suppression device (low voltage MOV, “Transzorb,” or R/C) as close as possible to the inductive
device to reduce the generation of transients. Do not run this type of signal wiring along with other I/O or
DC in the same shielded cable. Inductive load wiring must be separated from other circuits in conduit by
using an additional cable shield on the offending cable.
In general, for optimum protection against high frequency transients and other disturbances, do not allow
installation of this Analyzer where its unshielded I/O and DC circuits are physically mixed with AC mains
or any other circuit that could induce transients into the Analyzer or the overall system. Examples of elec-
trical events and devices known for the generation of harmful electromagnetic disturbances include mo-
tors, capacitor bank switching, storm related transients, RF welding equipment, static, and walkie-talkies.
Process photometric analyzers, process moisture analyzers, and sampling systems are warranted to perform the
intended measurement, only in the event that the customer has supplied, and AMETEK has accepted, valid sample
stream composition data, process conditions, and electrical area classification prior to order acknowledgment. The
photometric light sources are warranted for ninety (90) days from date of shipment. Resale items warranty is limited
to the transferable portion of the original equipment manufacturer’s warranty to AMETEK. If you are returning
equipment from outside the United States, a statement should appear on the documentation accompanying the equip-
ment being returned declaring that the goods being returned for repair are American goods, the name of the firm who
purchased the goods, and the shipment date.
The warranty shall not apply to any equipment (or part thereof) which has been tampered with or altered after leav-
ing our control or which has been replaced by anyone except us, or which has been subject to misuse, neglect, abuse
or improper use. Misuse or abuse of the equipment, or any part thereof, shall be construed to include, but shall not
be limited to, damage by negligence, accident, fire or force of the elements. Improper use or misapplications shall be
construed to include improper or inadequate protection against shock, vibration, high or low temperature, overpres-
sure, excess voltage and the like, or operating the equipment with or in a corrosive, explosive or combustible me-
dium, unless the equipment is specifically designed for such service, or exposure to any other service or environment
of greater severity than that for which the equipment was designed.
The warranty does not apply to used or secondhand equipment nor extend to anyone other than the original pur-
chaser from us.
THIS WARRANTY IS GIVEN AND ACCEPTED IN LIEU OF ALL OTHER WARRANTIES, WHETHER
EXPRESS OR IMPLIED, INCLUDING WITHOUT LIMITATION AND WARRANTIES OF FITNESS OR OF
MERCHANTABILITY OTHER THAN AS EXPRESSLY SET FORTH HEREIN, AND OF ALL OTHER OBLIGA-
TIONS OR LIABILITIES ON OUR PART. IN NO EVENT SHALL WE BE LIABLE UNDER THIS WARRANTY
OR ANY OTHER PROVISION OF THIS AGREEMENT FOR ANY ANTICIPATED OR LOST PROFITS, INCI-
DENTAL DAMAGES, CONSEQUENTIAL DAMAGES, TIME CHANGES OR ANY OTHER LOSSES IN-
CURRED BY THE ORIGINAL PURCHASER OR ANY THIRD PARTY IN CONNECTION WITH THE PUR-
CHASE, INSTALLATION, REPAIR OR OPERATION OF EQUIPMENT, OR ANY PART THEREOF COVERED
BY THIS WARRANTY OR OTHERWISE. WE MAKE NO WARRANTY, EXPRESS OR IMPLIED, INCLUD-
ING WITHOUT LIMITATION ANY WARRANTIES OF FITNESS OR OF MERCHANTABILITY, AS TO ANY
OTHER MANUFACTURER’S EQUIPMENT, WHETHER SOLD SEPARATELY OR IN CONJUNCTION WITH
EQUIPMENT OF OUR MANUFACTURE. WE DO NOT AUTHORIZE ANY REPRESENTATIVE OR OTHER
PERSON TO ASSUME FOR US ANY LIABILITY IN CONNECTION WITH EQUIPMENT, OR ANY PART
THEREOF, COVERED BY THIS WARRANTY.
| xi
EC Declaration of Conformity
__________________________________________
Robert J. Fiore
2010 Manager of New Product Development
AMETEK Process & Analytical Instruments Division
5100 HD
Overview | 1-1
Tunable Diode Laser Spectroscopy Theory
Tunable Diode Laser Absorption Spectroscopy (TDLAS) is a spectroscopic
technique that uses a diode laser as the light source. The technology is extremely
selective. The laser line is very narrow in frequency so it can probe the analyte
gas without interference from other gases. It works according to the fundamental
principles of Beer’s Law. The Law indicates that for a constant path length, the
intensity of the incident light energy traversing an absorbing medium diminishes
exponentially with concentration.
Ln [I°/I] = S*L*N
Where:
I is the measurement of beam intensity when
tuned to the absorbing wavelength the analyte
Electronics Enclosure
The electronics enclosure houses the electronics, display, and moisture reference
cell and is made of stainless steel and built to withstand harsh environments
(IP65). Included in the electronic enclosure are:
Overview | 1-3
User Interface
Sample Cell
Liquid Separator
Cell Temperature Sensor
Heater
The sample inlet port, liquid filter drain and the exhaust port are located on
the side for the model 5100 HD.
