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50) 2022 Experimental Analysis of The Piezomagnetic Bao Sheng2022
50) 2022 Experimental Analysis of The Piezomagnetic Bao Sheng2022
334
MAGNETIC METHODS
The objective of this research is to investigate the evolution of the piezomagnetic field of 30CrNiMo8 steel under cyclic
tensile stress with variable amplitudes and asymmetrical cyclic tensile stress. The piezomagnetic field signal of an initially
undemagnetised 30CrNiMo8 steel specimen was recorded simultaneously during the whole loading process. It was found
that the magnetic field variation is in contrast to the variation of the applied stress during the elastic stage. However, the
magnetic field variation started to be consistent with the variation of the applied stress when approaching and entering
the plastic stage. A reasonable explanation was given for understanding this phenomenon. The Villari reversal point and
the tail reversal point occurred during the plastic stage, which can be used to characterise the transition state from the
elastic to plastic stage. The variations of the Villari reversal point and the tail reversal point under cyclic tensile stress with
variable amplitudes were slightly different from those under asymmetrical cyclic tensile stress.
Keywords: piezomagnetic field, cyclic tensile stress, Villari reversal, tail reversal, 30CrNiMo8 steel.
1. Introduction of the previous law of approach equation to include terms that are
analogous to those in the Rayleigh Law.
It is well known that the magnetic properties of a ferromagnetic Previous work mostly focused on the effects of stress on magnetic
material will be altered due to the applied mechanical stress, which properties under an applied magnetic field, such as susceptibility,
is called the piezomagnetic effect. This was first investigated by permeability, remanence and coercivity, as well as the hysteresis
Villari[1] in 1865. Since then, many studies have been carried out loop[17-19]. However, the variations of spontaneous magnetic signals
to explore the relationship between the piezomagnetic field and of ferromagnetic materials without demagnetisation under a wide
mechanical stress with an external applied magnetic field. Brown[2] range of stress in the geomagnetic field have not been investigated
successfully predicted the magnetisation-stress curve by replacing thoroughly. Recently, the piezomagnetic effect has attracted
the applied stress with an equivalent field, which exerts the same increased attention as a supplement of magnetic measurements for
effect on the domain walls as the applied stress. Bozorth et al[3,4] the evaluation of the stress state in ferromagnetic materials[20-22].
indicated that the effect of unidirectional stress on magnetisation It has been demonstrated that measuring spontaneous magnetic
depends on the magneto-striction of the material. Craik and Wood[5] field signals provides a promising tool with which to estimate
investigated the magnetisation variations induced by uniaxial the stress state in ferromagnetic materials. However, the strong
elastic stress in a constant applied magnetic field and found that coupling of stress and microstructure with magnetic properties in
the magnetisation variations under tensile stress are asymmetrical ferromagnetic materials makes it difficult to completely understand
to those under compressive stress in various ferromagnetic the complex effects of stress on magnetisation behaviours.
materials. Jiles and Atherton[6] indicated that the application of This paper continues and supplements the research into the
stress, whether compressive or tensile, causes the magnetisation to evolution of the piezomagnetic field of Q345 and U75V steels
approach the anhysteretic curve at a given constant field strength. subjected to cyclic tensile stress with variable amplitudes[23]. It was
Later, a physical model was developed by Sablik and Jiles[7] for the found that the magnetic field reversal points vary drastically during
coupling between magnetic and magnetostrictive hysteresis and for the initial loading cycles, especially before and after entering the
the effect of mechanical stress on both types of hysteresis. Based yield stage, and then change gradually during the plastic stage.
on the law of approach, Jiles[8] proposed an improved model theory The initial drastic variations of the magnetic field reversal points
of the magnetomechanical effect considering the stress-dependent may be utilised to characterise the transition state from elastic to
magnetostriction and the anhysteretic magnetisation curve. plastic deformation. In this paper, cyclic tensile stress with variable
This model theory was successively verified by experimental amplitudes and asymmetrical cyclic tensile stress were exerted on
results[9-13]. Further work was carried out to modify and 30CrNiMo8 steel, respectively. The corresponding piezomagnetic
improve the model theory of the magnetomechanical effect.