Sample Cell
The sample cell consists of :
• Sample tube
• Gold-front surfaced mirror
• InGaAs Detector
• GRIN lens
Overview | 1-5
Detector
Two light-sensitive detectors are typically used, one for the sample cell and one
for the reference. The detectors output a voltage proportional to the intensity of
the light striking the active area. The type of detectors used varies depending on
the wavelength, which in turn depends on the analyte(s).
GRIN Lens
GRIN is short for graded-index or gradient index. One of the most important
advantages of GRIN lenses compared to classical lenses is that the optical
surfaces of GRIN lenses are flat. This is very important for creating a good
quality joint between the lens and the fiber optics. The GRIN lens in the TDLAS
focuses the laser/fiber-optics package to detect the best signal.
The sample flows from the inlet thru a Genie filter where any liquid condensate
is removed. The liquid removed flows down the drain vent connection on the
side of the 5100 HD. The gas sample then flows thru the sample cell. Cell
pressure and temperature are monitored using pressure and temperature sensors
respectively. The cell is heated to a maximum of 150C.
Laser Configuration
The laser output is coupled to a single mode fiber, which in turn is connected to
a fiber optic splitter. The splitter is used to divide the optical power for use in the
sample and reference measurements, respectively. The ‘sample’ output is coupled
to the cell assembly by means of a fiber/Gradient Refractive INdex (GRIN) lens
combination. ‘Reference’ out put is also similarly coupled to the reference cell.
The GRIN lens helps collimate the output of the single mode fiber and direct the
beam through the sample and reference cells. The beam is reflected by a mirror
at the other end of the cell and is received by a light-sensitive detector at the
originating end.
Measurement
The detector converts the light energy received to an electrical signal and sends
it for signal processing and the analyte concentration determination. WMS and
signal processing are digital providing enhanced quality of analyzer response.
The reference cell is used to lock the output wavelength of the laser diode. The
sealed reference cell contains a known concentration of the analyte in a host gas,
which has no absorbance in the spectral range of interest. A block diagram of the
wavelength-locking algorithm employed by the instrument is shown in the figure
below. Two nested levels of temperature control are employed to maintain the
operation of the DFB laser at the proper wavelength. The first level is a simple
PID control loop, which maintains the laser at a target temperature. In the second
level, the outer control loop, the spectra of the analyte samples in the reference
cells are monitored. Minor shifts in the observed peak positions are used as a
feedback signal for the temperature set point of the inner control loop. Thus, the
outer-control loop provides a fine adjustment for the inner-control loop.
Built-in verification
External calibration is time consuming, especially for polar species like water
with long equilibration times. Model 5100 HD uses a sealed reference cell
(containing moisture vapor in a buffer gas that does not absorb in the spectral
range of interest) for quick analyzer verification. The analyzer response is
compared to the value of the analyte concentration in the reference cell and the
analyzer performance is verified continuously.
Measurement
Fiber optics conduct the laser beam through the GRIN lens to the sample
cell. When the beam reaches the mirror at the end of the cell, it is reflected so
that it continues upward back through the cell until it enters the detector. The
detector converts the information from the beam into an electrical signal that is
transmitted to the microprocessor. The software then processes the signal and
determines the analyte concentration.
Overview | 1-7
Controller Communications
All analyzer functions are controlled by microprocessors housed within the
electronics enclosure. These include:
The Model 5100 HD is configured, and analyzer parameters are set, using either
the analyzer display and keypad, or the Web Interface. The 4-line x 20-character
VFD provides moisture data, system operating parameters, system messages, and
alarm conditions. The 20-button keypad on the front of the unit is used to set or
change operating parameters and system values. There is a serial interface inside
the main electronics enclosure, which is intended for service use only.
The Herriott sample cell is constructed with two mirrors, compared to the standard
cell with one. The two mirrors are facing each other at both ends of the sample
cell. The laser light is reflected back and forth between the mirrors many times,
increasing the path length of the light through the sample gas. This increase in path
length creates a proportional increase in sensitivity to the analyte. The rest of the
analyzer remains the same as for a standard sample cell.
Overview | 1-9
High Temperature Sample Cell Option
Spool Piece
Purge Lines
(1/8” compression ports)
Space-Coupled Option
This option is used for certain application (e.g. O2 measurement) where fiber optics
are not the best approach. Instead of fibers, conventional optical components are used
to direct the laser light through the sample cell. The reference cell is in series optically
with the sample cell, creating a combined path. The reference cell absorption is then
subtracted from the total to get the sample concentration. The sample system and
electronics for this option are the same as for the standard analyzer.