Schneider et al[14] proposed a model based on the measured
l Submitted 01.03.22 / Accepted 13.04.22
differential susceptibility of the normal magnetisation curve and
the saturate hysteresis curve. The stress effective field from energy Sheng Bao, Yan Li, Zhengye Zhao, Tao Jiang* and Huangjie Lou are
considerations and stress demagnetisation derived from measured with the College of Civil Engineering and Architecture, Zhejiang
data where stress demagnetisation is a major consideration. University, Hangzhou, Zhejiang 310058, China.
Li and Jiles[15,16] developed a new and improved equation for *Corresponding author. Email: cetjiang@zju.edu.cn
modelling the magnetomechanical effect based on an extension
field variations during the whole loading process were analysed and springs to install the electronic extensometer. The magnetic signals
the differences from those of Q345 and U75V steels were discussed. (B-field) were detected using an APS 428D fluxgate magnetometer
with an accuracy of 0.1 nT. The selected range of the magnetometer
was ±10,000 nT. The installation of the test apparatus is shown
2. Experimental details in Figure 3. Each specimen was vertically mounted between the
The material used in this research is 30CrNiMo8 steel, which is upper and lower grips of the testing machine when being loaded.
a low-alloy quenched and tempered steel mainly used in high- The magnetic probe was installed on the upper grip of the testing
pressure vessels and characterised with high strength and excellent machine with a rigid non-magnetic support and aimed at the
fatigue resistance. The chemical composition and mechanical middle-upper part of a specimen with an angle of 45°. The distance
properties of the steel are listed in Tables 1 and 2, respectively. The between the tip of the magnetic sensor and the surface of the
stress-strain curve of the 30CrNiMo8 steel is shown in Figure 1. It specimen was about 10 mm. A relatively large variation in both
can be observed that the 30CrNiMo8 steel exhibits an elastic stage, the horizontal and normal components of the magnetic field could
a plastic stage with a 0.2% offset yield strength of about 800 MPa be monitored by positioning the probe closely and at a slant with
and a necking stage. Tensile specimens were machined into smooth respect to the sample, which can be found in prior publications[24,25].
plates with a thickness of 4 mm according to the Chinese standard Shielded by a cylindrical Mu-metal tube, the magnetic probe only
GB/T228-2002. The dimensions of the specimen are shown in recorded the magnetic field component parallel to the cylindrical
Figure 2. axis of the probe. To determine the magnetic field interference
from the external environment, such as
the grips of the testing machine and the
Table 1. Chemical composition (wt%) of the 30CrNiMo8 steel
electronic control system, experiments on
C Si Mn P S Cr Ni Mo non-magnetic specimens made of aluminium
0.26-0.34 ≤0.4 0.5-0.8 ≤0.025 ≤0.035 1.8-2.2 1.8-2.2 0.3-0.5 and copper have been carried out in prior
publications[20-22]. The results showed that the
background field does not significantly disturb the piezomagnetic
Table 2. Mechanical properties of the 30CrNiMo8 steel field originating from the specimen.
disappear immediately in cycle 4. Identically, as the maximum the maximum B-field starts to appear during the unloading process.
applied stresses in cycles 5-7 are all less than the yield strength, the During the unloading process, the B-field first increases and then
Villari reversal point and the tail reversal point do not occur during decreases leading to the occurrence of Bmax. The point where Bmax
the loading and unloading processes. It can be seen from cycle 8 occurs is slightly away from the point where the applied stress is the
that the Villari reversal point and the tail reversal point appear smallest as the number of the loading cycle increases. For example,
again due to the maximum applied stress of cycle 8 (840 MPa) being Bmax is 1475 nT in cycle 24 and the corresponding stress is 190 MPa,
larger than the yield strength. The difference between the B-field which is quite close to the minimum stress (175 MPa), while Bmax
of the Villari reversal point and the tail reversal point is 8 nT in is 1481 nT in cycle 30 and the corresponding stress is 262 MPa,
cycle 8, which greatly increases to 115 nT in cycle 10 as the maximum which is greatly larger than the minimum stress. During the loading
applied stress increases from 840 MPa in cycle 8 to 920 MPa in process, there is a change in the decreasing rate of the B-field and
cycle 10. Then, the difference between BV and BT reduces to a the minimum B-field occurs at the point where the applied stress is
relatively steady level of about 80 nT in cycles 11-13, though the the largest. Though the variation of the B-field of step 3 is slightly
maximum applied stress continually increases from 940 MPa in different from that of steps 1 and 2, it is still in contrast to the
cycle 11 to 980 MPa in cycle 13. It can be observed that the B-field variation of the applied stress.