Overview | 1-11
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Specifications | 2-1
Parameter Specification
Depends on analyte and availability:
H2O: 1854nm (25789JE)
CO2: 2004 nm (25834JE)
Wavelength
O2: 763 nm (25895JE)
H2S: 1575 nm (25881JE)
CO2 (high range): 1581 nm (25889JE)
25789JE, Class 1m
25834JE, Class 1m
Laser Classification 763 nm, Class 3b
1575 nm, Class 3b
1581 nm, Class 3b
Independent linearity H2O in CH4: +/- 4 ppmV (.53 mAU) or +/- 2%,
whichever is greater
H2O in non-absorbing background: +/- 1 ppmV (.16
mAU) or 2%, whichever is greater
CO2 in non-absorbing background: +/- .1% CO2 (10
mAU) or 2% of reading, whichever is greater
O2 in non-absorbing background: +/- .1% O2 (1.32
mAU) or 2% of reading, whichever is greater
H2S in non-absorbing background: +/- .1% H2S (.36
mAU) or 2% of reading, whichever is greater
Specifications | 2-3
-20C to +150C (-4 F to +302 F) Gas-phase samples
Sample Temperature
only
Pollution Degree 2
This chapter contains information on the installation and setup of the 5100 HD
Analyzer including:
• Analyzer Requirements:
- Location
- Mounting
- Wiring
- Sample Pressure Requirements
• Installation Connections:
- User-Supplied Items
- Gas Connections
- Signal Connections
- Communication Connections
- Alarm Relay Connections
- User Interface
- Initial Startup
Location
The Model 5100 HD Analyzer is wall-mounted; ensure that there is adequate clearance
when mounting and select a readily accessible position for the analyzer to allow for
routine maintenance. The location should be free from excessive vibration and the
ambient temperature should be -20 °C to 50 °C (-4 °F to 122 °F) without external
heating or cooling. Shade must be provided for the analyzer. Do not mount in direct
sunlight. Shade from luminaires.
• Allow a minimum of 8 inches (20.3 cm) on both sides and the bottom of the
unit for space for system output cables and the AC mains supply conduit.
• Allow a minimum of 4 inches (10.2 cm) on the top of the unit to allow
access to mounting hardware should the unit need to be removed from the
wall.
• Provide adequate clearance at the bottom and sides of the unit for routing
of gas supply line and vent lines.
• The access door(s) to the enclosures swing out when open. Be sure to allow
space for door swing.
Mounting Requirements
C C
26.5” High x 32.7” Wide x 11.9 “ Deep
GENIE FILTER
OVEN ENCLOSURE SAMPLE CELL
HINGE DOOR DRAIN OUTLET ELECTRONIC
1/4" UNION 1/4" UNION ENCLOSURE VENT TERMINAL BOX
ELECTRONICS ENCLOSURE SHOWN WITH COVER
HINGE DOOR REMOVED
B (SEE SHEET 2) B
5100 HD (Doors Closed):
Dimensions
PRODUCT LINE
A LINE
REMOVE BURRS AND BREAK SHARP EDGES
TOOL/FIXTURE
IN HOUSE ONLY
CONFIDENTIAL AMETEK
PROCESS & ANALYTICAL INSTRUMENTS DIV. A
REPRODUCTION PROHIBITED WITHOUT 150 FREEPORT ROAD
1/2" CONDUIT 3/4" CONDUIT DIMENSIONS ARE IN INCHES
TOLERANCES:
PERMISSION BY AMETEK P & AI DIVISION PROCESS & ANALYTICAL INSTRUMENTS DIVISION PITTSBURGH, PENNSYLVANIA 15235 U.S.A.
OPENING OPENING FRACTIONAL 1/32"
ANGULAR: MACH 30'
TWO PLACE DECIMAL .010
DRAWN BY NAM DD-DD-DD XXXXXXXXXX
RR-RR-RR
THREE PLACE DECIMAL .005
SURFACE ROUGHNESS 125
DOC. CONT. DCT
XXXXXXXXXX
ENGR. APPR. EGA RR-RR-RR
SIZE DWG. NO. REV
B 204-164 R
MATERIAL FINISH
ORIG. ISSUE OI DD-DD-DD
SCALE SHEET 1 OF 1
8 7 6 5 4 3 2 1
Wiring
• All wiring conductor ratings should be for the minimum temperature required
for the analyzer but not less that 50° C (122° F).
• For AC mains supply wiring, use between 12 and 14 American Wire Gauge
(AWG) or equivalent metric between 3.3 mm2 and 2.1 mm2.
• The terminal blocks in the customer connection box are sized for 0.2 - 4.0
mm2 (AWG 24 - 12) wire, 1 conductor per block, torque between 0.6 nm and
0.8 nm (85.1 to 113.5 in-oz).
• For optimum noise protection, connect the analyzer mains supply wiring to a
circuit separate from any that could introduce transients into the system.
• Remove the cover of the customer connection box by removing the screws
holding it in place and lifting the cover upward and away from the box.
• Locate the power entry terminal block to make connections to the AC power
line.
• Thread the AC mains supply wiring through the conduit entry port on the
customer connection box and connect as shown below.
The 5100 HD must be ordered for either 120 VAC or 240 VAC since the oven
heater is voltage-specific.
User-Supplied Items
Interconnect Wiring
The user must supply all wiring for serial communication, analog output
(max cable resistance <900 Ohms), and alarm relays. Recommended wire is
22 gauge, twisted/shielded pair.
The terminal blocks in the customer connection box are sized for 02 - 4.0
mm2 (AWG 24 - 12) wire, 1 conductor per block, torque between 0.6 nm and
0.8 nm (85.1 to 113.5 in-oz).
A sample cell pressure sensor located in the electronics box is used to monitor
inlet pressure (shown below).
Gas Connections
Locate the analyzer as close as possible to the sample source and install a main
process shut-off valve at the sample tap. All connections to the 5100 HD are
made using 1/4”tubing (6mm for metric option) compression fittings. These
fittings are located on the right side of the system enclosure. They include:
sample inlet, liquid separator drain, and sample exhaust.
When connecting the sample line, minimize the amount of time that
the analyzer gas fittings are left open. Otherwise significant amounts
of moisture may be introduced into the sample cell from the ambient
air.
1. Remove the fitting caps from the sample inlet fitting and exhaust fitting.
Keep the fitting caps in case you have to ship the analyzer or if it has to be
disconnected for an extended period of time.
2. Connect the sample input tube to the analyzer sample inlet valve.
3. Connect the exhaust tube to the analyzer exhaust. The exhaust must be vented to an
appropriate vent system.
4. The separator inside the sample section removes entrained liquids and
particulates from the gas before it passes through the sample cell. For this
reason, the bypass or drain valve is left OPEN to allow the residue to exit the
analyzer. Ensure that the valve is turned slightly to the OPEN position.
Check the filter on the liquid separator for contamination every two
weeks and replace if necessary. Once you determine a pattern as to how
NOTE long the filter can be used, you can adjust the time interval between
replacements. Check and, if necessary, replace after any known process
event.
5100 HD Separator
The following suggestions will help to minimize issues with the sampling
system:
2. Any condensate that drains from the membrane filters may contain hazardous
and/or corrosive substances. Handle with caution and dispose of properly.
• Using the contact input, there are two methods to connect a switch contact to
the I/O ports:
There are two methods that can be used to connect the output current loop to the
I/O ports.
• Voltage Input
On the analog board find Header J2, place jumpers between Pins 1 and 3,
and between Pins 2 and 4. See the following figure. Connect the positive (+)
input to the Current Input + terminal, and the negative (-) input to the Current
Input – terminal.
Input resistance is 2.5 K Ohms. Maximum input voltage is 6.25 Volts.
NOTE
Current input range is 4-20 mA. Input resistance between Pins 4 and
5 is 100 Ohms.
NOTE
ISOCOM
2W-
2W+
The 5100 HD is equipped with a termination resistor that can be used for the last
unit on the network. Jumper J7 on the MCU board allows you to place a 120-
Ohm termination resistor into the RS-485 circuit. See the following figure.
There are four (4) relay alarms available for the 5100 HD. The relays are
configured in the software. The settings available for the alarms are: Disable,
Concentration, Data Valid, System Alarm, and Normally Open/Normally Closed
(NO/NC).
1. Disconnect the power from the analyzer and remove the cover on the
customer connection box by removing the screws that hold the cover in
place.
2. Thread the cable or conduit through the entry port on the side of the customer
connection box near the relay connection terminals and connect the wiring to
the relay terminals. See the following figure:
Ratings for the Relay Alarms are as follows: Contact rating is 100 VA
max, 1.0 A switching, 2.5 A max carry, 60 VDC/30 VAC max switching.
NOTE
When using the Ethernet interface on the 5100 HD, the minimum requirement for
the Ethernet cable is a CAT 5e (maximum 100 m) cable to connect the analyzer
to the network. The maximum distance between the analyzer and the hub is
100 m. For outdoor analyzer installations, hazardous locations, and/or lengths
greater than 100 m, special requirements may be necessary. Contact your network
administrator for more information.
1. Disconnect the power from the analyzer and remove the cover on the
customer connection box.
2. Route the Ethernet cable through the cable entry port and into the box.
4. Route the cable to the network connection in the plant and connect it.
Overview of Keypad
CALIB Used to define on-demand calibration settings.
Navigation Keys
Arrow Keys Scroll up, down, left, and right through menu
items and system value lists.
Number Keys (0 through 9) Enter values. Use the period (.) to enter numbers
that require a decimal point.
To select an item, use the arrow keys to scroll through the menu items until the
small arrowheads point to your choice as shown below. When you come to the
end of the selections under that menu item, the display will go back to the top of
the list.
Overview of Display
There is also a series of blips after the “status” message (Sampling . . . .) that
repeat to indicate the analyzer is functioning.
2. AMETEK recommends you adjust the sample inlet pressure to between -4.5
PSIG and 10 PSIG.
3. Turn on the power at the source. Boot-up information will appear on the
analyzer display followed by the operation screen. Lines 3 and 4 of the
display will flash various messages and alarm conditions at start-up.
4. When the sample flow starts, the analyzer will adjust to normal operating
mode.
5. Adjust the inlet valve so that approximately 2000 ml/min of natural gas is
flowing through the analyzer.
6. Set the flow rate of the flowmeter to about 1200 ml/min for air to correspond
to the natural gas flow rate of about 2000 ml/min.
7. Use the software to set up your analyzer parameters (See Chapter 4 of this
manual).
The user interface consists of the display screen on the front of the Model 5100
HD Analyzer and the keypad. Use the arrow keys, BKSP, ENTER, SPACE, num-
bers, and period to set the parameters for your analyzer.
Figure 4-1a. Keypad and display for the Model 5100 HD Analyzer.
Line 1 - - Concentration
Line 2 - - Status
Line 3 - - Alarm Message
Line 4 - - Alarm Value
System Alarm
Test
NO/NC Normally Open
Normally Closed
Relay 2 Disable
System Alarm
Test
NO/NC Normally Open
Normally Closed
Relay 3 Disable
System Alarm
Test
NO/NC Normally Open
Normally Closed
Relay 4 Disable
System Alarm
Test
NO/NC Normally Open
Normally Closed
Figure 4-2.