amplitude has a dramatic increase in the second plastic stage,
increasing from 800 nT in cycle 8 to 1760 nT in cycle 13.
first increases and then decreases as the applied stress decreases U75V steels. On the other hand, as well as the matrix phase, there
during the unloading process. Thus, there are two extreme points may be a second phase existing in 30CrNiMo8 steel with the Cr
of the B-field in the loading and unloading processes. It should addition. As reported in[27-28], the second-phase particle-like Cr
be noted that the minimum B-field occurs at the point where the atom will redissolve in the matrix phase under severe plastic
applied stress is the largest in cycles 31-38. Therefore, the extreme deformation. That is, the second phase in 30CrNiMo8 steel may
point of the B-field in the loading process may not be defined as the disappear during the plastic stage, thereby eliminating the magnetic
Villari reversal point and the extreme point in the unloading process property difference between 30CrNiMo8 steel and the Q345 and
may not be denoted as the tail reversal point. With the number of U75V steels.
the loading cycle increasing, the difference
between the minimum B-field and the B-field
at the end of the unloading process gradually Table 5. Chemical composition (wt%) of Q345 and U75V steels
decreases. In cycle 31, the minimum B-field
Material C Si Mn P S V
is 1410 nT, which is less than the B-field
Q345 0.12-0.20 0.20-0.60 1.20-1.60 ≤0.035 ≤0.035 0.02-0.15
at the end of the unloading process by
53 nT. In cycle 38, the difference between the U75V 0.70-0.78 0.50-0.80 0.70-1.05 ≤0.030 ≤0.030 0.04-0.12
minimum B-field and the B-field at the end
of the unloading process decreases to 3 nT. It is interesting that the Figure 9 displays the variations of the applied stress and the
minimum B-field starts to occur at the end of the unloading process corresponding magnetic field response during the plastic stage
from cycle 39. In cycle 39, the B-field at the end of the unloading of specimen 3. Compared with the B-field variation at step 4, the
process is 1441 nT. This is less than the B-field corresponding to the B-field variation becomes more stable and regular when entering
maximum stress, which is 1444 nT. The extreme point of the B-field the plastic stage. It can be seen from cycles 41-60 that the Villari
in the loading process can be referred to as the Villari reversal point reversal point and the tail reversal point occur in the loading and
and the extreme point in the unloading process can be denoted unloading processes, respectively. The B-field of the tail reversal
as the tail reversal point in cycles 39 and 40. In other words, a point is always larger than that of the Villari reversal point.
transition of the variation trend of the B-field occurs between However, the Villari reversal points are not as conspicuous as those
cycle 38 and cycle 39. Before cycle 39, the variation of the B-field in Figure 4, which shows the experimental results of specimen 1.
is in contrast to the variation of the applied stress; however, the It can be observed that the Villari reversal point is quite close to
variation of the B-field starts to be consistent with the variation of the point where the applied stress is the largest. The difference
the applied stress from cycle 39. between the B-field of the Villari reversal point and the B-field
corresponding to the maximum stress is rather small. For example,
BV is 1520 nT in cycle 45 and the corresponding stress is 800 MPa,
which is quite close to the maximum stress (825 MPa). The B-field
corresponding to the maximum stress is 1517 nT, which is slightly
less than BV by 3 nT.
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