Menu map for Model
5100 HD Analyzer
*Indicates a value must be entered.
Enable
Span Only
Zero Only
Duration (sec)*
Internal (hr)*
Time (00.00.00)*
Enable
Span Value*
Zero Value*
19200
Parity None
Even
Odd
Month Month *
Day Day*
Hour Hour*
Minute Minute*
Second Second*
kPa
Fahrenheit
Open
Relay 2 Close
Open
Relay 3 Close
Open
Relay 4 Close
Open
12 mA
20 mA
Enable
DHCP Disable
Enable
IP Address Address*
Subnet Subnet*
Gateway Gateway*
Hydrogen
Helium
Methane
Ethane
Propane
Butane
Natural Gas
Carbon Dioxide
Special
Air
Nitrogen
Analyte Units
Analyte Units
(See Moisture Analyte
Map Below)
SPAN/ZERO
Span Check Yes Span
CHECK
No
<Target>*
Enable
System Alarm
Test
NO/NC Normally Open
Normally Closed
Relay 2 Disable
System Alarm
Test
NO/NC Normally Open
Normally Closed
Relay 3 Disable
System Alarm
Test
NO/NC Normally Open
Normally Closed
Relay 4 Disable
System Alarm
Test
NO/NC Normally Open
Normally Closed
Disable
Select this alarm function to disable the alarm for the associated relay.
Data Valid
Select this alarm function to set the alarm to recognize corrupt data.
System Alarm
Select this function to trigger an alarm when the system malfunctions.
Test
Select this function to test the relay alarm settings.
NO/NC
Select this function to define the default relay position.
• NC = Normally Closed
• NO = Normally Open
Max Concentration
Enter the reading equivalent to 20 mA.
Min Concentration
Enter the reading equivalent to 4 mA.
Example:
To scale the analog output to represent a 0 to 100 PPMV range enter the follow-
ing settings:
Modbus
Selects the communication setup. The Modbus protocol transmission mode
implemented is Remote Terminal Unit (RTU) with the analyzer operating as a
slave device.
Slave Address*
9600
MODBUS Baud Rate
19200
Time Out (ms)*
• Slave Address
Enter the Slave Address.
• Baud Rate
Select the baud rate at which you transfer data (9600 or 19200). The default
is 9600.
Year
Select Year and enter the 4-digit value for the year.
Month
Select Month and enter the numerical value for the month.
Day
Select Day and enter the numerical value for the day.
Hour
Select Hour and enter the numerical value for the hour using the 24-hour clock.
Minute
Select Minute and enter the numerical value using the 24-hour clock.
Sec
Select Sec and enter the numerical value for the seconds.
psia
Press Disply Units
kPa
Celsius
Temp Disply Units
Fahrenheit
SYSTEM Close
TEST RELAYS Relay 1
TEST
Open
Close
Relay 2
Open
Close
Relay 3 Open
Close
Relay 4 Open
4 mA
TEST ANALOG
12 mA
OUTPUT
20 mA
Test Relays
Tests the relay contacts by toggling them Close / Open.
Enable
NETWORK NETWORK*
Disable
Enable
DHCP*
Disable
IP ADDRESS*
SUBNET*
GATEWAY*
Network
Enables or disables the Ethernet network. Select Enable or Disable.
DHCP
Dynamic Host Configuration Protocol (DHCP). Choose Enable to open the com-
munication protocol or Close to disable it.
IP Address
Defines the network of the analyzer and is a required parameter. Enter the IP ad-
dress for your network.
Subnet
Defines the subnet to which the analyzer belongs. Analyzers in the same subnet
can communicate locally without going through a router (Gateway). Enter your
network subnet.
Gateway
This function defines the Gateway IP address for the network to allow local net-
work traffic to be sent to another network. Enter the Gateway address.
Units
Use the Unit function to select the unit of measurement for the analyzer. (The
map below is shown as an example using moisture.)
PPMV
LB/MMSCF
MG/NM3
Select the unit for the readings from the list. Press Enter.
If you choose either Dew Point C (dewC) or Dew Point F (dewF), you must also
select one of the following:
To begin, the analyzer should be in normal operating mode, and sampling. Press
the ENTER key, and the main menu selections will appear on the display:
To perform a Span Check, scroll to that selection and press ENTER. The follow-
ing screen will be displayed (for H2O in this example):
To change the target value to match the applied analyte concentration, press the
enter key. The screen below will appear, prompting you for the new value.
The passcode is “123”. It is not necessary to press ENTER after typing the
passcode. The software will perform the span automatically once “123” is keyed.
If the password is incorrect, the software will display the message “Incorrect
Passcode”.
After spaning, the analyzer will return to the “Span/Zero Check” screen.
Tec temperature high “TEC Hi Limit Alrm” Laser temperature is above the
setpoint
Tec temperature low “TEC Lo Limit Alrm” Laser temperature is below the
setpoint
Cell temperature high “Cell Hi Limit Alrm” Sample cell temperature is above the
setpoint
Cell temperature low “Cell Lo Limit Alrm” Sample cell temperature is below the
setpoint
Cell Pressure high “Pres Hi Limit Alrm” Sample cell pressure is above the
setpoint
Cell Pressure low “Pres Lo Limit Alrm” Sample cell pressure is below the
setpoint
Ethernet Connection
Use an Ethernet cable to connect the 5100 HD to the network. The minimum
requirement for the Ethernet cable is a CAT 5e. The maximum distance between
the analyzer and the hub is 100 m.
1. Disconnect the power from the analyzer and remove the cover on the customer
connection box.
2. Route the Ethernet cable through the cable entry port (see below) and into the
box.
2. Plug the cable into the LAN RJ45 connector.
3. Route the cable to the network connection in the plant and connect it.
To connect to the 5100 HD Analyzer web interface, you need to know the IP
Address used by your network. The IP Address can be found by using the analyzer
display to navigate to TEST CONFIG, then Network, then IP Address.
• Open any browser (Internet Explorer, Netscape, etc.) and type the IP
Address into the address box and click Return.
Example:
http://10.52.236.54
The Home page displays a graphic of the analyzer indicating current parameters
and location of the following:
• Reference Temperature
• Sample Cell Temperature
• Laser Temperature
• Sample Cell Pressure
3. Menu Buttons
- Home
- Alarms
- Trends
- Spectra
- Settings
Trend and spectral data are stored in temporary memory. For security reasons,
temporary data cannot be stored directly on a computer or network.
Alarms
The Alarms window displays any active analyzer alarm condition as determined
by the built-in Diagnostics. A maximum of 15 active alarms and warnings can be
displayed. If there are more than 15, you can use the scroll arrows to go through
the list. The most recent event is at the top of the list. If there are no active
alarms, the screen will be empty.
The Alarms History window displays a history of Alarms and Warnings that have
been reset along with the time and date that the alarm was triggered. The activity
that caused the alarm, warnings, system and other events can be displayed using
the check boxes for the Alarm Filter Messages. This screen is Read-only.
The Trends window displays the most recent data held in short-term memory at
the upper-right edge of the Trend chart. Since data cannot be saved, use the Print
Screen key or other sceen capture methods to copy and paste data screens for
troubleshooting.
Click the Get Trend button to refresh the display with the most
recent data, after changing the interval or selecting a different
NOTE parameter.
Click on the down arrow to the right of the interval window to change the time
interval for the current trend:
Settings: Relays
Using the Relay display window, you can set up parameters for up to four relays.
• Concentration Limits
High and Low limits
• System Alarm
Triggers to indicate a system alarm condition.
Changes are not saved to the instrument until the “Save” button is
pressed.
NOTE
Use the Current Output display window to set the parameters for a single
current output.
• Offset (Low)
Enter the value for the offset.
• Output Type
4-20 mA DC
0-20 mA DC
Changes are not saved to the instrument until the “save” button is
pressed.
NOTE
Ethernet
• IP Address
Cannot be modified when DHCP is checked. When DHCP is not checked a
static IP address can be assigned.
• IP Subnet Mask
Defines the subnet to which the analyzer belongs. You can communicate with
devices in the same Subnet locally without going through a router.
• Time
The local instrument time can be set here.
• Date
You can use the calendar icon to select the correct date.
Modbus
• Baud
Use the drop-down list box, select the baud rate.
• Parity
Use the drop-down list boc to select parity.
• Stop Bits
Use the drop-down list box to select stop bits.
• Modbus Address
Enter the Modbus address for the instrument.
• Modbus Timeout
Enter the number of milliseconds (msec) before Modbus communication will
time out.
• Date Format
Use the drop-down list box to select the date format.
• Decimal Point
Use the drop-down list box to select either decimal point or period.
Changes are not saved to the instrument until the “Save + reset”
button is pressed. The instrument will reset and communications will
NOTE need to be reestablished from the browser window. Please note that
the IP address may change when the instrument is restarted if DHCP
is chosen as the IP address type.
Maintenance | 6-1
Cleaning
Cleaning the exterior of the analyzer is required occasionally to remove dust and
other debris. Use a damp cloth to clean the analyzer’s exterior, including the
keypad and display.
The battery’s expected life-span is greater than five years; therefore, it is impor-
tant to order and stock a battery when your analyzer is approaching five years
from the original manufacture date.
Before proceeding, test the area around the analyzer for flammable
gases. If an explosive gas atmosphere is present, do not power down
the analyzer or any alternate power sources that supply power to
the analyzer components. Proceed only when the area is found to be
safe.
2. While wearing a grounding wrist strap, use an appropriate tool to remove the
battery from the MCU board. Insert the new battery.
3. Take all necessary precautions to safely power up the analyzer and prepare
it for operation.
Before proceeding, test the area around the analyzer for flammable
gases. If an explosive gas atmosphere is present, do not power down
the analyzer or any alternate power sources that supply power to
the analyzer components. Proceed only when the area is found to be
safe.
4. Close the analyzer enclosure doors and secure them with their latches to al-
low the analyzer to warm up to operating temperature and stabilize.
5. check the System Time and system Date (System screen, SETUP menu)
and set them to the current time and date.
Maintenance | 6-3
Containment System Leaks
• Always leak check the system after servicing it. Use a leak-check liquid solu-
tion, or apply pressure and check for any drop over time – indicating a leak. Do
not apply more than 45 psig or component damage could result.
• Before disconnecting a compression fitting, first mark the fitting to show the
alignment of the fitting body and nut(s). When re-assembling, tighten the fitting
back to this original orientation, and then tighten slightly more to ensure a good
seal.
o Ensure that tube end is pushed all the way to the stop inside the fitting
body.
o Tighten finger-tight.
• When reassembling a sample cell, ensure than all screws are tightened suffi-
ciently to bring the cell pieces into contact (bottom out).
Maintenance | 6-19
6-20 | Model 5100 HD Analyzer
AUTO CAL FEATURE
Feature Overview:
Auto Cal works in two basic ways: as a validation “check”, or as a calibration span/
zero adjustment.
A validation (i.e. check or bump) consists of challenging the analyzer with a zero
gas, span gas, or both – and observing the difference between the applied gas
value(s) and the analyzer readings. It does not include any adjustment of either the
span or zero settings in the analyzer software. Therefore, the analyzer readings will
remain the same for a given gas after the validation event as they were before it.
A calibration span is very similar, in that the same zero and/or span gasses are
introduced into the analyzer. The difference is that the analyzer adjusts itself so that
the zero and/or span values in the software are changed. These changes result in the
analyzer readings matching more closely the actual standard gas concentration(s)
that were entered by the user. The analyzer readings, therefore, will be different
for a given gas after the calibration event than they were before it. Please note that
the span and zero adjustments only affect two points on the calibration curve for
the analyzer. A full, multi-point calibration is done on each analyzer by AMETEK
before the equipment leaves the factory, The span and zero changes performed later
in the field by the Auto Cal feature do not replace this original factory calibration –
they adjust it.
The Auto Cal feature operates on a timer principle. The user enters a time of day
that the Auto Cal event is to occur, as well as an interval. The analyzer will then
initiate an Auto Cal periodically, after each successive interval. For example, if the
user sets an Auto Cal time of 3:00 pm, and an interval of 24 hours, the analyzer will
perform the Auto Cal that day at 3pm (or the following day if the user performed
the setup after 3 pm), and everyday thereafter at 3pm.
Appendix A | A-1
Please note that the real-time clock in the analyzer must be set cor-
rectly for the analyzer to properly schedule and perform these opera-
tions. Instructions for setting the clock may be found in Chapter 4.
NOTE
Alarms: History
4. The first menu option listed is “Ena/Dis”. Selecting this option allows
the user to enable or disable the Auto Cal feature. Any Auto Cal schedule set up
previously will not occur if “Disable” is selected.
Appendix A | A-3
5. The second menu option is “Mode”. This allows the user to select between
“Span & Zero”, “Zero only”, and “Span only”.
Appendix A | A-5
7. Next is “Interval (hr). This is the wait time (in hours) between successive
Auto cal events. Again, type in a new value and press Enter if necessary. If no
change is needed, press Backspace to exit.
8. Next is “Time (00.00.00)”, which is the time of day for the first Auto cal
to occur. Enter the time in military format. For example, 3 pm would be 15:00:00
10. Next is “Zero value”, the concentration of the applied zero gas (typically
Appendix A | A-7
zero). Change if necessary.
11. The last selection is “Auto Adjust”, which establishes whether or not a
Appendix A | A-9
Span and Zero Tolerances:
For both a check and a calibration (i.e. either with Auto Adjust enabled or dis-
abled) the analyzer uses the following tolerances to determine what happens:
So, for a zero check or adjustment, the analyzer tolerance requirement is +/-2%
of full scale. For example, with a full scale range of 0-5%, the tolerance require-
ment is +/-2% of 5%, or +/- 0.1%.
For a span check or adjustment, the tolerance is +/-5% of the span gas. For ex-
ample, if 2% gas is used for span, the span tolerance is 5% of 2%, or +/-0.1%
If either the zero or span reading is outside of the required tolerances, the analyz-
er will display an alarm (which can also be tied to an alarm relay). In the case of
a span or zero check, the analyzer will display a message identifying whether the
problem was with the zero, span, or both. It will, however, return to normal op-
eration and continue to read process gas. In the case of a calibration adjustment,
the analyzer will NOT make the adjustment for a value outside of the tolerance.
It will display the alarm(s), and return to normal operation, without any zero or
span change being performed.
The user can force the analyzer to accept a zero or span (even for readings
outside of the tolerance) only by using the manual Zero/Span feature outlined in
Chapter 4. This is the only way to clear a span or zero alarm.
This analyzer has been customized with the ability to read in a dry contact clo-
sure. To accomplish this, wire the poles of the external switch to the two wires
labelled “CONTACT CLOSURE” in the wiring enclosure (under the main elec-
tronics cabinet). Upon detecting the switch closure, the analyzer will display an
alarm message, which may also be mapped to an alarm relay.
Two laser diodes are used – one for each measuring range. The 5100 HD em-
ploys the same laser device for both ranges, but different wavelengths are used
to ensure an optimal match of absorption strength and sample cell path length for
each range.
The following two pages show a general arrangement drawing for this configura-
tion of the 5100 HD. A heated sample line entry boot is used for both the process
gas inlet and return to process lines. Unlike other 5100 HD versions, there is no
membrane separator/filter included in the analyzer oven. Accordingly, there is no
drain port or valve. The only operational maintenance is cleaning of the sample
cells as necessary.
Appendix B | B-1
8 7 6 5 4 3 2 1
33.2
OVEN ENCLOSURE
C C
B B
30.4
DOOR CLEARANCE
PRODUCT LINE REMOVE BURRS AND BREAK SHARP EDGES
AMETEK
A TDLAS TOOL/FIXTURE CONFIDENTIAL PROCESS & ANALYTICAL INSTRUMENTS DIV. A
IN HOUSE ONLY REPRODUCTION PROHIBITED WITHOUT 150 FREEPORT ROAD
DIMENSIONS ARE IN INCHES
PERMISSION BY AMETEK P & AI DIVISION PROCESS & ANALYTICAL INSTRUMENTS DIVISION PITTSBURGH, PENNSYLVANIA 15235 U.S.A.
TOLERANCES:
FRACTIONAL 1/32"
ANGULAR: MACH 30' DRAWN BY RJF 09-19-14 GENERAL ARRANGEMENT DRAWING
TWO PLACE DECIMAL .010
DOC. CONT. RJF 09-19-14
THREE PLACE DECIMAL .005 5100 HD, DUAL-RANGE H2S, Ja
SURFACE ROUGHNESS 125
A ENGR. APPR. RJF 09-19-14
SIZE DWG. NO. REV
SEE SHEET 2 FOR WIRING INFORMATION MATERIAL ORIG. ISSUE RJF 09-19-14
9000-161-VE SCALE SHEET
450-209
1 OF 2 B A
8 7 6 5 4 3 2 1
8 7 6 5 4 3 2 1
RETURN TO PROCESS
SAMPLE IN
D D
LOW-RANGE SAMPLE CELL
C C
FLOW DIAGRAM
LAN CONNECTOR
IN TOP OF
ENCLOSURE
B B
Appendix B | B-3
SCALE SHEET OF 2
2 B A
8 7 6 5 4 3 2 1
Replacement Parts List
Sensor
COLDFIRE MCU ASSEMBLY 64 Mbit FLASH TESTED (FRU USE 100-2045S) P/N 100-2045S
CONNECTOR, MOD JACK, 8P8C, COUPLER SHIELDED P/N 19875JE
DISPLAY KEYBOARD 5100 P/N 25759JE
POWER SUPPLY 180W 7.5A X 24V DC P/N 25893JE
CONVERTER, D-D, 24V INPUT, 5V OUTPUT, 5 CHAN P/N 25894JE
O-RING, VITON, #019, 13/16” ID, 15/16” OD, 5100-NCM P/N 42760JE
O-RING, #018, VITON P/N 42906JE
STANDARD SAMPLE CELL, EP/SI COATED P/N 7000-919SE
LONG PASS HERRIOT CELL, EP/SI COATED P/N 7000-920-SE
LOW RANGE LASER ASSEMBLY (80597SE ANALOG BOARD WITH MATCHED 255881JE
H2S 1575 NM LASER) P/N 7001-174-TE
HIGH RANGE LASER ASSEMBLY (80597SE ANALOG BOARD WITH MATCHED 255881JE
H2S 1575 NM LASER) P/N 7001-175-TE
SAMPLE OVEN HEATER ASSEMBLY (76589SE HEATER EXTRUSION WITH 301-0462 120V
HEATER CARTRIDGE) P/N 7001-176-TE
INSULATION BOTTOM 5100 NCM P/N 76036KE
GASKET, OVEN INNER, DUAL LASER P/N 76398KE
GASKET, OVEN INNER, DUAL LASER P/N 76399KE
GASKET, BOX CONNECTION, 5100 HD P/N 76405KE
GASKET, CONNECTION BOX TO MAIN, 5100 HD P/N 76406KE
GASKET, CONDUIT FLANGE, 5100 HD P/N 76431KE
ASSY SAMPLE CELL 5100 HD P/N 76477SE
ASSY PRESSURE TRANSDUCER 5100 HD P/N 76580SE
GASKET, SAMPLE CELL CONDUIT, 5100 HD P/N 76630KE
ASSY REFERENCE CELL 5100 HD P/N 76638SE
SAMPLE CELL RTD P/N 76647SE
RAIL, DIN, 35MM X 7.5MM PERORATED, 75MM LONF, 5100 HD P/N 76779KE
ASSY, CABLE, 180W TRACO POWER SUPPLY, 5100 HD P/N 76793SE
ASSY, CABLE, POWER SUPPLY TO D-D CONVERTER, 5100 HD P/N 76794SE
ASSY PCB CUSTOMER CONNECTION BOARD 5100 DUAL LASER P/N 80579SE
ASSY PCB DETECTOR 5100 P/N 80583SE
ASSY PCB OVER-TEMP CONTROLLER BOARD FOR DUAL LASER TDLAS P/N 80584SE
ASSY PCB ANALOG INTERFACE 5100 HD P/N 80591SE
When ordering, provide the serial number of your analyzer to ensure proper parts are ordered:
AMETEK
Process & Analytical Instruments Division
150 Freeport Road
Pittsburgh, PA, USA 15238
Phone: (412) 828-9040 Fax: (412) 826-0399